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Lake Charles Clean Energy, LLC

Lake Charles Clean Energy Project


Document ID
4200 STPD MeOH Unit S-03848 P59001-X 0
Job No. Doc. No Rev.
Page Item No.
Product polisher unit
1 of 4
09-X-0001

Process Specification
for
09-X-0001
Product polisher unit

Revision Description Date Made By Chd. By Appd. By


0 First Issue 23-Aug-2013 RKUM GOPA JYH
Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
Lake Charles Clean Energy, LLC
Lake Charles Clean Energy Project
Document ID
4200 STPD MeOH Unit S-03848 P59001-X 0
Job No. Doc. No Rev.
Page Item No.
Product polisher unit
2 of 4
09-X-0001

Datasheet for General Reactor


General Equipment Information
Design case EOR
Location Outdoor

Operating Data
Inlet
Temperature 113 F Pressure 34 psig
Liquid flow 350000 lb/h Liquid density 48.02 lb/ft
Outlet
Temperature 113 F Pressure 26 psig
Liquid flow 350000 lb/h Liquid density 48.02 lb/ft

Reactor Vessel
Mechanical Design Conditions
Fluid description Methanol
Design temperature (min.) 14 F Design pressure (min.) psig
Design temperature (max.) 220 F Design pressure (max.) 1) 225 psig
Vessel
Inner diameter 117 107 in Tangent to tangent distance 296.5 in
Construction code ASME Sec. VIII Stress relieving According to code
Construction material CS Corrosion allowance 0.125 in
Insulation purpose None Insulation thickness in
Top head type Spherical Bottom head type Spherical

Catalyst Bed
Reactor Inlet Arrangement
Type Deflector plate
Layers (from Top)
Description Size Volume Unit Height Unit Rem.
Amberlyst 15 wet 600-850 m 1458 ft 281 in 2)
Ceramic balls 1" 63 ft 26.75 in
Catalyst Bed Support
Type Ellipsoidal dish Topsoe standard 3-1998/U
Ellipsoidal dish diameter 59 in Perforated dish diameter 47.25 in
Design Load for Catalyst Bed Support
Catalyst/inert weight 86360 lb Total design weight (as load) 9.6 psi
Design pressure drop 8.1 psi Total design load 17.7 psi

Nozzles and Connections


Ref. No. SizeDescription Nozzle Device
A 1 8" 10"
Inlet
B 1 8" 10"
Outlet
H 1 12" Handhole Catalyst unloading pipe
M 1 24" Manhole
Catalyst unloading pipe details (nozzle H)
The catalyst unloading pipe is to be filled with 1" ceramic balls and the pipe must extent 4" above the wire mesh.
The inclination of the pipe is to be minimum 30 to horizontal downwards.
A handhole retaining plate is to be installed, reference is made to Topsoe standard 4-1320/U.

Remarks
1 Design pressure to be verified against shut-off pressure of P-0006 A/B and P-0008 A/B during detailed engineering.
2 Maximum expected inlet concentration of TMA in polisher unit is 50 ppb wt.

L2 DC1 C1 rkum 1603475


Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
Lake Charles Clean Energy, LLC
Lake Charles Clean Energy Project
Document ID
4200 STPD MeOH Unit S-03848 P59001-X 0
Job No. Doc. No Rev.
Page Item No.
Product polisher unit
3 of 4
09-X-0001

117 107

A
M

d
T.L.
296.5

262.75

T.L.
18.25

Deflector plate
h = 1.5 x inlet nozzle size, minimum 12 inch

d = 1.5 x inlet nozzle size, minimum 12 inch

All sketch measurements are indicated in inches.


Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS
Lake Charles Clean Energy, LLC
Lake Charles Clean Energy Project
Document ID
4200 STPD MeOH Unit S-03848 P59001-X 0
Job No. Doc. No Rev.
Page Item No.
Product polisher unit
4 of 4
09-X-0001

117 107

T.L.

Wire mesh SS304 1)


Detail A
Wire mesh SS304 2)
6

Perforated area

47.25
59
H
Wire mesh
1" balls Detail A.

Notes:
1. SS304 wire mesh to be placed below the catalyst bed:
- Double layer of 0.007x0.007 inch, wire =0.0055 inch (top)
- 0.125x0.125 inch, wire =0.025 inch (middle)
- 0.375x0.375inch, wire =0.075 inch (bottom)
Size of wire meshes:
- 0.007x0.007 inch mesh to be extended 4 inch up against the reactor inner wall and catalyst chute
- 0.125x0.125 inch mesh to fit with reactor inner wall and catalyst chute
- 0.375x0.375 inch mesh to fit with reactor inner wall and catalyst chute
Wire meshes to be tighten against catalyst chute with labyrint seal arrangement
indicated in detail a. However, 0.1875 inch SS liner is not required around catalyst chute. 0.03125 inch SS
seal strip to be welded directly to catalyst chute.

2. SS304 wire mesh on ellipsoidal dish: double layer of wire mesh: 0.375x0.375 inch opening, wire 0.075 mm
perforation of ellipsoidal dish: 0.75 inch, pitch 1.3125 inch

All sketch measurements are indicated in inches.


Information contained herein is confidential; it may not be used for any purpose other than for which it has been
issued, and may not be used by or disclosed to third parties without written approval of Haldor Topse A/S.
RESEARCH | TECHNOLOGY | CATALYSTS

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