Professional Documents
Culture Documents
TITLE PAGE
GROUP 22
GROUP PERSONNEL:
Arif Hendrawan (1406531763)
Nafila Wajdi (1406531675)
Renno Afriansyah (1406577783)
Yoga Wiranoto (1506800350)
Yusran Fachry Reza (1406531826)
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durability are in sequence 80 years, 60 years, and 50 years. So, current best existing
product is Aspen Aerogels.
Insulation in cryogenic storage and pipelines has become a necessity as the
demand of cryogenic liquid and LNG grows up. Since heat leak is of major concern
in the design of storage and transfer systems for such cryogenic liquids, selecting
the proper thermal insulation to use on such system is vitally important. The strategy
is to understand the concept and make a comparison between one another so that
we could generate a new and better cold insulation product.
In order to make our product happened; we determined our product concept
by evaluating the existing concept, new concepts, do concept screening, and the last
concept scoring to select the best concept for our cryogenic insulation product.
On the screening step, we eliminated several concepts that are not feasible.
On the first screening stage, we eliminated the concepts based on its possibilities to
be implemented and we got 11 concepts to proceed to the next step. In this step, we
eliminated concepts based on our screening criteria. The criteria are thermal
conductivity, thermal expansion, lifespan, cost, health and safety, combustibility,
vapour-water transmission, service temperature, and vermin resistance.
Those remaining concepts need to be scored with nine selection criteria using
weight percentage which is already mentioned above as criteria. The weight
percentage based on our intention and the customers requirement. The highest
weight scores are 15% of each thermal conductivity, thermal expansion, cost, and
health and safety. The concept which has the highest score is Silica Aerogel.
The final concept is then tested to the user by interview and emails to
determine whether the concepts are working or not which is resulted to a potential
customer. From 25 respondents, 17 of the correspondents are interested and willing
to use the product in the future.
In product positioning, we used conceptual mapping to help us compared our
product with our competitors that would affect products quality and to determine
users interest. In the product description, we defined our product specification based
on the chosen product concept. We also compare all of our product specification
our with existing commercial product. Through this comparison, we know what
would be our strength the specification that our competitors are a lack of.
Praise to Allah, the Cherisher and Sustainers of the world; God who has been
giving all His Blessing and Mercy for writer to complete this Assignment 1 Report
of Chemical Product Design entitled Insulation in Cryogenic, Pipelines, Storage
and Air-conditioning.
This final report is submitted to fulfill one of the requirements in Chemical
Product Design Class as capstone course of Chemical Engineering Major in
Universitas Indonesia.
In the completion this report, the writer really gives his regards and thanks
for people who has given guidance and help, they are:
1. Prof. Dr. Ir. Widodo Wahyu Purwanto, DEA., Dr. rer. nat. Ir. Yuswan Muharam
M.T. , Dr. Ing. Ir. Misri Gozan M.Tech., Ir. Dewi Tristantini, M.T., PhD., and
others Lecturers, who has given their best guidance to the writer in writing a great
quality report and well developed chemical product.
2. The informant and respondent of our questionnaire that helps indirectly to begin
this report
3. Imas Mega Pratiwi, Giovanni Anggasta, Raden M. Fatih, Nugrahirani Hijrianti as
the lecturer assistants of Chemical Product Design 2017 who gives suggestion and
guidance to the writer in writing this final report.
4. Our Parents, who always give their supports, prayers, and blessing.
5. Our beloved friends in Chemical Engineering Department batch 2014 who always
give their supports.
6. All of our correspondents who spend their time to fill our questionnaire.
Finally, the writer realizes there are unintended errors in writing this final
report. The writer really appreciates all readers giving their suggestion to improve
its content in order to be made as one of the good examples for the next report.
Depok, March 2017
Writer team
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LIST OF GROUP MEMBERS
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TABLE OF CONTENTS
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CHAPTER 1
INTRODUCTION
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As we know that there are many types of insulation material available in the
market. Insulation materials are generally divided into three main types : fibrous
insulation, cellular insulation, and granular insulation (Bahadori, 2015). Fibrous
insulation is composed of small diameter fibres which finely divide the air space.
The most widely used insulations of this type are glass fibre and mineral wool.
Cellular insulation is composed of small individual cells separated from each other.
The cellular material may be glass or foamed plastic such as phenolic foam or nitrile
rubber. Granular insulation is composed of small nodules which may contain voids.
Example of these insulations are calcium silicate and vermiculite which no longer
used because of asbestos which can cause fibrotic lung disease (National Cancer
Institute, 2015).
The problem with cold insulation is that if installation is finished impoperly,
it will cause heat leak through the system, and depends on the environment where
the system is installed, in this case where the temperature of the system is below
dew point of ambient air, it will cause condensation which will be reached at some
distance inside the later of insulation. This condensate could freeze, which can
render the insulation futile by increasing the thermal conductivity and the
possibility of corrosive or electrolytic attack on metal surface (Bahadori, 2015). In
case of fire, certain insulation systems may generate appreciable quantities of
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smoke and toxic fumes if ignited which is not safe for personnel and evironment
(Environmental Protection Agency, 2017). The cold insulation requirements shall
be determined with due consideration to safety aspects as well as to process aspects
and with the objective to minimise life cycle cost (Bahadori, 2015).
By interpreting and analyzing the data which our team has gathered from
interviews and literature review, we believe that there are lots of spaces for
improvement in order to design a cold insulation which are not only prevent basic
needs such as preventing heat gain to some extent and extreme temperature
difference but also highly durable, occupationally safe, easy to maintain, and has a
competitive price.
1.2 Objective
Authors aim to design a cold insulation for cryogenic application which is
occupationally safe, highly durable, easy to maintain, and has a competitive price.
1.3 Problem Identification
Identification of problems from cold insulation product are as follows:
The existing product could cause skin irritation due to contact with
insulation material
The existing product could cause lung and respiratory problems due to
inhaling material dust
The existing product is still vulnerable to condensation, freezing, and even
corrosion
The existing product is not really durable due to extreme temperature
difference
The existing product is quiet expensive for a low thermal conductivity value
The existing product needs skilled individuals to install and maintain which
is hard to find.
1.4 Problem Formulation
What are the best possible materials that can be used in order to design
occupationally safe, highly durable, easy to maintain, and has a competitive price
cold insulation?
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CHAPTER 2
REVIEW OF LITERATURE
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best insulation for low to medium temperatures where compression and/or vibration
is not a factor.
However, where higher temperatures are encountered, the air or gas voids
need to be reduced in size to minimize the convection within the voids and this is
achieved by increasing the density of the insulation (TIASA, 2001). Density may
be increased to a point where the solids content of the insulation is such that the
heat bridge of the solids overcomes the insulating effect of the voids. It follows
therefore, that by encasing a container of heat with thermal insulation material the
reverse heat flow will be retarded with resultant reducing energy loss and cost.
The word retarded is important because no matter how much insulation is
applied, the reverse flow of heat to ambient can never be stopped. The primary
reasons for insulation are many and varied, the main ones being (TIASA, 2001):
To conserve energy
To reduce heat loss or gain
To maintain a temperature condition
To maintain the effective operation of equipment or chemical
reaction
To assist in maintaining a product at a constant temperature
To prevent condensation
To create a comfortable environmental condition
To protect personnel
The type and thickness of insulation depend on the foregoing primary
reasons together with the parameters of the specific conditions. Economic thickness
is the thickness of insulation, which will result in minimum total cost of energy
losses plus the cost of the erected insulation. The calculation of economic thickness
is complex and in some cases is overruled by the other listed primary reasons, which
can make the calculation unnecessary. The exception is when retro fitting of
insulation is envisaged. Retro fitting is the application of additional insulation to
existing insulation to further reduce heat loss or gain in order to reduce the cost of
energy losses.
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In such an event, and in the case of cold rooms, it is better that the water
vapour has an unhindered path to the cold surface to enable it to be drawn off by
the refrigeration equipment. In the case of pipe work and vessels, it is preferable
that the water vapour has free passage to the cold surface where the resultant water
or ice will be encased by the insulation. A break in the vapour barrier of the
insulation system will eventually cause the system to fail but its effective life will
have been prolonged by a design which permits the through transmission of water
vapour.
Whatever the primary reason for cold insulation, it should be designed to
prevent condensation. Condensation occurs when water vapour in the atmosphere
comes in contact with a surface at a temperature of less or equal to the dew point.
Therefore, if the surface temperature is less than the dew point, condensation will
occur. The presence of condensation on the warm side of the vapour barrier has no
detrimental effect on the insulation but, nevertheless, it is a condition, which has to
be avoided. To prevent condensation, the insulation thickness should be so designed
that temperature on the warm side of the vapour barrier is above the dew point
(TIASA, 2001).
In calculating the thickness of insulation required to prevent condensation,
it is prudent to know or assume conditions of high relative humidity. If the fluid
inside the pipe or vessel is likely to remain static for long periods when the ambient
temperature is below the freezing point of the fluid, it is important that this shall be
stated. Also, the fluid in small diameter pipes may be especially susceptible to
freezing, particularly if the rate of flow is intermittent or slow, it may be necessary
to consider the use of supplementary means of heating, possibly only in local areas,
like heat tracing.
2.2.1 Application of Cold Insulation
All insulation should fit snugly around piping and equipment. On low
temperature insulation work all attachments to the piping or equipment and
projecting through the insulation should also be insulated for a distance of four
times the thickness of the basic insulation from the point where the projection is
exposed. All the insulation and the vapour barrier should be continuous at pipe
supports. Where metal cradles preformed to the outside diameter of the insulation
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are provided at the pipe supports the cradle should be designed to prevent undue
compression of the insulation due to the weight of the insulated pipe (TIASA,
2001).
Joint Sealers and Adhesives
All materials intended for use for cryogenic insulation of pipes and vessels
should be checked for their suitability at low temperatures and if, for example,
no acceptable joint mastic is available for -196C (liquid oxygen, nitrogen, etc)
then only the joints on the outer layer on a multi-layer system should be sealed.
Joint sealers and adhesives should be completely compatible with the insulation,
vapour barrier and the item being insulated (refer manufacturers
recommendations).
When insulating low temperature pipe work, it is advisable to create
circumferential vapour dams extending from the bare pipe to the vapour seal on
the warm side of the insulation. The longitudinal spacing of the dams is arbitrary
and as a guide, 2m, for very low temperatures to 10m for, say chilled water,
should be considered. The purpose of the dams is to prevent the failure of long
sections of pipe insulation should the warm side vapour seal be ruptured in any
way.
Support For Insulation
The following can support insulation:
Adhesive
Pins plastic or nylon
Strapping bands for large cylindrical surfaces
Pressure-sensitive tape for small diameter surfaces
Pre-installed insulation support rings, normally used on large vertical
vessels.
Vapour Barriers
The following tables provides a guideline for the required water vapour
permeance for different plant cold surface temperatures:
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Structural Barriers
Often prefabricated to exact dimensions required and ready to install, these
are rigid sheets of reinforced plastic, galvanized, aluminium or stainless steel
jacketing - flat, corrugated or embossed.
Membran Barriers
Metal foils, laminated foils and treated papers, plastic films and sheets, and
coated felts and paper - these are either part of the insulation as supplied or can
be supplied separately.
Coating Barriers
In fluid form as a paint or mastic (or semi-fluid of the hot-melt variety) the
material can be asphaltic, resinous or polymeric. These provide a seamless
coating but require time to dry and are normally reinforced with a membrane
sandwiched between layers. Special attention must be given to vapour sealing
of protrusions, joints or any other discontinuities such as glands, local to valve
spindles or mechanical drives, etc.
Protection of Insulation
Protection of the insulation may consist of metal cladding or a coating
system. Metal and non-metallic finishes should generally be as per the
insulation guideline for hot insulation. However, care should be taken where
piping and equipment is being clad; the cladding should be manufactured and
installed so as to prevent the vapour barrier being punctured. Cushioning
material applied between screws or rivets and vapour barrier, or other suitable
means, would be a normal practice.
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a. Cellular Glass
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Industrial: tank bases, vessels, piping and equipment, cold stores and marine
applications.
Buildings: roofs, floors, walls (internal and external), car park decks, soffits.
b. Cork
Figure 2. 2 Cork
(Source : https://www.greenbuildingadvisor.com)
Density : and range, if applicable
Thermal Conductivity
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Density : 10 to 80 /3
Thermal Conductivity
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Mechanical Properties
Compressive strength : 1 to 8 /2 at 5 % deformation
Flexural strength : N/a
Thickness Range : Available from 15 to 150mm
Forms available : Blown Fibre, Pipe Sections, Rolls, Slabs
Typical Uses and Application
Glass mineral wool is available in a wide range of forms ranging
from flexible rolls to rigid slabs and preformed pipe sections. It is
particularly suitable for thermal and acoustic applications in the H & V
sector and is also used as both a thermal and an acoustic insulation in
transport, shipping, building and industrial applications.
d. Phenolic Foam
Density : 35 to 120 /3
Thermal Conductivity
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For cold insulation, we can replace heat loss with heat gain.
2.6 Arranging Insulation in Equipments
To Arrange insulation in equipment, we must know the appropriate steps in
accordance with existing standards and to prevent mistakes that can be ruin an
insulation system. Below are some steps that can help us in Arrange insulation in
equipment (TIASA, 2001).
2.6.1 Pre-Insulation
Before insulation is applied; all surfaces to be insulated shall be
thoroughly cleaned to remove dirt, oil, moisture, loose rust or any other
foreign matter.
Pressure and leak testing, it is recommended that pressure and leak
testing be carried out and any repairs effected prior to application of
insulation. In many cases this is a statutory requirement.
Heat transfer cement and heat tracing, if a temperature is to be
maintained by means of external heat sources such as heat tracers, heat
transfer cement may have to be applied to improve the heat transfer
from the tracer in severe cases. The manufacturers recommendations
should be consulted.
Corrosion protection, where the operating temperature is less than
130C and the equipment or pipe work is other than austenitic alloy, the
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surfaces should be coated with a suitable paint. It has been found that
below this temperature corrosion conditions can occur.
Pre-Installation support, Insulation supports shall be installed prior to
the application of the insulation.
2.6.2 Designing Insulation Systems
Factors that influence the design of an insulation system are
(TIASA, 2001):
Location of Plant
Indoors
Outdoors protected from the weather
Outdoors exposed to the weather
Shape, size and elevations all need to be taken into consideration
Temperature Condition
The normal operating temperatures
The extreme temperature if other than normal operating
temperature
Any fluctuating temperature
Duration of extreme or fluctuating temperatures
Surrounding Atmospheric Condition
Ambient temperature
Relative humidity to establish dew point for cold insulation
Flammable conditions
Potentially corrosive atmosphere
Acidic conditions in atmosphere
Air flow over insulated surface (wind velocity)
Special or Service Conditions Requirements
Resistance to compression, for example, foot traffic
Resistance to fire
Resistance to vibration
Resistance to mechanical damage
Resistance to corrosive fluids or gases
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CHAPTER 3
NEEDS AND IDEAS
3.1. Needs
Since heat always flow from a higher temperature region to one at a lower
temperature, there is a continuous flow of heat from outside to the refrigerated
space, whether it is through walls or floor. To limit the amount of such heat flow,
it becomes necessary to use good insulating material for the system. In this case,
the temperature difference between the outside and the refrigerated space is large.
Thus it becomes essential to use insulation.
Heat transfer, as we have studied, occurs due to conduction, convection and
radiation. For reducing the heat flow through the walls and roofs of cold storages,
the heat flow due to conduction and convection has to be reducted. The heat flow
due to conduction can be reduced by the use of materials having a low-heat
conductivity. The heat transfer through convection can be reduced by having very
small closed air cells in the insulation material. Based on this theory, we conclude
that the basic needs is that an insulating material should have a low-heat
conductivity and a number of small closed air cells for good insulation.
The insulation strategy is to minimize radiative heat transfer, minimize
convective heat transfer, and introduce a minimum of solid conductance media.
Factors considered in the selection of the most suitable insulation include it
ruggedness, convenience, volume, weight, ease of fabrication and handling, and of
course thermal effectiveness and cost.
The existing insulation product hasnt been able to answer the needs of
consumers yet who are well marked by complaints regarding the operational costs,
and performances.However, we can meet consumer expectations related to this
product by listen to their voices at the beginning of this project.Thus, we do survey
in orderto identify the needs of existing consumers.
3.2. Consumer Requirement
Consumer requirement is consumer ideas that have been surveyed,
analyzed, and examined where those consumer voices are affecting the
sustainability of product design and development.
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Based on Figure 3.1 which is extracted from the survey, it can be seen that
from we got 12 respondentswhich comes from PT Pagoda Sakti, Air Liquide, and
Huntsman Indonesia as producing company of insulation, and also several user
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Insulation
To avoid any heat loss/leak or to that able to
keep maintain low temperature of prevent heat
Why do you use the the gas in liquid phase and in the leak and
1 insulation system on same time to keep maintain the maintain the
the equipment? phase and avoid pressure change temperature
in the systems. In addition, of the
external insulation will help to system
mitigate any external corrosion
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Insulation that
At hinges, joints, and cable holes. can be placed
What part on your
at hinges,
equipment is most
3 joint, cable
vulnerable to the
At the top of gas storage tank holes, and at
heat-leak?
top of the
storages.
What types of Panel insulation in form of sheets.
insulation are
4
installed on your
Loose-fill insulation
equipment?
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Need
Needs
Number
A RETAILING
6. Insulation with a competitive price
B PRODUCT PERFORMANCE
Insulation that has thermal conductivity minimum as low as
1.
0.03 W/m.K
2. Insulation that is able to withstand thermal expansion
3. Insulation that is able to withstand wear or pressure
Insulation that is firm and ductile enough to withstand hit or
5.
crash
8. Insulation that is easy for maintenance and services
9. Insulation that can withstand water absorbtion
C PRODUCT PERCEPTION
Insulation that is able to withstand extreme external
4.
condition
Insulation that is easily installed to every length and size of
7.
the system
After grouping has been done, grading or ranking is done to know how
important these needs for insulation for low-temperature product. Needs rank
consists of :
1 undesirable needs
2 not important needs
3 nice to have needs
4 highly desirable needs
5 essential needs
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Need
Needs Rank
Number
A RETAILING
6. Insulation with a competitive price 4
B PRODUCT PERFORMANCE
Insulation that has thermal conductivity minimum as low as
1. 5
0.03 W/m.K
2. Insulation that is able to withstand thermal expansion 5
3. Insulation that is able to withstand wear or pressure 4
Insulation that is firm and ductile enough to withstand hit or
5. 3
crash
8. Insulation that is easy to maintain or to service 4
9. Insulation that can withstand water absorbtion 3
C PRODUCT PERCEPTION
4. Insulation that is able to withstand extreme external condition 3
Insulation that is easily installed to every length and size of
7. 3
the system
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CHAPTER 4
SPECIFICATION
1.
4.1. List of Metrics
The focus in this chapter is translating what customer needs from the previous
chapter into product specification. This chapter, we define the specification of the product
to all of needs which has been grouped and given rank into dimension and then giving unit
based on the specification. By changing the qualitative form into the quantitative one, it
helps us to determine what we should do in the future to reach our goal to produce the
desirable product.
Table 4. 1 List of Metrics
Metric Need
Metric Rank. Units
No. Nos.
1 1 Thermal conductivity 5 W/mK
o
2 2 Service temperature range 5 C
3 3 Durability 4 Year
4 3,8 Combustibility 3 Combustible/Non
5 3,9 Water vapour transmission 4 gm/Nh
6 4 Density 4 kg/m3
7 4,5 Thickness range 2 Mm
8 6 Unit manufacturing cost 5 US$/m2
9 7,8 Time to assamble 1 S
10 8,9 Surface spread to flame 3 Class
2. (Source: Reproduce from the literature)
4.2. Metrics & Needs
The next step is making a matrix of needs and metrics. This step will help
us to see if there are some needs which have a same metric units. If there are some
needs that have same metric unit, that doesnt mean we have to erase one or some
of it. Because therere some needs that has subjective specification, its possible to
have needs that have same metric.
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10
1
2
3
4
5
6
7
8
9
Water vapour transmission
Service temperature range
Time to assamble
Thickness range
Combustibility
Durability
Density
Need
Insulation that has thermal conductivity minimum as low
1
0.03 W/m.K
2 Insulation that is able to withstand thermal expansion
3 Insulation that is able to withstand wear or pressure
Insulation that is able to withstand extreme external
4 condition
Insulation that is firm and ductile enough to withstand hit
5 or crash
6 Insulation with a competitive price
Insulation that is easily installed to every length and size
7 of the system
8 Insulation that is easy to maintain
9 Insulation that can withstand water absorbtion
4. (Source: Reproduce from the interview & literature)
5.
4.3. Benchmarking Existing Product
As conceptual product that will move forward to its production scale, our
product needs benchmarking. Benchmarking is a way to determine the superiority
of our products to be the production of other products that similar and have been
producing in the market. The necessity to conduct benchmarking is vital, because
we will produce a product that must be able to compete with existing products in
the market overally.
The result from benchmarking also help us to project the market segment
for our product, so we can analyze which variable require to scale up, and or further
modification so it will meet both the market share and customer needs.
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Arabian
Metric Need Aspen
Metric Rank. Units Rockwool Fiberglass
No. No. Aerogels
Insulation
Thermal
1 1 5 W/mK 0.021 0.038 0.028
conductivity
Service
(-56) (-18)
2 2 temperature 5 o
C 0 250
6 450
range
3 3 Durability 4 year 80 60 50
Combust-
4 3,8 Combustibility 3 Non Non Non
ible/Non
Water vapour
5 3,9 4 gm/Nh Zero N/a N/a
transmission
6 4 Density 4 kg/m3 160 120 64
Thickness 12.7
7 4,5 2 Mm 5-10 20 120
range 650
Unit
8 6 manufacturing 5 US$/m2 25 5.5 0.58
cost
Time to
9 7,8 1 s 7200 N/a 10800
assamble
Surface spread
10 8,9 3 Class N/a 1 1
to flame
6. (Source: Reproduce from the interview & literature)
4.4. Target Value for Each Metric
After we listed competitors specifications, we need to make the specification for
our product. The specification of our product is based on ideal value and marginal value.
Ideal value is a value we hope our product could be reach while marginal value is an
acceptable value. Marginal value is obtained based on the interview toward the respondents
and the expertise. Ideal values are obtained by selecting the ideal specification from the
best product. We use the specification from the existing product as reference because we
could not find it from any literature. Own values are obtained by discussing together with
all of our members to select the minimum value that our product should have.
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Unit
8 6 5 US$/m2 0.11 64 5.5 10
manufacturing cost
7200 -
9 7,8 Time to assamble 1 S 9000
10800
Surface spread to
10 8,9 3 Class 14 1
flame
7. (Source: Reproduce from the interview & literature)
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CHAPTER 5
INTRODUCTION
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A. Cryogenic
1. What is the meaning of cryogenic?
2. On what temperature cryogenic is occur?
3. What is the principle work of cryogenic?
4. Whether high temperature effects cryogenic system?
5. How does mechanisms of cryogenic?
B. Insulation
1. What is the meaning of insulation?
2. What is the function of insulation?
3. What kind of insulation that is provide for cryogenic?
4. What is the effect of insulation for environment?
5. What factor does it make relevant to cryogenic insulation?
6. How does insulation mechanisms on cryogenic temperature?
7. Whether the thickness affects the heat transfer to the insulation?
C. Storage and Piping
1. Are storage and piping freeze at low temperatures?
2. What will happen if pipe at low temperature dont coated by
insulation?
3. What size of pipe that is optimal for coating?
4. How long does it take time for coating the pipe?
5. What is usually stored in cryogenic storage?
6. What effect the ease of the installation on the pipe and storage?
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We can see on the mind map in Figure 1.1, there are several categories of
ideas that are often used by cold insulation customers to keep their equipment
from heat gain.
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Polyisocyanurate
Fiberglass
Plastic Fiber
Cellulose
No-vacuum
Blow in Fiber Glass
Mineral
Fiber glass
Rigid Fibrous
Mineral
Cementiticus
Polyurethane
Micro Fiberglass
Multi-layer Insulation
Vacuum
Vaccuum panels
Aerogels
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Polyethylene Bubbles
Reflective System
Plastic Films
Aerogels
Blanket
Foam Composites
Silica Aerogel
Cold Insulation New Concept Non-vaccum
MLI
Integrating
Aerogel Composite Blanket
W ood Fibre
Hemp
Natural
Cork
Flax
Figure 5. 2 Mind map of new concept
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Micro Fiberglass
Polysterene
Fine Perlite Hi-vacuum
Foam Boards Polyurethane
Multi-layer Insulation
Vaccuum Polyisocyanurate
Vaccuum Panels
Fiberglass
Layer Composite Insulation Soft-vaccuum
Batts and Roll Mineral
Aerogels
Plastic Fiber
Polyethylene Bubbles
Reflective System Celulose
Plastic Films
Cold Insulation Non-Vaccuum Blow-in Fiber Glass
Aerogels
Blanket Mineral
Foam Composite
Fiber Glass
Polymide Foams Spray Rigid Fibrous
Mineral
Wod Fiber Non-Vaccuum
Cementiticus
Hemp Natural
Phenolic
Cork Sprayed Foam
Polyisocyanurate
Silica Aerogel
Polyurethane
Aerogel Composite Blanket
Integrating
Layered Composition Insulation
MLI
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CHAPTER 6
CONCEPT SELECTION
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Concept Insulation
Description
Number Materials
Foam Glass Serves temprature range -180 C to 120 C,
Since no diffusion can take place, the material
is watertight and efficient barrier against soil
1
humidity. Mostly used underground or
underwater because it is able to withstand
hydrostatic pressure and chemical erosion.
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Concept Insulation
Description
Number Materials
Aerogel is a synthetic porous ultralight
Aerogel material derived from a gel, in which the liquid
component of the gel has been replaced with a
gas. The result is a solid with extremely low
7 density and low thermal conductivity. Silica
aerogel is the most common type of aerogel.
Aerogel is currently considered the newest
invention for cryogenic insulation materials.
Icynene H2 Icynene H2 Foam Lite
Foam Lite is a spray-applied open cell, water blown, low
density polyurethane foam. The product is
8
prepared from two liquid components,
isocyanate and resin H2FoamLite, and is
yellowish in colour.
(Source : Authors Personal Data)
There are two stages of screening process. On the first stage of screening
process, we would eliminate concept based on their possibilities to be implemented
on the product. On the second stage, concepts would be eliminated based on the
screening criteria that we made. The criteria are made based on the customer needs
which have been determined on the previous assignment.
6.2 Concept Screening
After identifying problems by splitting it into sub-problems and searching
for existing and new ideas, the next step we do to design cryogenic insulation
product is screening the concepts The purpose of concept screening is to reduce the
many product concepts generated to a relative few that will get additional
refinement and analysis. We also have chosen selection criterias which are related
to key customer needs. The concepts screening procedures we do is listed below:
1. Prepare the screening matrix
2. Rate the concepts
3. Rank the concepts
4. Combine and improve the concepts
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Concept
Product Concept
Number
1 Polyethylene Bubbles
2 Plastic Films
3 Iron Aerogel
4 Foam Composite
5 Polyimide Foams
6 Wood Fibre
7 Hemp based material
8 Flax based material
9 Cork
10 Silica Aerogel
Aerogel with Composite Blanket with Carbon
11
Dispersion
Layered Composite Insulation with Fiberglass Paper
12
and Fumed Silica Dispersion
13 MLI (Aluminum Foil and Fiber Glass Paper Spacer)
(Source : Authors Personal Data)
Screening 1
Several concepts which has been listed above come from both of existing
product concepts and new product concepts. The concepts that came from
brainstorming may be logical, redundant, foolish, or vague. We now need to weed
out some of the concepts that seem to be impractical before going to the next step.
The impractical concepts will be classified in three classes: redundant (R), foolish
(F), or vague (V). Here below is the list of rejected concepts from the first screening.
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Number Criteria
1 Thermal conductivity
2 Thermal expansion
3 Lifespan
4 Cost-effective
5 Health and safety
6 Combustability
7 Vapor-moisture transmission
8 Service temperature
9 Vermin and fungus resistance
(Source : Authors Personal Data)
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The first criterion is health and safety. Every effort should be made to avoid
the use of asbestos or asbestos containing materials in the insulation system. In
those cases where the use of such material is unavoidable due to the lack of a
technically acceptable substitute or any other means, the prior agreement of the user
to their use shall be obtained. Safety regulations on the use and application of
asbestos or asbestos-containing materials shall be observed . Reference shall be
made to the appropriate instructions from manufacturers for health and safety.
Certain finishing cements are strongly alkaline when wet and may cause skin
irritation.
The second criterion is thermal conductivity. A low thermal conductivity is
desirable to achieve a maximum resistance to heat transfer. Therefore, for any given
heat loss, a material of low thermal conductivity will be thinner than an alternative
material of high conductivity. The thermal conductivity of most insulating materials
varies with temperature and with bulk density, so that both these factors shall be
considered. It is the normal practice of manufacturers to provide tables or graphs
showing thermal conductivities for each of their standard products at a range of hot-
face temperatures together with the relevant cold-face temperatures used for the
tests. The information shall also include the bulk density for each material tested.
The third criterion is thermal expansion. Due to thermal cyclic or shock, an
insulation is suspectible to changes in its dimensional form which can cause the
material to shrink, swell, slump, and warp. These phenomena can cause the
insulation material effectiveness to decrease which can render the insulation futile.
The property of cryogenic insulation material also have to be consistent that it can
be considered constant because a good insulation can stand a wide range of harsh
conditions without change in properties considerably. Most thermal insulating
materials have a lower thermal expansion coefficient than metals. Differential
thermal movement between insulated surface, insulation, and outer finish shall be
considered.
The fourth is is combustability. Not all the thermal insulating materials in
common use are nonflammable. Some of them, often used for refrigeration systems,
are entirely of organic composition and thus may constitute afire hazard, or they
may emit smoke and toxic fumes. Designers of thermal insulation systems shall
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therefore consider the process conditions and the plant arrangement before deciding
whether or not the proposed thermal insulating material might contribute to the
spread of fire, however initiated, and they shall vary their choice of material
accordingly. Some insulating materials that contain organic bonding agents,
although generally suitable for the anticipated service temperature, may in fact
constitute a fire risk through a phenomenon of internal selfheating. This hazard may
be accentuated if air can enter into material of low bulk density, or by convection
current induced with insulated vertical pipe work.
The fifth one is vapor permeability. The purpose of the vapor barrier is to
reduce, and if possible to prevent, the ingress of water vapor into the insulating
material, Thus, the barrier shall always be applied to the warmer surface of the
material. It may take the form of a coating or sheet material resistant to the passage
of water vapor, i.e., of low permeability, and the sealing of joints and overlaps shall
be effective. Insulating materials that consist substantially of closed cells possess
an inherent resistance to the passage of water vapor, but open-cell insulants and
loosefill porous materials are readily permeable to water vapor. Since it is essential
to prevent the deposition of moisture, with the consequent risk of ice formation
within the insulating material in those zones that are below the freezing point, the
use of an effective vapor barrier is an important technical requirement.
The sixth criterion is lifespan. The cryogenic insulation product must be able
to perform its required function over a lengthy period under conditions without
excessive maintenance or repair. These added values can prolong the durability of
the material so that the maintenance cost can be lowered and the optimum operating
condition can be achieved. The required life of the insulation system shall be
considered because this affects the annual cost and hence the economic thickness.
If the plant has only a short life, a cheap insulation system may be adequate; if the
plant has a longer life, a more expensive insulation system with longer life may be
the more economic.
The seventh one is cost effective. As we know it, nearly all industries which
use cryogenic insulation is profit-driven. So that material cost is a critical
consideration that someone must take in order to choose the best material possible
to minimize heat gain to their system as low as possible without sacrificing the other
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options. This criterion is also connected with labor cost which will be explained in
the next paragraph. The point is a good insulation can lower the labor cost as well
as material cost.
The eighth one is anti-fungi and vermin. The resistance of insulation to
vermin, insects, and fungal growth can be important, particularly in cold stores for
goods. Insulation surfaces likely to become wet shall not befinished with materials
that may be attacked by these agencies. Finishing with nonabsorptive materials is
desirable for severe cases.
The ninth one is service temperature range. Choosing an insulation with a
wide service temperature range can help ensure process control. It also reduces the
number of different materials needed to meet different temperature requirements
and it can help minimize material costs as well as purchase confusion. And, an
insulation with a wide service temperature range reduces the likelihood of the
material being exposed to temperatures outside of its range - which can lead to
system failure and costly repair and reinsulation.
6.2.2 Rate the Concepts
For each concept, the each criterion should be rated as plus (+), zero (0), or minus
(-).
Plus (+) means that its better than preference concept.
Zero (0) means that its the same as preference concept.
Minus () means that its worse than preference concept.
6.2.3 Rank the Concepts
Rank of the concept can be made by summing all of the criterion rating for
each concept. Ranking the concepts used to review screening result and to check
which concept is qualified for most criteria and can go to the next step, which is
concept scoring.
For the reference, we use Polyurethane Foam. It is due to the most widely
used Polyurethane Foam as cold insulation material. The upcoming concepts are
compared to Polyurethane Foam for each criterion.
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Product Concept
Criteria
Reference 1 2 3 4 5 6 9 10 11 12 13
Thermal
0 - - + + 0 - - + + + +
Conductivity
Thermal Expansion 0 0 + + 0 + + - + 0 0 0
Lifespan 0 + + + + + - - + + + +
Ease of Use 0 + + + 0 + + + + + + +
Cost-effective 0 + 0 0 0 + + + - - - -
Health and Safety 0 0 0 + + + + + + + + +
Combustability 0 - - 0 0 + - - 0 0 - -
Vapour-moisture
0 - - + + 0 - 0 + + + +
transmission
Service temprature 0 - - + 0 - - + + + + +
Vermin and fungus
0 + + + + + - - + + + +
resistance
Amount + 0 4 4 8 5 7 4 4 8 7 7 7
Amount - 0 4 4 0 0 1 6 5 1 1 2 1
Total Amount 0 0 0 8 5 6 -2 -1 7 6 5 6
Ranking 0 5 5 1 4 3 7 6 2 3 4 3
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in which it is used and under the conditions anticipated, will not ignite, burn,
support combustion, or release flammable vapors when subjected to fire or heat.
Some industrial applicaitons insulation materials are also required to meet certain
surface burning chaaracteristics, usually assessede by means of a flame spread
index (FSI) and a smoke developed index (SDI). When a material is required to
meet certain values of flame spread index and smoke developed index, it usually
must be tested in accordance with ASTM.
G. Water vapor permeability (Weight = 10%)
Water vapor permeability is defined as the time rate of water vapor
transmission through unit area of flat material of unit thickness induced by unit
vapor pressure differential between the two specific surfaces under specified
temperature and humidity conditions. The permeability of a material is expressed
in terms of the weight of the water vapor transmitted through a unit thickness of the
material, divided by the vapor pressure differential, the time, and the area of the
material. Hence, the lower the permeability, the more resistance it is to the diffusion
of moisture vapor through a given thickness of it. Since it is essential to prevent the
deposition of moisture, with the consequent risk of ice formation within the
insulating material in those zones that are below the freezing point, the use of an
effective vapor barrier is an important technical requirement.
H. Service temperature (Weight = 5%)
When choosing an insulation material for any given service, one major
concern is system-operating temperature (minimum/maximum) and the proper
insulation material designed for use within those operating parameters. Insulation
materials intended operating temperature ranges for insulation materials are
normally specified by the insulation material manufacturers. When selecting an
insulation material, this recommended range should be the first consideration. It
may be necessary for the specifier to look at the combinations of maximum and
minimum tests results plus all associated properties to determine the need fot one
type of material for an inner layer and another type for the outer layer.
I. Vermin and fungus resistance (Weight = 5%)
The resistance of insulation to vermin, insects, and fungal growth can be
important, particularly in cold stores for goods. Insulation surfaces likely to become
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wet shall not befinished with materials that may be attacked by these agencies.
Finishing with nonabsorptive materials is desirable for severe cases.
6.3.2 Rate the Concepts
The rating at this stage is based on group discussion and literature. Here is
the rating of the concept compared to reference product.
Table 6. 6 Rating the Concepts Value
Relative performance Rating
Bad 1
Enough 2
Good 3
Great 4
Excellent 5
(Source : Authors Personal Data)
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Rati Criteria
ng A B C D E F G H I
k value =>
1 0,12 5.10-3/oC <2,5 years 41-50$/m3 Asbestos Combustible 20 gm/Nh 200-300 K Organic
W/(m.K)
k value =<
2 0,12 1.10-3/oC <5 years 31-40$/m3 - - 15 gm/Nh 150-300 K -
.
W/(m K)
k value =<
3 0,06 5.10-4/oC <10 years 21-30$/m3 - - 10 gm/Nh 100-300 K -
W/(m.K)
k value =<
4 0,03 1.10-5/oC <20 years 11-20$/m3 - - 5 gm/Nh 50-300 K -
W/(m.K)
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3 5 10 11 13
Criteria Weight Weighted Weighted Weighted Weighted Weighted
Rating Rating Rating Rating Rating
Score Score Score Score Score
Thermal
15% 3 0,45 2 0,3 4 0,6 4 0,6 5 0,75
Conductivity
Thermal
15% 4 0.6 4 0.6 4 0.6 4 0,6 4 0.6
Expansion
Lifespan 10% 4 0.4 3 0.3 4 0.4 3 0.3 3 0.3
Cost-effective 15% 4 0.6 4 0.6 3 0.45 2 0.3 2 0.3
Health and
15% 5 0.75 5 0.75 5 0.75 5 0.75 5 0.75
safety
Combustibility 10% 5 0.5 5 0.5 5 0.5 5 0.5 5 0.5
Vapor
10% 3 0.3 3 0.3 4 0.4 4 0.4 4 0.4
permeability
Service
5% 4 0.2 2 0.1 4 0.2 3 0.15 3 0.15
temperature
Vermin &
fungus 5% 5 0.25 5 0.25 5 0.25 5 0.25 5 0.25
resistance
Sum 100% 4.05 3.70 4.15 3.85 4,00
Rank - 2 5 1 4 3
(Source : Authors Personal Data)
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The pie chart above shows how 25 respondents see through our concept
product, based on silica aerogel as our insulation product. There are 17 of
respondent thought they are very interested, due they believe to Indonesia potency
for the recycled raw material of silica aerogel. 7 of respondents thought they are
somewhat interested because they find it interesting but not yet know the beneficial
quality of it. 1 of respondents chose to not interested at all because their expertise
is not for cryogenic temprature, only for chiller, thus the insulation material does
not need to be that advance.
9 of the 25 respondent play role as industry experts, 4 of them are would likely
to buy the product we offer, 4 would like to take a sample, and 1 is not willing to
buy.This proves that our product has demand, hence has a potential customers.
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CHAPTER 7
FINAL PRODUCT
Arabian
Aspen Own
Criteria Rockwool Fiberglass
Aerogels Product
Insulation
Thermal conductivity 4 3 4 5
Thermal expansion 4 3 4 5
Lifespan 5 5 5 5
Cost-effective 4 4 4 3
Health and safety 5 5 4 5
Combustibility 5 5 5 5
Vapor-moisture
5 3 3 4
transmission
Service temperature 4 3 4 5
Vermin and fungus
5 4 5 5
resistance
(Source : Authors Personal Data)
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The rating is given from 1 to 5. Rating 5 is given for the best, while rating
1 for the worst. The figure 3.1 below would describe the position of our product
compared with its competitors based on the criteria above.
Thermal conductivity
5
Vermin and fungus
4 Thermal expansion
resistance
3
2
Service temperature 1 Lifespan
0
Vapor-moisture
Cost-effective
transmission
a. Thermal Conductivity
Increasing temperature of a system happen when heat coming from the
environment into the system. For the insulation system, we need to prevent the
heat gain into the system. Heat transfer occurs in an insulation system occurs
by conduction. Based on fouriers law we can determine that the incoming heat
is proportional to the thermal conductivity of a material. Thus, the smaller value
of the thermal conductivity of a material, the better the insulation system would
be. Rating 5 is given to insulation system which has thermal conductivity
around 0.021 W/mK. Meanwhile rating 1 is given to insulation system which
has thermal conductivity above 0.03 W/mK. We rated our product as 5 in this
criteria because own product has thermal conductivity 0.021 W/mK. We gives
Aspen Aerogel 5 too because has thermal conductivity 0.021 W/mK.
Meanwhile based on benchmarking from assignment 1 Rockwool is given 3
rating and Arabian Fiberglass Insulation is given 4 rating.
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b. Thermal Expansion
When the tenperature of material is decreasing significantly, it affects
the material to shrink. Shrinking of the material affects the value of thermal
conductivity to raise up, resulting heat that enters into the system becomes
bigger. From the literature (Bahadori, 2014) we know that the shrinking process
is proportional to the value of thermal expansion coefficient, bigger the thermal
expansion coefficient of material affects the increasing of shrinking process.
Rating 5 is given to the insulation which has thermal expansion coefficient close
to 2 105 / and the smaller rating is given to the insulation that has thermal
expansion coefficient far from 2 105 / . We rated our product as 5 because
has thermal expansion coefficient 2.5 105 / .
c. Lifespan
The insulation system will be better when it can be used for long periods
of time. Beside to decreasing preparation procees, it will reduce the costs in a
work project. Rating 5 is given to the insulation which has close to 30 years of
lifespan and the smaller rating is given to the insulation that has below 30 years
of lifespan. For all existing product we gives 5 rating based on benchmarking
data from assignment 1. For own product is given 5 rating because has 80 years
of lifespan
d. Cost-effective
One of the most important aspects in a work project is the amount of
costs that we used. From economics approach we know that small capital we
spend will be good on the sustainability of projects. Our insulation material tend
to be difficult to make and hard to find so have a high selling price. So, we give
3 rating for own product.
e. Health and Safety
The insulation system has to use material that can not harm the
environtment and worker on the work place. Health and safety is a parameter to
determiner whether the product is harmful or can cause some side-effect like
allergy when being used. our products use natural ingredients that have a
low content of chemicals so that has low possible of carcinogenic, mutagen,
neurotoxic, and reproductive toxic. That is why our product has 5 rating.
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f. Combustibility
Cryogenic industry tend to work in high pressure conditions. the higher
the pressure in the system it will be very susceptible to the occurrence of an
explosion. So that, the insulation for this situation has to use non combustible
material. Rating 5 is given to the insulation material that non combustible.
Meanwhile rating 1 is given to the insulation material that combustible. Own
product use non combustible material so the rating is given as 5
g. Vapor Moisture Transmission
For whatever purpose cold insulation is required, the insulation system
is only as good as its vapour barrier and the care with which it is installed. A
vapour barrier is a membrane of very low permeance placed on the warm side
of insulation to limit the flow of water vapour into the insulation. Rating 5 is
given to the insulation that has water vapour transmission close to 0 /
and the smaller rating is given to the insulation that has water vapour
transmission far from 0 /. Own product has water vapour transmission
0 / so we gives 5 rating
h. Service Temperature
The insulation material has the ability to stick to a certain temperature .
Materials that we use on cryogenic insulation purpose should has range
temperature below 150 to maintain a cryogenic product at a certain phase.
Rating 5 is given for the insulation that has service temperature below 150 .
From properties of material that we use we know that own product has service
temperature 1800 so we can gives 5 rating for own product.
i. Vermin and Fungus Resistance
The resistance insulation to vermin insect and hungel growth can be
important, particularly in hold stores for good. Insulation surfaces lightly to
become wet shall not definish with materials that maybe attack by this agencies.
Finishing with non absorptive materials is desireable for severe cases. Because
own product is made from non organic material we conclude that own product
can be resist to vermin and fungus. 5 rating is given to our product because of
vermin and Fungus Resistance
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the previous study. This concept will lead to our final specification on this product.
The final specifications of our products are given in the table below.
Table 7. 2 Product Specification
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Product
Characteristic Brief Description
Description
Insulation with maximum
Preventing heat gain from
Mechanism thermal protection with minimal
environment to the system.
weight and thickness.
Primary:
Polyvinyl
Material Chloride
Secondary:
Kraft
4 m x 1.5 m
Volume
x 1.5 m
Package
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Ingredients
Chemical Name Percent Brief Description
Synthetic Amorphous
25-40% as reinforcing fillers
Silica
a highly efficient
thickener, sebum absorber
Methylsilylated Silica 10-20% and soft focus agent
(impacts the appearance of
fine lines and wrinkles)
Polyethylene terephthalate an excellent water and
10-20%
(PET or polyester) moisture barrier material
Fibrous Glass (textile to improves the strength of
10-20%
grade) the composites
Magnesium Hydroxide 0-5% as a fire retardant
prevents the radiation of
Aluminum Foil 0-5% heat by reflecting it back at
the source.
(Source : various literatures)
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The choosing of silica aerogel as the main material based on the value of
thermal conductivity and service temperature that can be applied perfectly on
cryogenic insulation. Silica aerogel has the thermal conductivity 0.021 /
which makes this material to be good to prevent heat gain from the environtment to
a system. When heat gain has minimized, there will be no the change of temperature
of a system so we can maintain the temperature of a system to be constant. When
this is happen the goal of insulation system will be achieved.
The other important reason to choose silica aerogel is on the healty and
safety factor. Health and safety is a parameter to determiner whether the product is
harmful or can cause some side-effect like allergy when being used. our
products use natural ingredients that have a low content of chemicals so that
has low possible of carcinogenic, mutagen, neurotoxic, and reproductive toxic.
For whatever purpose cold insulation is required, the insulation system is
only as good as its vapour barrier and the care with which it is installed. A vapour
barrier is a membrane of very low permeance placed on the warm side of insulation
to limit the flow of water vapour into the insulation. Silica aerogels has 0 /
of water vapour transmission which means this material ability to prevent the flow
of water vapour into the insulation is good. The flow of water into the insulation
should be prevented to maintain the temperature of system to be contstant.
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CHAPTER 8
CONCLUSION
From chapter 1 until chapter 4 in this report, we conclude several things, they are:
1. The use of thermal insulation is to prevent heat gain which cause energy
consumption to skyrocket by simply providing resistance to heat flow
during heat transfer mechanisms.
2. Basic requirement for insulation system is due to their thermal conductivity.
The lower the number of thermal conductivity the less the flow of heat is.
3. The insulation strategy is to minimize radiative heat transfer, minimize
convective heat transfer, and introduce a minimum of solid conductance
media.
4. Based on the consumer requirements, the insulation product should be able
to meet the following criteria: have low thermal conductivity, able to
withstand thermal expansion, pressure, hit or crash, and is easy for
maintenance and services.
5. After benchmark to several existing products Aspen Aerogels, Rockwool,
and Arabian Fiberglass we obtain their specifications. The existing
products thermal conductivity are sequentially 0,021; 0,038; 0,028 W/m.K.
The service temprature range are consecutively -156 6 oC; 0 250 oC; -
18 450 oC. Their durability are in sequence 80 years, 60 years, and 50
years. So, current best insulation product is Aspen Aerogels.
6. There are two concepts from existing product. For the new concept, we propose
non-vacuum system with some new materials, there are reflective system,
blanket, spray, natural, and integrating.
7. Our new concept is divided into six materials of cold insulation including:
reflective system, blanket, spray, natural, and integrating.
8. From 13 respective concepts, we eliminate 2 concept through preliminary
elimination of vague, foolish, and redundant concept. From the 11 individual
concepts, we scored and compared them to the reference product with several
criteria and reduced them into 5 concept with a small highest score.
9. Based on 25 correspondent results. 17 of them are interested with our selected
concept, 7 are somewhat interested, and 1 is not interested.
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10. Out of 9 respondent as industry experts, 4 of them are would likely to buy the
product we offer, 4 would like to take a sample, and 1 is not willing to buy.This
proves that our product has demand, hence has a potential customers.
11. The selected concept is better than reference concept in some criteria which are
thermal conductivity, thermal expansion, lifespan, combustability, water-vapor
transmission, and service temprature.
12. The final specification of our insulation for cryogenic storage and pipeline is a
silica aerogel insulation, which the silica raw material is obtained through a
recycled silica gel. Hence, the insulation product we offer would become more
cost effective.
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REFERENCES
1.
2. ASTM Standard C1696, 2015, "Standard Guide for Industrial Thermal
Insulation Systems," ASTM International, West Conshohocken, PA, 2015,
www.astm.org.
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United States of America:McGraw-Hill Companies, Inc.
4. Aspen Aerogels, Inc. 2013. PIPE INSULATION FOR COLD SERVICE.
Northborough: Aspen Aerogels, Inc.
5. Arabian Fiberglass Insulation Co., Ltd. 2015. Heavy Density Pipe
Insulation Product. Dammam: AFICO
6. Cengel, Yunus A. 2008. Thermodynamics An Engineering Approach. 7 th.
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7. Van ness, Smith and Abbott. 2005. An Introduction to Chemical
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9. Fesmire, J.E., Rouanet, S., and Ryu, J., "Aerogel-Based Cryogenic
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2017.
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14. Bahadori, Alireza. Thermal Insulation Handbook for the Oil, Gas, and
Petrochemical Industries. Oxford: Gulf Professional, 2014. Print.
15. "Asbestos Exposure and Cancer Risk." National Cancer Institute. N.p., n.d.
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Environmental Protection Agency, 02 Feb. 2017. Web. 9 Feb. 2017.
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