ICL CALIBRATION LABORATORIES, INC. an ISONEC 17025 and ANSUNCSL Z540-1 accredited 1601 Dectar Avenue Sute 118 Sturt, FL 24004 USA “The snncalts in ASTM and lebortonthemometrs 8 hycrometers eevee saeT 0087 eee ene meen om rere wee chute com Setting new standards in catbraton excelence! Report No. U185901_ $0: 129456 (Ghent: SAMPLE CUSTOMER Bate report issued: 05 16-2017 Page T of 3 pages CALIBRATION REPORT FOR PRT & READOUT THE INSTRUMENT DESCRIBED BELOW WAS EXAMINED AND TESTED IN ICL'S ISO/EC 17025 ACCREDITED CALIBRATION LABORATORY. USING MST TRACEABLE REFERENCE STANDARDS, IN ACCORDANCE WITH ICL'S ISONEC 17025 CALIBRATION PROCEDURE REFERENCED BELOW. THIS CALIBRATION MEETS THE REQUIREMENTS OF ISONEC 17025, ANSUINCSL 2540. 1-7994, (WHICH SUPERCEDED AND REPLACED Mit‘STD 456624), AND THE 150-9000 AND QS-9000 SERIES OF QUALITY STANDARDS. (CUSTOMER INFORMATION ‘SAMPLE CUSTOMER ‘STREET ADORESS City, STATE 2P PURCHASE ORDER NUMBER: NOT AVAILABLE ‘SUBMITTED BY: SAMPLE COMPANY DATES DATE CALIBRATED: 05-16-2011 NEXT OUE (SPECIFIED BY CLIENT): May 16, 2012 INSTRUMENT DESCRIPTION ‘SENSOR INFORMATION: MANUFACTURER: HART SCIENTIFIC ‘MODEL NO:5614 SERIAL NO: X300XX DESCRIPTION: 4 wire 100 Ohm secondary standard PRT TEMPERATURE RANGE: -196/420C. ACCURACY TOLERANCE: +/- SEE BELOW SENSOR IMMERSION: Minimum 6 inches recommended [READOUT DEVICE INFORMA TION: MANUFACTURER: HART SCIENTIFC ‘MODEL NO: 715028 ‘SERIAL NO: 300000 READOUT RESOLUTION: .001 ACCURACY TOLERANCE: *7- SEE BELOW “AS FOUND" READOUT CALIBRATION CONSTANTS: Gal0: 010002 C2!100: 0.0009 Cal400- 0.0011 NO CHANGES WERE MADE TO THESE CONSTANTS. NOTE: THE ACCURACY TOLERANCE FOR THIS SYSTEM CALIBRA TION (SENSOR AND READOUT) IS THE ROOT SUM SQUARE OF THE ACCURACY TOLERANCE OF THE SENSOR AND THE ACCURACY TOLERANCE OF THE READOUT DEVICE. SCALE TESTED: °C RESULTS OF PHYSICAL EXAMINATION THE PHYSICAL CONDITION OF THIS INSTRUMENT WAS SATISFACTORY AND IT APPEARED THAT ALL SYSTEMS WERE FUNCTIONAL. [NO INSULA TION RESISTANCE TEST WAS PERFORMED ON THIS SENSOR. THE CONDITION OF THIS INSTRUMENT WAS SATISFACTORY WITH NO VISUALLY APPARENT DEFECTS, UNLESS NOTED BELOW. CALIBRATION PROCEDURE USED {C1 Procedure 05, which is drawn from ASTM E-77, ASTM E-644 and ASTM E1137.ICL CALIBRATION LABORATORIES. INC. Report No. U185901_ $0. 123456 Gent: SAMPLE CUSTOMER Date report issued: 05-16-2011 Page 2 of 3 pages RESULTS OF CALIBRATION Note: the ’As Found! readings were observed using coelticients resident in the non-volatile memory of he clent's readout, which were: IPW: 100.027 of: -7.52808E-04 bé:-302112E-05 8:7 44288E-04 D8: -& 80212-05 "AS FOUND’ VALUES: NomaL TEST ACTUAL TEST TEMPERATURE TEMPERATURE 9-010°¢ ACCEPT LIMIT* PMU MEASUREMENT. te ord UNCERTAINTY k=2 0.0160°% 020329; 920330; 070333; C 0:00: 020257; 0:010°C -0:008°¢ © 0:0160°C AS CAN BE DETERMINED FROM THE INFORMATION PRESENTED IN THE TABLE ABOVE, ONE OR MORE OF THE ‘AS FOUND" READINGS (OF THIS DEVICE WERE EITHER BEYOND THE ‘ACCEPT LIMIT”, RESULTING IN A DECLARATION OF ‘MARGINAL’, OR WERE BEYOND THE ‘ACTUAL TOLERANCE. ACCORDINGLY, AN ADJUSTMENT WAS UNDERTAKEN. THE NEW RESISTANCE AT THE TRIPLE POINT OF WATER (RTPW) VALUE OBSERVED WAS ENTERED INTO THE READOUT DEVICE, AND THE CALIBRATION WAS REPEATED TO OBTAIN THE ‘AS LEFT” VALUES SHOWN IN THE FOLLOWING TABLE. Now RIPW vestance athe tole pon of woter) vate: 100.0305 Revised caeicons geod er tof voter [bw GROS OP AAOEE-OF Be -SOETTRE-0S 8-7 4288608 be: -8.802126.05 "AS LEFT VALUES: NOMINAL TEST ACTUAL TEST READING CORRECTION ACCEPT LIMIT* PIF == MEASUREMENT TEMPERATURE TEMPERATURE or uur Ts ors} UNCERTAINTY k=2 9.0109¢ 9.010°¢ 9.010%¢ Pass 490:000°C 399356" 400: 005°C PASS: 200000'c = 138:396°¢ © 99:88aec Pass S381834°C © =38l834ec == 3818326 PASS: -196:000°C | -135.645°C — -195.652°C PASS O:010°C '0:010°C 0:003°C PASS “ACCEPT LIMITis) The acceptance limits) shown above representa statistical evelsetion of the instrument's tolerance relative tothe uncertainty of the measurement. If require, the acceptance init is set To 9 value smater than the tolerance. The difference between the tolerance ard the acceptance it the ‘querd band” The guard Band imposed fo reduce the probability of ase acceptance IPFA), Ora false failure, fo less than 2% PME Accordingly, there ae three possible calibration outcomes: 1. PASS The callrotion result falls within the interval desenbed by the test point + or - (the tolerance MINUS the guard band). 2. MARG**\ marginal "The calbration result ‘horderine’. of indeterminate 3 therefore statistically and metrelogicaly imprudent {0 declare that the instrument is defintively either istolerance” or ‘out-of tolerance” 3 Fail "The calibration result falls outside the interval described by the test point + oF - (the tolerance PLUS the guard band) The methodlogy and equations used for determination of guard bands and acceptance limits comply with the requirements of ANSINCSL 2840.3 (Our best measurement capabilties are: at Liguld Nitrogen (approximately -196C), +/-6.2 mK: from -80 to OC. +/- 8.9 mK: at OC, o7. 39 mk: at GTC (TP), «7-1-9 mK: rom 0.0} fo 100, +," 8.5 MK: trom 100 to 200C, "9.4 mk: trom 200 to 300G, + 9.8 mk: from 300 to 420C, +/- 14 mK: from 420 9 500, +/-0.034C: from 500 9 700C, +/-0.26C; trom 700 t0 1000C, +/-0.86C. Those Uncertainties have been calculated utlizing the methods eleboreted i NIST Technical Note 1297 and the ANSI-NCSL document 2-540-2 ‘entitled ‘Guide o the Expression of Uncertainty ip Measurement. commonly referred 103s the ‘GUM”. & coverage factor of 2 sigma (k= 2) has been anphed 10 the Standard uncertainty inorder fo express the expanded uncertainty at approximately 8 95% confidence level. THE UNCERTAINTIES PRESENTED ABOVE IN THE ‘RESULTS’ TABLE WILL BE LARGER THAN OUR SYSTEM UNCERTAINTIES, AS THE RESOLUTION OF THIS READOUT, -0.001°C. AND OTHER CONTRIBUTIONS HAVE BEEN FACTORED INTO THE CALCULATION. THE EXPANDED UNCERTAINTIES (K = 2) REPORTED HERE DO NOT CONTAIN ESTIMATES FOR (1) ANY EFFECTS THAT MAY BE INTRODUCED BY TRANSPORTATION OF THE INSTRUMENT BETWEEN ICL AND THE USER'S LABORATORY. (2) DRIFT OF THE INSTRUMENT, (3) HYSTERESIS OF THE INSTRUMENT, OR (4) ANY MEASUREMENT UNCERTAINTIES INTRODUCED BY THE USER. LABORATORY ENVIRONMENTAL CONDITIONS: TEMPERATURE: 23°C +/: 2°C RELATIVE HUMIDITY: BETWEEN 40% AND 60% ALL TEMPERATURES GIVEN IN THIS REPORT ARE THOSE DEFINED BY THE INTERNATIONAL TEMPERATURE SCALE OF 1990 (/TS-90) THIS CALIBRATION WAS PERFORMED BY: J. JEFF KELLY THE CALIBRATION PERFORMED AND DOCUMENTED BY THIS CALIBRATION REPORT'S A FULL SCALE CALIBRATION AND NO LIMITATIONS OF USE ARE IMPOSED ON THIS INSTRUMENT.ICL CALIBRATION LABORA TORIES. INC. Report No. U185901_ $0: 123466 Ghent: SAMPLE CUSTOMER Date report issued: 05-16-2011 Page 3 of 3 pages TRACEABILITY INFORMATION This calibration is receoble to NIST through an unbroken chein of comparisons. The reference standard is used to calibrate the transfer ‘Standord, which i tun 3 used to calibrate the client's instrament. Each step in the chain hilly documented. and measurement Uncertainty ot each step has been colevisted. (Our NIST primary reference thermometer trom -196 to 420C is 2 Rosemount 162CE, 25.5 Ohm SPAT. seria! no. 5206, Calibrated by NIST on Apri 1, 2008. NIST GMP-11 recommends @ 36 month calbration cycle for SPATs.. Transfer standords PRT fre calibrated against this reference standard annually. (Our primary standerd for temperatures above 420C to 1000C is a Hart Scientific mode! 6624 10 Ohm platinum resistance ‘thermometer, senal number 0108, our MTE-243, celloreted traceable fo NIST by Hart Scientific. (COMPARATORS USED IN PERFORMANCE OF THIS CALIBRATION Comparator (MTE# Manufacturer TEM maine bach au mart Gosom sair bach © 239 Hart Scientific S0S0H Sait bach © 240 Hart Seiencific 7080 ale bath 033, Hart Scientific EN comparator, 220 Mart Scientific ‘Tow Maine bath sh Hart Scientific TRANSFER AND CHECK STANDARDS USED IN PERFORMANCE OF THIS CALIBRATION Tronster Standard MMTEs Manufacturer NextDue Position FEN cqh porayy 32 Mart Scientific 03/29/12 Standard 4ob:eo0-c Sesecis per 0332353 Mart Scientific 06/01/11 Standard ber iz0s 363 Mart Seiencific 06/01/11 Check standard 200.000°¢ Der 0992252 Mart Scientific 96/01/11 Standara, pr iz08 363 Hart Scientific 06/01/11 Check standard -38.034°C Far irss 306 Mart Scientific 06/01/11 Standard Bar isi 305 Mart Scientific 06/01/11 Check “standard -196.000°C Ber 0541237 Mart Scientific 06/01/11 Standara Seaecis Pr ii00 390 Hart Scientific 06/01/11 Check standard o.o10"c | Tpw cell Ba2217 32 Hart Scientific 03/29/12, Standard "THERMOMETER READOUT(S) USED TO READ THIS UUT AIL readings of this sensor were observed using customer’s readout /n: XOOUX ICL CALIBRATION LABORATORIES, INC. ‘Ae ISO1EC 17025 8 ANSINCS 25401 ected taatery Ameen Ase or taba AcettenCerteate 1526.01 J. Jett Kelty, Technical Director Deborah i. Weber, Quaity Deputy ‘This document prepared by LORI PARR and reviewed by KAREN MANGOLD DATE CALIBRATED: 05-16-2011 __RECALIBRATION DATE SPECIFIED BY CLIENT: May 16, 2012 MIST GMP-11 (Mar 03), ‘Good Measurement Practice for Assignment and Adjustment of Calioration Intervals for Standards’ cautions that, “Temperature standards are dynamic with use. Shock, contammation and other factors can cause Gil rom accepted values" Table 407 GMP-1T recommends recalibration of iquidin-glass thermometers, standard thermictors and PRTs at 12 month tervals. Liquid:nsglass thermometers used for Tempereture Ciical Parameters” should be recalrated at 6 month intarvais. NIST GMP-11 is ‘avafable for download in Adobe -pd format on our website at worw.iellas. com Flow the lnk for ‘Downloads ‘The user should be aware that any number of factors may cause this instrument to dnft out of calibration before the specified caliration interval has expied. This calibration report may not be reproduced except in full without the express written permission of ICL Calibration Laboratories, nc. This report applies only tothe item calibrated. This calibration report shal not be used to clsim product endorsement by the A2LA.