08

08/05/2017 13:41:56
Welcome to Minitab, press F1 for help.
Box-Behnken Design
Factors: 3 Replicates: 1
Base runs: 15 Total runs: 15
Base blocks: 1 Total blocks: 1
Center points: 3
Response Surface Regression: FAME% versus Residence ti, Amount of ca, ...
The analysis was done using coded units.
Estimated Regression Coefficients for FAME%
Term Coef SE Coef T P

Constant 94.3000 0.6900 136.657 0.000
Residence time 4.2500 0.4226 10.058 0.000
Amount of catalyst 0.0625 0.4226 0.148 0.888
Methanol to oil ratio 1.3625 0.4226 3.224 0.023
Residence time*Residence time 1.8625 0.6220 2.994 0.030
Amount of catalyst* -5.8625 0.6220 -9.425 0.000
Amount of catalyst
Methanol to oil ratio* -3.5625 0.6220 -5.727 0.002
Methanol to oil ratio
Residence time*Amount of catalyst 1.0500 0.5976 1.757 0.139
Residence time*Methanol to oil ratio -3.3500 0.5976 -5.606 0.002
Amount of catalyst* 0.1750 0.5976 0.293 0.781
S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%
Analysis of Variance for FAME%
Source DF Seq SS Adj SS Adj MS F P

Regression 9 395.671 395.671 43.9634 30.78 0.001
Linear 3 159.382 159.382 53.1275 37.19 0.001
Square 3 186.866 186.866 62.2886 43.60 0.001
Interaction 3 49.422 49.422 16.4742 11.53 0.011
Residual Error 5 7.142 7.142 1.4285
Lack-of-Fit 3 7.142 7.142 2.3808 * *
Pure Error 2 0.000 0.000 0.0000
Total 14 402.813
Estimated Regression Coefficients for FAME% using data in uncoded units
Term Coef
Constant -9449.94
Residence time 14.3475
Amount of catalyst 113.175
Methanol to oil ratio 19530.0
Residence time*Residence time 0.0186250
Amount of catalyst* -23.4500
Amount of catalyst
Methanol to oil ratio* -10133.3
Residence time*Amount of catalyst 0.210000
Residence time*Methanol to oil ratio -17.8667
Amount of catalyst* 18.6667

Constant 94.3000 0.6900 136.657 0.000
Residence time 4.2500 0.4226 10.058 0.000
Amount of catalyst
S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Regression 9 395.671 395.671 43.9634 30.78 0.001
Linear 3 159.382 159.382 53.1275 37.19 0.001
Square 3 186.866 186.866 62.2886 43.60 0.001
Interaction 3 49.422 49.422 16.4742 11.53 0.011
Residual Error 5 7.142 7.142 1.4285
Lack-of-Fit 3 7.142 7.142 2.3808 * *
Pure Error 2 0.000 0.000 0.0000
Total 14 402.813
Obs StdOrder FAME% Fit SE Fit Residual St Resid

1 4 96.800 95.663 1.035 1.138 1.90
2 13 94.300 94.300 0.690 0.000 0.00
3 3 84.400 85.063 1.035 -0.662 -1.11
4 7 93.800 93.063 1.035 0.738 1.23
5 9 83.700 83.625 1.035 0.075 0.13
6 11 86.400 86.000 1.035 0.400 0.67
7 12 86.400 86.475 1.035 -0.075 -0.13
8 6 98.100 98.838 1.035 -0.737 -1.23
9 2 94.100 93.438 1.035 0.662 1.11
10 1 85.900 87.038 1.035 -1.137 -1.90
11 14 94.300 94.300 0.690 0.000 0.00
12 5 84.700 83.638 1.035 1.062 1.78
13 10 83.000 83.400 1.035 -0.400 -0.67
14 15 94.300 94.300 0.690 0.000 0.00
15 8 93.800 94.863 1.035 -1.063 -1.78
Term Coef
Constant -9449.94
Amount of catalyst

Constant 94.3000 0.6900 136.657 0.000
Residence time 4.2500 0.4226 10.058 0.000
Amount of catalyst
S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Regression 9 395.671 395.671 43.9634 30.78 0.001
Linear 3 159.382 159.382 53.1275 37.19 0.001
Square 3 186.866 186.866 62.2886 43.60 0.001
Interaction 3 49.422 49.422 16.4742 11.53 0.011
Residual Error 5 7.142 7.142 1.4285
Lack-of-Fit 3 7.142 7.142 2.3808 * *
Pure Error 2 0.000 0.000 0.0000
Total 14 402.813

1 4 96.800 95.663 1.035 1.138 1.90
2 13 94.300 94.300 0.690 0.000 0.00
3 3 84.400 85.063 1.035 -0.662 -1.11
4 7 93.800 93.063 1.035 0.738 1.23
5 9 83.700 83.625 1.035 0.075 0.13
6 11 86.400 86.000 1.035 0.400 0.67
7 12 86.400 86.475 1.035 -0.075 -0.13
8 6 98.100 98.838 1.035 -0.737 -1.23
9 2 94.100 93.438 1.035 0.662 1.11
10 1 85.900 87.038 1.035 -1.137 -1.90
11 14 94.300 94.300 0.690 0.000 0.00
12 5 84.700 83.638 1.035 1.062 1.78
13 10 83.000 83.400 1.035 -0.400 -0.67
14 15 94.300 94.300 0.690 0.000 0.00
15 8 93.800 94.863 1.035 -1.063 -1.78

Term Coef
Constant -9449.94
Amount of catalyst
The analysis was done using uncoded units.

Constant -9449.9 1513.84 -6.242 0.002
Residence time 14.3 3.02 4.758 0.005
Amount of catalyst
S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Regression 9 395.671 395.671 43.9634 30.78 0.001
Linear 3 159.382 81.429 27.1430 19.00 0.004
Square 3 186.866 186.866 62.2886 43.60 0.001
Interaction 3 49.423 49.423 16.4742 11.53 0.011
Residual Error 5 7.142 7.142 1.4285
Lack-of-Fit 3 7.142 7.142 2.3808 * *
Pure Error 2 0.000 0.000 0.0000
Total 14 402.813

1 4 96.800 95.662 1.035 1.138 1.90
2 13 94.300 94.300 0.690 0.000 0.00
3 3 84.400 85.062 1.035 -0.662 -1.11
4 7 93.800 93.062 1.035 0.738 1.23
5 9 83.700 83.625 1.035 0.075 0.13
6 11 86.400 86.000 1.035 0.400 0.67
7 12 86.400 86.475 1.035 -0.075 -0.13
8 6 98.100 98.837 1.035 -0.737 -1.23
9 2 94.100 93.437 1.035 0.663 1.11
10 1 85.900 87.037 1.035 -1.137 -1.90
11 14 94.300 94.300 0.690 0.000 0.00
12 5 84.700 83.637 1.035 1.063 1.78
13 10 83.000 83.400 1.035 -0.400 -0.67
14 15 94.300 94.300 0.690 0.000 0.00
15 8 93.800 94.862 1.035 -1.062 -1.78
11/05/2017 14:35:26

Retrieving project from file: 'C:\Users\user\Desktop\MINITAB.MPJ'

Constant -9449.9 1513.84 -6.242 0.002
Residence time 14.3 3.02 4.758 0.005
Amount of catalyst
S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Regression 9 395.671 395.671 43.9634 30.78 0.001
Linear 3 159.382 81.429 27.1430 19.00 0.004
Square 3 186.866 186.866 62.2886 43.60 0.001
Interaction 3 49.423 49.423 16.4742 11.53 0.011
Residual Error 5 7.142 7.142 1.4285
Lack-of-Fit 3 7.142 7.142 2.3808 * *
Pure Error 2 0.000 0.000 0.0000
Total 14 402.813

1 4 96.800 95.662 1.035 1.138 1.90
2 13 94.300 94.300 0.690 0.000 0.00
3 3 84.400 85.062 1.035 -0.662 -1.11
4 7 93.800 93.062 1.035 0.738 1.23
5 9 83.700 83.625 1.035 0.075 0.13
6 11 86.400 86.000 1.035 0.400 0.67
7 12 86.400 86.475 1.035 -0.075 -0.13
8 6 98.100 98.837 1.035 -0.737 -1.23
9 2 94.100 93.437 1.035 0.663 1.11
10 1 85.900 87.037 1.035 -1.137 -1.90
11 14 94.300 94.300 0.690 0.000 0.00
12 5 84.700 83.637 1.035 1.063 1.78
13 10 83.000 83.400 1.035 -0.400 -0.67
14 15 94.300 94.300 0.690 0.000 0.00
15 8 93.800 94.862 1.035 -1.062 -1.78

Constant -9449.9 1513.84 -6.242 0.002
Residence time 14.3 3.02 4.758 0.005
Amount of catalyst
S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Regression 9 395.671 395.671 43.9634 30.78 0.001
Linear 3 159.382 81.429 27.1430 19.00 0.004
Square 3 186.866 186.866 62.2886 43.60 0.001
Interaction 3 49.423 49.423 16.4742 11.53 0.011
Residual Error 5 7.142 7.142 1.4285
Lack-of-Fit 3 7.142 7.142 2.3808 * *
Pure Error 2 0.000 0.000 0.0000
Total 14 402.813

1 4 96.800 95.662 1.035 1.138 1.90
2 13 94.300 94.300 0.690 0.000 0.00
3 3 84.400 85.062 1.035 -0.662 -1.11
4 7 93.800 93.062 1.035 0.738 1.23
5 9 83.700 83.625 1.035 0.075 0.13
6 11 86.400 86.000 1.035 0.400 0.67
7 12 86.400 86.475 1.035 -0.075 -0.13
8 6 98.100 98.837 1.035 -0.737 -1.23
9 2 94.100 93.437 1.035 0.663 1.11
10 1 85.900 87.037 1.035 -1.137 -1.90
11 14 94.300 94.300 0.690 0.000 0.00
12 5 84.700 83.637 1.035 1.063 1.78
13 10 83.000 83.400 1.035 -0.400 -0.67
14 15 94.300 94.300 0.690 0.000 0.00
15 8 93.800 94.862 1.035 -1.062 -1.78

Constant -9449.9 1513.84 -6.242 0.002
Residence time 14.3 3.02 4.758 0.005
Amount of catalyst
S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Regression 9 395.671 395.671 43.9634 30.78 0.001
Linear 3 159.382 81.429 27.1430 19.00 0.004
Square 3 186.866 186.866 62.2886 43.60 0.001
Interaction 3 49.423 49.423 16.4742 11.53 0.011
Residual Error 5 7.142 7.142 1.4285
Lack-of-Fit 3 7.142 7.142 2.3808 * *
Pure Error 2 0.000 0.000 0.0000
Total 14 402.813

1 4 96.800 95.662 1.035 1.138 1.90
2 13 94.300 94.300 0.690 0.000 0.00
3 3 84.400 85.062 1.035 -0.662 -1.11
4 7 93.800 93.062 1.035 0.738 1.23
5 9 83.700 83.625 1.035 0.075 0.13
6 11 86.400 86.000 1.035 0.400 0.67
7 12 86.400 86.475 1.035 -0.075 -0.13
8 6 98.100 98.837 1.035 -0.737 -1.23
9 2 94.100 93.437 1.035 0.663 1.11
10 1 85.900 87.037 1.035 -1.137 -1.90
11 14 94.300 94.300 0.690 0.000 0.00
12 5 84.700 83.637 1.035 1.063 1.78
13 10 83.000 83.400 1.035 -0.400 -0.67
14 15 94.300 94.300 0.690 0.000 0.00
15 8 93.800 94.862 1.035 -1.062 -1.78
Residual Plots for FAME%
30/05/2017 15:34:07

Retrieving project from file: 'C:\USERS\USER\DESKTOP\MATLAP\MINITAB.MPJ'
* WARNING * Error attempting to open or read Graphics file 'Residual Plots
* for FAME%'.
* WARNING * Error attempting to open or read Project file.

Constant -9449.9 1513.84 -6.242 0.002
Residence time 14.3 3.02 4.758 0.005
Amount of catalyst
S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Regression 9 395.671 395.671 43.9634 30.78 0.001
Linear 3 159.382 81.429 27.1430 19.00 0.004
Square 3 186.866 186.866 62.2886 43.60 0.001
Interaction 3 49.423 49.423 16.4742 11.53 0.011
Residual Error 5 7.142 7.142 1.4285
Lack-of-Fit 3 7.142 7.142 2.3808 * *
Pure Error 2 0.000 0.000 0.0000
Total 14 402.813

1 4 96.800 95.662 1.035 1.138 1.90
2 13 94.300 94.300 0.690 0.000 0.00
3 3 84.400 85.062 1.035 -0.662 -1.11
4 7 93.800 93.062 1.035 0.738 1.23
5 9 83.700 83.625 1.035 0.075 0.13
6 11 86.400 86.000 1.035 0.400 0.67
7 12 86.400 86.475 1.035 -0.075 -0.13
8 6 98.100 98.837 1.035 -0.737 -1.23
9 2 94.100 93.437 1.035 0.663 1.11
10 1 85.900 87.037 1.035 -1.137 -1.90
11 14 94.300 94.300 0.690 0.000 0.00
12 5 84.700 83.637 1.035 1.063 1.78
13 10 83.000 83.400 1.035 -0.400 -0.67
14 15 94.300 94.300 0.690 0.000 0.00
15 8 93.800 94.862 1.035 -1.062 -1.78
31/5/2017 14:23:47

Retrieving project from file: 'G:\MINITAB.MPJ'

Constant -9449.9 1513.84 -6.242 0.002
Residence time 14.3 3.02 4.758 0.005
Amount of catalyst
S = 1.19520 PRESS = 114.28

R-Sq = 98.23% R-Sq(pred) = 71.63% R-Sq(adj) = 95.04%
Source DF Seq SS Adj SS Adj MS

Regression 9 395.671 395.671 43.963
Linear 3 159.382 81.429 27.143
Residence time 1 144.500 32.343 32.343
Amount of catalyst 1 0.031 4.960 4.960
Methanol to oil ratio 1 14.851 51.250 51.250
Square 3 186.866 186.866 62.289
Residence time*Residence time 1 24.005 12.808 12.808
Amount of catalyst*Amount of catalyst 1 116.000 126.901 126.901
Methanol to oil ratio*Methanol to oil ratio 1 46.861 46.861 46.861
Interaction 3 49.423 49.423 16.474
Residence time*Amount of catalyst 1 4.410 4.410 4.410
Residence time*Methanol to oil ratio 1 44.890 44.890 44.890
Amount of catalyst*Methanol to oil ratio 1 0.123 0.123 0.123
Residual Error 5 7.142 7.142 1.428
Lack-of-Fit 3 7.142 7.142 2.381
Pure Error 2 0.000 0.000 0.000
Total 14 402.813
Source F P
Regression 30.78 0.001
Linear 19.00 0.004
Residence time 22.64 0.005
Amount of catalyst 3.47 0.121
Methanol to oil ratio 35.88 0.002
Square 43.60 0.001
Residence time*Residence time 8.97 0.030
Amount of catalyst*Amount of catalyst 88.83 0.000
Methanol to oil ratio*Methanol to oil ratio 32.80 0.002
Interaction 11.53 0.011
Residence time*Amount of catalyst 3.09 0.139
Residence time*Methanol to oil ratio 31.42 0.002
Amount of catalyst*Methanol to oil ratio 0.09 0.781
Residual Error
Lack-of-Fit * *
Pure Error
Total

1 4 96.800 95.662 1.035 1.138 1.90
2 13 94.300 94.300 0.690 0.000 0.00
3 3 84.400 85.062 1.035 -0.662 -1.11
4 7 93.800 93.062 1.035 0.738 1.23
5 9 83.700 83.625 1.035 0.075 0.13
6 11 86.400 86.000 1.035 0.400 0.67
7 12 86.400 86.475 1.035 -0.075 -0.13
8 6 98.100 98.837 1.035 -0.737 -1.23
9 2 94.100 93.437 1.035 0.663 1.11
10 1 85.900 87.037 1.035 -1.137 -1.90
11 14 94.300 94.300 0.690 0.000 0.00
12 5 84.700 83.637 1.035 1.063 1.78
13 10 83.000 83.400 1.035 -0.400 -0.67
14 15 94.300 94.300 0.690 0.000 0.00
15 8 93.800 94.862 1.035 -1.062 -1.78

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08/05/2017 13:41:56

Welcome to Minitab, press F1 for help.

The analysis was done using coded units.

Estimated Regression Coefficients for FAME%

Term Coef SE Coef T P

S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Analysis of Variance for FAME%

Source DF Seq SS Adj SS Adj MS F P

Estimated Regression Coefficients for FAME% using data in uncoded units

The analysis was done using coded units.

Estimated Regression Coefficients for FAME%

Term Coef SE Coef T P

S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Analysis of Variance for FAME%

Source DF Seq SS Adj SS Adj MS F P

Obs StdOrder FAME% Fit SE Fit Residual St Resid

Estimated Regression Coefficients for FAME% using data in uncoded units

The analysis was done using coded units.

Estimated Regression Coefficients for FAME%

Term Coef SE Coef T P

S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Analysis of Variance for FAME%

Source DF Seq SS Adj SS Adj MS F P

Obs StdOrder FAME% Fit SE Fit Residual St Resid

Estimated Regression Coefficients for FAME% using data in uncoded units

The analysis was done using uncoded units.

Estimated Regression Coefficients for FAME%

Term Coef SE Coef T P

S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Analysis of Variance for FAME%

Source DF Seq SS Adj SS Adj MS F P

Obs StdOrder FAME% Fit SE Fit Residual St Resid

Welcome to Minitab, press F1 for help.

The analysis was done using uncoded units.

Estimated Regression Coefficients for FAME%

Term Coef SE Coef T P

S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Analysis of Variance for FAME%

Source DF Seq SS Adj SS Adj MS F P

Obs StdOrder FAME% Fit SE Fit Residual St Resid

Estimated Regression Coefficients for FAME%

Term Coef SE Coef T P

S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Analysis of Variance for FAME%

Source DF Seq SS Adj SS Adj MS F P

Obs StdOrder FAME% Fit SE Fit Residual St Resid

The analysis was done using uncoded units.

Estimated Regression Coefficients for FAME%

Term Coef SE Coef T P

S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Analysis of Variance for FAME%

Source DF Seq SS Adj SS Adj MS F P

Obs StdOrder FAME% Fit SE Fit Residual St Resid

Residual Plots for FAME%

Welcome to Minitab, press F1 for help.

The analysis was done using uncoded units.

Estimated Regression Coefficients for FAME%

Term Coef SE Coef T P

S = 1.195 R-Sq = 98.2% R-Sq(adj) = 95.0%

Analysis of Variance for FAME%

Source DF Seq SS Adj SS Adj MS F P

Obs StdOrder FAME% Fit SE Fit Residual St Resid

Residual Plots for FAME%

Welcome to Minitab, press F1 for help.