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27.01.

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27.01.2006 N 40



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16 ( 5 .) 3
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18 25, 50, 100 10
19 0,1, 0,2, 1,0, 2,0, 5,0 10,0 10
20 50, 100, 250, 500 3
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23 250 10
24 3, 6, 25 10
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26 5, 10, 2 10
27 10 50
28 12 () 50
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27.01.2006 N 40


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1 "", ""
2 25% ""
3 "", ""
4 "", ""
5 "", ""
6 0,2%
7 "", ""
8 "", "" " , 0 1"
9 "", ""
10 "", ""
11 BSTFA + 1% TMCS bis (trimethylsilyl) trifluoroacetamide + 1% trimethylchlorosilane
12 ()
13 "", ""
14 "", ""
15
16 , ,
17 "", ""
18 "", ""
19 "", ""
20 - Helix Potatia
21 "", ""
22 "", ""
23 "", ""
24 "", ""
25 "", ""
26 "", ""
27 "", ""
28
29 "", ""
30 "", ""
31
32 "", ""
33 "", ""
34 "", ""
35 "", ""
36 "", ""
37 "", ""
38 "", ""
39 "", ""
40 "", ""
41 "", ""
42 "", ""
43 "", ""
44 "", ""
45 "", ""
46 "", ""
47 "", ""
48 "", ""
49 - "", ""
50 "", ""
51 ( ) "", ""
52 98%
53 "", ""
54 "", ""
55 "", ""
56 98%
57 MBTFA N-methyl-bis-triflyoroacetamide
58 MBTFA N-methyl-N-trimethylsilil-triftoracetamide
59 MTBSTFA N-tret-buthyldimethylsilil-N- methyltriftoracetamide
60 "", ""
61 "", ""
62 "", ""
63 "", ""
64 / ""
65 / ""
66 "", ""
67 () ""
68 "", ""
69 1- "", ""
70 2- "", ""
71 "", ""
72 "", ""
73 "", ""
74 "", ""
75 N-a- "", ""
76 B- "", ""
77 "", ""
78 - "", ""
79 ()
80 33%
81 70%
82 ""
83 ( ) "", ""
84 155 (-1500, 1540)
85 PFPA Pentafluoropropionic anhydride
86 "", ""
87 "", ""
88 "", ""
89 "", ""
90 "", ""
91
92
93 -
94 - ""
95 - ""
96 - ""
97 - ""
98 - ""
99 - ""
100 - ""
101 ""
102 () ,

103 ""
104 ()
105 "", ""
106 X-100,(X-305)
107 1,2,3--(2-)-
108 ""
109 ""
110
111 TFAA trifluoroacetic anhydride
112
113 , pH 0 - 12,
114 ""
115 ""
116 "", ""
117 2- "" " " "", ""
118 C-22 (: -545, , , )
119 "", ""
120 "", ""
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27.01.2006 N 40



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27.01.2006 N 40


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27.01.2006 N 40



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27.01.2006 N 40


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27.01.2006 N 40



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27.01.2006 N 40


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27.01.2006 N 40



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27.01.2006 N 40


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27.01.2006 N 40



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27.01.2006 N 40


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27.01.2006 N 40

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27.01.2006 N 40


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