A GOOD WAY OF PRESENTING DATA

IR1
Table 1: Assignment of peaks for the IR spectrum of Sample A

Intensity of
Wavenumber range (cm-1) Assignment
Peaks
3649.32, 3375.43 Weak O-H stretch
3062.96, 3030.17 Medium sp2 C-H Stretch
2956.87, 2924.09, 2862.36 Medium sp3 C-H Stretch
2229.71 Strong CH Stretch
1959.68, 1897.95, 1799.59,
Weak Aromatic Overtones
1707.00
1600.92, 1583.56, 1483.26,
Medium Aromatic Ring Stretching
1448.54
Aromatic out of plane
788.89, 686.66 Strong
bending

Table 2: Assignment of peaks for the IR spectrum of Sample B

Intensity of
Wavenumber range (cm-1) Assignment
Peaks
3003.17 Medium sp2 C-H Stretch
2956.87 - 2835.36 Medium sp3 C-H Stretch
1869.02, 1845.88 Weak Aromatic Overtones
1589.34, 1577.77, 1458.18,
Medium Aromatic Ring Stretching
1440.83
Strong, Phenyl Alkyl Ether
1247.02, 1031.92
Medium Stretch
Aromatic out of plane
821.68 Strong
bending
599.86 Strong C-Br Stretching

Table 3: Assignment of peaks for the IR spectrum of Sample C

Intensity of
Wavenumber range (cm-1) Assignment
Peaks
3448.72 3215.34 Strong 1o Amine
3061.03, 3020.53 Strong 2
sp C-H Stretch
2964.59, 2931.80, 2872.01 Strong sp3 C-H Stretch
1921.10, 1890.24, 1780.30 Weak Aromatic Overtones
1618.28, 1583.56, 1496.76,
Strong Aromatic Ring Stretching
1456.26
1215.45 1273.02 Medium C-N Stretch

1 Adopted from Justin LimEdited by FM Fung

 Aromatic out of plane
750.31 Strong
bending
NMR
Relative
J
Chemical number of
Peak Multiplicity Proton Integration Coupling
Shift Values protons
No of the peaks Assignment Ratio constants
(ppm) causing the
(Hz)
peaks
1.2263
1 1.2507 Triplet Hc 6.9542 7 7.32
1.2740
1.5828
1.5945
2 1.6042 Quintet Hh/Hh 7.2580 7 3.51
1.6130
1.6247
1.9734
3 1.9811 Multiplet Hi/Hi 7.5542 8 2.31
1.9850
4 2.0367 Singlet Ha 6.5374 7 -
5 2.4360 Singlet Hd 3.8265 4 -
4.0781
4.1015
6 Quartet Hb 4.2556 4 7.02
4.1258
4.1492
7 5.6627 Singlet Hj 3.0096 3 -
- 7.2600 - Solvent - - -
7.3145
8 Doublet He 2.0877 2 7.89
7.3408
7.7596
9 Doublet Hf 2.2147 2 7.89
7.7859
10 9.9579 Singlet Hg 1.0000 1 -