UPVC

Elements KG % RATIO
1. MEK added in reactor at room
THF 655 28.634% 2.Aerosil 200 and calcuim sterat
Aerosil 200 45 1.967% 3.after mixing dd THF and cycloh
MEK 562.5 24.590% 4. Heating start for 30 mints whe
Cyclohexanone 512.5 22.404% 5.add Solvim 250 and solvim 27
Paraloid KM 376 10 0.437% 6.start cooling aggitate 2 hrs
Solvim 250 250 10.929% 7. Start sampling
Solvim 275 250 10.929% 8.adjust viscosity in range.
calcium sterate 2.5 0.109290%

Total 2287.5
first Sample
for Adjustment visc 6250 cps
MEK 75 35.29412% added
THF 75 35.29412% M 30
Cyclohexanone 62.5 29.41176% T 30
Total 212.5 C 25
total 85
 d in reactor at room temperature @30 c and agitation starts
0 and calcuim sterate added in MEK and aggitation speed raises to 60 hz with temperature @31 c
ng dd THF and cyclohexane propor aggitation
tart for 30 mints when temperature @ 38 or 40 comes , heating off
m 250 and solvim 275
ng aggitate 2 hrs

cosity in range.

2nd sample 3rd Sample

visc 5110 visc 4480
added
35% M 11 35%
35% T 11 35%
29% C 9 29%
total 31
ture @31 c