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CN 101353305 B 1/6 }n

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3
CN 101353305 B 2/6 }n

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CN 101353305 B 3/6 }n

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CN 101353305 B 5/6 }n

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@~:fUH~ 130 C J;f@Jt~~5l7-K, ~J ~ifilili~ 100 C, JJoJ\it'ri~Jt;ff 2 1J\ S1 J1@1J! IX
tt~ffl ~t'E. iWf{X5ti9r, ~ffi,~fi*Z-Wicrr*l - TW~B~l&$ 99. 5% ~ffl Kar 1 Fischer
Ti trator ?tHr*Z- Wictr*l - TW~B~15"7-K.S. o. 15 %;I[X 10 ~ 30ml/kg B~Jf.S.xt:*: M
:fo~,~i'. ~*Z-Wttr*l- rw~, *mi!{:ll{tffl, m1,;-~ 10% s~*Z-Wttr*l- rw~s~tPJ
M~*:*:Msm*mMH~~,tE~~~~~ffl mm*~~1-:r~Z-Mrr*l-T~ 0

x:ll
[0061] ~~{} 3
[0062] ffi-ftt1-:rS1, P] &@~~NJ\tr*l 1 Wte;, iETWJ 2 Wte;;fP{t1tff o. 01 Wte;, JJoiH~
130C, :3f PJ &@~~ B~imAffi~, tEtfltiI!GJt;ff;fP@ltt~:;{;T itt:ff W~1t&@, 3 &@~~ B~
.11)'::S; 7 S11f Jt&@, :ff~ffl1@Jt~*:'i=xt &@~1@Jt~~5lW$ JE&@~ilf&~if{~f 1l0C
J, PJ &@~NAMm: o. 8 Wte;, {11tff o. 005 Wte;, JJom:ff~~ilflttE 130C, jffi,}\ffi~JE?t
Jt;ff &@ 2 1J\S1 J, fii Z-Wictr*l -TW~:tilrfb, 1@Jt~~5lJ~ifilili~ B0CJittif ~ T -
1JC11Jnx~ :OOffi-1JC11Jnx~~fflW~1t&@1-:~B~7-K:fP~~1ttr*Jre:'i=i;&lt 5%~ 10 %B~iJnxii,
1Ei~11i1iJJoJ\&@~JtJt1l 30 ?ttrr, mr:'i=?t ~J, t!Pili T ~&=1i ;ffi-=1_x11i~~Uffl-=t1t
s~7J<:fo~~1ttr*Jre:'i:1;&1t 5%~ 10 %s~11i1i, 1Ei~11i1iJJoJ\&@~JtJt1l 30 ?ttrr, mr:'i=
5t ~J, t!Plli T ~&:ii ;@ffi -1JC11Jnx~~ffl-=f1$Jt;fo~~1ttr*Jre:'i=1;&lt 5%~ 10 %B~iftx
ii, 1Ei~11Jnx1iJJoJ\&@~JJt1-'F' 30 ?ttrfi, mr:'i=?t~J, t!Plli T ~&:ii ;ilfox~3'G*J, &@~
:fHH~ 130C J;f@Jt~~5l7-K, ~J ~ifilili~ l00C, JJoJ\it'ri~Jt;ff 2 1J\S1 J1@1J! IXtt~ffl ~
t'E.iWf1X5ti9r' ~ffi,~fi*Z-Wictr*l - TW~B~l&$ 99. 5% ~ffl Kar 1 Fischer Ti trator
o

5tttr*Z-W1crr*l-TW~B~15"7-K.S. o. 15% ;tX 10 ~ 30ml/kg B~JfU.S.xt:*: m;t;fP~l'a~i:D


~* l. Wictr*l - TW~, *m!{:ll{tffl, ffl 15"~ 10 %B~* l. Wictr*l - TW~ B~tAJf4PJ*:*:
Msm*mMH~~,tE~~~~~fflmm*~~1-:r~Z-Mtr*l-T~x:ll
[0063] ~~{} 4
[0064] ffi=ttt1-:rS1, PJ &@~~NJ\tr*l 1 Wte;, iETWJ 2 Wte;;fP{t1tJfU o. 01 Wte;, JJoiH~
130 C, :3f PJ &@~ ~ B~imAffi~, tEtfltiI!GJt;ff ;fP@l tt~:;{;T ittif W~1t&@, 3 &@~ ~ B~
.11)'::S; 7 S11f Jt&@, :ff~ffl1@Jt~*:'i=xt &@~1@Jt~~5lW$ JE&@~ilf&~if{~f 1l0C
J, PJ &@~NAMm: o. 8 Wte;, {11tJfU o. 005 Wte;, JJom:ff~~ilflttE 130 C, jffi,}\ffi~JE
?tJt;ff &@ 2 1J\S1 J, fii Z-Wictr*l- TW~:tilrfb, 1@Jt~~5lJ ~ifilili~ B0C Jitt:ff ~ T
-~N~:OOffi-~N~~fflffi-ftt1-:rS1ffi-~N~~ili~&:*~~~~~re:'i=*lt
7
CN 101353305 B 6/6 }n

5%~ 10%B~iJnxil,tEi~iftxilJJoJ\&@~J~t-'!': 30 7ttrfi,fftlt5t~J,t!Fl:Br~Jl:1l ;~


= 1JC iJnx15tlU ffl ** W~ 1t&@jjJ_'f P>G B~ 7-K:fl ~ $(.1,t ~ @cJf i;&Jl'. 5%~ 1o%B~ iJnxil, tE i~
{Jnx1,&jJQJ\&@~J~1-'f: 30 7ttrr, fft1f7t ~J, t!HB r ~Jjj,& ;@~ - 1JC{jnx1Jt;;fUffl -=f1tJt;fP
~$(.1t~@c1fi;&Jl'.7J 5%~ 10 %B~iftxil, tEi~iJnxilJJoJ\&@~J~t-'!': 30 7ttrr, fft1f7t ~J,
t!Fili r ~JJl1l ;iJnx15t:3'EitJ, &@~fr1H~ 13oc JtrnJt~mlJt, ~J ~ifiH~ 1ooc, JJoJ\
ittt~~t-'!': 2 !J\ S1 ] trniJt o IfXttlUffl ~t 'E. il1X7t i9r' ~ffi,~ 1i* G W5trr*l~ - TW~ B~ L&~ 7J
99. 5%alUfflKarlFischer Titrator'5ti9r*Z,W5trrtl~=-Tw~s~137-K.S.7J0.15%;I[X 10~
30ml/kg B~JfU.S.xt:*: l M:fP~l'a~~ o ~*Z,W5trr*l~ - TW~, *m !tll1tffl, ffl13~ 10 %B~
*Z,Mrr*l~-T~~~M~~:*:Msm*mMH~~,ft~~~~~ffl mm*R~ 0

f=B~ Z,W5trr*l~ -TW~x:ll


[0065] * *
R ~ mffl Jt1m ~ :i:!Hf R ~ B~ ~ 1, -~,ltt:J} *HiE B~ JI_ 1* % A *tt!f~ [E] Jlt' xit
o

M~-~*~'*R~~L~~~~~mR~~~~*R~~~~ffi~~~~*R~&
lUJ}-*4=5t~ili B~*R~ s~f!E, ffi L~B~~~**t~ili*R~ s~f!E, IEIJ1tft-'=5*R~ B~
&~J}-*4=5ffl~~13-~~f!E~~ff~~~m@~JJ~~fflft&~J}*-=f=5~f!E~o

8
CN 101353305 B
1/2 }n

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120C---130C

TBC ffl. ir

F&ATBC

9
CN 101353305 B 2/2 ]n

fT -f1Ht.1f!J
iE T lf
Xitl:!3*
l 20C,......130C

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-~1i~
TBC ffl it
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lf tr=rn, fflHt1f!J
J,j" EJf *
fll.t1*~ 120C Ji fiY. 2 ,j, n-t
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ATBC ffl..Hi

a N-1 U==lkilltltfl Nllt~ 11211


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10

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