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C
1H A P T E R

Introduction to
Radiographic Testing

Harold Berger, Industrial Quality, Incorporated,


Gaithersburg, Maryland (Part 3)
Holger H. Streckert, General Atomics, San Diego,
California (Part 4)
Marvin W. Trimm, Westinghouse Savannah River
Company, Aiken, South Carolina (Parts 1 and 2)
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PART 1. Nondestructive Testing1

Nondestructive testing (NDT) has been sampling. Sampling (that is, less than
defined as comprising those test methods 100 percent testing to draw inferences
used to examine or inspect a part or about the unsampled lots) is
material or system without impairing its nondestructive testing if the tested sample
future usefulness.1 The term is generally is returned to service. If the steel is tested
applied to nonmedical investigations of to verify the alloy in some bolts that can
material integrity. then be returned to service, then the test
Strictly speaking, this definition of is nondestructive. In contrast, even if
nondestructive testing includes spectroscopy used in the chemical testing
noninvasive medical diagnostics. X-rays, of many fluids is inherently
ultrasound and endoscopes are used by nondestructive, the testing is destructive if
both medical and industrial the samples are poured down the drain
nondestructive testing. Medical after testing.
nondestructive testing, however, has come Nondestructive testing is not confined
to be treated by a body of learning so to crack detection. Other discontinuities
separate from industrial nondestructive include porosity, wall thinning from
testing that today most physicians do not corrosion and many sorts of disbonds.
use the word nondestructive. Nondestructive material characterization
Nondestructive testing is used to is a growing field concerned with material
investigate specifically the material properties including material
integrity of the test object. A number of identification and microstructural
other technologies for instance, radio characteristics such as resin curing, case
astronomy, voltage and amperage hardening and stress that have a direct
measurement and rheometry (flow influence on the service life of the test
measurement) are nondestructive but object.
are not used specifically to evaluate Nondestructive testing has also been
material properties. Radar and sonar are defined by listing or classifying the
classified as nondestructive testing when various techniques.1-3 This sense of
used to inspect dams, for instance, but nondestructive testing is practical in that it
not when they are used to chart a river typically highlights methods in use by
bottom. industry.
Nondestructive testing asks Is there
something wrong with this material? In
contrast, performance and proof tests ask
Does this component work? It is not Purposes of
considered nondestructive testing when Nondestructive Testing
an inspector checks a circuit by running
electric current through it. Hydrostatic Since the 1920s, the art of testing without
pressure testing is another form of proof destroying the test object has developed
testing, one that may destroy the test from a laboratory curiosity to an
object. indispensable tool of fabrication,
Another gray area that invites various construction and manufacturing
interpretations in defining nondestructive processes. No longer is visual testing of
testing is future usefulness. Some material materials, parts and complete products
investigations involve taking a sample of the principal means of determining
the inspected part for testing that is adequate quality. Nondestructive tests in
inherently destructive. A noncritical part great variety are in worldwide use to
of a pressure vessel may be scraped or detect variations in structure, minute
shaved to get a sample for electron changes in surface finish, the presence of
microscopy, for example. Although future cracks or other physical discontinuities, to
usefulness of the vessel is not impaired by measure the thickness of materials and
the loss of material, the procedure is coatings and to determine other
inherently destructive and the shaving characteristics of industrial products.
itself in one sense the true test object Scientists and engineers of many
has been removed from service countries have contributed greatly to
permanently. nondestructive test development and
The idea of future usefulness is relevant applications.
to the quality control practice of The various nondestructive testing
methods are covered in detail in the

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literature but it is always wise to consider fluctuates and reverses at low or high
objectives before details. How is frequencies. Frequency of stress reversals
nondestructive testing useful? Why do increases with the speeds of modern
thousands of industrial concerns buy the machines and thus parts tend to fatigue
testing equipment, pay the subsequent and fail more rapidly.
operating costs of the testing and even Another cause of increased stress on
reshape manufacturing processes to fit the modern products is a reduction in the
needs and findings of nondestructive safety factor. An engineer designs with
testing? certain known loads in mind. On the
Modern nondestructive tests are used supposition that materials and
by manufacturers (1) to ensure product workmanship are never perfect, a safety
integrity and, in turn, reliability; (2) to factor of 2, 3, 5 or 10 is applied. However,
avoid failures, prevent accidents and save because of other considerations, a lower
human life (see Figs. 1 and 2); (3) to make factor is often used that depends on the
a profit for the user; (4) to ensure importance of lighter weight or reduced
customer satisfaction and maintain the cost or risk to consumer.
manufacturers reputation; (5) to aid in New demands on machinery have also
better product design; (6) to control stimulated the development and use of
manufacturing processes; (7) to lower new materials whose operating
manufacturing costs; (8) to maintain characteristics and performance are not
uniform quality level; and (9) to ensure completely known. These new materials
operational readiness. create greater and potentially dangerous
These reasons for widespread and problems. As an example, an aircraft part
profitable nondestructive testing are was built from an alloy whose work
sufficient in themselves but parallel hardening, notch resistance and fatigue
developments have contributed to its life were not well known. After relatively
growth and acceptance. short periods of service some of these
aircraft suffered disastrous failures.
Increased Demand on Machines Sufficient and proper nondestructive tests
could have saved many lives.
In the interest of greater speed and As technology improves and as service
reduced cost for materials, the design requirements increase, machines are
engineer is often under pressure to reduce subjected to greater variations and to
weight. This can sometimes be done by wider extremes of all kinds of stress,
substituting aluminum alloys, magnesium creating an increasing demand for
alloys or composite materials for steel or stronger or more damage tolerant
iron but such light parts may not be the materials.
same size or design as those they replace.
The tendency is also to reduce the size.
These pressures on the designer have Engineering Demands for Sounder
subjected parts of all sorts to increased Materials
stress levels. Even such commonplace Another justification for nondestructive
objects as sewing machines, sauce pans tests is the designers demand for sounder
and luggage are also lighter and more
heavily loaded than ever before. The stress
to be supported is seldom static. It often
FIGURE 2. Boilers operate with high internal steam pressure.
Material discontinuites can lead to sudden, violent failure
with possible injury to people and property.
FIGURE 1. Fatigue cracks caused damage to aircraft fuselage,
causing death of flight attendant and injury to passengers
(April 1988).

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materials. As size and weight decrease and of several others. Loss of such production
the factor of safety is lowered, more is one of the greatest losses resulting from
emphasis is placed on better raw material part failure.
control and higher quality of materials,
manufacturing processes and
workmanship.
An interesting fact is that a producer of Applications of
raw material or of a finished product Nondestructive Testing
sometimes does not improve quality or
performance until that improvement is Nondestructive testing is a branch of the
demanded by the customer. The pressure materials sciences that is concerned with
of the customer is transferred to all aspects of the uniformity, quality and
implementation of improved design or serviceability of materials and structures.
manufacturing. Nondestructive testing is The science of nondestructive testing
frequently called on to deliver this new incorporates all the technology for
quality level. detection and measurement of significant
properties, including discontinuities, in
items ranging from research specimens to
Public Demands for Greater Safety finished hardware and products in service.
The demands and expectations of the By definition, nondestructive testing
public for greater safety are apparent methods are means for examining
everywhere. Review the record of the materials and structures without
courts in granting high awards to injured disruption or impairment of serviceability.
persons. Consider the outcry for greater Nondestructive testing makes it possible
automobile safety, as evidenced by the for internal properties or hidden
required automotive safety belts and the discontinuities to be revealed or inferred
demand for air bags, blowout proof tires by appropriate methods.
and antilock braking systems. The Nondestructive testing is becoming
publicly supported activities of the increasingly vital in the effective conduct
National Safety Council, Underwriters of research, development, design and
Laboratories, the Occupational Safety and manufacturing programs. Only with
Health Administration and the Federal appropriate nondestructive testing
Aviation Administration in the United methods can the benefits of advanced
States, as well as the work of similar materials science be fully realized. The
agencies abroad, are only a few of the information required for appreciating the
ways in which this demand for safety is broad scope of nondestructive testing is
expressed. It has been expressed directly available in many publications and
by passengers who cancel reservations reports.
following a serious aircraft accident. This
demand for personal safety has been
another strong force in the development
of nondestructive tests. Classification of Methods
In a report, the National Materials
Rising Costs of Failure Advisory Board (NMAB) Ad Hoc
Committee on Nondestructive Evaluation
Aside from awards to the injured or to adopted a system that classified
estates of the deceased and aside from techniques into six major method
costs to the public (because of evacuation categories: visual, penetrating radiation,
occasioned by chemical leaks), consider magnetic-electrical, mechanical vibration,
briefly other factors in the rising costs of thermal and chemical/electrochemical.3 A
mechanical failure. These costs are modified version is presented in Table 1.1
increasing for many reasons. Some Each method can be completely
important ones are (1) greater costs of characterized in terms of five principal
materials and labor; (2) greater costs of factors: (1) energy source or medium used
complex parts; (3) greater costs because of to probe object (such as X-rays, ultrasonic
the complexity of assemblies; (4) greater waves or thermal radiation); (2) nature of
probability that failure of one part will the signals, image or signature resulting
cause failure of others because of from interaction with the object
overloads; (5) trend to lower factors of (attenuation of X-rays or reflection of
safety; (6) probability that the failure of ultrasound, for example); (3) means of
one part will damage other parts of high detecting or sensing resultant signals
value; and (7) part failure in an integrated (photoemulsion, piezoelectric crystal or
automatic production machine, shutting inductance coil); (4) method of indicating
down an entire high speed production or recording signals (meter deflection,
line. When production was carried out on oscilloscope trace or radiograph); and
many separate machines, the broken one (5) basis for interpreting the results (direct
could be bypassed until repaired. Today, or indirect indication, qualitative or
one machine is tied into the production quantitative and pertinent dependencies).

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The objective of each method is to Classification Relative to Test


provide information about the following Object
material parameters: (1) discontinuities
and separations (cracks, voids, inclusions Nondestructive testing techniques may be
delaminations and others); (2) structure or classified according to how they detect
malstructure (crystalline structure, grain indications relative to the surface of a test
size, segregation, misalignment and object. Surface methods include liquid
others); (3) dimensions and metrology penetrant testing, visual testing, grid and
(thickness, diameter, gap size, moir testing. Surface/near-surface
discontinuity size and others); (4) physical methods include tap, potential drop,
and mechanical properties (reflectivity, holography and shearography, magnetic
conductivity, elastic modulus, sonic particle and electromagnetic testing.
velocity and others); (5) composition and When surface or surface/near-surface
chemical analysis (alloy identification, methods are applied during intermediate
impurities, elemental distributions and manufacturing processes, they provide
others); (6) stress and dynamic response preliminary assurance that volumetric
(residual stress, crack growth, wear, methods performed on the completed
vibration and others); (7) signature object or component will reveal few
analysis (image content, frequency rejectable discontinuities. Volumetric
spectrum, field configuration and others); methods include radiography, ultrasonic
and (8) abnormal sources of heat. testing, acoustic emission testing and less
Terms used in this block are further widely used methods such as
defined in Table 2 with respect to specific acoustoultrasonic testing and magnetic
objectives and specific attributes to be resonance imaging. Through-boundary
measured, detected and defined. techniques described include leak testing,
The limitations of a method include some infrared thermographic techniques,
conditions required by that method: airborne ultrasonic testing and certain
conditions to be met for method techniques of acoustic emission testing.
application (access, physical contact, Other less easily classified methods are
preparation and others) and requirements material identification, vibration analysis
to adapt the probe or probe medium to and strain gaging.
the object examined. Other factors limit No one nondestructive testing method
the detection or characterization of is all revealing. That is not to say that one
discontinuities, properties and other method or technique of a method is
attributes and limit interpretation of rarely adequate for a specific object or
signals or images generated. component. However, in most cases it
takes a series of test methods to do a
complete nondestructive test of an object

TABLE 1. Nondestructive testing method categories.


Categories Objectives

Basic Categories

Mechanical and optical color; cracks; dimensions; film thickness; gaging; reflectivity; strain distribution and magnitude; surface
finish; surface flaws; through-cracks
Penetrating radiation cracks; density and chemistry variations; elemental distribution; foreign objects; inclusions; microporosity;
misalignment; missing parts; segregation; service degradation; shrinkage; thickness; voids
Electromagnetic and electronic alloy content; anisotropy; cavities; cold work; local strain, hardness; composition; contamination;
corrosion; cracks; crack depth; crystal structure; electrical conductivities; flakes; heat
treatment; hot tears; inclusions; ion concentrations; laps; lattice strain; layer thickness; moisture content;
polarization; seams; segregation; shrinkage; state of cure; tensile strength; thickness; disbonds
Sonic and ultrasonic crack initiaion and propagation; cracks, voids; damping factor; degree of cure; degree of impregnation;
degree of sintering; delaminations; density; dimensions; elastic moduli; grain size; inclusions;
mechanical degradation; misalignment; porosity; radiation degradation; structure of composites; surface
stress; tensile, shear and compressive strength; disbonds; wear
Thermal and infrared anisotropy, bonding; composition; emissivity; heat contours; plating thickness; porosity; reflectivity; stress;
thermal conductivity; thickness; voids; cracks; delaminations; heat treatment; state of cure; moisture;
corrosion
Chemical and analytical alloy identification; composition; cracks; elemental analysis and distribution; grain size; inclusions;
macrostructure; porosity; segregation; surface anomalies
Auxiliary Categories
Image generation dimensional variations; dynamic performance; anomaly characterization and definition; anomaly
distribution; anomaly propagation; magnetic field configurations
Signal image analysis data selection, processing and display; anomaly mapping, correlation and identification; image
enhancement; separation of multiple variables; signature analysis

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or component. For example, if surface situations, if internal discontinuities were


cracks must be detected and eliminated to be detected, then ultrasonic testing or
and the object or component is made of radiography would be the selection. The
ferromagnetic material, then magnetic exact technique in either case would
particle testing would be the obvious depend on the thickness and nature of
choice. If that same material is aluminum the material and the types of
or titanium, then the choice would be discontinuities that must be detected.
liquid penetrant or electromagnetic
testing. However, for either of these

TABLE 2. Objectives of nondestructive testing methods.

Objectives Attributes Measured or Detected

Discontinuites and separations


Surface anomalies roughness; scratches; gouges; crazing; pitting; inclusions and imbedded foreign material
Surface connected anomalies cracks; porosity; pinholes; laps; seams; folds; inclusions
Internal anomalies cracks; separations; hot tears; cold shuts; shrinkage; voids; lack of fusion; pores; cavities; delaminations;
disbonds; poor bonds; inclusions; segregations
Structure
Microstructure molecular structure; crystalline structure and/or strain; lattice structure; strain; dislocation; vacancy;
deformation
Matrix structure grain structure, size, orientation and phase; sinter and porosity; impregnation; filler and/or reinforcement
distribution; anisotropy; heterogeneity; segregation
Small structural anomalies leaks (lack of seal or through-holes); poor fit; poor contact; loose parts; loose particles; foreign objects
Gross structural anomalies assembly errors; misalignment; poor spacing or ordering; deformation; malformation; missing parts
Dimensions and metrology
Displacement; position linear measurement; separation; gap size; discontinuity size, depth, location and orientation
Dimensional variations unevenness; nonuniformity; eccentricity; shape and contour; size and mass variations
Thickness; density film, coating, layer, plating, wall and sheet thickness; density or thickness variations
Physical and mechanical properties
Electrical properties resistivity; conductivity; dielectric constant and dissipation factor
Magnetic properties polarization; permeability; ferromagnetism; cohesive force
Thermal properties conductivity; thermal time constant and thermoelectric potential; diffusivity; effusivity; specific heat
Mechanical properties compressive, shear and tensile strength (and moduli); Poissons ratio; sonic velocity; hardness; temper and
embrittlement
Surface properties color; reflectivity; refraction index; emissivity
Chemical composition and analysis
Elemental analysis detection; identification, distribution and/or profile
Impurity concentrations contamination; depletion; doping and diffusants
Metallurgical content variation; alloy identification, verification and sorting
Physiochemical state moisture content; degree of cure; ion concentrations and corrosion; reaction products
Stress and dynamic response
Stress; strain; fatigue heat treatment, annealing and cold work effects; residual stress and strain; fatigue damage and life (residual)
Mechanical damage wear; spalling; erosion; friction effects
Chemical damage corrosion; stress corrosion; phase transformation
Other damage radiation damage and high frequency voltage breakdown
Dynamic performance crack initiation and propagation; plastic deformation; creep; excessive motion; vibration; damping; timing of
events; any anomalous behavior
Signature analysis
Electromagnetic field potential; strength; field distribution and pattern
Thermal field isotherms; heat contours; temperatures; heat flow; temperature distribution; heat leaks; hot spots; contrast
Acoustic signature noise; vibration characteristics; frequency amplitude; harmonic spectrum and/or analysis; sonic and/or
ultrasonic emissions
Radioactive signature distribution and diffusion of isotopes and tracers
Signal or image analysis image enhancement and quantization; pattern recognition; densitometry; signal classification, separation;
and correlation; discontinuity identification, definition (size and shape) and distribution analysis;
discontinuity mapping and display

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nondestructive testing at the end of a


Value of Nondestructive manufacturing process. This approach will
ultimately increase production costs.
Testing When used properly, nondestructive
The contribution of nondestructive testing saves money for the manufacturer.
testing to profits has been acknowledged Rather than costing the manufacturer
in the medical field and computer and money, nondestructive testing should add
aerospace industries. However, in profits to the manufacturing process.
industries such as heavy metals, though
nondestructive testing may be reluctantly
accepted its contribution to profits may
not be obvious to management. Overview of
Nondestructive testing is sometimes Nondestructive Testing
thought of only as a cost item. One
possible reason is industry downsizing.
Methods
When a company cuts costs, two To optimize the use of nondestructive
vulnerable areas are quality and safety. testing, it is necessary first to understand
When bidding contract work, companies the principles and applications of all the
add profit margin to all cost items, methods. This book features radiographic
including nondestructive testing, so a testing (Fig. 3) only one of the
profit should be made on the nondestructive testing methods. Several
nondestructive testing. However, when other methods and the applications
production is going poorly and it is associated with them are briefly described
anticipated that a job might lose money, next.
it seems like the first corner that
production personnel will try to cut is Visual Testing
nondestructive testing. This is
accomplished by subtle pressure on Principles. Visual testing (Fig. 4) is the
nondestructive testing technicians to observation of a test object, either directly
accept a product that does not quite meet with the eyes or indirectly using optical
a code or standard requirement. The instruments, by an inspector to evaluate
attitude toward nondestructive testing is the presence of surface anomalies and the
gradually improving as management objects conformance to specification.
comes to appreciate its value. Visual testing should be the first
Nondestructive testing should be used nondestructive testing method applied to
as a control mechanism to ensure that an item. The test procedure is to clean the
manufacturing processes are within design surface, provide adequate illumination
performance requirements. It should and observe. A prerequisite necessary for
never be used in an attempt to obtain competent visual testing of an item is
quality in a product by using knowledge of the manufacturing processes
by which it was made, its service history,
potential failure modes and related
industry experience.
FIGURE 3. Representative setup for radiographic test.
Applications. Visual testing provides a
means of detecting and examining a
Radiation source variety of surface discontinuities. It is also

FIGURE 4. Visual test using borescope to


view interior of cylinder.

Specimen
Void

Image plane Discontinuity images

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the most widely used method for surface discontinuities, seams, cracks, laps,
detecting and examining for surface porosity and leak paths.
discontinuities associated with various
structural failure mechanisms. Even when Magnetic Particle Testing
other nondestructive tests are performed,
visual tests often provide a useful Principles. Magnetic particle testing is a
supplement. For example, when the eddy method of locating surface and slightly
current testing of process tubing is subsurface discontinuities in
performed, visual testing is often ferromagnetic materials. It depends on the
performed to verify and more closely fact that when the material or part under
examine the surface condition. This test is magnetized, discontinuities that lie
verification process can impact the in a direction generally transverse to the
evaluation process associated with other direction of the magnetic field will cause a
nondestructive test methods being used. leakage field to be formed at and above
The following discontinuities may be the surface of the part. The presence of
detected by a simple visual test: surface this leakage field and therefore the
discontinuities, cracks, misalignment, presence of the discontinuity is detected
warping, corrosion, wear and physical by the use of finely divided ferromagnetic
damage. particles applied over the surface, with
some of the particles being gathered and
held to form an outline of the
Liquid Penetrant Testing discontinuity. This generally indicates its
Principles. Liquid penetrant testing (Fig. 5) location, size, shape and extent. Magnetic
reveals discontinuities open to the particles are applied over a surface as dry
surfaces of solid and nonporous materials. particles or as wet particles in a liquid
Indications of a wide spectrum of carrier such as water or oil.
discontinuity sizes can be found regardless Applications. The principal industrial uses
of the configuration of the workpiece and of magnetic particle testing are for final,
regardless of discontinuity orientations. receiving and in-process testing; for
Liquid penetrants seep into various types quality control; for maintenance and
of minute surface openings by capillary overhaul in the transportation industries;
action. The cavities of interest can be very for plant and machinery maintenance;
small, often invisible to the unaided eye. and for testing of large components. Some
The ability of a given liquid to flow over a of the typically detected discontinuities
surface and enter surface cavities depends are surface discontinuities, seams, cracks
principally on the following: cleanliness and laps.
of the surface, surface tension of the
liquid, configuration of the cavity, contact
angle of the liquid, ability of the liquid to Eddy Current Testing
wet the surface, cleanliness of the cavity Principles. Based on electromagnetic
and size of surface opening of the cavity. induction, eddy current testing (Fig. 6) is
Applications. The principal industrial uses used to identify or differentiate among a
of liquid penetrant testing are final
testing, receiving testing, in-process
testing and quality control, maintenance
and overhaul in the transportation FIGURE 6. Representative setup for eddy current test.
industries, in plant and machinery
maintenance and in testing of large Primary electromagnetic field
components. The following are some of Coil in eddy current probe
the typically detected discontinuities:

Direction of
FIGURE 5. Liquid penetrant indication of primary current
cracking.

Induced field

Direction of eddy
currents
Conducting specimen
Eddy current strength
decreases with
increasing depth

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wide variety of physical, structural and Applications. An important industrial use


metallurgical conditions in electrically of eddy current testing is on heat
conductive ferromagnetic and exchanger tubing. For example, eddy
nonferromagnetic metals and metal parts. current testing is often specified for thin
The method is based on indirect wall tubing in pressurized water reactors,
measurement and on correlation between steam generators, turbine condensers and
the instrument reading and the structural air conditioning heat exchangers. Eddy
characteristics and serviceability of the current testing is also used often in
parts being examined. aircraft maintenance. The following are
With a basic system, the part is placed some of the typical material
within or adjacent to an electric coil in characteristics that can be evaluated by
which high frequency alternating current eddy current testing: cracks, inclusions,
is flowing. This excitation current dents and holes; grain size and hardness;
establishes an electromagnetic field coating and material thickness;
around the coil. This primary field causes dimensions and geometry; composition,
eddy current to flow in the part because conductivity or permeability; and alloy
of electromagnetic induction. Inversely, composition.
the eddy currents affected by all
characteristics (conductivity, permeability, Ultrasonic Testing
thickness, discontinuities and geometry)
of the part create a secondary magnetic Principles. Ultrasonic testing (Fig. 7) is a
field that opposes the primary field. The nondestructive method in which beams of
results of this interaction affect the coil sound waves at a frequency too high to
voltage and can be displayed in a variety hear are introduced into materials for the
of methods. detection of surface and subsurface
Eddy currents flow in closed loops in discontinuities in the material. These
the part or air. Their two most important acoustic waves travel through the material
characteristics, amplitude and phase, are with some attendant loss of energy
influenced by the arrangement and (attenuation) and are reflected at
characteristics of the instrumentation and interfaces. The reflected beam is displayed
test piece. For example, during the test of (or reduces the display of transmitted
a tube the eddy currents flow sound) and is then analyzed to define the
symmetrically in the tube when presence and locations of discontinuities
discontinuities are not present. However, or discontinuities.
when a crack is present, then the eddy Applications. Ultrasonic testing of metals
current flow is impeded and changed in is widely used, principally for the
direction, causing significant changes in detection of discontinuities. This method
the associated electromagnetic field. can be used to detect internal

FIGURE 7. Representative setups for ultrasonic testing: (a) longitudinal wave technique; (b) shear wave
technique.

(a) (b)

Crack

Crack

Time

Bolt Entry surface

Back surface Crack

a b
Transducer
Skip distance
Crack

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discontinuities in most engineering The source of acoustic emission energy


metals and alloys. Bonds produced by is the elastic stress field in the material.
welding, brazing, soldering and adhesive Without stress, there is no emission.
bonding can also be ultrasonically Therefore, an acoustic emission test
examined. Inline techniques have been (Fig. 8) is usually carried out during a
developed for monitoring and classifying controlled loading of the structure. This
materials as acceptable, salvageable or can be a proof load before service; a
scrap and for process control. Other controlled variation of load while the
applications include testing of piping and structure is in service; a fatigue, pressure
pressure vessels, nuclear systems, motor or creep test; or a complex loading
vehicles, machinery, structures, railroad program. Often, a structure is going to be
rolling stock and bridges and thickness loaded hydrostatically anyway during
measurement. service and acoustic emission testing is
used because it gives valuable additional
Leak Testing information about the expected
performance of the structure under load.
Principles. Leak testing is concerned with Other times, acoustic emission testing is
the flow of liquids or gases from selected for reasons of economy or safety
pressurized or into evacuated components and a special loading procedure is
or systems intended to hold fluids. The arranged to meet the needs of the acoustic
principles of leak testing involve the emission test.
physics of fluid (liquids or gases) flowing
Applications. Acoustic emission is a
through a barrier where a pressure
natural phenomenon occurring in the
differential or capillary action exists.
widest range of materials, structures and
Leaking fluids (liquid or gas) can
processes. The largest scale events
propagate from inside a component or
observed with acoustic emission testing
assembly to the outside, or vice versa, as a
are seismic and the smallest are small
result of a pressure differential between
dislocations in stressed metals.
the two regions or as a result of
The equipment used is highly sensitive
permeation through a barrier. The
to any kind of movement in its operating
importance of leak testing depends on the
frequency (typically 20 to 1200 kHz). The
size of the leak and on the medium being
equipment can detect not only crack
leaked. Leak testing encompasses
growth and material deformation but also
procedures that fall into these basic
functions: leak location, leakage
measurement and leakage monitoring.
Applications. Like other forms of FIGURE 8. Acoustic emission testing setup in which eight
nondestructive testing, leak testing has a sensors permit computer to calculate location of crack
great impact on the safety and propagation.
performance of a product. Reliable leak
testing decreases costs by reducing
number of reworked products, warranty Acoustic
repairs and liability claims. The most event
common reasons for performing a leak
test are to prevent the loss of costly Preamplifier
materials or energy; to prevent
contamination of the environment; to
ensure component or system reliability;
and to prevent the potential for an
explosion or fire.

Acoustic Emission Testing


Principles. Acoustic emissions are stress
waves produced by sudden movement in
stressed materials. The classic source of
acoustic emission is discontinuity related
deformation processes such as crack
growth and plastic deformation. Sudden Computer
movement at the source produces a stress
wave that radiates out into the structure
and excites a sensitive piezoelectric sensor.
As the stress in the material is raised,
emissions are generated. The signals from Test
one or more sensors are amplified and object
measured to produce data for display and
interpretation.

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such process as solidification, friction, through the connection produces an


impact, flow and phase transformations. increase in surface temperature of the
Therefore, acoustic emission testing is also connection.
used for in-process weld monitoring, Applications. There are two basic
detecting tool touch and tool wear during categories of infrared and thermal test
automatic machining, detecting wear and applications: electrical and mechanical.
loss of lubrication in rotating equipment, The specific applications within these two
detecting loose parts and loose particles, categories are numerous. Electrical
detecting and monitoring leaks, applications include transmission and
cavitation, flow, preservice proof testing, distribution lines, transformers,
in-service weld monitoring and leak disconnects, switches, fuses, relays,
testing. breakers, motor windings, capacitor
banks, cable trays, bus taps and other
Infrared and Thermal Testing components and subsystems. Mechanical
applications include insulation (in boilers,
Principles. Conduction and convection
furnaces, kilns, piping, ducts, vessels,
are the primary mechanisms of heat
refrigerated trucks and systems, tank cars
transfer in an object or system. However,
and elsewhere), friction in rotating
electromagnetic radiation is emitted from
equipment (bearings, couplings, gears,
a heated body when electrons in that
gearboxes, conveyor belts, pumps,
body change to a lower energy state.
compressors and other components) and
Thermal testing involves the
fluid flow (steam lines; heat exchangers;
measurement or mapping of surface
tank fluid levels; exothermic reactions;
temperatures when heat flows from, to or
heating, ventilation and air conditioning
through a test object. Temperature
systems; leaks above and below ground;
differentials on a surface, or changes in
cooling and heating; tube blockages;
surface temperature with time, are related
systems; environmental assessment of
to heat flow patterns and can be used to
thermal discharge; boiler or furnace air
detect anomalies or to determine the heat
leakage; condenser; turbine air leakage;
transfer characteristics of an object. For
pumps; compressors; and other system
example, during the operation of an
applications).
electrical breaker, a hot spot detected at
an electrical termination may be caused
by a loose or corroded connection (see Other Methods
Fig. 9). The resistance to electrical flow There are many other methods of
nondestructive testing, including optical
methods such as holography,
FIGURE 9. Infrared thermography of shearography and moir imaging; material
automatic transfer switches of emergency identification methods such as chemical
diesel generator. Hot spots appear bright in spot testing, spark testing and
thermogram. spectroscopy; strain gaging; and acoustic
methods such as vibration analysis and
tapping.

Introduction to Radiographic Testing 11


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PART 2. Management of Radiographic Testing

Radiography may be considered the most


effective nondestructive testing method
merely because of its universal use and
Management of
acceptance in industry. Radiography can Radiographic Testing
be used to test most types of solid Programs
material. Exceptions include materials of
Management of a radiographic testing
very high or very low density. Neutron
program will require consideration of
radiography, however, can often be used
many items before a program can produce
in such cases. There is wide latitude both
the desired results. Six basic questions
of material thickness that can be tested
must be answered before a true direction
and in the techniques that can be used.
can be charted. They are as follows.
Usually conditions that result in a two
percent or greater difference in 1. Are regulatory requirements in place
through-section thickness can usually be that mandate program characteristics?
detected. 2. What is the magnitude of the program
Radiography has three main that will provide desired results?
advantages: (1) detection of internal 3. What provisions must be made for
discontinuities, (2) detection of significant personnel safety and for compliance
variations in composition and with environmental regulations?
(3) permanent record of test data. 4. What is the performance date for a
Compared to other nondestructive test program to be fully implemented?
methods, radiography can be expensive. 5. Is there a cost benefit of radiographic
Large capital costs and space allocations testing?
may be required for radiographic 6. What are the available resources in
activities. Cost may be reduced if personnel and money?
equipment of smaller size or lower energy Once these questions are answered, then a
requirement can be used. The magnitude recommendation can be made to
of potential test activities, however, must determine the best path forward. Three
be considered before limits are placed on primary paths are (1) service companies,
the test facility. (2) consultants and (3) in-house programs.
There are three major limiting factors Though these are primary paths, some
that must be considered before programs may on a routine or on
radiography becomes the method of as-needed bases require support personnel
choice. from a combination of two or more of
1. Discontinuity detection depends on these sources. Before a final decision is
radiation beam orientation. In general, made, advantages and disadvantages of
radiography can detect only features each path must be considered. Therefore,
that have a thickness change in a the following are details that must be
direction parallel to the radiation considered.
beam.
2. Radiography typically involves the Service Companies
transmission of radiation through the
part or component, in which case 1. Who will identify the components
both sides of the part must be within the facility to be examined?
accessible. 2. Will the contract be for time and
3. Radiation safety is always necessary to materials or have a specific scope of
a successful operation. work?
In addition, radiographic images (in 3. If a time and materials contract is
the form of film or digital images) may awarded, who will monitor the time
need to be stored for years to comply with and materials charged?
quality assurance or regulatory 4. If a scope of work is required, who is
requirements. technically qualified to develop and
approve it?
5. What products or documents (test
reports, trending, recommendations,
root cause analysis and others) will be
provided once the tests are completed?

12 Radiographic Testing
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6. Who will evaluate and accept the 2. What are the regulatory requirements
product (test reports, trending, (codes and standards) associated with
recommendations, root cause analysis program development and
and others) within your company? implementation?
7. Do the service company workers 3. Who will develop a cost benefit
possess qualifications and analysis for the program?
certifications required by contract and 4. How much time and resources are
by applicable regulations? Will other available to establish the program?
contractors be required to take care of 5. What are the qualification
related matters such as radiation requirements (education, training,
safety? experience and others) for personnel?
8. Do the service company workers 5. Do program personnel require
require site specific training (confined additional training (radiological safety,
space entry, electrical safety, hazardous confined space entry or others) or
materials and others) or clearance to qualifications?
enter and work in the facility? 6. Are subject matter experts required to
9. If quantitative tests are performed, do provide technical guidance during
program requirements mandate personnel development?
equipment calibration? 7. Are procedures required to perform
10. Does the service company retain any work in the facility?
liability for test results? 8. If procedures are required, who will
develop, review and approve them?
9. Who will determine the technical
Consultants specifications for test equipment?
1. Will the contract be for time and
materials or have a specific scope of
work?
2. If a scope of work is required, who is Test Procedures for
technically qualified to develop and Radiographic Testing
approve it? The conduct of facility operations
3. Who will identify the required (in-house or contracted) should be
qualifications of the consultant? performed in accordance with specific
4. Is the purpose of the consultant to instructions from an expert. This is
develop or update a program or is it to typically accomplished using written
oversee and evaluate the performance instructions in the form of a technical
of an existing program? procedure. In many cases codes and
5 Will the consultant have oversight specifications will require the use of a
responsibility for tests performed? technical procedure to perform required
6. What products (trending, tests.
recommendations, root cause analysis The procedure process can take many
and others) are provided once the tests forms, including general instructions that
are completed? address only major aspects of test
7. Who will evaluate the consultants techniques. Or a procedure may be
performance (test reports, trending, written as a step-by-step process requiring
recommendations, root cause analysis a supervisors initial or signature after
and other functions) within your each step. The following is a typical
company? format for an industrial procedure.
8. Does the consultant possess
qualifications and certifications 1. The purpose identifies the intent of the
required by contract and by applicable procedure.
regulations? 2. The scope establishes the latitude of
9. Does the consultant require site items, tests and techniques covered
specific training (confined space entry, and not covered by the procedure.
electrical safety, hazardous materials 3. References are specific documents from
and others) or clearance to enter and which criteria are extracted or
work in the facility? documents satisfied by
10. Does the consultant retain any implementation of the procedure.
liability for test results? 4. Definitions are needed for terms and
abbreviations that are not common
knowledge to people who will read the
In-House Programs procedure.
5. Statements about personnel requirements
1. Who will determine the scope of the address specific requirements to
program? Will the radiation source be perform tasks in accordance with the
isotopes or X-ray machines? Will the procedure issues such as personnel
images be recorded on film or on qualification, certification, access
digital media? clearance and others.

Introduction to Radiographic Testing 13


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6. Equipment characteristics, calibration 6. The source intensity (total quantity of


requirements and model numbers of penetrating rays) will directly affect
qualified equipment must be specified. the exposure time. Increased exposure
7. Safety issues must be addressed because time may affect safety requirements.
of the nature of penetrating radiation.
8. The test procedure provides a sequential
process to be used to conduct test Selection of Imaging
activities. Typically an image is the end product of a
9. Acceptance criteria establish component radiographic examination. The image may
characteristics that will identify the be the captured output of a radioscopic or
items suitable for service. electronic imaging system. Its format may
10. Reports (records) provide the means to be a hard copy (film or paper), a computer
document specific test techniques, image file or a video monitor displaying
equipment used, personnel performing an image in real time.
activity, date performed, test results,
compliance with environmental 1. The first consideration is the ability to
regulations and safety procedures. detect discontinuities of interest.
11. Attachments may include (if required) 2. Examination environment.
items such as report forms, instrument 3. Image handling requirements include
calibration forms, qualified equipment provisions for processing, evaluation
matrix, schedules and others and transmitting of images.
Once the procedure is completed,
typically an expert in the subject matter Interpretation
performs a technical evaluation. If the Interpretation may be complex. The
procedure is deemed adequate (meeting interpreter must have a knowledge of the
identified requirements), the expert will following: (1) the radiographic process
approve it for use. Some codes and (radiation source, exposure technique,
standards also require the procedure to be image storage system and other means
qualified that is, demonstrated to the used to obtain the image); (2) the item
satisfaction of a representative of a being examined (its configuration,
regulatory body or jurisdictional material characteristics, fabrication
authority. process, potential discontinuities and
other aspects); and (3) the acceptance
criteria.
Test Specifications for
Radiographic Testing
A radiographic specification must Standards and
anticipate a number of issues that arise Specifications for
during testing. Radiographic Testing
Standards have undergone a process of
Source Selection peer review in industry and can be
The radiation source requirements (energy invoked with the force of law by contract
level, intensity and physical size) to detect or by government regulation. In contrast,
the target discontinuities must be a specification represents an employers
determined. instructions to employees and is specific
1. The selected means of imaging may to a contract or work place. Specifications
dictate source energy and intensity may form the basis of standards through a
levels. review process. Standards and
2. The radiation source may need to be specifications exist in three basic areas:
mobile for use in various locations. equipment, processes and personnel.
3. The energy level (ability to penetrate) 1. Standards for equipment include
of the radiation sources affects calibrated electronic radiation sources
radiographic contrast. Radiographic and isotope sources. Standardized
contrast is an element of image reference objects such as image quality
sensitivity. indicators (penetrameters), calibrated
4. The physical size of the radiation density strips and radiation survey
emitting surface affects the geometric meters would also fit into this
unsharpness of the radiographic category.
image.
5. High energy levels may increase safety
issues because of increased shielding
requirements.

14 Radiographic Testing
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2. ASTM International and other 2. ANSI/ASNT CP-189, Standard for


organizations publish standards for Qualification and Certification of
test techniques. Some other standards Nondestructive Testing Personnel
are for quality assurance procedures resembles SNT-TC-1A but also
and are not specific to a test method establishes specific attributes for the
or even to testing in general. Tables 3 qualification and certification of
and 4 list some of the standards used nondestructive testing personnel.
in radiographic testing. A source for However, CP-189 is a consensus
nondestructive testing standards is the standard as defined by the American
Annual Book of ASTM Standards.5 National Standards Institute (ANSI). It
3. Qualification and certification of test is recognized as the American standard
personnel are discussed below, with for nondestructive testing. It is not
specific reference to recommendations considered a recommended practice; it is
of ASNT Recommended Practice No. a national standard.6
SNT-TC-1A.4 3. The ASNT Central Certification Program
(ACCP), unlike SNT-TC-1A and
CP-189, is a third party certification
process. Currently it has identified
Personnel Qualification qualification and certification
and Certification attributes for Level II and Level III
nondestructive testing personnel. The
One of the most critical aspects of the test American Society for Nondestructive
process is the qualification of test Testing certifies that the individual has
personnel. Nondestructive testing is the skills and knowledge for many
sometimes referred to as a special process. nondestructive testing method
The term simply means that it is very applications. It does not remove the
difficult to determine the adequacy of a responsibility for the final
test by merely observing the process or determination of personnel
the documentation generated at its qualifications from the employer. The
conclusion. The quality of the test is employer evaluates an individuals
largely dependent on the skills and skills and knowledge for application of
knowledge of the inspector. company procedures using designated
The American Society for techniques and identified equipment
Nondestructive Testing (ASNT) has been a for specific tests.7
world leader in the qualification and
certification of nondestructive testing
personnel for many years. By 1999, the Selections from
American Society for Nondestructive ASNT Recommended Practice
Testing had instituted three major
programs in place for the qualification No. SNT-TC-1A
and certification of nondestructive testing To give an overview of the contents of
personnel. these documents, the following items are
1. ASNT Recommended Practice specified in the 1996 edition of
No. SNT-TC-1A provides guidelines for SNT-TC-1A. (For the purpose of this
personnel qualification and discussion the quantities cited are those
certification in nondestructive testing. that address radiographic testing only.)
This recommended practice identifies Scope. This recommended practice has
the specific attributes that should be been prepared to establish guidelines for
considered when qualifying the qualification and certification of
nondestructive testing personnel. It nondestructive testing personnel whose
requires the employer to develop and specific jobs require appropriate
implement a written practice knowledge of the technical principles
(procedure) that details the specific underlying the nondestructive test they
process and any limitation in the perform, witness, monitor or evaluate.
qualification and certification of This document provides guidelines for the
nondestructive testing personnel.4 establishment of a qualification and
certification program.
Written Practice. The employer shall
establish a written practice for the control
and administration of nondestructive
testing personnel training, examination
and certification. The employers written
practice should describe the responsibility
of each level of certification for
determining the acceptability of materials
or components in accordance with
applicable codes, standards, specifications
and procedures.

Introduction to Radiographic Testing 15


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Table 3. Some radiographic standards published by ASTM International.


C 638-92 (1997), Standard Descriptive Nonmenclature of Constituents of Aggregates for Radiation-Shielding Concrete
E 94-00, Standard Guide for Radiographic Examination
E 155-00, Standard Reference Radiographs for Inspection of Aluminum and Magnesium Castings
E 170-99e1, Standard Terminology Relating to Radiation Measurements and Dosimetry
E 186-98, Standard Reference Radiographs for Heavy-Walled (2 to 4 1/2-in. [51 to 114-mm]) Steel Castings
E 192-95 (1999), Standard Reference Radiographs for Investment Steel Castings of Aerospace Applications
E 242-95 (2000), Standard Reference Radiographs for Appearances of Radiographic Images as Certain Parameters Are Changed
E 272-99, Standard Reference Radiographs for High-Strength Copper-Base and Nickel-Copper Alloy Castings
E 280-98, Standard Reference Radiographs for Heavy-Walled (4 1/2 to 12-in. [(114 to 305-mm]) Steel Castings
E 310-99, Standard Reference Radiographs for Tin Bronze Castings
E 390-95, Standard Reference Radiographs for Steel Fusion Welds
E 431-96, Standard Guide to Interpretation of Radiographs of Semiconductors and Related Devices
E 446-98, Standard Reference Radiographs for Steel Castings Up to 2 in. (51 mm) in Thickness
E 505-96, Standard Reference Radiographs for Inspection of Aluminum and Magnesium Die Castings
E 592-99, Standard Guide to Obtainable ASTM Equivalent Penetrameter Sensitivity for Radiography of Steel Plates 1/4 to 2 in. (6 to 51 mm) Thick
with X Rays and 1 to 6 in. (25 to 152 mm) Thick with Cobalt-60
E 666-97, Standard Practice for Calculating Absorbed Dose from Gamma or X Radiation
E 689-95 (1999), Standard Reference Radiographs for Ductile Iron Castings
E 746-02, Standard Test Method for Determining Relative Image Quality Response of Industrial Radiographic Film
E 747-97, Standard Practice for Design, Manufacture and Material Grouping Classification of Wire Image Quality Indicators (IQI) Used for Radiology
E 748-95, Standard Practices for Thermal Neutron Radiography of Materials
E 801 (2001), Standard Practice for Controlling Quality of Radiological Examination of Electronic Devices
E 802-95 (1999), Standard Reference Radiographs for Gray Iron Castings Up to 4 1/2 in. [114 mm]) in Thickness
E 803, Standard Test Method for Determining the L/D Ratio of Neutron Radiography Beams
E 975-00, Standard Practice for X-Ray Determination of Retained Austenite in Steel with Near Random Crystallographic Orientation
E 999-99, Standard Guide for Controlling the Quality of Industrial Radiographic Film Processing
E 1000-98, Standard Guide for Radioscopy
E 1025-98, Standard Practice for Design, Manufacture, and Material Grouping Classification of Hole-Type Image Quality Indicators (IQI) Used for Radiology
E 1030-00, Standard Test Method for Radiographic Examination of Metallic Castings
E 1032-95, Standard Test Method for Radiographic Examination of Weldments
E 1114-92 (1997), Standard Test Method for Determining the Focal Size of Iridium-192 Industrial Radiographic Sources
E 1161-95, Standard Test Method for Radiologic Examination of Semiconductors and Electronic Components
E 1165-92 (2002), Standard Test Method for Measurement of Focal Spots of Industrial X-Ray Tubes by Pinhole Imaging
E 1254-98, Standard Guide for Storage of Radiographs and Unexposed Industrial Radiographic Films
E 1255-96, Standard Practice for Radioscopy
E 1320-00, Standard Reference Radiographs for Titanium Castings
E 1390-90 (2000), Standard Guide for Illuminators Used for Viewing Industrial Radiographs
E 1411-95, Standard Practice for Qualification of Radioscopic Systems
E 1441-00, Standard Guide for Computed Tomography (CT) Imaging
E 1453-93 (1996), Standard Guide for Storage of Media That Contains [sic] Analog or Digital Radioscopic Data
E 1475-97, Standard Guide for Data Fields for Computerized Transfer of Digital Radiological Test Data
E 1496-97, Standard Test Method for Neutron Radiographic Dimensional Measurements
E 1570-00, Standard Practice for Computed Tomographic (CT) Examination
E 1647-98a, Standard Practice for Determining Contrast Sensitivity in Radioscopy
E 1648-95 (2001), Standard Reference Radiographs for Examination of Aluminum Fusion Welds
E 1672-95 (2001), Standard Guide for Computed Tomography (CT) System Selection
E 1734-98, Standard Practice for Radioscopic Examination of Castings
E 1735, Standard Test Method for Determining Relative Image Quality of Industrial Radiographic Film Exposed to X-Radiation from 4 to 25 MV
E 1742-00, Standard Practice for Radiographic Examination
E 1814-96, Standard Practice for Computed Tomographic (CT) Examination of Castings
E 1815-96 (2001), Standard Test Method for Classification of Film Systems for Industrial Radiography
E 1894-97, Standard Guide for Selecting Dosimetry Systems for Application in Pulsed X-Ray Sources
E 1931-97, Standard Guide for X-Ray Compton Scatter Tomography
E 1936-97, Standard Reference Radiograph for Evaluating the Performance of Radiographic Digitization Systems
E 1955-98, Standard Radiographic Examination for Soundness of Welds in Steel by Comparison to Graded ASTM E 390 Reference Radiographs
E 2002-98, Standard Practice for Determining Total Image Unsharpness in Radiology
E 2033-99, Standard Practice for Computed Radiology (Photostimulable Luminescence Method)
E 2116-00, Standard Practice for Dosimetry for a Self-Contained Dry-Storage Gamma-Ray Irradiator
F 629-97, Standard Practice for Radiography of Cast Metallic Surgical Implants
F 947-85 (1996), Standard Test Method for Determining Low-Level X-Radiation Sensitivity of Photographic Films
F 1035-91 (1997), Standard Practice for Use of Rubber-Cord Pie Disk to Demonstrate the Discernment Capability of a Tire X-Ray Imaging System

16 Radiographic Testing
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TABLE 4. Some standards and practices for radiographic testing and for radiation safety.
Issuing Organization Representative Standards and Related Documents

American National Standards Institute ANSI N43.9-1991, Gamma Radiography Specifications for Design and Test of Apparatus
(revision and redesignation of ANSI N432-1980)
ANSI PH2.8-1975, Sensitometry of Industrial X-Ray Films for Energies up to 3 Million Electron
Volts, Method for.
See also ASME and ASNT.
American Society of Mechanical Engineers ANSI/ASME B31.1, Power Piping
ANSI/ASME B31.3, Process Piping
ASME Boiler and Pressure Vessel Code: Section I Power Boilers
ASME Boiler and Pressure Vessel Code: Section III Components
ASME Boiler and Pressure Vessel Code: Section V Power Boilers
ASME Boiler and Pressure Vessel Code: Section VIII Pressure Vessels
ASME Boiler and Pressure Vessel Code: Section XI Inservice Inspection of Nuclear Vessels
ASME PTC 19-1, Performance Test Codes, Supplement on Instruction and Apparatus
American Society for Nondestructive Testing ASNT Recommended Practice No. SNT-TC-1A
ANSI/ASNT CP-189, ASNT Standard for Qualification and Certification of Nondestructive Testing
Personnel
American Society for Testing and Materials See Table 3
American Petroleum Institute API 510, Pressure Vessel Inspection Code: Maintenance Inspection, Rating, Repair and Alteration
API 570, Piping Inspection Code: Inspection, Repair, Alteration, and Rerating of In-Service Piping
Systems
API 650, Welded Steel Tanks for Oil Storage
API 1104, Welding, Pipelines and Related Facilities
American Water Works Association AWWA D100-96, Welded Steel Tanks for Water Storage
American Welding Society AWS D1.1, Structural Welding Code Steel
AWS D1.5, Bridge Welding Code
Canadian General Standards Board CAN/CGSB-48-GP-2M, Spot Radiography of Welded Butt Joints in Ferrous Materials
CAN/CGSB-48.3-92, Radiographic Testing of Steel Castings
CAN/CGSB-48.5-95, Manual on Industrial Radiography
CAN/CGSB-48.9712-95, Non-Destructive Testing Qualification and Certification of Personnel
Deutsche Institut fr Normung DIN 6814, Terms and Definitions in the Field of Radiological Techniques
DIN 6832-2, Radiographic Cassettes; Test for Light-Proofness and Test for Contact between
Radiographic Film and Intensifying Screen
DIN 25 430, Safety Marking in Radiation Protection
DIN 54 115, Non-Destructive Testing; Radiation Protection Rules for the Technical Application of
Sealed Radioactive Sources
DIN EN 444, Non-Destructive Testing; General Principles for the Radiographic Examination of
Metallic Materials Using X-Rays and Gamma-Rays
DIN EN 12 681, Founding Radiographic Inspection
DIN EN 14 096, Non-Destructive Testing - Qualification of Radiographic Film Digitisation Systems
European Committee for Standardization CEN 584, Non Destructive Testing Industrial Radiographic Film
EN 12 679, Non-Destructive Testing Determination of the Size of Industrial Radiographic
Sources Radiographic Method
International Organization for Standardization ISO 2504, Radiography of Welds and Viewing Conditions for Films Utilization of
Recommended Patterns of Image Quality Indicators (I.Q.I.)
ISO 7004, Photography Industrial Radiographic Film Determination of ISO Speed and
Average Gradient When Exposed to X- and Gamma-Radiation
ISO 3999, Apparatus for Gamma Radiography
ISO 9712, Nondestructive Testing Qualification and Certification of Personnel
ISO 9915, Aluminium Alloy Castings Radiography Testing
ISO 11 699, Non-Destructive Testing Industrial Radiographic Films
Japanese Standards Association K 7091, Testing Method for Radiography of Carbon Fibre Reinforced Plastic Panels Edition 1
K 7521, Dimensions for Photographic Film in Sheets and Rolls for Medical, Industrial and Dental
Radiography
Z 4560, Industrial Gamma-Ray Apparatus for Radiography
Korean Standards Association A 4907, Film Marker of Radiography
A 4921, Industrial X-Ray Apparatus for Radiography
M 3910, Dimensions for Photographic Film in Sheets and Rolls for Medical, Industrial and Dental
Radiography
National Council on Radiation Protection NCRP 61, Radiation Safety Training Criteria for Industrial Radiography
Occupational Safety and Health Administration 29 CFR 1910, Occupational Safety and Health Standards [Code of Federal Regulations:
Title 29, Labor]
Society of Automotive Engineers SAE AMS 2635C, Radiographic Inspection
SAE ARP 1611A, Quality Inspection Procedure, Composites, Tracer Fluoroscopy and Radiography
SAE AS 1613A, Image Quality Indicator, Radiographic
SAE AS 7114/4, NADCAP Requirements for Nondestructive Testing Facility Radiography

Introduction to Radiographic Testing 17


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Education, Training, Experience (12 in.) on a standard jaeger test chart.


Requirements for Initial Qualification. This test should be administered annually.
Candidates for certification in Written Examination for NDT Levels I
nondestructive testing should have and II. The minimum number of
sufficient education, training and questions that should be administered in
experience to ensure qualification in the written examination for radiographic
those nondestructive testing methods for test personnel is as follows: 40 questions
which they are being considered for in the general examination and 20
certification. Table 5 lists the questions in the specific examination. The
recommended training and experience number of questions is the same for Level
factors to be considered by the employer I and Level II personnel.
in establishing written practices for initial
qualification of Level I and II individuals Practical Examination for NDT Level I
for radiographic testing. and II. The candidate should demonstrate
ability to operate the necessary
Training Programs. Personnel being nondestructive test equipment, record
considered for initial certification should and analyze the resultant information to
complete sufficient organized training to the degree required. At least one selected
become thoroughly familiar with the specimen should be tested and the results
principles and practices of the specified of the nondestructive test analyzed by the
nondestructive test method related to the candidate.
level of certification desired and
applicable to the processes to be used and Certification. Certification of all levels of
the products to be tested. nondestructive testing personnel is the
responsibility of the employer.
Examinations. For Level I and II Certification of nondestructive testing
personnel, a composite grade should be personnel shall be based on
determined by a simple averaging of the demonstration of satisfactory qualification
results of the general, specific and in accordance with sections on education,
practical examinations described below. training, experience and examinations, as
Examinations administered for modified by the employers written
qualification should result in a passing practice. Personnel certification records
composite grade of at least 80 percent, shall be maintained on file by the
with no individual examination having a employer.
passing grade less than 70 percent. The
examination for near vision acuity should Recertification. All levels of
ensure natural or corrected near distance nondestructive testing personnel shall be
acuity in at least one eye such that recertified periodically in accordance with
applicant can read a minimum of jaeger the following: evidence of continuing
size 2 or equivalent type and size letter at satisfactory performance; reexamination
a distance of not less than 305 mm in those portions of examination deemed
necessary by the employers NDT Level III.
Recommended maximum recertification
intervals are three years for Level I and
Level II and five years for Level III.
TABLE 5. Recommended training and experience for These recommendations from
radiographic testing personnel according to SNT-TC-1A are cited only to provide a
ASNT Recommended Practice No. SNT-TC-1A.4 flavor of the specific items that must be
Level I Level II considered in the development of an
in-house nondestructive testing program.
Radiographic Testing However, if an outside agency is
High school graduatea 39 h 40 h contracted for radiographic test services,
Two years of collegeb 29 h 35 h then the contractor must have a
Work experiencec 3 mo 9 mo qualification and certification program to
satisfy most codes and standards.
Neutron Radiographic Testing
High school graduatea 28 h 40 h
Central Certification
Two years of collegeb 20 h 40 h
Work experiencec 6 mo 24 mo Another standard that may be a source for
compliance is contained in the
a. Or equivalent. requirements of the International
b. Completion with a passing grade of at least two years of engineering or Organization for Standardization (ISO).
science study in a university, college or technical school.
The work of preparing international
c. Work time experience per level. Note: for Level II certification, the
experience shall consist of time as Level I or equivalent. If a person is standards is normally carried out through
being qualified directly to Level II with no time at Level I, the required technical committees of the International
experience shall consist of the sum of the times required for Level I and Organization for Standardization, a
Level II and the required training shall consist of the sum of the hours worldwide federation of national
required for Level I and Level II.
standards bodies. Each ISO member body
interested in a subject for which a
technical committee has been established

18 Radiographic Testing
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has the right to be represented on that 6. Be aware of any potentially explosive


committee. International organizations, atmospheres. Determine whether it is
governmental and nongovernmental, in safe to take your equipment into the
liaison with the International area.
Organization for Standardization, also 7. Do not enter any roped off or no entry
take part in the work. areas without permission and
Technical Committee ISO/TC 135, approval.
Non-Destructive Testing Subcommittee 8. When working on or around moving
SC 7, Personnel Qualification, prepared or electrical equipment, remove pens,
international standard ISO 9712, watches, rings or objects in your
Nondestructive Testing Qualification and pockets that may touch (or fall into)
Certification of Personnel.8 In its statement energized equipment.
of scope, ISO 9712 states that it 9. Know interplant communication and
establishes a system for the qualification evacuation systems.
and certification, by a certification body, 10. Never let unqualified personnel
of personnel to perform industrial operate equipment independently
nondestructive testing (NDT) using any of from qualified supervision.
the following methods: (a) eddy current 11. Keep a safe distance between you and
testing; (b) liquid penetrant testing; any energized equipment. In the
(c) magnetic particle testing; (d) United States, these distances can be
radiographic testing; (e) ultrasonic found in documents from the
testing and that the system described in Occupational Safety and Health
this International Standard may also Administration, the National Fire
apply to visual testing (VT), leak testing Prevention Association (National
(LT), neutron radiography (NR), acoustic Electric Code),9 the Institute of
emission (AE) and other nondestructive Electrical and Electronics Engineers
test methods where independent (National Electrical Safety Code)10 and
certification programs exist. The other organizations.
applicability of ISO 9712 to radiographic 12. Be aware of the personnel
testing therefore depends on activity of responsibilities before entering a
the national certifying body. confined space. All such areas must be
tested satisfactorily for gas and oxygen
levels before entry and periodically
thereafter. If odors are noticed, or
Safety in Radiographic unusual sensations such as earaches,
Testing dizziness or difficulty in breathing are
experienced, leave the area
To manage a radiographic testing immediately.
program, as with any test program, the 13. Notice that the safety considerations
first obligation is to ensure safe working listed above are applicable to many
conditions. The following are components test methods. Because ionizing
of a safety program that may be required radiation can hurt people, additional
or at least deserve serious consideration. precautions are needed for
1. Identify the safety and operational radiographic testing and are discussed
rules and codes applicable to the areas, in a separate chapter.
equipment and processes being Most facilities in the United States are
examined before work is to begin. required by law to follow the
2. Provide proper safety equipment requirements in the applicable standard.
(protective barriers, hard hat, safety Two Occupational Safety and Health
harnesses, steel toed shoes, hearing Standards in the United States that should
protection and others). be reviewed are Occupational Safety and
3. Provide necessary training in radiation Health Standards for general industry11 and
safety. the Occupational Safety and Health
4. Before the test, perform a thorough Standards for the Construction Industry.12
visual survey to determine all the Personnel safety is always the first
hazards and identify necessary consideration for every job.
safeguards to protect test personnel
and equipment.
5. Notify operative personnel to identify
the location and specific equipment Ensuring Reliability of Test
that will be examined. In addition, a
determination must be made if signs Results
or locks restrict access by personnel. When a test is performed, there are four
Be aware of equipment that may be possible outcomes: (1) a discontinuity can
operated remotely or may started by be found when a discontinuity is present;
time delay. (2) a discontinuity can be missed even
when a discontinuity is present; (3) a
discontinuity can be found when none is

Introduction to Radiographic Testing 19


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present; and (4) no discontinuity is found


when none is present. A reliable testing
process and a qualified inspector should
find all discontinuities of concern with no
discontinuities missed (no errors as in
case 2, above) and no false callouts
(case 3, above).
To achieve this goal, the probability of
finding a discontinuity must be high and
the inspector must be both proficient in
the testing process and motivated to
perform a maximum efficiency. A reckless
inspector may accept parts that contain
discontinuities, with the resultant
consequences of possible inservice part
failure. A conservative inspector may
reject parts that contain discontinuities
but the inspector also may reject parts
that do not contain discontinuities, with
the resultant consequences of unnecessary
scrap and repair. Neither inspector is
doing a good job.

Summary
As noted in this discussion, many factors
must be considered before a program of
radiographic testing can begin at a facility.
To manage a nondestructive testing
program many options must be
considered. The final decision for a path
forward must be based on requirement
documents (codes, standards or
specifications) and what is best for your
company. If a person in a position of
responsibility lacks the expertise for this
critical decision, the industry has many
talented individuals willing to assist. The
American Society for Nondestructive
Testing is a place to begin the decision
making process.

20 Radiographic Testing
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PART 3. History of Radiographic Testing13

and compressibility of liquids. As a


Rntgen director of the Physical Institute at
Wrzburg, Rntgen had freedom to
Wilhelm Conrad Rntgen (Fig. 10) made pursue scientific ideas that were of
his momentous discovery of X-rays on interest to him. In 1895, he began
Friday, 8 November 1895, in his collecting the equipment needed to
laboratory at the University of Wrzburg investigate luminescence effects. He
in Germany. The importance of this new studied early work by people before him
kind of ray was recognized immediately Faraday, Geissler, Hittorf and Crookes,
The see-through property of X-rays created for example as well as the more current
a sensation, not only in the scientific work of fellow German scientist Philipp
community but also in the popular press. Lenard. These scientists and others had
By early January 1896, newspapers around studied luminescence in gases and solids
the world carried news of these new rays using a partially evacuated tube, popularly
and their ability to pass through flesh and known as a crookes tube.14 This was
other materials. The newspaper accounts typically a pear shaped glass tube,
correctly predicted the tremendous impact containing two electrodes. When a high
that X-rays were to have on medical voltage was put between the electrodes,
diagnosis. Rntgen and other early X-ray the positively charged ions from the gas
workers showed X-ray images of things: bombarded the negative electrode,
Rntgen took X-ray images of his causing the release of electrons, then
shotgun, a compass and weights in a box. called cathode rays. The electrons caused
Much experimental work ensued in an luminescence in the partial gas filling, in
almost playful atmosphere, as researchers the glass walls of the tube or in other
radiographed hundreds of different kinds materials placed in their path.
of objects. Industrial applications of a sort
were found almost immediately, in the
sense that artillery shell casings were
among the objects so examined. It was
decades before nonmedical uses of X-rays FIGURE 10. Wilhelm Conrad Rntgen.
became important.
Clearly, the practical uses for X-rays
have gone well beyond the early concepts.
Immediate medical uses foreseen included
setting of broken bones and location of
foreign objects bullets, pins, coins and
others. Medical applications have now
expanded to include diagnosis of diseases
such as tuberculosis, malfunctions such as
blockages of the circulatory system and
the detection of many abnormalities such
as tumors and calcium loss in bones.
X-rays are now used for medical therapy,
to identify and analyze materials, to
inspect industrial materials and, a use all
airplane travelers recognize, to inspect
baggage and packages. The methods
include fluoroscopy and film radiography
the two methods Rntgen used and
more modem techniques such as
electronic radioscopy, tomography,
backscatter imaging, radiation gaging,
diffraction, fluorescence and others.

Preliminary Work
Rntgen was a respected scientist before
the X-ray discovery, having published
work on specific heat, optical phenomena

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Discovery the general public. One of his mailed set


of reprints and photographs went to his
Rntgen was an institute director, with
friend Ernst Warburg in Berlin. Warburg
graduate students and assistants available
displayed the material as a poster exhibit
as needed. However, as was his usual
at the 50th anniversary meeting of the
custom, Rntgen did many experimental
Berlin Physical Society in 1896. Many saw
studies himself. His laboratory was only
the exhibit in one corner of the hall.
one floor down from his living quarters in
Another of his private communications
the Physical Institute, so it was easily
went to a second college friend, Professor
available to him as he desired. All was in
Franz Exner in Vienna. Exner showed the
readiness on the afternoon of Friday,
pictures to several fellow scientists. One of
8 November 1895. Rntgen had his
them, Professor Ernst Lecher visiting from
covered tube and a darkened laboratory
Prague, was so fascinated by the pictures
when he energized the cathode ray tube
that he asked Exner if he could borrow
and noticed luminescence from a barium
them overnight. Lecher shared the
platinocyanide screen on a table about
pictures with his father, Z. Lecher, editor
2 m (7 ft) away. The luminescence was
of the Vienna Presse newspaper. Lechers
definitely associated with the tube,
January 1896 article in the Vienna Presse
turning on only when the tube was
newspaper extolled the potential of these
energized. Rntgen knew the effect could
new X-rays, correctly pointing out the
not be cathode rays, because they
benefits for medical diagnosis. The news
penetrate only a short distance in air. He
quickly spread around the world,
was intrigued; he investigated.
appearing in many newspapers within the
He quickly learned about the
following week. Rntgen received more
penetrating power of these new rays; they
than 1000 pieces of mail in the first week
penetrated paper, wood, metal and flesh.
following the press announcement.
The rays made shadow pictures on
Within days, scientists everywhere, using
fluorescent screens and on film.
crookes tubes, were repeating Rntgens
Nevertheless, he was skeptical about his
observations and confirming his results.
discovery. As he became totally consumed
Once the news was out, there were
in a seven week intensive study he
many offers of honors, lectures and visits.
commented to his friend, Theodor Boveri,
However, Rntgen turned down most
I have discovered something interesting
such overtures. One he could not refuse
but I do not know whether or not my
was a royal invitation. Rntgen gave a
observations are correct. At the same
demonstration of X-rays before Kaiser
time, as a scientist, he was excited. He
Wilhelm II and his court in January 1896.
knew he must report his findings and
As a result of this summons to the court,
obtain feedback from fellow scientists.
Rntgen was awarded the Royal Order of
Because the new rays darkened a
Merit, an award that permits one to use
photographic plate, he could take pictures
the title von, as an indication of nobility.
and share them with others. One of these
Rntgen never made the formal
early pictures in December 1895 was a
application for the noble rank and refused
15 min exposure showing the bones in
to use the term von in his name.
the hand of his wife, Bertha. Other early
Another summons he could not turn
pictures taken with the new rays included
down was a call from his own university.
weights in a box, a compass, a piece of
In January 1896, he lectured on his
metal and a shotgun. He recognized that
discovery before the Physical Medical
he must publish his results so that they
Society in Wrzburg and gave the first
could be shared with others in the
public demonstration before an
scientific community. His first technical
overflowing audience. The image of
paper on X-rays, On a New Kind of Rays:
Rntgens lecture was captured in a 1961
A Preliminary Communication, was
painting (Fig. 11). During the lecture
published in the annals of the Wrzburg
Rntgen radiographed the hand of his
Physical Medical Society in December
fellow university professor and well
1895.15 The reprints were ready by the
known anatomist, Albert von Kolliker.
new year. As he mailed reprints and
Kolliker was so enthused by the discovery
photographs to colleagues, Rntgen said
that he announced that the new rays
to Bertha, Now the devil will be to pay,
should be called roentgen rays, as they are
clearly a premonition of the coming
still in Europe and within the medical
drastic change in his life.
community. The lecture and
demonstration were greeted with
Fame enthusiastic applause. It was to be
Rntgen was apprehensive as he sent Rntgens only formal public lecture on
reprints and pictures to colleagues in X-rays.
January 1896, but he probably had no The commercial community took note
idea of what was in store for him. There of Rntgens discovery.14,16 An American
was tremendous interest in his new rays, industrial group was said to offer Rntgen
both from the scientific community and a fortune for rights to his discovery.

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Rntgen was similarly approached by Crookes was always rejecting


many industrial groups, including a photographic plates because they were
documented overture by Max Levy of a fogged, most likely from X-ray exposure.
German company. However, Rntgen Philipp Lenard, who had helped Rntgen
remained true to his scientific calling, obtain one of his thin window tubes, had
saying that discoveries and inventions noticed that an electric charge some
belong to humanity and that they should distance away from his lenard tube was
not in any way be hampered by patents, discharged but he did not investigate
licenses or contracts, nor should they be fully.17
controlled by any one group. One well documented early notice of
Edison, the renowned American X-rays occurred in the physics laboratory
inventor, was quoted as saying about of Arthur W. Goodspeed at the University
Rntgens attitude, After they have of Pennsylvania.18 He was visited in
discovered something wonderful, February 1890, by photographer William
someone else must look at it from the Jennings to do some photography with
commercial point of view. One must see spark discharges. After the young men
how to use it and how to profit from it finished with the spark equipment,
financially. Edison was among the first of Goodspeed showed Jennings his crookes
many Americans to investigate X-rays. He tube equipment in operation. Jennings
quickly designed and built X-ray tubes had several unexposed, covered
and a fluorescent screen fluoroscope, photographic plates on the table during
making use of the Edison discovery that a the crookes tube demonstration; he had
calcium tungstate phosphor screen gave placed several coins for his carfare on top
very bright X-ray images. Edison of the stack of plates. On returning to his
exhibited an X-ray fluoroscope at the laboratory, he processed the plates and
National Electrical Exposition at the found a curious image of several round
Grand Central Palace in New York in May objects. He dated and filed the plate, only
1896. The Exposition gave the general to bring it back at Goodspeeds request
public a rare opportunity to see X-ray after the news of the X-ray discovery.
pictures. They could document that they had made
Obviously, with crookes tubes in use in an X-radiograph five years before
laboratories around the world, it is clear Rntgens discovery. Goodspeed and
that many people before Rntgen had Jennings merely brought the radiograph
produced X-rays. Once the discovery was to public attention, never claiming any
announced, many scientists recognized credit for discovering X-rays.
that X-rays had been responsible for Rntgen himself published two
strange effects they had noticed (but not additional scientific papers about X-rays.
followed up) from earlier experiments. On a New Kind of Rays, Continued,15
was published by the same Wrzburg
publication in March 1896 and was
followed by Further Observations on the
FIGURE 11. Rntgen demonstrates X-rays in 1896. Properties of X-Rays,19 published in
March 1897 by the Prussian Academy of
Sciences. His three scientific papers
presented thorough results about X-rays.
His investigations showed the
penetrating power of the new rays as
related to the density of the absorber and
the effect on fluorescent materials and
photographic film. Rntgen took pinhole
pictures to confirm that the source of the
X-ray emission was the point where the
cathode rays struck the glass wall or a
metal target. He recognized the
nonuniform distribution of the X-ray
emission from the target and found the
fundamentals of the inverse square law
for decreasing X-ray intensity with
increasing distance from the target. He
tried without success to deflect the X-ray
beam with a magnet or an electric field.
His attempts to demonstrate reflection
and diffraction were likewise without
success. His experiments did produce
evidence that the new rays caused
electrical conductivity in air and that
heavy metal targets such as platinum
produced more intense X-ray beams than

Introduction to Radiographic Testing 23


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glass or aluminum targets. His three recognition that gas in the body can help
papers on X-rays gave the basic outline organs, an early concept of a
information about X-rays to the world.20 contrast medium.

Early Medical Applications Introduction of Additional


The medical use of X-rays began Radiation Sources
immediately. It was straightforward to In 1898 Marie Sklodowska Curie (Fig. 12)
recognize the usefulness of X-rays to find and Pierre Curie published research
foreign objects in the body and to help showing the discovery of two new
set broken bones. There are many radioactive elements, polonium and
documented instances of such radium, laying the foundation for gamma
applications as early as January and radiography.
February 1896. The first recorded X-ray The early X-ray tubes were partially
picture in the Americas was taken by evacuated glass bulbs. Metal targets and
Arthur W. Wright of Yale University, in curved cathodes were quickly added to
January 1896. This was quickly followed increase X-ray output. Nevertheless, it was
by X-ray work at other universities. a challenge to operate these early gas
Men recognized for early work in what tubes consistently The gas pressure
has become medical radiology include changed because of outgassing of the
Francis H. Williams, a doctor at the walls and other heating effects. One of
Boston City Hospital, and William J. the first X-ray related patents was for a
Morton, a New York City physician.21 technique of controlling the tube gas
Williams used X-rays to study anatomy, pressure (issued March 1896 to Siemens).
both diseased and normal. He used Among the early uses of radioscopy,
fluoroscopy and film radiography to study fluoroscopes similar to those at todays
the thorax, for determining the outline of airports were used during World War I to
the heart, for diagnosis of tuberculosis inspect packages for contraband
and other medical studies. Williams had (Fig. 13).22
the advantage of working with two It was in this background that William
Massachusetts Institute of Technology D. Coolidge (Fig. 14) of General Electric
scientists, Charles Norton and Ralph introduced the hard vacuum, hot cathode
Lawrence, whose work advanced early X-ray tube, truly a significant advance in
X-ray technology. Mortons wide ranging X-ray technology.23 This new X-ray tube
pioneering X-ray work included the concept brought much improved
reproducibility and ease of operation to
X-ray technology and prepared the way
for high energy X-ray use. The patent for
FIGURE 12. Marie Sklodowska Curie (1928). this landmark X-ray development was
issued in 1916.24

FIGURE 13. Radioscopic system for detection of contraband


(circa 1910).

24 Radiographic Testing
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Knipping26,27 and from the pioneering


X-Rays for Nondestructive work of the father and son Bragg team.
28,29 X-ray diffraction is a widely used
Testing method to identify and analyze
materials.25 Some idea of the impact that
X-ray diffraction has had on science is
X-Ray Diffraction given by noting that twenty Nobel
Rntgens early X-ray work included physics prizes have been awarded for
unsuccessful attempts to show diffraction achievements in crystallography.30
effects by directing the rays through a fine
slit. This effect was successfully shown
later following the 1909 work of Walter
Radiography
and Pohl.25 It was Max von Laue who first Early advances in X-ray nondestructive
thought of using the regular order of a testing were being made in many
crystal to diffract X-rays. Experimental countries around the world.
confirmation of this now important and Documentation of early X-ray work in the
widespread use of X-rays came from United Kingdom and in Germany
Laues work with Friedrich and describes work going back to the time of
World War I. The early work in the United
Kingdom, particularly the armament
related X-ray nondestructive testing work
FIGURE 14. William Coolidge, inventor of X-ray tube: of V.E. Pullin, is well described by
(a) posing with 1 MeV tube; (b) X-ray tube. Halmshaw.31 An excellent description of
early work in Germany shows many
(a) examples of radiographic nondestructive
testing, including field test systems dating
from the 1920s.32 A recent summary of
X-ray history is given in the X-ray
centennial issue of Insight, including
articles about X-ray development in the
United Kingdom and in Germany.33
Early work in the United States is
documented in patents.34,35 Despite these
early efforts and many demonstrations of
X-rays for material examination,24
radiographic nondestructive testing did
not become important commercially until
World War II. In the United States,
workers in nondestructive testing cite the
early work of Horace Lester (Fig. 15) at the

FIGURE 15. Horace Lester.

(b)

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Watertown Arsenal (Fig. 16) as laying the Horace Lester attended this 1929 X-ray
groundwork for our present use of lecture and contributed to the discussion
radiography.36,37 Lesters work was included with the published article.
significant because it clearly demonstrated Lesters comment discussed the increasing
that X-rays could be used to locate use of steel forgings and welded structures
internal discontinuities in castings, welds instead of castings because engineers
and other metal forms and that these believed that these substitutes for
discontinuities could lead to premature castings are free from hidden defects and
failure. Lesters contributions were also therefore more reliable. He went on to
important because of his preeminent point that his work at Watertown Arsenal
position in the metallurgical field.38,39 showed that the assumption of soundness
However, there was significant work done for forgings and welds was not true.
in the United States in radiographic Wheeler Davey also attended the lecture
nondestructive testing even before Lesters and contributed to the discussion. Daveys
landmark research. An excellent review of comment may strike a responsive chord
early X-ray nondestructive testing work is even today: the authors bring out the
given in the 1929 Fink and Archer paper fact, previously emphasized by Lester, that
for ASM International, when it was called there are few cases where it is good
the American Society for Steel Treating.40 economic sense to use radiography for
The paper cites 108 references, with 46 of 100 per cent inspection.
these dating during the period 1915-1921. It was in this environment of
Prominent among the early citations is unfavorable economics for widespread use
the work of Wheeler R. Davey, who did of nondestructive testing that the
research on radiographic nondestructive American Society for Nondestructive
testing at the General Electric Research Testing began.
Laboratory (1914 to 1926) and later at
Penn State University. The Alcoa team of
Fink and Archer described X-ray exposure
techniques for aluminum and steel, American Society for
including the use of fluorescent and lead Nondestructive Testing
screens. This 1929 paper is given credit for
the first public description for the use of The society was started officially by a
lead intensifying screens.41 charter from the state of Massachusetts
dated August 1941. Prominent among the
nine signers of the original charter are the
first two names, Philip D. Johnson and
Carlton G. Lutts. Lutts served as the first
FIGURE 16. Laboratory of Horace Lester at Watertown president of the American Industrial
Arsenal, Watertown, Massachusetts. Radium and X-Ray Society during its
initial year of operation, 1941-1942. The
new societys first conference was held at
Massachusetts Institute of Technology in
October, 1941, highlighted by a
presentation (later called the Mehl Honor
Lecture) by Charles W. Briggs.
Formed as it was in late 1941, the
society was in place as the United States
entered World War II in December 1941.
The war effort required increasing
emphasis on product reliability and
nondestructive testing. The fledgling
society was there to provide a needed
forum for the exchange of nondestructive
testing information. The new society
journal, first called Industrial Radiography
and issued in the summer of 1942, played
a key role in spreading knowledge about
nondestructive testing.
Ralph Turner, ASNT national president
during 1971-1972 and an ASNT historian,
reflected on the early years of the Society:
The Society has not done badly. Perhaps
the most fortunate event was its
inadvertent birth just before World
War Il.42 Clearly the war years gave a
needed push to help the new society
survive and grow during the crucial
formative years.

26 Radiographic Testing
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An early recognition was that States Capitol (September 1985) and the
nondestructive testing included methods Statue of Liberty (October 1985).
other than radiography. Liquid penetrants The journal has also provided an
and magnetic particles were in wide use opportunity for commercial development
and other methods such as ultrasonic of X-ray technology. Early advertisers in
testing were becoming important. With the journal included equipment suppliers
Volume 5 in the summer of 1946, the such as General Electric, Keleket, North
journal name and mission were expanded American Philips, Picker and
to Industrial Radiography & Non-Destructive Westinghouse, film suppliers such as
Testing. In the fall of 1947 the name of Agfa-Ansco, DuPont and Eastman Kodak;
the society was changed to the Society for and tube/accessory suppliers such as
Non-Destructive Testing. The hyphen in Bar-Ray Products, Machlett, Pako and Ray
the name disappeared in 1952. The Proof Corporation. Only a few of these
journal expanded publication to early X-ray companies continue to supply
bimonthly (instead of quarterly) in 1953 the X-ray nondestructive testing market
and became a monthly journal in 1964, at in the 21st century; others, Keleket and
the same time changing the journal name Machlett, for example, have disappeared
to Materials Evaluation.43 By 1967 many completely.
other countries had nondestructive testing Many of the society honors and awards
societies and there had been five have had a radiation connection. The
International Conferences on Coolidge Award, named for William D.
Nondestructive Testing (now called World Coolidge, the inventor of the hard
Conferences), so it seemed appropriate to vacuum X-ray tube (Fig. 14), was
change the society name again; it became presented from 1953 to 1964 for
the American Society for Nondestructive outstanding contributions to the
Testing (ASNT). advancement of nondestructive testing
ASNT can be proud of its role in using X-rays. The Lester Honor Lecture,
advancing the state-of-the-art of named for the X-ray pioneer Horace
nondestructive testing and X-ray Lester (Fig. 15), has been presented since
technology. The national conferences, the 1943. The Mehl Honor Lecture, named for
section meetings for local information Robert Mehl, an early contributor to
exchange, the topical conferences, the gamma radiography,44 has been presented
societys international participation, the since 1941. Although the honor lectures
Nondestructive Testing Handbook series and are named for men known for their work
educational and personnel activities all in radiation, the topics of the lectures
provided opportunities for exchange of cover the entire field of nondestructive
nondestructive testing information. The testing.
early issues of the journal were heavily Throughout the society history there
weighted toward X-ray technology, has been a clear division of effort in
reflecting the original name of the society. advancing nondestructive testing between
Early contributors to the journal included the American Society for Nondestructive
many respected engineers and scientists. Testing and the American Society for
Early issues contained articles by Arthur Testing and Materials Committee E-7 on
Barkow, Charles Barrett and George Clark Nondestructive Testing, organized in
(all of whom made early contributions to 1938.45 The American Society for Testing
the advancement of X-ray diffraction), and Materials activity produces consensus
James Bly and Gerold Tenney (whose standards for nondestructive testing
work included developments in high methods and applications. The American
energy radiography), Donald OConnor Society for Nondestructive Testing efforts
(whose group at the Naval Ordnance provide a forum for information
Laboratory, with colleagues Edward exchange, education and personnel
Criscuolo and Daniel Polansky, certification. The role of the two
contributed much to the early X-ray organizations was recognized early, as
nondestructive testing standards), Leslie indicated in a 1942 letter from Horace
Ball (an early user of X-ray technology in Lester, Chairman of American Society for
the aircraft field), Donald Kerst, the Testing and Materials E-7.
developer of the betatron, film research There are many individuals who
workers Herman Seeman and George remain active in both the American
Corney and many others whose names Society for Testing and Materials
and works were well known. Committee E-7 and the American Society
Along the way there have been many for Nondestructive Testing, thereby
noteworthy radiographic applications. providing a strong link between the two
Materials Evaluation readers may recall the nondestructive testing organizations.
following: the Vatican Pieta (June 1964),
the worlds largest radiograph (November
1964), the Liberty Bell (February 1976), a
lighthouse (March 1980), the United

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Advances in Radiographic
Technology
The period from 1935 to 1960 saw
improvements in technology and
techniques for radiation safety,46 gamma
radiography,47-49 portable X-ray
machines,49,50 high voltage
radiography51-53 and nucleonic gaging.54
Radiographic testing found new
applications, in metals,55 shipbuilding56
and particularly in the aviation
industries.57-59
Although radiographic testing is still
performed essentially in the same
through-transmission, direct shadowing
way that Rntgen used 100 years ago, the
twenty-first century has much better
X-ray sources, detectors and
understanding of image quality factors
like scatter and unsharpness. In addition,
of course, the industry today has a large
arsenal of techniques for example,
electronic radioscopy, computed
tomography, backscatter imaging,
laminography, dual energy,
microradiography, flash techniques and
in-motion radiography. The commercial
X-ray market for equipment, accessories
and supplies is still primarily weighted
toward medical fields but other X-ray
applications contribute to what is
estimated to be a $12 billion annual
market. In addition to the medical and
traditional nondestructive testing
applications, industry uses X-ray
diffraction and other analytical methods
such as fluorescence, radiation methods
for material modification, X-ray
lithography, radiation gaging and the ever
expanding use of X-rays for security.
Looking toward the future, only one
thing is clear the technology will
continue to advance. Obvious directions
are the increasing use of computerized
instrumentation, automated testing and
greater use of nondestructive test
techniques in process control
applications. Regardless of the new
directions that nondestructive testing and
X-ray technology may take in the coming
century the American Society for
Nondestructive Testings roles of
education, information exchange and
personnel certification will continue.
Thanks to the superb investigative
talents of Wilhelm Conrad Rntgen, our
generation enjoys many benefits from
Rntgens rays. The new edition of the
Nondestructive Testing Handbook is a good
time to remember past achievements.

28 Radiographic Testing
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PART 4. Units of Measure for Radiographic


Testing

Multipliers
Origin and Use of SI In science and engineering, very large or
System very small numbers with units are
expressed by using the SI multipliers,
In 1960 the General Conference on prefixes of 103 intervals (Table 9). The
Weights and Measures established the multiplier becomes a property of the SI
International System of Units. Le Systme unit. For example, a millimeter (mm) is
International dUnits (SI) was designed so 0.001 meter (m). The volume unit cubic
that a single set of measurement units centimeter (cm3) is (0.01 m)3 or 106 m3.
could be used by all branches of science, Unit submultiples such as the centimeter,
engineering and the general public. decimeter, dekameter (or decameter) and
Without SI, this Nondestructive Testing hectometer are often avoided in scientific
Handbook volume could have contained a and technical uses of SI because of their
confusing mix of obsolete variance from the 103 interval. However,
centimeter-gram-second (CGS) units, dm3 and cm3 are commonly used. Note
imperial units and the units preferred by that 1 cm3 is not equal to 0.01 m3.
certain localities or scientific specialties. Nevertheless, in equations, submultiples
SI is the modern version of the metric such as centimeter (cm) or decimeter (dm)
system and ends the division between are often avoided because they disturb the
metric units used by scientists and metric
units used by engineers and the public.
Scientists have given up their units based
on centimeter and gram and engineers
made a fundamental change in TABLE 7. SI derived units with special names.a
abandoning the kilogram-force in favor of Relation
the newton. Electrical engineers have to Other
retained their ampere, volt and ohm but Quantity Units Symbol SI Unitsb
changed all units related to magnetism.
Table 6 lists the seven SI base units. Capacitance farad F CV1
Table 7 lists derived units with special Catalytic activity katal kat s1 mol
names. Table 8 gives examples of Conductance siemens S AV1
conversions to SI units. In SI, the unit of Energy joule J Nm
time is the second (s) but hour (h) is Frequency (periodic) hertz Hz 1s1
recognized for use with SI. Force newton N kgms2
For more information, the reader is Inductance henry H WbA1
referred to the information available
Illuminance lux lx lmm2
through national standards organizations
and specialized information compiled by Luminous flux lumen lm cdsr
technical organizations.60-63 Electric charge coulomb C As
Electric potentialc volt V WA1
Electric resistance ohm VA1
Magnetic flux weber Wb Vs
TABLE 6. SI base units. Magnetic flux density tesla T Wbm2
Plane angle radian rad 1
Quantity Unit Symbol
Power watt W Js1
Length meter m Pressure (stress) pascal Pa Nm2
Mass kilogram kg Radiation absorbed dose gray Gy Jkg1
Time second s Radiation dose equivalent sievert Sv Jkg1
Electric current ampere A Radioactivity becquerel Bq 1s1
Temperature kelvin K Solid angle steradian sr 1
Amount of substance mole mol Tempersature, celsius degree celsius C K
Luminous intensity candela cd Timea hour h 3600 s
Volumea liter L dm3
a. Hour and liter are not SI units but are accepted for use with the SI.
b. Number one (1) expresses dimensionless relationship.
c. Electromotive force.

Introduction to Radiographic Testing 29


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convenient 103 or 103 intervals that


make equations easy to manipulate.
TABLE 9. SI prefixes and multipliers.
In SI, the distinction between upper
and lower case letters is meaningful and Prefix Symbol Multiplier
should be observed. For example, the
meanings of the prefix m (milli) and the yotta Y 1024
prefix M (mega) differ by nine orders of zetta Z 1021
magnitude. exa E 1018
peta P 1015
tera T 1012
giga G 109
SI Units for Radiography mega M 106
The original discoveries of radioactivity kilo k 103
helped establish units of measurement hectoa h 102
based on observation rather than precise deka (or deca)a da 10
physical phenomena. Later, scientists who
decia d 101
worked with radioactive substances (or
centia c 102
who managed to manufacture radioactive
beams) again made circumstantial milli m 103
observations that were then used for micro 106
measurement purposes. This practical nano n 109
approach was acceptable at the time, but pico p 1012
a broader understanding of physics and femto f 1015
the modern practice of using only one atto a 1018
unit for a quantity has led to the zepto z 1021
modification of many of the original units yocto y 1024
(see Tables 10 to 12). In the SI system,
radiation units have been given a. Avoid these prefixes (except in dm3 and cm3) for
science and engineering.
established physical foundations and new
names where necessary.

TABLE 8. Examples of conversions to SI units.


Quantity Measurement in Non-SI Unit Multiply by To Get Measurement in SI Unit

Angle minute (min) 2.908 882 104 radian (rad)


degree (deg) 1.745 329 102 radian (rad)
Area square inch (in.2) 645 square millimeter (mm2)
Distance angstrom () 0.1 nanometer (nm)
inch (in.) 25.4 millimeter (mm)
Energy British thermal unit (BTU) 1.055 kilojoule (kJ)
calorie (cal), thermochemical 4.184 joule (J)
Power British thermal unit per hour (BTUh1) 0.293 watt (W)
Specific heat British thermal unit per pound 4.19 kilojoule per kilogram per kelvin (kJkg1K1)
degree fahrenheit (BTUlbm1F1)
Force (torque, couple) foot-pound (ft-lbf) 1.36 joule (J)
Pressure pound force per square inch (lbfin.2) 6.89 kilopascal (kPa)
Frequency (cycle) cycle per minute 601 hertz (Hz)
Illuminance footcandle (ftc) 10.76 lux (lx)
phot (ph) 10 000 lux (lx)
Luminance candela per square foot (cdft2) 10.76 candela per square meter (cdm2)
candela per square inch (cdin.2) 1 550 candela per square meter (cdm2)
footlambert (ftl) 3.426 candela per square meter (cdm2)
lambert 3 183 (= 10 000/) candela per square meter (cdm2)
nit (nt) 1 candela per square meter (cdm2)
stilb (sb) 10 000 candela per square meter (cdm2)
Radioactivity curie (Ci) 37 gigabecquerel (GBq)
Ionizing radiation exposure roentgen (R) 0.258 millicoulomb per kilogram (mCkg1)
Mass pound (lbm) 0.454 kilogram (kg)
Temperature (difference) degree fahrenheit (F) 0.556 kelvin (K) or degree celsius (C)
Temperature (scale) degree fahrenheit (F) (F 32)/1.8 degree celsius (C)
Temperature (scale) degree fahrenheit (F) (F 32)/1.8) + 273.15 kelvin (K)

30 Radiographic Testing
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Physical Quantities Mesures) permitted the units given in


Table 11 (curie, roentgen, rad and rem) to
Three physical quantities in particular are
continue to be used with the SI until
widely used as measurement units the
1998.61-63 However, these units must not
electronvolt (eV), the speed of light (c)
be introduced where they are not
and the unified atomic mass unit (u).
presently used. The National Institute of
Their precise values, however, are
Standards and Technology strongly
obtained experimentally.
discourages the continued use of curie,
Electronvolt. The electronvolt is the roentgen, rad and rem.61-63 The American
kinetic energy acquired by an electron in National Standards Institute, the
passing through a potential difference of American Society for Testing and
1 V in vacuum; 1 eV = 1.602 176 462 Materials, the Institute of Electrical and
1019 J with a combined standard Electronics Engineers, the International
uncertainty of 6.3 1027 J.63,64 The Organization Standardization (ISO) and
electronvolt is accepted for use with SI. and the American Society for
Speed of Electromagnetic Radiation. The Nondestructive Testing all support the
quantity c represents the speed of light, replacement of older English units with SI
that is, the speed of electromagnetic units.
waves in vacuum; 1 c = 299 792 458 ms1 Becquerel Replaces Curie. The original
exactly (670 616 629 mih1). The speed of unit for radioactivity was the curie (Ci),
light is a physical quantity but can be simply the radiation of one gram of
used as a unit of measure. radium. Eventually all equivalent
Unified Atomic Mass Unit. The unified radiation from any source was measured
atomic mass unit (u) is 121 of the mass of with this same unit. It is now known that
the atom of the nuclide carbon-12; 1 u = a curie is equivalent to 3.7 1010
1.660 538 731027 kg with a combined disintegrations per second. In SI, the unit
standard uncertainty of 1.3 for radioactivity is the becquerel (Bq),
1034 kg.63,64 which is one disintegration per second.
Because billions of disintegrations are
required in a useful source, the multiplier
Radiation Measurement prefix giga (109) is used and the unit is
Because of existing practice in certain normally seen as gigabecquerel (GBq).
fields and countries, the International Coulomb per Kilogram Replaces
Committee for Weights and Measures Roentgen. The unit for quantity of
(CIPM, Comit Internationale des Poids et electric charge is the coulomb (C), where

TABLE 10. Physical quantities used as units. Values of physical quantities are experimentally obtained and
may only be approximated in SI. Conversions are provided here for descriptive purposes.
Physical Quantity Symbol Multiply by SI Unit SI Symbol

Electronvolt a eV 1.6 1019 joule J


Speed of electromagnetic waves in vacuum c 2.997 924 58 108 meter per second ms1
Unified atomic mass unit a,b u 1.66 x 1027 kilogram kg
a. Approved for use with SI.
b. Mass of unified atomic mass unit is 121 of the mass of the atom of the nuclide carbon-12.

TABLE 11. Conversion to SI radiographic units.


Traditional Unit Symbol Multiply by Resulting SI Unit SI Symbol

Curie Ci 3.7 1010 becquerel Bq


37 gigabecquerel GBq
Rad rad a 102 gray Gy
10 milligray mGy
Rem rem 102 sievert Sv
10 millisievert mSv
Roentgen R 2.58 104 coulomb per kilogram Ckg1
258 microcoulomb per kilogram Ckg1

a. The abbreviation rd may be used for radiation absorbed dose where there is possibility of confusion with radian
(rad), the SI unit for plane angle.

Introduction to Radiographic Testing 31


3RT01_LAYOUT(001_036) 10/2/02 1:34 PM Page 32

1 C = 1 A 1 s. The original roentgen (R) roentgen converts to millisieverts on a


was the quantity of radiation that would one-to-ten basis.
ionize 1 cm3 of air to 1 electrostatic unit Exposure charts were often made by
of electric charge, of either sign. It is now using curie minutes at a source-to-film
known that a roentgen is equivalent to distance in inches squared. This was
258 microcoulombs per kilogram of air written Ciminin.2. Exposure charts
(258 Ckg1 of air). This corresponds to made in SI use gigabecquerel minutes for
1.61 1015 ion pairs per 1 kg of air, which a source-to-film distance in centimeters
has then absorbed 8.8 mJ (0.88 rad, where squared, where 1 Ciminin.2 =
rad is the obsolete unit for radiation 50 GBqmincm2. Table 12 lists some of
absorbed dose, not the SI symbol for these compound units.
radian).
Gray Replaces Rad. The roentgen (R) was
an intensity unit but was not
representative of the dose absorbed by TABLE 12. Compound radiographic units.
material in a radiation field. The radiation Traditional Multiply Resulting
absorbed dose (rad) was first created to Unit by SI Unit
measure this quantity and was based on
the erg, the energy unit from the old RCi1h1 at 1 m 0.27 mSvGBq1h1 at 1 m
centimeter-gram-second (CGS) system. In Ciminin.2 50 GBqmin.cm2
the SI system, the unit for radiation dose Rmin1 a 0.01 Gymin1
is the gray (Gy). The gray is useful because Rmin1 b 0.01 Svmin1
it applies to doses absorbed by matter at a
R 2.58 104 Ckg1
particular location. It is expressed in
energy units per mass of matter or in a. Absorbed dose.
joules per kilogram (Jkg1). The mass is b. Dose absorbed by human body.
that of the absorbing body.
Sievert Replaces Rem. The SI systems unit
for the dose absorbed by the human body
(formerly rem for roentgen equivalent man;
also known as ambient dose equivalent,
directional dose equivalent, dose equivalent,
equivalent dose and personal dose equivalent)
is similar to the gray but includes quality
factors dependent on the type of
radiation. This absorbed dose has been
given the name sievert (Sv) but its
dimensions are the same as the gray, that
is, 1 Sv = 1 Jkg1.

Compound Units
Exposure to ionizing radiation could be
measured in roentgens with an ionization
chamber that, when placed 1 m (39 in.)
from the radiation source, provided
necessary information one roentgen
per curie per hour at one meter (RCi1h1
at 1 m), for example. The numbers,
however, had limited physical meaning
and could not be used for different
applications such as high voltage X-ray
machines.
The roentgen per hour (Rh1) was used
to designate the exposure to an ionizing
radiation of the stated value. Because the
radiation received from 1 Rh1 was
considered about equal to 1 rem, the
relationship is approximated as 1 Rh1 =
0.01 Gyh1 = 10 mGyh1.
A previously popular unit, roentgen per
curie per hour at one meter (RCi1h1 at
1 m), is expressed in SI units as
millisievert per gigabecquerel per hour at
one meter (mSvGBq1h1 at 1 m), such
that 1 mSvGBq1h1 at 1 m =
3.7 RCi1h1 at 1 m. In this relationship,

32 Radiographic Testing
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Introduction to Radiographic Testing 35

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