Professional Documents
Culture Documents
Engineering
Qatar University
(CHME 324)
Chemical Engineering Lab 1
[Laboratory Manual]
Fall 2016
College of Engineering
Qatar University
CHME-324
Laboratory Manual
(Fluid Mechanics and Heat Transfer Lab)
September, 2016
Contents
Laboratory Manual .............................................................................................................. 1
Contents ............................................................................................................................... i
Preface ................................................................................................................................ iii
Syllabus .............................................................................................................................. iv
General Guidelines ............................................................................................................. xi
Title Page (Full Report) .................................................................................................................... xii
Rubrics Components ......................................................................................................................... 13
Lab Rule Observations and Compliance........................................................................................... 17
Guidelines for Technical Report Writing ......................................................................................... 18
Using Excel (Level 1): Plotting curves using Excel ......................................................................... 22
Using Excel (Level 2): Applying Curve Fits Modeling.................................................................... 21
A Practical Guide to Error Analysis ................................................................................................. 28
Fluid Mechanics Experiments ........................................................................................... 31
F1: Fluid Friction in Pipes ................................................................................................................ 32
1. Objective ................................................................................................................................ 32
2. Introduction and Theory ......................................................................................................... 32
3. Experimental Setup and Procedure ........................................................................................ 37
4. Report Requirements .............................................................................................................. 38
5. References .............................................................................................................................. 39
6. Experimental Data Log Sheet for Experiment (F1) ............................................................... 40
F2: Flow Meter Demonstration Apparatus ....................................................................................... 41
1. Objective ................................................................................................................................ 41
2. Introduction and Theory ......................................................................................................... 41
3. Experimental Setup and Procedure ........................................................................................ 46
4. Report requirements ............................................................................................................... 47
5. References .............................................................................................................................. 48
6. Experimental Data Log Sheet for Experiment (F2) ............................................................... 49
F3: Energy Losses in Bends and Fittings .......................................................................................... 50
1. Objectives ............................................................................................................................... 50
2. Introduction and Theory ........................................................................................................ 50
3. Experimental Setup and Procedure ........................................................................................ 55
4. Report Requirement ............................................................................................................... 56
5. References .............................................................................................................................. 57
6. Experimental Data Log Sheet for Experiment (F3) ............................................................... 58
F4: Centrifugal Pump Performance .................................................................................................. 61
1. Objective: ............................................................................................................................... 61
2. Background and Theory ......................................................................................................... 61
3. Experimental Setup and Procedure ........................................................................................ 66
4. Report requirements ............................................................................................................... 70
5. References .............................................................................................................................. 70
Heat Transfer Experiments ............................................................................................... 71
H1: Conduction along a Simple Bar ................................................................................................. 72
H2. Lumped capacity model ............................................................................................................. 81
H3: Heat Exchanger .......................................................................................................................... 84
Preface
The fluid mechanics and heat transfer laboratory at Qatar University provides a promising setting to
help chemical engineering students become better engineering practitioners. They get hands on
experience of working with laboratory setups the theories of which they studied in Fluid Mechanics
and Heat Transfer courses. This course helps to reinforce and enhance the understanding of fluid
mechanics and heat transfer learned in theoretical courses.
This edition of the Chemical Engineering Laboratory I (CHME 324) manual comes as a result of
needing to improve contents and better organization of the previous edition in accordance with
various suggestions received from faculties and students. The lab safety, lab rule observations, and
guidelines for preparing laboratory reports are incorporated herein this edition.
It is hoped that with the latest modifications, students and instructors will find this edition of the
manual clear and easier to follow and use.
However, our target in the future is to develop this laboratory further with new experimental setups
and further improvements in the laboratory manual. This is an ongoing process. The continued help
and support of the Department of Chemical Engineering and its faculties in preparing this manual is
highly acknowledged.
Syllabus
COLLEGE OF ENGINEERING
Instructor Information
Name: Dr.Ahmed Elkhatat
Academic title: Teaching Assistant
Office:BCR-219
Phone: 4403-4153
E-mail: ahmed.elkhatat@qu.edu.qa
Office Hours:
(1) Please send me email for appointment if you want to discuss anything related to the
course in the following timings.
A-Sunday: 10:30-11:30 am (Office hours Room-C07)
B- Tuesday: 10:30-11:30 am (Office hours Room-C07)
C-Thursday: 10:30-11:30 am (Office hours Room-C07)
(2) You also can contact me by email anytime and I will respond to your questions if I am
available.
TA Information
N/A
Class/Laboratory Schedule
Day/Time/Location:
1) L51: Sunday, 3:30-6:20 pm. G113/G217/G224.
2) L54: Monday, 3:30-6:20 pm. G113/G217/ G224.
3) L01: Wednesday, 3:30-6:20 pm. G113/G217/ G224.
Coordinator Information
Name: Mohammad Hasan Arshad
Academic title: Teaching Assistant
Office: College of Engineering Building, Corridor 7, G228
Phone: 4403- 4151
E-mail: marshad@qu.edu.qa
Course Information
Catalog Description:
Experiments in Fluid Flow and Heat Transfer: Frictional Pressure Losses in Pipes & Fittings, Pump
Performance, Convection, and Double Pipe and Shell & Tube Heat Exchangers.
Credits:
1
Contact Hours:
3
Textbook(s):
Chemical Engineering Laboratory I Manual
References:
Ron Darby. Chemical Engineering Fluid Mechanics, Ed.2. CRC Press (2001)
Holman, J.P. "Heat Transfer", McGraw Hill, New York (1997).
Geankoplis, C.J. "Transport Processes and Separation Process Principles", Prentice Hall, New
Jersey (2003).
Fox, R.W., McDonald, A.T., and Pritchard, P.J. "Introduction to Fluid Mechanics", John Wiley and
Sons, New Jersey (2006)
Course Objectives:
Experimental study of heat transfer and fluid flow. Emphasis is on open laboratory projects with
electronic instrumentation; experimental design with analytical, numerical and graphical analysis of
data
Topics Covered:
Total 9
Method of Instruction:
Laboratory Experiments. Instructor will give a tutorial at the beginning of the semester on how to
use statistical analysis, and use the results to interpret data meaningfully.
Assessment Methods and Grading Policy
Computer/Software Usage
Microsoft Word and Excel
Laboratory Projects
Applicable
Attendance is Mandatory according to University Policies. More than 25% absence will not
qualify you for the course credit.
You can contact by email any time and I will respond to your questions if I am available.
You can also send me email for an appointment if you want to discuss anything related to the
course.
The Tool of communication will BB (blackboard). It will be the student's responsibility to
check the announcements.
The university Plagiarism/Cheating policy will be strictly followed (Check Student
Integrity Code).
General Guidelines For Submitting Reports.
(1) The report should be submitted as a Word file (not PDF) on the SafeAssignment
(BB), Excell Calculations should be submitted as well on Safeassignment.
(2) Full report shall include: Title Page, Abstract, Introduction, Methodology
[experiment Setup, Procedure, Sample Calculation], Results and Discussion,
Conclusion, References.
(3) Deadline of Reports submission is 10 days starting from the day of conducting the
Experiment (By 12:00 noon) (for example: 1: If your Lab is on Sunday, your
submission deadline will be Wednesday 12:00 noon) - (2: If your Lab is on
Monday, your submission deadline will be Thursday 12:00 noon) - (2: If your Lab
is on Thursday, your submission deadline will be Sunday 12:00 noon).
(4) Take care: Late Submittion will be (10% for the first day, 25% for the second day,
50 % for the third day, 100% for the fourth day).
(5) Team Leader will be responsible for fairly distributing of the tasks in the reports,
and also will be responsible for submitting the reports via SafeAssign or by email.
The students of the Department of Chemical Engineering shall follow Qatar Universitys Student
Integrity Code. Practices violating this code include (but are not limited to):
Cheating or copying in any student assignments
Plagiarism in any submitted work: Such as the use of the work, ideas, images or words of
someone else without his/her permission; use of someone else's wording, name, phrase,
sentence, paragraph or essay without using quotation marks, and misrepresentation of the
sources that were used.
Inappropriate Collaboration: Such as working with someone else in developing, organizing or
revising a submitted work without acknowledging that person's help. This work may include: a
project, a paper, an oral presentation, a research, a design project or a take-home examination,
use of tutors for writing, editing or fabricating a submitted work, and use of unauthorized
assistance in all cases of submitted work.
Attending an exam or any academic activity or obligation in replacement of another student
Dishonesty in examinations and submitted work: Such as submission of non-original paper,
test result, work and materials; any form of communication between or among students during
examination; cheating from another student during examination; copying from another's paper,
giving unauthorized assistance, obtaining unauthorized advance knowledge of examination
questions, and the use of mechanical or marking devices or procedures for the purpose of
obtaining false scores on machine-graded examinations; submitting any material prepared by
or purchased from another person or company.
Deliberate falsification of data
Helping or attempting to help another student to commit an act of academic dishonesty
Interference with other students' work
Violating this code can result in penalties following the Universitys regulations.
Declaration
This syllabus and contents are subject to changes in the event of extenuating circumstances. The
instructor (with approval of the Head of Department) reserves the right to make changes as
necessary. If changes are necessitated during the term of the course, the students will be notified by
email communication and posting the notification on the online teaching tool Blackboard. It is
students responsibility to check on announcements made while they were absent.
Qatar University
College of Engineering
Department of Chemical Engineering
General Guidelines
Title of the
Experiment:
Date of experiment: Date of
submission:
Name ID Participation
Group
Team Leader
Student 1
Student 2
Student 3
Grades:
Item Grades Score
Spelling, grammar, sentence
05
Report presentation structure
Appearance and formatting 05
Abstract 10
Introduction and Theory 05
Experimental Setup / Procedure Experimental Setup / Procedure 05
Raw Data 05
Sample Calculation 10
Results and Discussions Analysis of Data: [Statistical
15
Analysis, Tables and Figures]
Discussions/Interpretation 25
Conclusion 10
Citation and References 05
Total 100
Comment
Rubrics Components
Rubric Component Poor Fair Good Excellent
The report Prepares report
The report contains Prepares report that is
contains some that is
Spelling, grammar, frequent spelling free from
spelling and grammatically
sentence structure and grammatical grammatically
grammatical sound with few
[5 Marks] mistake. mistakes.
error. errors.
[Marks:0.5-1.5]. [Marks: 4-5]
[Marks: 1.5-2.5] [Marks: 2.5-4]
Does not Complies Complies to Complies fully to
comply with partially with prescribed prescribed format,
the prescribed the prescribed format. uses creativity in
format. format. Uses adequate presenting graph and
Graphs and Uses fair quality graphs table to analyze and
tables are quality graphs and table to interpret experimental
Appearance and
badly and table to analyze and data.
formatting
presented. analyze and interpret [Marks: 4-5]
[5 Marks]
[Marks:0.5-1.5]. interpret experimental
experimental data.
data. [Marks: 2.5-4 of 5]
[Marks: 1.5-2.5]
Basis
In this course you are asked to submit seven technical reports. Therefore, your reports should
seek to inform, instruct, and often to persuade that its interpretation of the data is the correct one.
In general,
(1) Report format should be A4 plain white paper. Pages must be numbered. Margins are to be
kept at a minimum one inch on each side. Each section should begin on a new page.
(2) Every table, graph, chart, drawing etc. must have a number and a title to identify it and
must be referenced in the text body of the report. Figures, charts, and drawings usually have
their numbers and titles below, whereas tables have their numbers and titles above. Use
Arabic numbers for all. Symbols, subscripts, abbreviations, superscripts and letters must be
defined the first time they occur in the text.
(3) Use past tense, passive voice, and third person to describe what was done. Pronouns as I, we,
he should be avoided
(4) Backup your judgments with data and scientific facts and avoid sensationalism.
(5) Plagiarism is not permitted, always give a reference to the source of any piece of information
you copy of the literature. Cite your references as you proceed through the report using
embraced a number (e.g., [1], [2]) and match a list of numbered references at the end of
your report. References must occur in (sequential) order in the body of your report, therefore
before you mention or cite reference [4], for example, you must have referred to references
[1], [2], and [3] and so on.
The following items are required for your technical written report. The report must be organized in
the order listed below with each section beginning on a new page.
1. Title Page.
2. Abstract.
3. Table of Contents.
4. List of Tables.
5. List of Figures.
6. Introduction.
7. Experimental Setup and Procedure.
a. Experimental Setup.
b. Procedure.
8. Results and discussion
a. Raw Data (Original Data).
b. Sample Calculation.
c. Analysis of Data: [Statistical Analysis, Tables and Figures].
d. Discussions/Interpretation
9. Conclusions
10. References
11. Appendices (If any)
1. Title Page
Use title page provided to you.
2. Abstract
The abstract is the only basis for another reader's decision whether or not your work is of
relevance to him. This requires careful writing. It should briefly state the Background, Statement of
Purpose, Summary of Procedure, Summary of Results and Significance of Findings). An abstract
should not exceed two-thirds of a page. The abstract is best written after you finish the write up of
your report and before you prepare the Table of Contents.
3. Table of Contents
List every division and heading in the report and give the number of the page on which it
starts to appear. It is essential that titles and subtitles match those occurring in the text. Therefore, the
best approach here is to cut the titles and headings from the body of the report and paste them in the
Table of Contents. It is evident thus that this part of the report is best written after preparing the final
report in its ultimate organized structure.
4. List of Tables
List every table along with its title and give the number of the page on which it appears.
5. List of Figures
List every drawing and graph with its title and give the number of the page on which it
appears.
6. Introduction
This is intended to give the unfamiliar reader the required background so that he/she can
follow up and understand your work. Use your own words to provide some background information
about your experiments and a discussion of why the experiment was carried out (i.e., the importance
of the study). Include enough information about the theory needed for a reader who is unfamiliar with
the topic of your experiment. This section also contains the background for the calculations and the
derivation of the equations involved. Sources of equations and derivations should be referenced and
the equations must be numbered. The last paragraph in the introduction must bring into focus the
direct objective(s) of the performed experimental work.
processed correctly with no mistakes, and graphs and tables should be resented professionally.
Moreover, the quality of the results should be analyzed statistically (e.g. Standard deviation, AAD%
etc.). Discussions/Interpretation, Results must be discussed and compared with theory and/or
literature. Each table or graph should be explained in writing and the trends of the curves must be
justified. Sources of errors, if any, and their relation to the obtained data must be stated. Different
paragraphs must be used to discuss different tables or graphs. Always refer to figure number when
discussing this figure. Trends of results should be explained well with the physical principle learned
in the corresponding theory course.
9. Conclusions
10. References
All references cited in the report should be listed in the order of their appearance in the report.
Your text and lab manual can serve as your primary source material, but you should search out and
use other sources. A proper reference for a book should include the name of the author(s), the title,
the publishers, and place and year of publications (e.g., S. E. Kegley, and J. Andrews, The Chemistry
of Water, University Science Books, California, 1998). For a journal article, the reference should
include the name of the author(s), the article title, the journal title and volume number, the year in
which this issue was published and the page numbers on which the article begins (e.g., G. Bassel, N.
Dural, and A. L. Hines, Liquid-liquid equilibria of sulfolane-benzene pentane, Industrial and
Engineering Chemistry Research, Volume 28, 1989, 1369- 1374).
11. Appendices
Extra calculations, derivations, calibrations and methods of analysis should appear in these sections.
1. Highlight the data in both columns, and then press Insert Scatter Scatter
with only markers.
You will get the graph (as shown below) without axis title.
2. Remove any letters or words from the graph. Add the title for x-axis (horizontal) as follows:
Layout Axis Titles Primary Horizontal Axis Titles Title Below Axis (then write
the title)
Then add the title for y-axis (vertical) as follows: Layout Axis Titles Primary
Vertical Axis Titles Rotate Title (then write the title). Do not forget to write the
UNITS as well.
Trendline More Trendline Options select Linear tick Display equation on chart
2) The general shape looks linear, so its equation is Y=mX+C (where, m and C are
variables)
3) To build the model, you have to put initial estimation values for (m) and (C) (fore
example m=1, c=1)
4) Create a column (Y model) and built its equation (Y=mX+C) (Note: here X=B3,
m=$H2, and C=$I2) ($ is used to freeze the cell while filling the column.
6) As these data are a model not actual data, so it is better to draw them as a line, not
scatter points
7) As you see, this model doesnt fit the experimental data set, because (m and C)
are not correct values, so, in order to make it fit Least Square Curve Model will be
used
a. Create (Error^2) column with equation (Ymodel Y)^2 (why squared ?
Because without square some data will be positive an some will be
negative, so in order to exclude all signs square will be applied to all
values.
c. Since the squared error is high we will try to reduce it by changing the
values of both (me and C) until error become minimum.
d. You can judge your data from (Average Absolute Deviation)
exp erimental theoritica l 100
AAD
theoritica l n
e. Create another column (Error Diviation) and use the equation (=Abs(Y-
model Y)/y)*100) and fill the column, then calculate the Average
Absolute Deviation (AAD)
f. Now, we will use solve to make the irritation to have the minimum value
for (Error^2)
i. DataSolver
ii. Set ObjectiveChose the submission f Error^2
iii. To:Min
iv. By Changing variable cellselect m and C cells.
v. Solve
g. As you see, the Y model becomes fitted to the dataset, and the Error^2
become the minimum, and the AAD is 14.35%
h. The Y model can be improved by removing the outliers (any point lies an
abnormal distance from from other points), and use the solver agan to
recalculate the data. the Error^2 becomes the minimum, and the AAD is
7.15%.
( )
=
In these equations, (n) is the number of independent measurements, (Xi ) is the value of
the measured quantity (X) in the (n) experiment, and (Xave) is the average value of (X)
from then experiments.( SD) is often expressed as a percentage:
% = %
In statistical terms, these equations express the expected random differences between the
results of individual but identical measurements of the same quantity. Assuming a
Gaussian distribution of the measured value, we expect that 67% of the measurements
will be within one SD from the average value, and 95% (one out of twenty) will be
within two SD from the average. In other words, if we would do an additional
experiment, we expect a 67% chance that that measured value will be with one SD from
Xave.
The (1 cm) is the absolute error in the height. The % (relative) error is (1/84)100% =
(1.2%). Therefore, in subsequent calculations using this cm, it is write cm = 841 (cm)
or = 84 cm 1.2%. The rules for using absolute or relative errors in subsequent
calculations are as follows:
1. For addition and subtraction: absolute error = (absolute errors)
2. For multiplication and division: %error = (% errors)
Example 1:
Weighing the mass of a sample by first weighing an empty beaker, then beaker +
sample, on a 1 mg balance.
Note that the errors add up, and that a small error in each of the two masses
becomes a large % error when the difference between the masses of the beaker
with and without sample is small!
Example 2:
Determine the density of a liquid by determining the mass of a given volume of
liquid. By using a1.00 mL micropipette (assuming that the 1.00 mL micropipette
delivers a volume of 1.000.02 mL) (0.02 mL half a drop).
Using again the previous 1 mg balance.
So far the method is the same as in the first example. To calculate the density:
() =
If more detail is needed a full discussion of error limits, statistical methods, and error
propagation calculations can be found for instance in:
D.P. Shoemaker, C.W. Garland, J.W. Nibler, Experiments in Physical Chemistry,
McGraw Hill International Editions, fifth edition, NY, USA, 1989, ISBN 0-07-100398.3
(or other editions of the same volume).
Fluid Mechanics
Experiments
Reynolds found that as the velocity of the flow increased, its characteristics were changed
from a laminar flow regime that is characterized by smooth and steady low to turbulent
flow regime, which is characterized by fluctuations and agitation in the flow.
Different laws of fluid resistance apply to laminar and turbulent flow. For a given fluid
flowing in a pipe, experiments show that for laminar flow, the hydraulic gradient
(friction losses per unit length) is proportional to the velocity of the flow, whereas for
turbulent flow, a power law relation is more appropriate.
The energy loss per unit mass in a pipe ( )can be determined from the equation
= = . ()
Since energy loss per unit mass in a pipe ( )can be related to kinetic energy per mass
( ) through Friction Coefficient , i.e.
= . ()
Then
= . ()
In circular pipes
= ( ) . ()
Where () is Fanning friction factor, thus
= ( ) . ()
P
In terms of head loss (hL = )
g
= = . ()
The hydraulic gradient
= . ()
So, the Fanning friction factor can be determined experimentally from head loss or
hydraulic gradient.
= . ()
There were different empirical equations for the determination of Fanning friction factor:
1) Fanning friction factor in laminar flow.
The Hagen poiseuille equation is used to determine Fanning friction factor in
laminar flow. This equation is valid for <2000
= . ()
factor
.
= [ + ] . ()
.
.
= ( ) . ()
A. Churchill equation (1977) can be used for all flow regimes, where it
represents the Fanning friction factor over the entire range of Reynolds
numbers within the accuracy of the data used to construct the Moody
diagram, including a reasonable estimate for the intermediate or transition
region between laminar and turbulent flow.
( )
= [( ) + ] . ()
( + )/
= . . . ()
+ .
[ ( )]
,
=( ) . ()
B. Moodys Chart
(1) The laminar region (for NRe < 2000) is described by the theoretical
HagenPoiseuille equation. In laminar flow the only fluid property that
influences friction loss is the viscosity (because the density cancels out).
Furthermore, the roughness has a negligible effect in laminar flow, as will
be explained shortly.
(2) The critical zone is the range of transition from laminar to turbulent
flow, which corresponds to values of NRe from about 2000 to 4000. Data
are not very reproducible in this range, and correlations are unreliable.
(3) The so-called transition zone in is the region where the friction factor
depends strongly on both the Reynolds number and relative roughness.
(4) The region in the upper right of the diagram where the lines of constant
roughness are horizontal is called complete turbulence, rough pipes or
fully turbulent. In this region the friction factor is independent of
Reynolds number (i.e., independent of viscosity) and is a function only of
the relative roughness.
(5) For turbulent flow in smooth tubes, the semiempirical Blasius models
represent the friction factor quite well. Whether a tube is hydraulically
smooth or rough depends upon.
The test apparatus (GUNT HM 150.11) allows to study the pressure losses in
pipes, piping elements and shut-off devices. In addition, the differential pressure method
is presented for measuring the flow rate.
The experimental unit contains six different pipe sections capable of being shut
off individually. The pipe sections are equipped with piping elements such as bends,
elbows and branches. In one pipe section, different shut-off devices and measuring
objects are installed to determine the flow rate. The measuring objects are made of
transparent material and provide excellent insight into the inner structure. The pressure
measuring points in the piping system are designed as annular chambers. This creates a
largely interference-free pressure measurement.
The experiments measure the pressure losses in pipes and piping elements, such
as branches and bends. The opening characteristic of the shut-off devices are also
recorded. The pressures are measured with tube manometers.
The experimental unit is easily positioned and securely on the work surface of the
HM 150 base module. The water is supplied and the flow rate measured by HM 150.
Alternatively, the experimental unit can be operated by the laboratory supply.
Technical Data
(1) Internal diameter of pipe work at the first measuring section d = 0.0168 m
Measuring length = 800 mm
(2) The internal diameter of the pipework at the second measuring section= d =
0.0268
Measurement length= 500 mm
(3) Roughness of pipe= 0.001 mm
Procedure
1. Connect The pressure gauge to desired measuring points (pipe 1, L=0.8 m,
D=0.0168).
2. Switch on the pump. Close the valve completely and check whether both levels of
manometers are same.
3. Start with lowest flow rate possible.
4. Take the manometer reading and measure flow rate by taking volume and time
reading.[Hint: make sure you take the time approximately close to 1 minute to
minimize the time error].
5. Repeat the same step for Pipe#2 [L=0.5 m, D=0.0268 m].
4. Report Requirements
1) Construct a relation between the flow rate and Reynold Number. Discuss the
obtained trend.
2) Calculate the Fanning friction factor of the pipe for each flow rate using equation
(9).
3) Using equation (9), construct a relation between head loss and velocity to find the
Fanning friction factor.
4) Calculate the friction coefficient of the pipe for each flow rate using equation (4)
5) Using equation (4), construct a relation between pressure loss and velocity to find
8) Simulation part: using theoretical calculation- find the pressure drop due to
friction in pipe flow for a fixed flow rate and length of pipe but vary the pipe
diameter as 0.0168 m, 0.02 m,0.025 m & 0.03 m. Hence establish the relation
between pressure drop and pipe diameter.
9) Ask your Instructor on the visualization model to show the effect of static head
and pipe diameter on the pressure drop.
5. References
1) Ron Darby. Chemical Engineering Fluid Mechanics, Ed.2. CRC Press (2001)
2) J.O Wilkes, Fluid Mechanics for Chemical Engineers, Prentice Hall, Boston,
(2005).
3) GUNT Instruction Manual, HM150.11 Fluid Friction Apparatus.
.
=============================================================
Pipe# 1 (d = 0.0168 m):L=800 mm
Figure 1:Schematic diagram of Venturi Flowmeter (on the left), and Industrial
Venturi Flow meter (on the right) (Source: Control Plus INC)
The Volumetric flow rate can be determined using the following equation,
( )
= . . ()
( )
2
Contraction Ratio for Vena Contracta (CC)= 2 = ( 2 ) . (For highly turbulent
flow 0.6)
The Volumetric flow rate can be determined using the following equation,
( )
= . . ()
( )
Table 2: Discharge Coefficient terms of Miller (1983) for different types of Orifice
flow meter
Fig 3: Miller (1983) Chart for Orifice Flow Meter (Ron Darby, 2011)
( )
=
( )
2) Using ( ) determine (()1 ). Where =
( )( )
= . . ()
Technical Details
Plate diameter: 20 mm
Orifice Pipe diameter: 51.9 mm
Throat diameter: 16 mm
Venturi
Pipe diameter: 26 mm
4. Report requirements
1. Derive the equation of Flow meter from both energy balance and mass balance
equations.
2. Find the discharge coefficient of both Venturi and Orifice meters experimentally,
and discuss the difference between the discharge coefficient for Venturi and
orifice.
1
Calibration was conducted by Eng. Arshad
Dr. Ahmed Elkhatat
48 CHME324 Laboratory Manual
3. Find the discharge coefficient of orifice meter using Miller (1983) chart, and
compare it with that one obtained experimentally.
4. Use the iteration method described above to calculate the flow rate of the Orifice
flow meter, and compare it with a flow rate obtained from Rotameter
5. Calculate % pressure recovery for both flow meters. Comment on the values with
reasons.
6. Calculate the loss coefficient in the Orifice meter, Discuss it.
5. References
(1) Ron Darby. Chemical Engineering Fluid Mechanics, Ed.2. CRC Press (2001).
(2) J.O Wilkes, Fluid Mechanics for Chemical Engineers, Prentice Hall, Boston,
2005.
Date:
Group Number:
.
==============================================================
OBSERVATION TABLE
Venturi Flow Meter Orifice Flow Meter
S.No Rotameter (cm)
h1 (mm) h2 (mm) h3 (mm) h1 (mm) h2 (mm) h3 (mm)
10
theoretical values.
In case of enlargement and contraction fittings, and due to changes in the cross section
area,there is a change in the static pressure. Thus, in order to compensate for this change
a correction to the kinetic energy should be involved.
1) For Sudden Epansion (Enlargement):
Head loss in the expansion ( ) is equal to the measured static pressure
( ) plus correction for kinetic head due to expansion ( ( )).
0.0625
= 4 ( ) where = 2
[log(3.7 )]
= + ( + )
, : 2K loss coefficient parameters.
:Internal diameter of the pipe that contains the fitting (in inches).
= + ( + . )
,
Figure 1. Energy Losses in Bends Apparatus (Front View on the left ) and
(Apparatus Diagram on the right)
Technical Details
Experimental Procedure
Experiment 1:
Measure loss across all the pipe fittings except the gate valve, which should be
kept fully open. Adjust the flow from the bench control valve and, at a given flow rate.
Start with lowest flow rate possible (idea is to have laminar flow regime for 2-3
trials) and then take height reading from all of the manometers after the levels have
steadied. In order to determine the volume flow rate, you should carry out a timed
volume collection using the volumetric tank .This is achieved by closing the ball valve
and measuring with a( stop watch) time taken to accumulate a known volume of fluid in
the tank, which is read from the sight glass. You should collect fluid for at least one
minute to minimize time errors.
Repeat this procedure to give a total of at least five sets of measurements of flow rate.
Experiment 2:
Measure loss across gate valve only. Clamp off the connecting tubes to the miter bend
pressure taping (to prevent air being drown into the system). Start with the gate valve
closed and open fully both the bench valve and the test rig flow control valve. Now open
the gate valve by approximately 25% (After taking up any back lash). For each of at least
5 flow rates, measure pressure drop across the valve from the pressure gauge; adjust the
flow rate by the use of the test rig flow control valve. Once measurements have started,
do not adjust the gate valve. Determine the volume flow rate by timed collections.
( Note: In order to open desire % of GATE valve, count no. of turns required to open the
valve completely and then open number of required turn for given % opening).
4. Report Requirement
(1) Using equation (1) or (2) determines the loss coefficient of the different fittings
you have. Compare between (Kf )of laminar and (Kf ) of turbulent flow regimes.
(2) Construct a relation using equation (1) or (2) to obtain the loss coefficient.
Discuss your results..
(3) From literature, find most possible theoretical expressions of (Kf).Compare them
with experimental results, and discuss the results.
(4) Study the relation between (Kf)and Reynold number.
5. References
(1) Ron Darby. Chemical Engineering Fluid Mechanics, Ed.2. CRC Press (2001).
(2) Armfield Instruction Manual, Losses in the bends F1-22, March 2004.
Date:
Group Number:
.
.
.
.
FITTINGS:
OBSERVATION TABLES
GATE VALVE
25% open
Gauge Reading Flow Rate Measurement
50% open
Gauge Reading Flow Rate Measurement
Notes/Observations
To obtain the characteristic curves such as the Input Power (P), efficiency (), and
the head generated (H) by the pump with respect to the flow rate (Q) obtained for a single
stage centrifugal pump operating at inherent speed and to use these pump curves to
explain and demonstrate the concepts of power management, energy conservation, and
cost savings (having to do with required pump power and pressures).
Most of Pumps can be broadly classified into: (1) Positive Displacement Pumps that
characterized by constant flow rate and variable head, and (2) Centrifugal Pumps, which
characterized by constant head and variable flow rate. The operation of centrifugal pump
is based on the transfer of the kinetic energy (angular momentum) from the rotating
impeller to the Fluid.
Figure (1) Centrifugal Pump (on the left; schematic diagram, and on the right;
industrial centrifugal pump) (Source: http://www.dccleaningsystem.com/)
size of the impeller, However, the volumetric flow rate (Capacity) of the centrifugal
pump depends on the flow resistance of the system, thats why it is variable.
This type of pump has two main components: an impeller and a stationary housing.
The impeller consists of a number of blades, usually curved, arranged in a regular pattern
around the shaft. Figure 1 is a picture of the different type of impellers used in the
centrifugal pump.
Pump Performance
Real pumps are never ideal and the performance of the pumps is determined
experimentally by the manufacturer and typically given in terms of pump curves.
Typically performance is given by curves of:
The operating characteristics of a centrifugal pump may be described or illustrated by
using graphs of pump performance. The three most commonly used graphical
representations of pump performance are:
(1) Efficiency versus capacity.
(2) Power versus capacity.
(3) Head versus capacity.
(4) NPSH versus capacity.
Mechanical Power: is equal to torque () times angular speed ()of the motor.
= = () = . . ()
-Where N=rotational speed of pump in RPM.
Since =
= = . . ()
[3] Pump Head
By solving equations (3) and (4) for pump head
=
= ()
From equation (5) it is obvious that:
So, Pump head is determined primarily by impeller size (R) and speed, and
pump efficiency.
Pump Head is independent of Fluid density, Thus, centrifugal pump develops the
same head regardless of its density or SP.GR.
Although Pump Head is independent of flow rate of the fluid, However, there is
a limitation of the flow that a given pump can handle. When, flow rate
approaches that limit, the developed head starts to drop off.
The maximum efficiency of most pumps occurs near the flow rate where the
head starts to drop significantly.
The head that is observed at the time when the flow is zero is called the shutoff
head and it simply means that the discharged valve is closed.
The optimum conditions for operation occur when the required 'duty point' of
head and flow coincides with a point of maximum efficiency. This point is
called Best efficiency point (BEP), Figure (2).
+ () + = + + () . ()
Figure (3) Representation of discharge head, suction head and total static head
(Source: Redrawn from http://www.pumpfundamentals.com)
Dr. Ahmed Elkhatat
65 CHME324 Laboratory Manual
Note that:
Liquid flows from the suction side to the discharge side.
Suction head is head available just before the pump, = +
Discharge head is the head of the exit from the pump, = + +
Pump head is head required for the pump, =
Thus, head required for the pump can be obtained by rearranging equation (7)
= + ( ) + (() + () )
Where = ( ) and, includes all pipes, fittings, etc
= + ( ) + ( ) . ()
Note that:
Equation (8) is System Pump Head Equation (System Curve).
Pump Head is a quadratic function of Q for highly turbulent flow (i.e. Constant )
Pump Head is a linear function of Q at laminar flow, because value is inversely
proportional to Reynold number.
[2]Procedure
[2.1] Preparation of Experiment
[2.3]Using Sofware
Technical Details
Orifice diameter d = 0.018m, Orifice discharge coefficient Cd = 0.61
Cross-sectional area of the pump inlet A1= 0.00029865 m2
Change in elevation head (Vertical distance between inlet and outlet = 0.048 m
4. Report requirements
(1) Calculate flow rate using orifice data for each case. Create a new column in
EXCEL sheet for this flow rate.
(2) Calculate efficiency using the flow rate you calculated (not from excel program),
and replace this efficiency with one calculated by the program.
(3) Generate pump characteristic curves by plotting Head, power input and efficiency
vs. flow rate for all the speed you studied. Discuss the trend in detail and justify it
and compare with the ideal pump curve one. Find BEP (best efficiency point) on
the graph.
(4) Generate a system curve for the giving pipe flow system provided by the
instructor (contact instructor to get data for system curve). Find the operating
point of the pump using system curve and pump curve.
(5) Create a suitable model for the relation between system curve and pump capacity,
and correlate this model with theory.
5. References
(1) Ron Darby. Chemical Engineering Fluid Mechanics, Ed.2. CRC Press (2001).
(2) J.O Wilkes, Fluid Mechanics for Chemical Engineers, Prentice Hall, Boston,
2005.
(3) Armfield Instruction Manual, Centrifugal pump demonstration unit FM 20,
January 2005.
Heat Transfer
Experiments
To solve the heat equation for a general long solid rod and to compare theoretical
predictions with the actual temperature measurements made in the lab.
To find thermal conductivity of brass and compare it with the value in the
literature.
If a plan wall of a thickness (x) and area (Ax) supports a temperature difference (T),
then according to Fourier law the heat transfer rate per unit time (q) by conduction
through the wall is found to be:
dT
q x Ax (1)
dx
dT
q x kAx (2)
dx
Where (q) is the conduction heat flow in the x direction, (Ax) is the cross sectional
area normal to the (x) direction and (k) is the thermal conductivity. The negative sign
implies that heat is transferred in the direction of decreasing temperature. In more general
cases, Fourier's Law becomes a vector relationship, which includes all directions of heat
flow.
T T T
q (iq x jq y kqz ) k (i j k ) (3)
x y z
The thermal conductivity (k) varies between different materials and can be a
function of temperature. Because of the enhancement of heat transfer by free electrons,
thermal conductivity is analogous to electrical conductivity and hence, metals that are
good conductors of electricity are also good conductors of heat. Figure 2 shows the
thermal conductivity of various materials at low pressures.
3. Experimental
3.1 Description of Experimental Setup
The apparatus we will be using in this experiment is the H940 Heat Conduction
Unit. There are four items to this unit. The first item is the transformer with a circuit
breaker attached. The transformer consists of two cords, one of which plugs into an AC
outlet and the other into the calibration unit.
The second item is the calibration unit. The calibration unit has two basic
functions. One, it delivers heater power to the heater element within the test unit, and
two, it calibrates the temperatures at each of the nine positions so they can be read by the
digital meter. The far right knob adjusts the amount of power delivered to the heater. The
knob to the left is the temperature selector switch, which will give the temperature at any
The third item is the test unit. The test unit consist two test geometries, an
insulated brass bar for which samples can be placed between the two ends and an
insulated disk. Both of these test geometries have a hose running through the cold end for
which cold water from the sink can be passed through (Figure 6-3-2). The purpose of
having cold water running through the end of the bar or disk is to remove heat that is
produced form the other end. Once the rate at which heat is generated is equal to the rate
at which heat is removed, steady state equilibrium conditions will exist. At this point the
temperatures will be constant throughout the bar or disk and readings can be taken. There
are two heater cords, one from the test bar and the other from the test disk. The cord for
the desired test connects into the heater plug located in the lower right hand corner of the
calibration unit.
The last item of the conduction unit is a box that contains the samples,
thermocouples, and conducting paste. The samples can be placed in the bar test unit by
releasing the clamps and sliding the cold bar end out. The samples fit in only one way.
The thermocouples must be placed in order from 1 to 8. There is a label on both the
calibration unit and the test unit letting you know was the number 1 thermocouple starts.
The conducting paste is a highly conductive compound which is designed to decrease
contact resistance when applied to the ends of the connecting bars.
Useful Data: brass sample Diameter: 25 mm
distances between the thermocouple sensors are as follows
x1-2 = x2-3 = x3-4 = x4-5 = x5-6 = x6-7 = x7-8 = 0.015m
Take a brass sample (25 mm Diameter) and coat each end including the apparatus
with conducting compound.
**Please note that the distances between the thermocouple sensors are as follows
x1-2 = x2-3 = x3-4 = x4-5 = x5-6 = x6-7 = x7-8 = 0.015m
To avoid burns, do not touch any metal or plastic surfaces on the hot end of the
sample or test unit.
Avoid using a high cooling water flow to prevent disconnection of the hose from
the test unit.
Do not exceed 20 W power delivery under any circumstances, and do not allow
the temperature to go above 100 C at any of the thermocouple locations.
Avoid using too much conducting paste as this may fry the unit.
5. Report Requirements
Derive governing energy equation (unsteady state included) for the heat
conduction case you studied in the lab. (Hint: Start with generation energy
equation and cancel the term not applicable to your case).
Write boundary and initial conditions.
Plot temperature profile along the length of cylinder at t=5min, 10 min, 15
minute, 20 min and 30 min. Comment on the plot with respect to the variation
with time. Did to get the steady state profile.
Plot steady state temperature profile and find thermal conductivity of brass
sample using slop of the temperature profile. Compare the value of thermal
conductivity with the values given in text.
6. References
J.P Holman, Heat Transfer, McGraw Hill, 2002.
Experimental. Operating and Maintenance Manual, PA HILTON, December
2005
Date:
Group Number:
OBSERVATION TABLE
Time T1 T2 T3 T4 T5 T6 T7 T8
q (W)
(min)
(oC) (oC) (oC) (oC) (oC) (oC) (oC) (oC)
5
10
15
20
30
Time V I T1 T2 T3 T4 T5 T6 T7 T8
q (W)
(min) (volts) (Amps)
(oC) (oC) (oC) (oC) (oC) (oC) (oC) (oC)
10
15
20
30
Time V I T1 T2 T3 T4 T5 T6 T7 T8
q (W)
(min) (volts) (Amps)
(oC) (oC) (oC) (oC) (oC) (oC) (oC) (oC)
10
15
20
30
Notes/Observations
Introduction
dT
q hA(T T ) c
d
and with initial condition T T0 at 0 the equation can be solved as
hA
T T
e cV
T0 T
which is the lumped capacity model in equation form. The results of the experimental
analysis should indicate that the difference between the object and liquid temperature
decay exponentially to zero as the time reaches infinity. The time constant is dependent
Dr. Ahmed Elkhatat
82 CHME324 Laboratory Manual
on the lumped thermal capacitance and resistance of the object to convection heat
transfer. The verification of the Biot number must first be established to determine the
validity of using the lumped capacitance model. This dimensionless number
hV A
k
must be less than 0.1 for the lumped capacity model to apply. The thermal conductivity
(k) is assumed constant, and all other quantities can be determined either directly from
the experiment or through analysis of the experimental results.
Useful data:
Diameter of sphere= 45 mm
Experimental set up :
Experimental procedure
1. Start with general energy balance to develop lumped capacity model equation for
unsteady state heat transfer for sphere (This can be done in theory part)
2. Case 1 (heating the shape in constant temperature bath): plot the temperature of
shape with time. Find the temperature of shape at t=1 minute. Using the lumped
capacity equation and this temperature value at given time, calculate heat transfer
coefficient of hot water inside bath. compare this value with the expected value of
h.
3. Calculate Biot number by using calculated value of h and known values of
thermal conductivity & diameter of sphere. comment on the value with respect to
the validity of lumped capacity model.
4. Case 2: Cooling of hot sphere at room temperature: search for the value of
convective heat transfer coefficient h for the case you studied (table 4-1 in your
heat transfer text book could be helpful). Calculate Biot number for the case you
studied. Comment on the value.
5. Draw temperature profile with time (cooling). Discuss the trend in detail. Plot
theoretical temperature on the same plot , compare both and discuss. Find the
value of h for air for which theoretical and experimental plot exactly matches.
compare this value with the one you found in literature.
1. Objectives:
2. Background
The process of heat exchange between two fluids that are at different temperatures
and separated by a solid wall occurs in many engineering applications. The device used
to implement this exchange is called a heat exchanger, and specific applications may be
found in space heating and air-conditioning, power production, waste heat recovery and
chemical processing. Heat exchangers are typically classified according to flow
arrangement and type of construction. In the first classification, flow can be
countercurrent or cocurrent (also called parallel). On the other hand, according to their
configuration, heat exchangers can be labeled as tubular, plate and shell & tube heat
exchangers.
The tubular heat exchanger is the simplest form of heat exchanger and consists of
two concentric (coaxial) tubes carrying the hot and cold fluids. Heat is transferred to/from
one fluid in the inner tube from/to the other fluid in the outer annulus via the metal wall
3. Theory
3.1 Experimental approach
3.1.1 Overall Efficiency
To design or predict the performance of a heat exchanger, it is essential to
determine the heat lost to the surrounding for the analyzed configuration. We can define a
parameter to quantify the percentage of losses or gains. Such parameter may readily be
obtained by applying overall energy balances for hot and cold fluids. If Qe is the heat
power emitted from hot fluid, meanwhile Qa the heat power absorbed by cold fluid
(neglecting potential and kinetic energy changes);
Qe mh Cph (Th,i Th,o ) (1)
Qa mc Cpc (Tc,o Tc,i ) (2)
m h , m c : Mass flow rate of hot and cold fluid, respectively.
Qa
Percentage of losses or gains P 100
Qe
The above formulas were deducted taking into account that hot fluid is rounded
by cold fluid. If the average cold fluid temperature is above the ambient air temperature
then heat will be lost to the surroundings resulting in P < 100%. If the average cold fluid
temperature is below the ambient temperature, heat will be gained resulting P> 100%.
3.1.2 Temperature efficiencies
Fig 1: Countercurrent and Co-current operation for a shell and tube heat exchanger
Th ,inlet Th ,outlet
Temperature efficiency for hot fluid h 100
Th ,inlet Tc,inlet
Tc ,outlet Tc ,inlet
Temperature efficiency for cold fluid c 100
Th,inlet Tc ,inlet
h c
Mean temperature efficiency m ,
2
Subscripts h and c stand for hot and cold, respectively.
Where,
t1 = T1-T4 ( temperature difference of hot and cold streams at one end)
t2 = T2-T3 ( temperature difference of hot and cold streams at other end)
heat exchangers they trade. Then, it is expected that the theoretical values differ from the
experimental ones, fundamentally due to the presence of bubbles. Of course,
experimental results are mandatory because they reflect real conditions of operation.
However, for heat exchanger selection it is convenience to have a methodology in order
to estimate the overall heat transfer coefficient or the size according to given temperature
range and flow specifications.
Before setting the equation that determines the Overall Heat Transfer Coefficient, lets
take some assumptions. The conduction resistance between hot and cold fluid could be
neglected, also resistance due to fouling.
1
Ui (5)
1 A A ln( ro / ri )
i i
hi ho Ao 2kL
Where
hi : Heat transfer coefficient of hot fluid [W/m2K]
ho : Heat transfer coefficient of cold fluid [W/m2K]
Ai: Heat transfer Area based on insider diameter
Ao: Heat Transfer Area based on outside diameter
ro: outside radius
ri: inside radius
L: heat transfer length
K: Thermal conductivity of tube material (steel)
In order to calculate hi and ho, the appropriate correlation will be used.
For flow in circular tubes:
NuD : 4.36 (Laminar flow, ReD < 2300)
Colburn equation
NuD : 0.023 ReD4/5 Pr1/3 (Turbulent flow, ReD > 2300)
hD
Nu D
k
Where D: Diameter of tube
k: Conductivity of fluid
If the tube is non circular, hydraulic diameter is used, instead.
4 Ac
Dh
P
Where Ac and P are the cross-sectional area and the wetted perimeter, respectively.
4. Experimental
Fig. 2: Heat Exchanger Service Unit with the Tubular Heat Exchanger installed.
The tubular heat exchanger consists of two concentric (coaxial) tubes carrying the
hot and cold fluids. The tubes are separated into two sections.
exchangers arranged in series in the form of a U. The hot water flows in the inner
tube and cold fluid in the outer annulus. The equipment allows the conversion from
Six temperature sensors are installed in the hot and cold fluid inlets, outlets and mid
positions.
Technical Data:
Each inner tube is constructed from stainless steel tube,8.3 mm ID, 9.5mm
OD.
Each outer annulus is constructed from clear acrylic tube, 12.0mm ID.
Each heat transfer section is 330mm long giving a combined heat transfer
5. Report requirements
Calculate overall efficiency, temperature efficiency and overall heat transfer
coefficient. Compare the results for concurrent and counter current cases.
Calculate theoretical overall heat transfer coefficient for counter current HE and
compare with the experimental one.
Plot experimental overall heat transfer coefficient against hot water temperature
and comment on the trend.
6. References
J.P Holman, Heat Transfer, McGraw Hill, 2002.
Instruction manual Computer Compatible Tubular Heat Exchanger HT 31,
Armfield, November 2004.