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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

目录 Contents

  • 1 安装准备 Installation preparation

    • 1.1 准备工作区 Preparing working-area

    • 1.2 工作台和搬运 Working plateform and Transportation

    • 1.3 安全 Safety

    • 1.4 安装说明 Installation instruction

      • 2 简介 Brief introduction

        • 2.1 安全须知 Safety introduction

        • 2.2 如何使用本手册 How to use this manual?

        • 2.3 操作过程中遇到无法解决的问题时的处理方法 Handling method

to inextricable problem during operation

  • 2.4 警告和注意 Warnings & Cautions

    • 3 概述 Summary

      • 3.1 简介 Brief introduction

      • 3.2 仪 器 基 本 描 述 : 部 件 说 明 Basic description of the

instrument:component descripition

  • 3.3 控制器 controller

    • 4 仪器操作 Instrumentation

      • 4.1 仪器的校正(操作前)calibration of the instrument(before

operation)

  • 4.2 如何使用 How to use the instrument?

  • 4.3 实验步骤 Testing steps

  • 4.4 试验方法 Testing way

    • 5 日常维护 Routine maintenance

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苏州宇诺仪器设备有限公司

REV

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

  • 5.1 警告和注意 Warnings&Cautions

  • 5.2 重要小结 Important brief summary

  • 5.3 校准仪器 Instrument calibration

6 故障排除 troubleshooting 7.氧指数法影响因素与讨论 Oxygen index influence factor and

discussion 附录 A 技术参数小结

Appendix A Technicl parameters brief

summary 附录 B 装箱清单 Appendix B Packing List

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苏州宇诺仪器设备有限公司

REV

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

1.安装准备 Installation preparation 1.1 准备工作区 Prepare working-area 在仪器安装人员到达之前,请事先做好以下准备工作:Please ensure the following preparation work ready before the installation personnel of instrument arrive 为仪器准备一个工作区 Preparing working-area 为仪器运至安装现场 Transport the instrument to the installation

site

准备好放置仪器的工作台 Place the working plateform of the instrument 注意 Cautions 此仪器任何有关的试验应由专业人员进行,否则有可能对仪器造成损

坏。

此仪器的对电源要求: 电压、频率保持稳定、接地良好 。 The instrument is working under high voltage and must be processed by professional personel,otherwise will result in instrument damage. Power supply requirement of the instrument. stable voltage and frequency . good grounding 1.2 工作台和搬运 Working plateform and Transportation 按以下要求安排工作台和进行搬运: Please arrange and transport working plateform as below requirement:

确保工作台坚固,可支撑机器重量。 Ensure the working plateform is strong enough to stand whole machine. 注意 Cautions

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

搬运时不要推拉仪器的控制器面板,仅能以仪器坚固的金属面为施力

点。

Please don’t push or pull the

operating panel during

transportation,can only take the hard metal appearance as point of force application for transportation. 1.3 安全 Safety 请始终具有安全意识。Keep safety awareness in mind always。 仪 器 内 的 部 件 只 能 由 专 业 人 员 进 行 操 作 。 Operate the inside component by professional personnel. 仪器的工作电压 220V。 Working voltage of the instrument is 220V. 警告 Warning 请确保断电后进行操作,以防止造成伤害。Please operate when power

supply interrupt in order to avoid hurt. 注意 Cautions 请在接地标志处接地线,否则可能会导致仪器损坏。Please connect ground wire in the earthing makr,otherwise may result in instrument damage. 1.4 安 装 说 明 Installation instruction

仪器名称 氧指数测定仪 型号 Instrument Name Digital Readout Oxygen Index Tester Model No. YN61037 搬运时不要推拉仪器的控制器面板,仅能以仪器坚固的金属面为施力 点。 Please

1、将仪器开箱后平放在通风橱内或工作平台上。取出燃烧筒内金属网,

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

放入配给的玻璃珠,再放入金属网、试样夹、套上玻璃燃烧筒。Open the instrument,and place on the draught cupboard or working plateform.Get the metal net out of incendiary cylinder and put glass bead,and then put metal net,sample holder and then put glass incendiary cylinder.

2、用随机附件中的塑料增强管将控制箱后的氧氮混合气体输出端与主

机底端的管连接头连接起来,并用管卡卡紧。注意:控制箱后面氮气、氧 气输入分别对应前面氮气、氧气调节方位,混合气输出端在中间。Connect the output end of trimix behind the control cabinet with plastic intensifier tube and host machine bottom and clamp tightly. Attention:

nitrogen and oxygen input match well the front nitrogen and oxygen adjusting position, trimix output is in the middle.

3、准备好氧气和氮气钢瓶,安好钢瓶上的减压阀。用随机附件中的塑

料增强管将控制箱后面板上的氮气、氧气接头分别与氧气,氮气钢瓶减压 阀输出端相连,并用管卡卡紧。钢瓶与减压阀由用户自备。Prepare oxygen and nitrogen cylinder, install the reducing valve.Connect the nitrogen and oxygen interface on the control cabinet behind board and their cylinder reducing valve output with plastic intensifier tube and clamp tightly. Cylinder and reducing valve should be prepared by the user. 4、点火器是专门为点火设计的点火枪。Igniter is a firing gun which is especially designed for ignition 5、 将燃烧桶安装在机座上。Install the burning barrels on the engine base. 2 简介 Brief introduction 本章包括以下内容:The chapter contains the following contents

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

. 如何使用本手册 How to use this manual? 操作过程中遇到无法解决的问题时的处理方法 Handling method to inextricable problem during operation 安全须知 Safety instruction 警告和注意 Warnings & Cautions 阅读并理解本章的内容。Please must read and underestand the contents of this Chapter 2.1 安全须知 Safety instruction 不正确按照本手册进行操作,可能会导致人身伤害的发生。Incorrect operation of this manual will result in possible personal injury. 此仪器在操作和维修过程中为防止人身伤害,在进行任何仪器操作前 都要首先阅读如下的安全措施,并严格遵循: In order to avoid personal injury, please must read the following safety precautions firstly before operating any instrument and follow strictly:

任何时候都要具有安全意识;Keep safety awareness in mind always; 在准备操作或维修此仪器前应阅读本手册的全部内容;All contents must be read when you start to operate the instrument or have maintenance 必须熟悉所有的安全特性和警告文字;Must be familiar with all security features and warning words; 严格按照国家的安全规程操作和维修此仪器;Must operate the

instrument or have maintenance strictly according to safety rules of Nations. 确保所有的操作和维修人员安全地使用和维护此仪器;Ensure all

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

operating personnel and maintenance personnel can use and maintenance this instrument safely 每日都对安全装置进行检查以确保其正常工作。Must inspect the

safety device every day and ensure it’s normal working

  • 2.2 如何使用本手册 How to use this manual?

本手册的目的是帮助您正确并安全地使用和维护 The purpose of this manual is to help you to use and maintenance correctly and safely. 本手册包含以下一些内容:This manual contains the following contents:

安装准备 Installation preparation 简介 Brief instruction 概述 Summary 仪器操作 Instrumentation 日常维护 Routine maintenance 故障排除 troubleshooting 氧指 数 法影 响因 素 与讨 论 Oxygen index influence factor and discussion 附录 Appendix

  • 2.3 操作过程中遇到无法解决的问题时的处理方法 Handling method

to inextricable problem during operation 当您在操作、维护过程中遇到无法解决的问题或不知如何进行下一步 操作时,请立即停止操作并联系本公司。When you meet inextricable problem during operation or maintenance or feel confused how to operate its next step, please stop operation and contact our company immediately 本公司联系方式:Contact info:

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

名称:苏州宇诺质检仪器有限公司 Name:Yunuo (Suzhou) Instrument Co.,Ltd. 地址:江苏省苏州市吴中区木渎镇金桥开发区木胥西路 26 号 Address:No 26,Muxuxi Rd,Jinqiao Development Zones,Mudu Town,Suzhou 电话:0512-82256088 Tel:0512-82256088 传真:0512-68560932 Fax:0512-68560932 2.4 警告和注意 Warnings & Cautions 在此手册中,警告(WARNINGS)警告操作人员避免可能的人身伤害, 注意(CAUTIONS)提醒操作人员防止可能发生的仪器损坏。如下一些通用 的 警 告 和 注 意 事 项 适 用 于 公 司 的 所 有 设 备 : In this manual, ” WARNINGS”:warn the operating personnel to avoid possible personal injury; ” CAUTIONS ” :remind the operating personnel to prevent possible instrument damage.The universal WARNINGS & CAUTIONS as below can apply to all equipments in Yunuo. 用户永远不能忽视此仪器的安全性能。User should never ignore the safety performance of the instrument. 非专业人员对仪器进行机械构件的拆卸或重新安装时,有可能损坏设 备或造成人身伤害。。Laypeople may damage the equipment or cause personal injury when he disassemble mechanical component of the instrument or make reinstallation. 在进行维修或维护操作前必须确保所有的电源均已断开。 Make sure all power supply are switch off before make maintenance or repair 必须随时保证仪器的正确接地,确保仪器的主电源极性连接正确。 Must ensure the proper grounding of the instrument any time and ensure the proper connecting of the main power supply polarity

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

记住此仪器的电源电压足以造成人身伤害。Keep in mind that the power voltage is enough to cause personal injury. 如果你所测试的材料有可能释放刺激性的或有毒雾气,必须连接合适 的排气设备,以把这些气体安全地排到外界空气里。 If the tested material may release pungent smell or toxic gas, please must connect exhaust equipment and drain the gas outside safely. 此外还有一些其它的专门用于此仪器的警告和注意事项,具体内容将 在本手册中出现,这些安全措施是附加的,但不能取代任何用户必须遵守 的其他安全标准。 More WARNINGS & CAUTIONS are included in this manual. These additional safety precautions can’t replace any other safety standard which all user must follow.

3.概述 Summary

本章内容包含 YN61037 氧指数测定仪的概述。 This chapter contains summary of YN61037 Digital readout oxygen index Tester

仪器名称 氧指数测定仪 型号 Instrument Name Digital Readout Oxygen Index Tester Model No. YN61037 记住此仪器的电源电压足以造成人身伤害。Keep in mind

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苏州宇诺仪器设备有限公司

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

3.1 简介 Brief introduction

氧指数测定仪:是符合国家标准 GB2406-2009 规定,用来测定聚合物 在燃烧过程中所需氧气浓度(体积百分比)的仪器。聚合物氧指数值是该 物质引燃后能保持燃烧 50 毫米或燃烧时间 3 分钟所需的氧、氮混合气体中 最低氧的体积百分比。该仪器结构简单,操作方便,可以作为鉴定聚合物 燃烧性能的一种手段,也可以作为一种相关的研究工具,从而对聚合物的 燃烧过程获得较好的认识。本仪器适用于塑料、橡胶、泡沫等材料的燃烧 性能的测试,其测定结果准确,再现性好。是研究、生产阻燃材料必不可 少的测试仪器。 OI Tester is compliant with GB2406-2009 and Used for testing the oxygen concentration (volume percent) needed when polymer is burning. With the following features:

(1) It’s simply structured, and easy to operate, (2) It can be used as a means of identifying polymer’s combustibility, also a relevant research tool. Thereby, we can get a better understanding of the polymer burning. (3) Suitable for testing plastic, rubber, bubble and other materials’ combustibility. (4) Its result is accurate. So, it’s an essential testing instrument when researching and producing antiflaming materials. 3.2 仪器基本描述:部件说明 Basic description of the instrument:

component description 要使用本仪器,必须首先了解以下的部件及其功能: Please learn well the following component and their function before operating the

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

instrument

.

流量计 flowmeter

压力表 piezometer

仪器名称 氧指数测定仪 型号 Instrument Name Digital Readout Oxygen Index Tester Model No. YN61037 instrument . 流量计

3.3 控制器 控制器包括以下部分:The controller includes the following part:

  • 1. 显示区 display area

  • 2. 操作键 operational key

3.3.1 示区 display area 液晶显示器。LCD

  • 3.3.2 操作键 operational key

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

电源开关键 power supply switch key:按此键机器通电。Press this key to have electricity 流量调节阀 flow adjusting valve:按此键调节流量。Press this key to adjust flow 减压阀 reducing valve:按此键调节压力。Press this key to adjust pressure 电位器调节旋钮 potentionmeter adjusting knob:校正氧浓度值。(在 机器背面)correct oxygen density value (behind the machine)

仪器名称 氧指数测定仪 型号 Instrument Name Digital Readout Oxygen Index Tester Model No. YN61037 电源开关键 power supply

4 仪器操作 Instrumentation 4.1 仪器的校正(操作前)calibration of the instrument(before operation)

校正满度:接通仪器电源,开启已知氧浓度值(钢瓶上有充气标定值) 的氧气钢瓶总阀并调节减压阀,压力为 0.25-0.4Mpa,顺时针调节仪器面板 右下角“稳压”阀,仪器压力表指示值为 0.1±0.01Mpa,反时针调节右边 压力表上方的“流量”旋键,流量计指示值为 10L±0.5L/min, 此时仪器数 显表显示的数值应符合已知氧浓度值,否则应调节“满度”,返时针关闭 “稳压”阀。 Full calibration: plug in and turn on the main valve of the

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

cylinder which has known oxygen density value (there is gasing calibration value on the cylinder) and adjust the reducing valve, pressure is 0.25-0.4Mpa;adjust the “stabilivolt” clockwise on the lower right corner of the instrument panel, the pressure display0.1±0.01Mpa;adjust the”flow” counter-clockwise on the

right side of the piezometer, flowmeter display 10L±0.5L/min.The display value no on the instrument is already compliant with known oxygen density value, otherwise should adjust ”full” and counter-clockwise close ”stabilivolt”

4.2 如何使用 how to use?

本章描述了的基本使用方法, 请按以下顺序进行操作:This chapter describe the basic using way. Please operate as follow steps:

1、根据 GB2406-2009 规定,燃烧桶内混合气体流速为 4±1 厘米/秒, 据此选择混合气体流量为 14.1L/min。也可以按特殊标准计算出所需流量。 公式为:燃烧筒截面积 X 流速(注意单位换算)。有的标准例如: GB/T5454-1997 直接给出了混合气体流量,参照此标准流量调整即可。As per GB2406-2009 requirement, mixed gas flow velocity in the burning barrels is 4±1cm/s,and thus get the mixed gas flow is 14.1L/min。 Can also calculate the required flow based on special standard. Formula: burning barrel sectional area X flow velocity(pay attention the the unit conversion).Some standard like: GB/T5454-1997 listed the mixed gas flow directly, and adjust the flow based on it.

2、按照所需要试验的试样标准规定选取制作试样,分别选用自撑材料

或非自撑材料的试样夹,装于高度可调的滑套顶端,如果高度超过标准要 求,可以卸下调高滑套将试样夹直接安装在滑套上。Making test sample based on sample standard, use self-supporting material test sample

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

holder or non self-supporting material test sample holder,install on the top of adjustable sliding sleeve.Can discharge the adjustable sliding sleeve and put the test sample holder on the sliding sleeve directly when the height is beyond of standard requirement.

3、满度调节。由于用户使用的氧气大多数是工业氧气,其纯度因产地

的不同而有所不同。所以在每次换氧气瓶时需要重新标定氧气浓度。方法 如下:氮气瓶关闭,氧气瓶打开,冲洗几分钟后。在控制箱内完全通氧气, 调节控制箱背后的“满度”旋钮,使前面显示的氧气浓度为氧气钢瓶的浓 度。一般情况下,参考值为 99.2%,或 99.3%左右。也可以直接询问氧气生 产厂家,确定其浓度,按此值调节。

Full scale adjusting

..

The

most oxygen which user use is industry

oxygen,and its purity is different due to different producing area.So please mark oxygen density when change the oxygen cylinder every time.See the following steps:close the nitrogen cylinder,open the oxygen cylinder and clean for several minitues.Make the control cabinet is full of nitrogen,adjust the”full scale” button behind of the control cabinet,change the previous oxygen density to be oxygn cylinder density.Generally,the reference value is 99.2% or about 99.3%.And also inquiry oxygen producer directly.

4、根据资料或经验选择最初的氧浓度,如无法了解,可在空气中点燃

试样,如试样燃烧很快,氧的最初浓度先定为 18%,如试样在空气中点燃后 马上熄灭,则根据点火的难易和离火后熄灭的情况选择氧浓度 25%或更高。 If still can’t learn about the oxygen density based on documents or experience,you can burn the test sample in the air.If the testing sample is burning quickly,and the oxygen density is 18%;if the testing sample extinguish immediately,please choose the oxygen

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仪器名称

氧指数测定仪

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Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

density 25% or more based on ignition difficulty and extingush situation after no fire.

5、关闭流量调节阀,和流量计上的流量调节阀,打开氧气、氮气钢瓶

阀门,调节减压阀,使输出压力在 0.2-0.3MPa 左右。然后调节稳压阀(稳 压阀在调节前,需将手钮盖拉出,调节后再推进去,在未拉出时,手钮是 不能转动的),使控制面板上的氧气、氮气压力表指示为 0.05-0.15MPa,然 后调节流量阀,按下面板上的电源按钮,打开电源。注意液晶显示表上的 氧的浓度,并注意混合气体的流量是否达到所需的流量。调节过程中,需 要比较小心和缓慢,在转动调节阀旋钮后,显示不会马上变化,原因是气 体需要在储气筒内充分混合。调节数值稳定后,需要等待 30 秒左右的时间 冲洗燃烧筒,使其内部的气体更为接近调节后的混合气体。 Close the flow adjusting valve and flo valve on the flowmeter,open the oxygen cylinder valve and nitrogen cylinder valve,adjust the reducing valve and make the pressure output about 0.2-0.3Mpa,then adjust pressure maintaining valve to keep oxygen and nitrogen pressure on the control panel to be 0.05-0.15MPa,then adjust the flow valve,press the power supply switch and turn on it. (before adjusting,please pull the hand knob cover and push in,the hand knob will not rotate if not pull out.)Pay attention to the oxygen density on the LDC screen and the mixed gas flow meets the required flow.Please remember to do it carefully and slowly during adjusting.The display will not have change immediately when move the adjusting valve knob,because the air should be mixed completely in the air cylinder.Waiting for 30 seconds after adjusting value is stable and then wash the burning barrel to make the inside air to be similar as adjustd mixed gas.

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

6、冲洗后,按标准要求点燃试样(点火器的使用按前面叙述),点燃

试样后,立即撤去火源。 Ignite the test sample as per standard requirement after washing( see the ignitor using as above-mentioned),move the fire ways at once after test sample burning.

7、试验后,按标准要求记录试验情况,填写试验报告。

Record the testing process as per standard and fill the testing report after test. 8、将仪器电源开关关闭; 断开主机电源开关和气源阀门,仪器及周 围打扫干净。 Turn off the instrument power supply; break the host power supply

switch and air source valve,keep the instrument and site clean and clear.

4.3 实验步骤 Testing steps:

1、取标准测试样品至少 15 根,对其编号整理,在试样的任意一端 50mm 处划线,把另一端插入燃烧柱内试验夹中,将试样垂直装在试样夹上,并 罩上燃烧筒。 Get the standard testing sample at least 15pcs, number each of them,mark any one side about 50mm,and insert another side to the testing fixture in the burning barrel,hang the test sample on the testing sample fixture and cover incendiary cylinder.

2、根据经验或试样在空气中点燃的情况,估计开始时的氧浓度。如在

空气中迅速燃烧,则开始试验时的氧浓度为 18%左右;在空气中缓慢燃烧或 时断时续,则为 21%左右;在空气中离开点火源即灭,则至少 25%。 Estimate the oxygen density based on experience or test sample burning in the air.If the testing sample is burning quickly,and the

工程设计

苏州宇诺仪器设备有限公司

REV

A

仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

oxygen density is 18%;if the testing sample burning slowly or intermittent, the oxygen density 21% ; and at least 25% when extingush after no fire. 3、打开氮气、氧气“稳压”阀,仪器压力表指示值为 0.1±0.01Mpa 并同时调节流量,使氮气、氧气混合流量为 10L±0.5L/min(球形浮子最大 直径处),此时数显窗口显示的数值,即为当前的氧浓度值(亦称氧指数值)。 若提高氧浓度则增大氧流量,减少氮流量,否则反之。并始终保持压力为 0.1±0.01Mpa 和总流量 10L/min 不变的速度流经燃烧筒,洗涤燃烧筒至少

30S。

Open the nitrogen pressure maintaining valve and oxygen pressure maintaining valve, and the pressure value on the instrument is 0.1 ±0.01Mpa and adjust the flow together to make nitrogen and oxygen mixed flow to be 10L±0.5L/min(the max diameter of spherical float) and the value displayed on the digital display window is just the value of oxygen density.If increase the oxygen density,then increase oxygen flow and decrease nitrogen flow;otherwise conversely. 4、然后用点火器(火焰长度 12mm—20mm)点燃试样顶端,确认试样上端 完全燃烧后撤走点火器. Use the ignitor(flame length is about 12mm-20mm) to ignite the top of test sample and withdraw after the top of test sample is burning completely. 5、开始计时,观察燃烧、记录燃烧现象。Start to timing,observe burning and record burning phenomenon.

6、燃烧结束后,换试样,根据燃烧现象调节氧浓度,重复前面的步骤。

Change the test sample after burning and repeat the previous steps and adjust oxygen density based on burning phenomenon.

工程设计

苏州宇诺仪器设备有限公司

REV

A

仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

4.4 试验方法 Testing method A、顶端点燃法 Top ignition method

1、点燃点火器,使点火器火焰的最底可见部分接触试样顶端并覆盖整

个顶表面,勿使火焰碰到试样的棱边和侧表面,同时开始计时。在确认试 样顶端全部着火后,立即移去点火器,同时再次计时,并观察试样燃烧的 长度。 Ignite the ignitor and make the flame bottom visible part can touch test sampe top and cover the whole top surface.Don’t make the flame to touch edge and side surface of the test sample. 2、当试样在 180 秒内燃烧前锋到达或超过上标线时,计时结束,调整 氧浓度,擦净燃烧筒和点火器表面的污物,使燃烧筒的温度回复到常温或 另换一个为常温的燃烧筒,进行下一次实验。 Timing is over when the test sample meets or exceeds the marking line in 180seconds;adjust the oxygen density,wipe the burning barrel and surface dirt on the ignitor.Make the next experiment after the temperature of burning barrel return back to normal or change another burning barrel with normal temperature. 3、若材料在 30s 内未点燃,移去点火器,并重新调整氧的浓度,重新 开始实验。 Move the ignitor if the material are not on ignition within 30 seconds,and adjust oxygen density and start experiment again. B、扩散点燃法:Diffused ignition method

1、点燃点火器,充分降低移动点火器,使火焰可见部分施加于试样顶

表面,同时施加于垂直侧表面约 6mm 长。开始计时。点燃试样时,火焰作 用时间最长为 30s,到 30s 后,开始 180s 计时。点燃试样时每隔 5s 左右稍 移开点火器观察试样,直至垂直侧表面稳定燃烧或可见燃烧部分的前锋到

工程设计

苏州宇诺仪器设备有限公司

REV

A

仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

达上标线处,立即移去点火器,开始计时,并观察试样燃烧长度。 Ignite the ignitor ,down and move the ignitor to make the flame visible part can touch the top surface of test sampe and put on vertical side surface about 6mm.Start timing.The longest action time of flame is 30s and start to timing for 180s after 30s.Move the ignitor left and right and observe the test sample every 5s til the vertical side surface burning or visible burning part reach marking line,then move the ignitor,start to timing and observe the the burning length of the test sample. 2、试样在 180 秒内燃烧前锋到达或超过下标线时计时结束。调整氧浓 度,擦净燃烧筒和点火器表面的污物,使燃烧筒的温度回复到常温或另换 一个为常温的燃烧筒,进行下一次实验。 Timing is over when the test sample meets or exceeds the marking line within 180s.Adjust oxygen density,wipe the burning barrel and surface dirt on the ignitor to make the temperature of burning barrel return back to normal or change another burning barrel with normal temperature.

3、试验结束后关闭电源、气源并清理残留物。

Switch off the power supply ,air source and clean the residue after testing.

5 日常维护 Routine maintenance

  • 5.1 警告和注意 Warnings& Cautions

在进行任何操作前,请务必仔细阅读以下内容:Please read the

following contents carefully before any operation:

警告 Warnings

  • 5.2 重要小结 Important brief summary

工程设计

苏州宇诺仪器设备有限公司

REV

A

仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

注意 Cautions 1、仪器使用的氧气、氮气钢瓶的内部压力不低于 1MPa,如果低于这个 压力,请及时更换。 The inside pressure of oxygen cylinder and nitrogen cylinder should not be less than 1Mpa,Please make replacement on time if the pressure is lower than 1Mpa. 2、点火器需要用打火机引火。Ignite the ignitor with lighter.

3、调节流量时用力要均匀,不要忽大忽小。

Adjust the flow evenly,don’t be unstable.

4、根据使用情况经常擦拭燃烧筒和点火器表面的污物,及时清除燃烧

筒内金属网上的燃烧滴落物,保证气体畅通。 Wipe the burning barrel and surface dirt of the ignitor termly and clean the burning dripping on the metal net of burning barrel to keep the smooth air.

5、如出现问题,请和我公司联系,请勿自行拆卸,尤其是元器件。

Please contact us if any problem.Don’t discharge the instrument by yourself,expecially for the component.

6、友情提醒:氧气、氮气钢瓶属于高压容器,使用时一定要远离火源,

注意安全。Friendly reminder:Keep the oxygen cylinder and nitrogen cylinder far away from fire source and be safety,as they are high pressure vessel. 5.3 校准仪器 Calibration instrument 通常只需定期检查仪器校准,如果校准值超出允许误差范围,则需要 对仪器进行校准。 Usually,calibrate the instrument termly.Calibrate the instrument once the calibration value is beyond of permissible

工程设计

苏州宇诺仪器设备有限公司

REV

A

仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

error range. 请每年检查一次仪器标定值以确保实验结果的一致。 Please inpect the instrument calibration value every year to ensure the same value as experiment result. 6、排除故障 Troubleshooting 当您对仪器进行了误操作或仪器出现故障时,如果在处置过程中出现 任何问题或按照给出的处置办法仍无法解决问题,请及时与本公司联系: 故障 可能的原因 检查步骤 解决方法。 If any problem of the instrument or misoperation,and still can’t solve as per our listed dealing method,please contact us:breakdown,possible reasons,inspect steps,solution. 7、氧指数法影响因素与讨论 Oxygen index influence factor and discussion 实验的影响因素较多,现在主要因素进行分析 Due to too many factors,now analyse main factors only:

(1)气体流速 gas-flow rate 实验时,气体流速越大,单位时间内通过燃烧筒的氧气量越大,这将 有助于试样的燃烧,而另一方面,过大的气体流速,带走大量热量,影响燃 烧。

The faster of the gas-flow rate,the more oxygen flow in the unit time and it will be helpful for test sample burning;on the other hand,overlarge gas-flow rate will take away mass heat and influence burning. (2)氧浓度控制和纯度 Oxygen density and purity 显然,氧浓度的提高有利于试样的燃烧,反之,则不利于试样的燃烧, 反之,则不利于试样的燃烧。为此,氧浓度的控制及气体系统接头应定期

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苏州宇诺仪器设备有限公司

REV

A

仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

校验。 Obviously,the higher oxygen density will be useful for test sample burning;otherwise,it’s bad for test sample burning.Therefore,oxygen density control and gas system joint should be calibrated termly. 通常我们将试验用氧气、氮气的纯度当做 100%,但是作为工业用气, 有一定误差。纯度越低,误差越大,另外钢瓶内压力的下降对氧的浓度也 有影响。 Usually,we regard oxygen and nitrogen purity to be 100%,but there is a little errorfor industrial gas.The lower purity,the bigger error;by the way,the decline of pressure in the cylinder has influence on the oxygen density. (3)试样尺寸及制备 试样燃烧的速率与试样形状、尺寸及制备方法 有关。如试样的厚度越小,越易点燃和燃烧。又如试样材料的不均匀将导 致点火的难易和燃烧行为的不同。因此,试样尺寸应精确测量并在规定范 围内。在要求严格时,就应考虑试样的制备方法及其处理。 Test sample size&making test sample burning speed is related with test sample shape,size and making method. (4)压强控制 有些聚合物其氧指数表现对减压敏感,这可能由于通 过不断除去产物而使聚合物的降解加速。 Pressure control Some polymer oxygen index is sensitive for the decompression,it may resulted by continously removing the propduct and speed up degradation of the polymer. (5)温度 温度对氧指数有很大的影响,在室温下温度对氧指数的影 响不大。在高温下各种聚合物氧指数对温度的关系各不相同。 Temperature Temperature has big influence on the oxygen

工程设计

苏州宇诺仪器设备有限公司

REV

A

仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

index.It has little influence under room temperature but has various influence on the polymer in high temperature. (6)增塑剂和填料 氧指数的试验值总是趋近最易挥发组分的氧指数, 即增塑剂的氧指数。 Plasticizer and padding The testing value of oxygen index is always the one which most volatile component,that’s oxygen index of plasticizer.

附录 A 技术参数小结 Appendix A Technicl parameters brief summary

技术参数如下: Technicl parameters as below:

1、燃烧筒内径 inner diameter of burning barrel: 100mm 2、燃烧筒高 height of burning barrel: 450mm 3、流量计精度 flowmeter precision: 2.5 level 4、压力表精度 piezometer precison: 2.5 level 5、压力表分辨率 piezometer precision resolution ratio :

0.01MPa

6、氧浓度指示表分辨率 resolution ratio of oxygen density indicator: 0.1% 7、气源 air source:GB3863 规定的氧气、GB3864 规定的氮气两瓶气 体均要调压阀。 GB3863 require oxygen cylinder to have pressure regulating valve,GB3864 require nitrogen cylinder to have pressure regulating valve. 8、试验环境 test environment: 温度 temperature 10-35℃, 湿 度 humidity 45-75% 9、输入压力 pressure input:0.2-0.3MPa 10、工作压力 working pressure:0.05-0.15MPa

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苏州宇诺仪器设备有限公司

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仪器名称

氧指数测定仪

型号

 

Instrument Name

Digital Readout Oxygen Index Tester

Model No.

YN61037

11、试样类型 testing type: 自撑材料和非自撑材料 self-supporting material and non self-supporting material 12、电源 power supply:220V,AC,50Hz 13、电流 electricity DC 1A

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