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The Evaluation of Varying Ductile Fracture Criteria for
3Cr20Ni10W2 Austenitic Heat-Resistant Alloy
Yu-Feng Xia, Gui-Chang Luo, Dong-Sen Wu, Guo-Zheng Quan, and Jie Zhou
School of Material Science and Engineering, Chongqing University, Chongqing 400044, China
Copyright 2013 Yu-Feng Xia et al. This is an open access article distributed under the Creative Commons Attribution License,
which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
Most bulk metal forming processes may be limited by ductile fracture, such as an internal or surface fracture developing in the
workpiece. Finding a way to evaluate the ductile fracture criteria (DFC) and identify the relationships between damage evolution
and strain-softening behavior of 3Cr20Ni10W2 heat-resistant alloy is very important, which, however, is a nontrivial issue that
still needs to be addressed in greater depth. Based on cumulative damage theory, an innovative approach involving heat physical
compression experiments, numerical simulations, and mathematical computations provides mutual support to evaluate ductile
damage cumulating process and DFC diagram along with deformation conditions. It is concluded that, as for strain-softening
material, ductile damage starts at work hardening phase, and the damage cumulation is more sensitive in work hardening phase
than in work softening phase. In addition, DFC of 3Cr20Ni10W2 heat-resistant alloy in a wide temperature range of 12031403 K
and the strain rate of 0.0110 s1 are not constant but change in a range of 0.0990.197; thus they have been defined as varying
ductile fracture criteria (VDFC) and characterized by a function of strain rate and temperature. According to VDFC diagram, the
exact fracture moment and position during various forming processes will be predicted conveniently.
350
= 0.01 s1 450
= 0.1 s1
300 400
1203 K 1203 K
250 350
True stress (Mpa)
300
400 500
True stress (Mpa)
1253 K
1253 K 400
300 1303 K
1303 K 300 1353K
200 1353K
200
1403K
100 1403K
100
0 0
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0
True strain True strain
(c) (d)
Figure 1: True stress-strain curves of 3Cr20Ni10W2 alloy at different strain rates and temperatures (a) 0.01 s1 , 12031403 K; (b) 0.1 s1 ,
12031403 K; (c) 1 s1 , 12031403 K; and (d) 10 s1 , 12031403 K.
of materials like yield stress and stress limit, though it is suitable process parameters and avoid the occurrence of frac-
affected by the working condition. Cockcroft and Latham ture. It is very significant to guide the practical production.
[29] have not expounded whether the critical damage value
depends on the temperature and strain rate. 2. Materials and Experimental Procedure
The main purpose of the present work is to analyze and
uncover the nature relationships between damage evolution The 3Cr20Ni10W2 austenitic heat-resistant alloy employed in
and deforming parameters of 3Cr20Ni10W2 heat-resistant the present investigation is provided in the form of bar with
alloy and furthermore to construct ductile fracture criteria the diameter of 100 mm. Its chemical compositions (wt. %)
histogram along with deforming parameters. An innovative are as follows: C 0.25, Si 1, Cr 20, Ni 10, Mn 1, W 2, and Fe
concept of damage sensitive rate is brought forth as the (balance). Before the experiment, the homogenized ingot was
essential intermediate quantity to determine ductile fracture scalped to diameter 10 mm and height 12 mm with grooves
criteria. As for the innovative approach, heat physical com- on both sides filled with machine oil mingled with graphite
pression simulations, numerical simulations, and mathemat- powder as lubrication to reduce friction between the anvils
ical computations are necessary, which induces that physical and specimen during hot compression tests. The specimens
experiments and numerical computations provide mutual were resistant heated to a certain temperature at a heating
support to determine the varying ductile fracture criteria rate of 1 K/s by a computer-controlled, servohydraulic Gleeble
(VDFC). Without a doubt, VDFC of 3Cr20Ni10W2 alloy 1500 machine, and held at a certain temperature for 180 s
make it possible to predict the exact fracture moment and by thermocoupled-feedback-controlled AC current to ensure
position during various forming processes. That is to say, the a uniform starting temperature and decrease the material
VDFC obtained in this work can help technicians to choose anisotropy. All the twenty specimens were compressed to
Advances in Mechanical Engineering 3
(a) (b)
Crack
(c) (d)
(e)
Figure 2: The specimen (a) as-received, (b) with a height reduction of 60% at temperature of 1253 K and strain rate of 10 s1 , (c) with a height
reduction of 80% at temperature of 1253 K and strain rate of 10 s1 (d) a height reduction of 60% at temperature of 1203 K and strain rate of
0.1 s1 , (e) and a height reduction of 60% at temperature of 1353 K and strain rate of 0.1 s1 .
a fixed true strain of 0.9163 (height reduction 60%) at the 3. Flow Stress Behavior and
temperatures of 1203 K, 1253 K, 1303 K, 1353 K, and 1403 K and Experiment Results
the strain rates of 0.01 s1 , 0.1 s1 , 1 s1 , and 10 s1 . During the
compressing processes the variations of stress and strain were The true compressive stress-strain curves of 3Cr20Ni10W2
monitored continuously by a personal computer equipped heat-resistant alloy are illustrated in Figures 1(a)1(d), which
with an automatic data acquisition system. In the tests, the show that both deformation temperature and strain rate have
temperatures of the specimens were controlled to within considerable influence on the flow stress of 3Cr20Ni10W2
0.1 K through three thermocouples adhibited affixed to the alloy. Comparing these curves with one another, it is found
specimens. that, for all of specimens after initial yielding, the flow stress
The true stress-strain relationships were derived from decreases monotonically with different softening rates. For a
the nominal stress-strain curves collected according to the specific strain rate, the flow stress decreases markedly with
following formula: = (1 + ), = ln(1 + ), where the increase in temperature. In contrast, for a specific tem-
is the true stress, the nominal stress, the true strain, perature, the flow stress generally increases with the increase
and the nominal strain. of strain rate due to an increase of dislocation density and
4 Advances in Mechanical Engineering
(a) (b)
Figure 3: The cross-sectional microstructure of 3Cr2Ni10W2 alloy (a) with a height reduction of 60% under temperature of 1203 K and strain
rate of 10 s1 (b) and a height reduction of 80% under temperature of 1253 K and strain rate of 10 s1 .
Top die
n
n SDx
RVE
S
In M
Workpiece
Axis of symmetry
Damage
A = 0.000
B = 0.0261 0.209
C = 0.0521
D = 0.0782
E = 0.104
F = 0.130 B
G = 0.156
H = 0.182
I = 0.209 0.139
Max
HGF E DC B Min
0.0695
B
Min 0.000
Max 0.209 0.000
Figure 6: The damage distribution of the height reduction 60% under temperature of 1253 K and strain rate of 0.01 s1 .
The results of heat physical compression experiments region. Therefore, macrocracks appear on the upsetting drum
are shown in Figure 2. Figure 2(a) shows the specimen firstly and then extend to the internal.
as-received; Figure 2(b) shows the deformed specimen with
a height reduction of 60% at temperature of 1253 K and strain 4. Basis for Damage Computation
rate of 10 s1 , on which no visible crack appears; Figure 2(c)
shows the deformed specimen with a height reduction of 4.1. Cockcroft-Lathams DFC. Generally, workability depends
80% at temperature of 1253 K and strain rate of 10 s1 , on on the local conditions of stress, strain, strain rate, and
which visible cracks appear; Figure 2(d) shows the deformed temperature in combination with material factors, such as the
specimen with a height reduction of 60% at temperature of resistance of a metal to failure. Failure in bulk metal forming
1203 K and strain rate of 0.1 s1 , on which no visible crack usually occurs as ductile fracture, rarely as brittle fracture.
appears; Figure 2(e) shows the deformed specimen with a Therefore, a ductile fracture criterion is very important and
height reduction of 60% at temperature of 1353 K and strain necessary for designing an optimum plastic forming process
rate of 0.1 s1 , on which cracks appear. without failure. According to various hypotheses, many
The microstructures on the section plane of specimen criteria for ductile fracture have been proposed empirically
were examined and analyzed under the optical microscope, as well as theoretically. Cockcroft and Latham [9, 1619],
as shown in Figure 3. Figure 3(a) shows the microstructure based on cumulative damage theory, developed a damage
on the cross section of the deformed specimen with a height computation module based on a critical value of the tensile
reduction of 60% under temperature of 1203 K and strain rate strain energy per unit volume, which has been widely applied
of 10 s1 . It can be seen that the deformed metal partially in the field of bulk forming with high reliability. Therefore, the
transforms to a microstructure of approximately equiaxed damage module of Cockcroft-Latham is convenient for both
defect-free grains which are predominantly bounded by experimental and numerical approaches is used in the present
high angle boundaries (i.e., a recrystallized microstructure) investigation to estimate if and where surface fracture occurs
by relatively localized boundary migration, and the grain during the deformation process. Cockcroft-Lathams damage
boundaries of the rest of untransformed metal reveal an uni- [9, 16, 17] can be expressed as an amount of work that the ratio
form vector in radial direction due to weak recovery for grain of maximum tensile stress to effective stress carries out
boundary torsion. Across the recrystallized microstructure, through the applied equivalent strain in a metal-working
no crack can be found. Figure 3(b) shows the microstruc- process; that is,
ture on the cross section of the deformed specimen with
a height reduction of 80% under temperature of 1253 K = d, (1)
and strain rate of 10 s1 . By comparison with Figure 3(a), 0
it can be seen that more deformed metal transforms to where is the total equivalent strain corresponding to
recrystallized microstructure due to higher mobility of grain fracture failure; the damage module is not based on a
boundaries (growth kinetics), and all the grains tend to micromechanical model to fracture but simply recognizes the
be more homogeneous due to stronger adaptivity for grain dependence of the critical at fracture upon the level of the
boundary migration. However, microcracks appear in the largest principal stress. In (1), the maximum damage value,
middle region of the section, which shows that the visible max , is named ductile fracture criteria (DFC), that is, the
cracks on the upsetting drum have extended from the surface critical damage value of the workpiece. The DFC value, max ,
to the center. According to elastic-plastic mechanics theory, is dependent on the material metallurgical properties such
in an upsetting process, the maximum stress appears on the as grain form, grain size, and nonmetallic inclusion content.
upsetting drum, while minimum stress appears in the middle The magnitude of cannot exceed max to failure; when the
6 Advances in Mechanical Engineering
0.30 0.20
0.25
0.16
Maximum damage
Maximum damage
0.20
0.12
0.15
0.08
0.10
0.04
0.05
0.00 0.00
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9
True strain True strain
1203 K 1353 K 1203 K 1353 K
1253 K 1403 K 1253 K 1403 K
1303 K 1303 K
(a) (b)
0.20
0.14
0.16 0.12
Maximum damage
Maximum damage
0.10
0.12
0.08
0.08 0.06
0.04
0.04
0.02
0.00 0.00
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9
True strain True strain
Figure 7: The maximum damage varying during compressing process at different temperatures and strain rates (a) 0.01 s1 , 12031403 K; (b)
0.1 s1 , 12031403 K; (c) 1 s1 , 12031403 K; and (d) 10 s1 , 12031403 K.
damage value of (1) reaches max , fracture will occur. For this time corresponding to fracture failure, and is the variable
reason, by comparing with max , the risk of material failure time increment used in the FE analysis.
during processing can be assessed.
In order to calculate by FE simulation, (1) has to be 4.2. Approach to Determine Cockcroft-Latham-Type DFC.
converted to an appropriate discrete expression that is con- From Figure 1, it can be seen that 3Cr20Ni10W2 heat-
venient for FE code: resistant alloy is a typical strain-softening alloy. As is well
known, for strain-hardening alloy the fracture criteria can
d
be determined by directly comparing the simulation with the
= d = d , (2) destructive experiments in terms of the critical deformation
0 d 0 0
level. However, for strain-softening alloy the ductile fracture
criteria can not be determined directly because it is difficult to
where is the equivalent strain rate as (1) calculated from find visible cracks on the surface of deformed billet and the
the individual principle strain-rate components, is the total stress-strain curveshave not apparent fracture points. Thus,
Advances in Mechanical Engineering 7
0.26 normal and its abscissa along the direction (as shown in
Figure 4) [20]. The value of the damage (, , ) attached
0.24
to the point in the direction and the abscissa is
0.22
(, , ) = ,
Maximum damage
0.20 (4)
0.18
where is the area of intersection of all the flaws with the
0.16 plane defined by the normal and abscissa and is the total
0.14 area at the intersection plane.
In (3), damage is bounded as 0 , where
0.12 is a critical damage value corresponding to the decohesion of
0.10
atoms in a representative volume element, = 0 represents
the undamaged RVE material, and = represents the
2.0 1.5 1.0 0.5 0.0 0.5 1.0 rupture failure in the remaining resisting area. As rupture
1 )
Lg (s failure has occurred, damage will keep increasing in a
1203 K 1353 K
growth rate near to zero or equal to zero with increasing
1253 K 1403 K deformation strain. It means that the damage will not be
1303 K sensitive to deformation.
0.9 0.55
0.8 0.50
0.45
0.7
0.6
0.35
0.5 0.30
0.4 0.25
0.3 0.20
0.15
0.2
0.10
0.1
0.05
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0
True strain True strain
0.40
Damage sensitive rate
0.40
0.35 0.35
0.30 0.30
0.25 0.25
0.20 0.20
0.15 0.15
0.10 0.10
0.05 0.05
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0
True strain True strain
Figure 9: The variation of damage sensitive rate under different temperatures and strain rates (a) 0.01 s1 , 12031403 K; (b) 0.1 s1 , 12031403 K;
(c) 1 s1 , 12031403 K; and (d) 10 s1 , 12031403 K.
no obvious regularity for the strain rates of 0.01 s1 , 0.1 s1 , Cockcroft-Latham damage (as (3)) in plastic deformation
and 10 s1 . In contrast, for a fixed temperature, at first, the (step ) at different temperatures and strain rates were
maximum cumulated damage decreases rapidly and then calculated and shown in Figures 9(a)9(d). It can be seen
slightly increases; finally, the damage value decreased again that, for all the deformation conditions, step decreases to the
(as shown in Figure 8). Further, it can be summarized that trough point rapidly before true strain 0.10.15, and then it
the changes in strain rate have a more significant effect on the slightly increases in true strain 0.150.2, soon after which it
cumulated damage. decreases to zero by slow degrees in true strain range 0.2
0.92. In this study, the zero point has a tolerance of 00.03,
5.2. Evaluation of Varying Ductile Fracture Criteria (VDFC). and it is assumed as the fracture time in tolerance limits. That
In order to evaluate the ductile fracture criteria, the fracture is to say, when step decreases to 0.03, it means that fractures
occurrence and the damage value at fracture time are nec- have appeared. To find the fracture time, the point arrays after
essary to be made certain. Based on the damage cumulating true strain 0.6 are picked out from each incremental ratio
processes as shown in Figure 7, the sensitive rates of varying curve and fitted linearly. The intersection of line fitted
Advances in Mechanical Engineering 9
1400
0.11
0.12
1365
0.16
0.13
0.14
Temperature (K)
DFC
DFC
0.15 0.15
0.14 0.14
0.12 0.13 0.13
1260 0.12 0.12
0.13
0.13 0.11 0.11
0.14 0.1 0.1
1225 0.17 0.09 0.09
0.16 0.14 0.16
0.18
50
1
14 50
.5
2.0 1.5 1.0 0.5 0.0 0.5 1.0 12 le
0
00 s ca
Tem 14
.5
1 00 g
Lg (s ) nL
0.5
per
atu 13 50 ei
rat
1
re ( 13
K) ain
Str
(a) (b)
Figure 10: The temperature and strain rate effect on the ductile fracture criteria of 3Cr20Ni10W2 alloy: (a) contour plot and (b) response
surface.
and horizontal axis is obtained, and it is made certain as the of 3Cr20Ni10W2 alloy, it should choose these deformation
fracture step. conditions to reduce fracture risk.
As the fracture time has been determined, and then based Comparing Figures 2 and 10, it is clear that the predict
on Figure 7, the fracture analysis step and the correspondent results of FEA corresponding to the experiment results. The
DFC under different deformation conditions can be evalu- crack initialization takes place at the edge of the workpiece
ated. The contour plot and response surface of DFC in Figures due to the maximum damage value. Besides, the fracture time
10(a)-10(b) indicate the nature influence of temperature and predicted based on the VDFC conforms to the experimental
strain rate on DFC of 3Cr20Ni10W2 alloy. Figures 10(a)- results.
10(b) show that DFC of 3Cr20Ni10W2 alloy are not constant
but change in a range of 0.0990.197, and thus they can
be defined as varying ductile fracture criteria (VDFC) and
6. Conclusion
described as a function of strain rate and temperature (as An innovative approach involving heat physical compression
in Table 1). In the scatter diagram, there is a valley under experiments, numerical simulations, and mathematical com-
the deformation conditions 12731353 K & 0.0320.316 s1 , putations was brought forth to evaluate the ductile damage
on both sides of which DFC value increases. What is worth cumulating process and DFC diagram along with various
explaining is that the forming process will be worse under deformation conditions for 3Cr20Ni10W2 alloy. The main
these conditions due to lower DFC, in addition to which, the conclusions can be summarized as follows.
deformation domains (12031253 K & 0.010.016 s1 , 1403
1453 K & 0.010.016 s1 , and 12031228 K & 0.1781.29 s1 ) (1) As for 3Cr20Ni10W2 alloy, a typical strain-softening
with lower fracture risk corresponding to higher VDFC material, ductile damage starts at work hardening
have been identified. Therefore, in bulk forming operations phase, and the damage cumulation is more sensitive
10 Advances in Mechanical Engineering
in work hardening phase than in work softening alloy, Transactions of Nonferrous Metals Society of China, vol.
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