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International Journal of Fatigue 29 (2007) 860868
Fatigue
www.elsevier.com/locate/ijfatigue
Received 7 December 2005; received in revised form 16 August 2006; accepted 10 September 2006
Available online 27 October 2006
Abstract
A threshold curve method was applied to study the fatigue behavior and fatigue blunt-notch sensitivity of austempered ductile iron
(ADI) of grade 2 (ASTM 897M-90), a material with an excellent combination of high strength, ductility, toughness, fatigue strength, and
wear resistance. The mechanical properties of ADI can be achieved by proper austempering treatments in relation to a unique micro-
structure consisting of acicular, carbide-free ferrite with carbon-enriched austenite. A mechanistic fatigue crack growth methodology that
uses an integrated threshold curve for fatigue crack propagation was applied to analyze its fatigue limit and the inuence of blunt
notches. The existence and nature of non-propagating cracks and their inuence on the denition of the fatigue limit was also analyzed.
Results show that the fatigue limit in ADI is controlled by a crack arrest. Ausferrite packet boundaries act as barriers for microstruc-
turally-small cracks due to a requirement for stage I growth in the ausferrite matrix. The strength of the barrier depends on the relative
orientations of the microstructure at the boundary. The fatigue limit of the ADI analyzed is inuenced by the micronotch eect of the
graphite nodules. However, it is possible to estimate a true matrix fatigue limit for the ausferrite microstructure, and the experimen-
tally measured limit may be described as an ADI or component fatigue limit.
2006 Elsevier Ltd. All rights reserved.
Keywords: Fatigue limit; Fatigue notch sensitivity; Microstructurally-small cracks; Crack growth threshold; Austempered ductile iron
0142-1123/$ - see front matter 2006 Elsevier Ltd. All rights reserved.
doi:10.1016/j.ijfatigue.2006.09.005
M.D. Chapetti / International Journal of Fatigue 29 (2007) 860868 861
Nomenclature
tration that is part of the casting design, it is important to respect to the fatigue limit up to a crack size a = d [12
understand its fatigue behavior so as to develop a useful 15]. For a microstructurally-small crack (MSC, the crack
assessment methodology for fatigue behavior predictions. length is of the order of the microstructural dimensions)
In this work, a mechanistic fatigue crack growth meth- initiated from a smooth surface, the fatigue limit at a given
odology that uses an integrated threshold curve for fatigue stress ratio R, DreR, denes the critical nominal stress range
crack propagation was applied to analyze the fatigue limit needed for continued crack growth (microstructural thresh-
and the fatigue notch sensitivity of an austempered ductile old). If the applied stress range Dr is smaller than DreR,
iron (ADI) of grade 2 (ASTM 897M-90). The existence and cracks (included in the microstructurally-small crack
nature of non-propagating cracks under the fatigue limit regime) are not initiated or are arrested at microstructural
and their inuence on the denition of the fatigue limit barriers located at depths smaller than d.
for blunt notches was also analyzed. On the other hand, for long or large cracks the threshold
stress for propagation decreases with increasing crack size
1.1. The small crack eect and the fatigue crack growth [1220]. The threshold for long cracks (LC, which have a
threshold crack length greater than that at which crack closure is
fully developed) is dened in terms of the threshold value
The eect of crack size on the fatigue crack propagation of the stress intensity factor range, DKthR, thus long cracks
threshold of many metals can be described conveniently by in constant amplitude loading can only grow by fatigue, if
means of the KitagawaTakahashi diagram, which relates the applied stress intensity factor range DK is greater than
the threshold stress with the crack size, as shown in DKthR.
Fig. 1. If the strongest microstructural barrier for fatigue In the physically small crack regime (PSC), which corre-
crack propagation is located at a given distance d from sponds to the transition between the microstructurally-
the material surface, the crack is non-damaging with small and long crack regimes (MSC and LC), the threshold
is below DreR and DKthR. Although in this regime the inu-
ence of microstructure is still important, it is the develop-
ment of crack closure, what governs the threshold level.
eR
Log. Threshold Stress, th
Crack propagation
Threshold, Kth
Physically
Microstructurally Small Cracks
Small Cracks
Extrinsic
Crack Initiation
KdR KthR
Microstructural Threshold KdR
d1 d2 d L0 l
Log. Crack Length, a d Crack Length, a
Fig. 1. KitagawaTakahashi-type diagram showing the threshold between Fig. 2. Fatigue crack propagation threshold as a function of crack length,
propagating and non-propagating cracks. dened by expression (1).
862 M.D. Chapetti / International Journal of Fatigue 29 (2007) 860868
Dierent models have been proposed to estimate the var- ditions. This concept is the basis for the resistance-curve
iation of the propagation threshold as a function of crack method [14,18,21], which needs to predict the variation of
length, while the crack is a small one, tending to a constant the propagation threshold as a function of crack length,
value for long cracks [14,16,17,21]. In a previous work [22] while the crack is a small one, tending to a constant value
an expression to estimate the threshold to fatigue crack for long cracks. The high-cyclic fatigue crack propagation
propagation as a function of crack length was obtained by behavior can be estimated for a given crack length range, if
Chapetti using only the smooth fatigue limit, DreR, the the crack growth rate as a function of the eective driving
threshold for long crack, DKthR, and the microstructural force for a given material is known. The initial crack length
characteristic dimension d (e.g. grain size). Below there is a is given by the position of the strongest microstructural
brief description of the model, which was used in this work. barrier, if the material is free of cracks or crack-like aws.
As mentioned before, small cracks grow to the rst The nal crack length is dened according to critical
microstructural barrier (e.g. grain boundary), and it is their parameters related to the loading conditions of the ana-
arrest what denes the fatigue limit. This is a material-based lyzed components.
limit (depending on the microstructural characteristic How to obtain the threshold for crack propagation for a
dimension, d). The model proposed in reference [22] is based given material, DKth, has been explained through expres-
on this concept and it estimates the material threshold for sions (1) and (2).
crack propagation from a depth given by the position d of To estimate the applied driving force DK for a given geo-
the strongest microstructural barrier, as follows (see Fig. 2): metrical and loading conguration, the following general
expression can be used [23]:
DK th DK dR DK thR DK dR b1 ekad c a P d: 1
p
For a crack length a = d, DKth = DKdR, and DKth tends to DK Y Drn pa; 5
DKthR for long cracks. In terms of threshold stress, we get: where Drn is the applied nominal stress range. The crack
DK dR DK thR DK dR 1 e kad
aspect ratio as a function of crack length has to be dened
Drth p a P d; 2 for the combination of component geometry and loading
Y pa
conditions, which allows the denition of the value of
where DKthR and DreR (and so DKdR), are all functions of parameter Y as a function of crack length.
the stress ratio R. The microstructural threshold for crack The quantitative analysis of fatigue crack growth
propagation, DKdR, is dened by the smooth fatigue limit requires a constitutive relationship of general validity to
DreR and the position d of the strongest microstructural be established between the rate of fatigue crack growth,
barrier, as follows [22]: da/dN, and some functions of the range of the applied
p
DK dR Y DreR pd ; 3 stress intensity factor, DK (crack driving force). Besides,
the threshold for the whole crack length range should be
where Y is the geometrical correction factor. In most cases, taken into account, including the short crack regime, where
the initiated microstructurally-small cracks can be consid- the fatigue crack propagation threshold is a function of
ered semicircular [1214], and the value of Y could then crack length. Among others, the following relationship
be 0.65. Furthermore, a total extrinsic threshold for crack meets these requirements [23]:
propagation, DKCR, is dened by the dierence between
da
the crack propagation threshold for long cracks, DKthR, C DK m DK m
th ; 6
and the microstructural threshold, DKdR, function of the dN
crack length. The parameter k can be estimated as a func- where C* and m are environmentally-sensitive material
tion of the same microstructural and mechanical parame- constants obtained from long crack fatigue behavior and
ters used to dene the material threshold to crack DKth is the crack growth threshold as a function of a and
propagation (DreR, d and DKthR), as follows [22]: R, and it also represents the eective resistance of the mate-
1 DK dR 1 DK dR rial to fatigue crack propagation. The fatigue crack propa-
k : 4 gation life for a given crack length range and a given
4d DK thR DK dR 4d DK CR
material can be obtained by integrating expression (6)
and using expression (1) for the threshold of the material
1.2. Fatigue crack propagation assessment (DKth), and a proper expression for the applied driving
force (DK) given by the analyzed loading and geometrical
The dierence between the total applied driving force conguration (expression (5)).
(dened by the applied stress distribution corresponding Nonetheless, the conditions for fatigue limit can be ana-
to a given geometrical and loading conguration, DK), lyzed assuming that it will be dened by the highest nomi-
and the threshold for crack propagation, DKth, denes nal stress level at which fracture does not occur; that is to
the eective driving force applied to the crack. By knowing say, the nominal stress above which the applied driving
the crack growth rate as a function of this eective driving force is greater than the resistance of the material for any
force for a given material, it is possible to estimate the high- crack length (da/dN > 0 in expression (6)). This analysis
cyclic fatigue crack propagation behavior in the given con- is presented below, following the description of the experi-
M.D. Chapetti / International Journal of Fatigue 29 (2007) 860868 863
mental procedure and results, as well as and the estima- run out. Between 10 and 12 specimens from each group
tions of the threshold curves and the applied driving forces were tested at several stress levels to obtain reliable SN
for dierent kt. curves and fatigue limits. The fatigue limit was estimated
as the highest stress level at which no failure was observed.
2. Experimental procedure and results Specimens that failed from casting defects (three of the
total number of specimens tested) were disregarded in
Blocks with a Y-shaped cross section where the web order to analyze the intrinsic fatigue properties of the
portion dimensions were 80 mm (high) 25 mm ADI. The inuence of casting defects will be fully
(thick) 230 mm (long) were cast in sand molds with addressed in a future paper.
the following chemical composition: 3.4% C, 2.63% Si, All fatigue test results are shown in Fig. 4. Fig. 5 shows
0.19% Mn, 0.90% Cu, 0.57% Ni, 0.048% Mg, 0.12% Mo, the fatigue limit, Dre, as a function of the theoretical stress
0.016% S, 0.041% P. The graphite structure in selected cast- concentration factor, kt. It can be seen that, when the con-
ing portions has the following measured data: average nod- centration factor increases from 1 to 2, fatigue limit
ule diameter of 51 lm, nodularity of 90%, and nodular decreases from 880 MPa to 520 MPa. However, if kt is fur-
count of about 100 nod/mm2. ther increased to 2.5, the fatigue limit reduces only 40 MPa.
Six specimens (each one of 225 mm in length and Below it will be shown that from this kt values the fatigue
12.5 mm in diameter) were initially machined from the limit is mainly given by the threshold for long cracks DKthR
web of the Y-blocks, followed by heat treatment. Speci- and the notch depth D.
mens were rst austenitized in salt bath at 900 C for
1.5 h , after which they were quenched in salt bath at
360 C for 1.5 h and then cooled in air. Mechanical proper-
kt
ties in this condition are 750 MPa in yield strength and 1.02
1020 MPa in tensile strength. The nal stages of machin- 1000 1.54
Applied Stress Range, n [MPa]
Fig. 3. Specimen dimensions in millimeters. A photograph of one of the specimen notches is also shown.
864 M.D. Chapetti / International Journal of Fatigue 29 (2007) 860868
Fig. 6. Examples of microstructural cracks found at specimens with dierent kt tested at stress levels just below the fatigue limit.
M.D. Chapetti / International Journal of Fatigue 29 (2007) 860868 865
3.1. The microstructural threshold and the strongest The threshold for long cracks and the position of the
microstructural barrier strongest microstructural barriers were estimated. In order
to estimate the threshold curve with Chapettis model, it is
In nodular cast iron, the cohesion between the graphite also necessary to estimate the resistance of the strongest
nodules and the matrix is low [24]. It can therefore be microstructural barriers. Because the existence of the
assumed that the nodules behave like holes, which give rise graphite nodules that act as holes inuences the stress eld,
to the formation of a crack in their equatorial plane. For the resistance of the strongest microstructural barriers can-
these small cracks the crack front delineated by the particle not be assumed to be equal to the smooth fatigue limit of
does not represent the equilibrium shape, which should be the ADI, as it can be done for continuous materials. How-
approximately a semicircle. Crack initiation will take place ever, by using the smooth fatigue limit of the ADI (DrADI eR ,
preferentially at the specimen surface and surface crack the position of the strongest microstructural barrier (2d),
growth will decrease eventually until the crack adopts an and the applied stress distribution calculated by consider-
equilibrium shape, as proposed in reference [24,25]. ing the inuence of the hole (graphite nodule), the smooth
Observations carried out in this work support those fatigue limit of the matrix (DrMatrix
eR , equal to the resistance
reported by references [11,24,25] (see Fig. 6), which show of the strongest microstructural barrier) can be roughly
that in absence of casting defects, micro-cracks are initiated estimated by using a trial-and-error method. The stress dis-
in graphite nodules and propagate following ferrite laths tribution in a microporous isotropic material with similar
that are perpendicularly oriented with respect to the notches to those shown in Fig. 3 was studied in a previous
applied maximum stress. Examples in Fig. 6 also show work [26], where the following expression was obtained for
how micro-cracks are arrested, when they nd ferrite tensile loading:
colognes unfavorably oriented regarding their propagation
Dryy x kt
directions. These changes in the orientation constitute the q 1 ebx ; 7
micro-structural barriers to crack propagation, where the Drn 1 4:5xR q
crack located rst from the graphite nodule seems to be
the strongest. where R is the nodule radius and b is an empirical constant
For an accurate assessment of the fatigue microcrack found to be 120 [1/mm] for all analyzed cases (D = 1 mm,
driving force, the nodule should not be considered a crack kt = 1.02, 1.54, 2, 2,55, q = 50, 2, 1, 0.5 mm, porous diam-
but a notch. Thus, it is necessary to determine a crack eter 20, 40, 60, 80, 100 lm, three-dimensional elastic anal-
driving force for small cracks inuenced by the nodule. ysis). The rst part of the right term of expression (7)
The problem lies in the analysis of the crack in a stress denes the stress concentration due to the notch, and the
eld inuenced by the nodule from which the microcrack term between branches denes the stress concentration
initiates. Then, if it is assumed that the nodules act as due to the micronotch (nodule) and is a function that tends
holes, the austempered ductile iron can be considered a to the unity for x/R values higher than 2; that is to say, the
microporous material. The distribution of microstructural inuence of the graphite nodule vanishes after a distance
barriers in the matrix can be then supposed to be dened similar to its size.
by the average size of the ausferrite packets (d = 40 lm).
From the evidence of Fig. 6 and by considering that the 4. Results and discussions
rst microstructural barriers are located at a distance
smaller than the average nodule size (50 lm), it is possible 4.1. Smooth fatigue limit
to assume that the strongest microstructural barrier is
actually the one located at a distance 2d from the macro- Fig. 7a shows the stress distribution obtained by using
notch root; that is to say, the rst barrier located at expression (7) for bending loading when a nominal stress
30 lm from the graphite nodule from which the micro- level of 880 MPa (fatigue limit) is applied to a smooth spec-
crack nucleates. imen with a micronotch of radius 50 lm. Here the micro-
Thus, in order to apply the threshold curve methodol- notch was conservatively considered to have a radius
ogy, the ADI should be regarded as an ausferrite material equal to the stated diameter of the graphite nodule, and
with an average size of the ausferrite lath length of about the crack was considered semicircular. Fig. 7 also shows
40 lm plus a distributions of microporous with and aver- the threshold curve for crack propagation corresponding
age size of about 50 lm. Assuming this, the strongest to a continuous matrix estimated with expression (2) by
microstructural barrier for the ausferrite material (continu- using the threshold for long cracks DKthR, the position of
ous matrix) would be located at a position d 40 lm from the strongest microstructural barrier d = 40 lm and its esti-
the specimen or notch surface. But for the ADI, it would be mated resistance DrMatrix
eR . It can be seen that the applied
located at a distance 2d 80 lm from the surface due to stress becomes equal to the threshold stress for crack prop-
the existence of the graphite nodule, as it is suggested by agation for a crack length a = 2d 80 lm. By using this
the experimental evidence shown in Fig. 6. procedure, the resistance of the strongest microstructural
866 M.D. Chapetti / International Journal of Fatigue 29 (2007) 860868
Threshold Curve, th
Applied Stress Distribution,
[MPa] n = eR = 880 MPa [MPa] n = e = 620 MPa
2 kt = 1.02 2 kt = 1.54
1000 1000
5 5
th
th
Graphite Graphite
Nodule Nodule
d 2d d 2d
2 2
0.01 0.10 1.00 0.01 0.10 1.00
a [mm] a [mm]
[MPa] n = e = 510 MPa n = e = 460 MPa
[MPa]
2 kt = 2 2 kt = 2.55
1000 1000
5 5
th th
Graphite Graphite
Nodule Nodule
d 2d d 2d
2 2
0.01 0.10 1.00 0.01 0.10 1.00
a [mm] a [mm]
Fig. 7. Stress distributions estimated by using expression (7) and threshold curves for crack propagation estimated with expression (2) for four dierent
stress concentration factors: kt = 0.02 (a), 1.54 (b), 2 (c) and 2.55 (d).
25 25
K n = eR = 880 MPa K n = e = 620 MPa
[MPa] [MPa]
20 kt = 1.02 20 kt = 1.54
K K
15 15
10 Kth 10 Kth
5 5 Graphite
Graphite
Nodule Nodule
d 2d d 2d
0 0
0.01 0.10 1.00 0.01 0.10 1.00
a [mm] a [mm]
25 25
K K n = e = 460 MPa
n = eR = 510 MPa
[MPa] [MPa]
20 kt = 2 20 kt = 2.55
15 K 15
Kth K
10 10 Kth
5 5 Graphite
Graphite
Nodule Nodule
d 2d d 2d
0 0
0.01 0.10 1.00 0.01 0.10 1.00
a [mm] a [mm]
Fig. 8. Applied driving forces as a function of crack length in terms of the applied stress intensity factor estimated by using expression (8) and threshold
curves for crack propagation estimated with expression (1) for four dierent stress concentration factors. kt = 0.02 (a), 1.54 (b), 2 (c) and 2.55 (d).
below the fatigue limit does not change with kt for the stud- 8, the fatigue limit is given by the mechanical threshold for
ied range and geometrical and loading conguration, and is long cracks for sharp notches (kt > 2.5), whereas the maxi-
given by the position of the strongest microstructural bar- mum length of non-propagating cracks observed below
rier located at a distance 2d from the specimen surface. Full the fatigue limit is then given by the applied stress level.
agreement with the experimental results can then be Finally, it should be noted that, despite the elasticity of
observed (see experimental results in Fig. 5 and estimated the macroscopic behaviour in all analyzed congurations,
ones in Fig. 7 or Fig. 8). there is some uncertainty over the application of linear-
Fatigue crack propagation threshold as a function of the elastic fracture mechanics to microcracks where cracks
crack depth is dened mainly by the smooth fatigue limit of sizes are comparable to the scale of the microstructure
the ADI, DrADIeR (fatigue limit without stress concentration), and crack-tip plasticity.
and the mechanical threshold for long cracks, DKthR. The
relative dierence between both values denes the existence 5. Conclusions
and nature of no-propagation cracks under fatigue limit
(See Figs. 1, 7 and 8). For a given threshold for long cracks In this work, the fatigue limit and the blunt-notch sensi-
(DKthR), an increase on DrADI eR will increase the fatigue tivity of an austempered ductile iron (ADI) of grade 2
notch sensitivity and also the crack length range for which (ASTM 897 M-90) were experimentally and theoretically
the propagation limit is dened as a mechanical propaga- analyzed by using a mechanistic fatigue crack growth
tion threshold. methodology that uses an integrated threshold curve for
It can be seen from Figs. 7 and 8 that the fatigue limit of fatigue crack propagation. The existence and nature of
the ADI is given by the rst eective microstructural barrier non-propagating cracks under the fatigue limit and their
for all kt analyzed. As it was observed for all non-propagat- inuence on the denition of the fatigue limit for blunt
ing cracks found just below the fatigue limit, their length is notches were also analyzed. Experimental results allowed
dened by the position of the rst microstructural barrier the denition of the necessary assumptions for the applica-
for blunt notches (kt < 2.5), and according to Figs. 7 and tion of the integrated threshold curve method.
868 M.D. Chapetti / International Journal of Fatigue 29 (2007) 860868
The observations demonstrate that the crack arrest con- [8] Krishnaraj D, Rao KV, Seshan S. AFS Trans 1989;98:34550.
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J Mater Sci 1994;29:493040.
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