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8810 - ORP
TABLE OF CONTENTS
1 APPLICATION
2 PROGRAMMATION
3 STARTING UP
4 REAGENT PREPARATION
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8810-ORP - SULPHIDE 1-100mg/l
1. APPLICATION :
The cell of the analyser is automatically filled O Press the UP/DOWN keys to select
with a constant and reproducible volume of "PROGRAMMATION".
sample. After alkaline conditioning,
sulphides are titrated directly by a solution O Press ENTER and hold on 5 seconds to enter
of copper II. The titration is followed by the PROGRAMMATION menu.
silver electrode.
The titration curve is increasing from a
potential of about -700 mV and the END 2.2 PM XXXX
POINT is located at -550 mV . The measuring
range is directly dependent on the O Select "PM XXXX" with the scroll keys.
concentration of the titrating reagent (cf :
5.1) O Press ENTER.
With this application, it is impossible to O Enter 4000 with the scroll keys.
calibrate automatically because of the great
O Press SELECT to change the digit.
instability of sulphide solution. For the same
reason, it is better to perform a process
O Enter 4600 with the scroll keys.
calibration than a manual one.
O Press SELECT to change the digit.
2. PROGRAMMATION : O Enter 4670 with the scroll keys.
2.1 PROGRAMMATION ACCESS :
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8810-ORP - SULPHIDE 1-100mg/l
O Enter or check the unit (g/l, mg/l, ...) and SAMPLE TIME : depending on your application,
press ENTER adjustable from 1 to 99 sec . (usually : 05 sec)
. (press ENTER)
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8810-ORP - SULPHIDE 1-100mg/l
OUT : Conc
2.6 CHEMICAL CLEANING :
The unit has been previously selected in the
O With the scroll key select "CLEANING" and UNIT submenu ( see 2.3.3 )
press ENTER.
Enter or check the following information : O With the scroll key select "ZERO" and adjust
your printer on the scale origin. (press ENTER)
FREQUENCY : XXX
depends on your application (press ENTER) O With the scroll key select "FULL" and adjust
your printer on full scale. (press ENTER)
SPRINKLER t. : 003 s ( press ENTER)
O With the scroll key select "CONC" and press
REAG. INJ. t. : 03 s (press ENTER) ENTER.
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8810-ORP - SULPHIDE 1-100mg/l
Now you are ready to start your process. In a 10 liters tank, pour 3 liters of demineralised
water. Add very slowly and under stiring 5
O Press SELECT to exit from the liters of concentrated sodium hydroxyde
PROGRAMMATION menu. solution (33-35%). Adjust to 10 liters mark with
demineralised water. Let it cool.
O With the scroll key select "START" and let
the analyser roll !
3.3 "PROCESS" CALIBRATION (If you have to In a 10 liters tank, pour 7 liters of demineralised
adjust the calibration slope). water. Then, add very slowly and under stirring
2 liters of concentrated nitric acid (65 %). Adjust
O Determine the sample concentration with a to 10 liters with demineralised water.
laboratory titration.
4. REAGENT PREPARATION
0 - 50 0.5 g/l 5 g