Professional Documents
Culture Documents
REF ERENCE MANUA L FOR U.S. MILK P OWDERS 2005 RE V ISED EDI T ION
Since 1995, the U.S. Dairy Export Council has been committed to
USDECUSA USDECMiddle East
developing educational materials on U.S. dairy ingredients based on info@usdec.org amfime@cyberia.net.lb
current scientific research. This manual is an update of the first two editions USDECChina USDECSouth America
usdec@prcon.com usdec@visualbyte.com.br
of the Reference Manual for U.S. Milk Powders. We have again attempted
USDECEurope USDECSoutheast Asia
to review the most current technical and scientific information available
usdec.europe@mistral-pr.co.uk usdec@pacrimassociates.com
consultants, researchers, Dairy Management Inc. and USDEC staff have USDECMexico USDECTaiwan
usdecmex@prodigy.net.mx usdec@prcon.com
shared their knowledge and contributed their resources to this new volume.
and other interested groups. We hope this new edition will continue to be a
Vronique Lagrange
Editor
U.S. Dairy Export Council
2 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
TABLE OF CON T EN T S
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 3
ACKNOWLEDGEMENTS
The U.S. Dairy Export Council wishes to
extend its appreciation to all the individuals,
companies and associations who American Dairy Products Institute Dairy Management Inc.
contributed to the development, review
The American Dairy Products Institute Formed in 1995, Dairy Management Inc. is
and production of this manual. In addition to
(ADPI) is the U.S. trade association of the the domestic and international planning and
the many experts in the field who cannot all
processed dairy products industry. ADPI management organization that builds
be listed here the U.S. Dairy Export Council
was established in 1986 by a merger of the demand on behalf of Americas dairy farmers.
would like to recognize the contribution
American Dry Milk Institute and the Whey DMI along with international, state and
of its member companies (list available
Products Institute. In 1987 the Evaporated regional organizations manage the American
at www.usdec.org), the American Dairy
Milk Association merged with ADPI. Dairy Association, the National Dairy Council
Products Institute, the California Dairy
and the U.S. Dairy Export Council.
Research Foundation, the Dairy Products Current Institute membership includes
Technology Center at California Polytechnic manufacturers of evaporated and dry milks, Dairy Management Inc.
State University, Dairy Management Inc., cheese and whey products, firms that provide 10255 West Higgins Road, Suite 900
Design Two Ltd. and the Wisconsin Center supplies and services to processors, and Rosemont, Illinois 60018-5616, USA
for Dairy Research. many companies that utilize processed dairy Phone: + 1-847-803-2000
products. The majority of ADPIs members Fax: + 1-847-803-2077
are located in the U.S., but the Institute has www.dairyinfo.com
many international members as well. www.innovatewithdairy.com
American Dairy Products Institute
116 North York Street
Suite 200
Elmhurst, Illinois 60126, USA
Phone: + 1-630-530-8700
Fax: + 1-630-530-8707
info@adpi.org
www.adpi.org
4 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
The U.S. Dairy Export Council provides The Councils headquarters is in Arlington,
support to international buyers and end- Virginia (adjacent to Washington, D.C.).
users of dairy products by:
U.S. Dairy Export Council
Working closely with trade partners and
2101 Wilson Blvd, Suite 400,
end-users around the world to develop and
U.S. Dairy Export Council nurture business relationships. Arlington, Virginia 22201, USA
Providing information about U.S. suppliers, Phone: + 1-703-528-3049
The U.S. Dairy Export Council (USDEC) Fax: + 1-703-528-3705
is an independent membership organization their products and capabilities.
www.usdec.org
that represents the interests of U.S. milk Supporting end-users and the trade with
producers, cooperative dairy companies, conferences and technical seminars aimed In addition, USDEC has set up a number of
dairy processors, export marketing and at providing training and guidance on the international offices with representatives in
trading companies, and suppliers to the dairy use of U.S. dairy products. China, Europe, Hong Kong, Japan, Mexico,
industry. USDECs members represent the Furnishing applications and usage ideas the Middle East, South America, South
vast majority of U.S. milk production and for U.S. dairy ingredients. Korea, Southeast Asia and Taiwan. Please
include companies with the widest varieties Helping drive the sale of U.S. dairy contact USDEC for further information
of dairy products available anywhere in products by creating and supporting and contacts.
the world. in-store and foodservice promotions.
Creating point-of-sale materials The U.S. Dairy Export Council provides
A function of USDEC is to unify the U.S. dairy highlighting the benefits of purchasing access to suppliers of the largest, safest milk
industrys international market development U.S. dairy products. supply in the world. USDEC has a global staff
efforts, so that the United States can be a in place to provide potential buyers with
more responsive supplier to international The U.S. Dairy Export Council facilitates a direct communication link to U.S. dairy
markets. USDEC works with U.S. suppliers communication between international buyers products suppliers.
to help them maximize all of the benefits of dairy products and U.S. suppliers by:
the industry has to offer: size, efficiency, Acting as a central contact point for
consistency, high-quality products, product international buyers and U.S. exporters,
applications support, and state-of-the- matching prospective buyers with
art technology. potential sellers.
Compiling and maintaining comprehensive
USDECs activities fall into three broad lists of buyers and sellers, which are
categories: provide on-going service to trade available to overseas customers
partners; bring potential buyers and sellers and members.
together to facilitate trade; and educate and Circulating product inquires from
support both U.S. dairy exporters and end- international buyers to a concentrated
users of U.S. dairy ingredients. list of U.S. suppliers to generate
price quotations.
Hosting international buying delegations
to familiarize end-users with the size and
scope of the U.S. industry.
Coordinating trade missions and
participating in trade shows in overseas
markets to help U.S. suppliers better
understand the needs of these markets.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 5
GLOSSARY
Some of the terms used in this manual have
synonyms that are used in related industries
or other countries. The intent of the following
list is to reconcile the terms used in this man-
ual with other frequently used terms and
closely related words.
Use of Terms
Synonym, closely related word or Whereas the terms nonfat dry milk
Term used in this manual or abbreviations. brief definition. and skim milk powder are used
ADPI American Dairy Products Institute. interchangeably in this manual and
www.adpi.org oftentimes by the trade, the terms are
Agglomerated Instantized actually defined by two different sets of
Anhydrous milk fat (AMF) Similar to butteroil. regulations and authorities (FDA/USDA
AMF: 0.15% moisture and 99.8% fat. and Codex Alimentarius). In addition,
Butteroil: 0.3% moisture and 99.6% fat. regulations of individual governments
DMI Dairy Management Inc. may differ. Please consult local
FDA Food and Drug Administration, United regulations for all pertinent information
States. www.fda.gov when purchasing milk powders, and for
Filled Recombined milk products where all or labeling purposes.
some of the milkfat is replaced with veg-
etable oil/fat.
Mt Metric tonne (or ton)
NFDM Nonfat dry milk. Defined in the United Whereas the terms dry whole milk
States Code of Federal Regulations, and whole milk powder are used
Title 21, volume 2, part 131.125. interchangeably in this manual and
(www.fda.gov) oftentimes by the trade, the terms are
Recombined The milk product resulting from the actually defined by two different sets of
combining of milkfat and milk-solids-
regulations and authorities (FDA/USDA
nonfat in one or more of the various forms
with or without water. This combination and Codex Alimentarius). In addition,
must be made so as to re-establish the regulations of individual governments
products specified fat-to-solids-nonfat may differ. Please consult local
ratio and solids-to-water ratio. regulations for all pertinent information
FAO/WHO 1973, Codex Alimentarius.
when purchasing milk powders, and for
Reconstituted The milk product resulting from the addition labeling purposes.
of water to the dried or condensed form
of the product in the amount necessary to
re-establish the specified solids-to-water
ratio. FAO/WHO 1973, Codex Alimentarius.
SMP Skimmed milk powder. Defined in Codex
Alimentarius Standard 207-1999
USDA United States Department of Agriculture.
www.usda.gov
WMP Whole milk powder. Defined in Codex
Alimentarius Standard 207-1999
DWM Dry whole milk. Defined in the
United States Code of Federal Regulations,
Title 21, volume 2, part 131.147.
(www.fda.gov)
USDEC The U.S. Dairy Export Council, producer of
this manual.
WPNI Whey Protein Nitrogen Index
6 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
T HE U. S. DA I RY I NDUS T RY AND E X P ORT I N I T I AT I V E S 1
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 7
1 T HE U. S. DA I RY I NDUS T RY AND E X P ORT I N I T I AT I V E S
Each year, U.S. manufacturers process The United States has been able to
1.1 OVERVIEW OF THE about 20 million mt of fluid milk products, achieve its current milk output through
U.S. DAIRY INDUSTRY 3.8 million mt of cheese, 900,000 mt of whey a combination of scientific and management
and lactose, 730,000 mt of milk powders, advancements at all levels of production,
The United States is the worlds largest cows 780,000 mt of yogurt, 615,000 mt of butter processing, regulation and marketing. In the
milk producer, producing about 76 million mt and 680,000 mt of ice cream and frozen dairy past 10 years, the country has increased milk
of milk per year, or close to 20% of the worlds products in over 1,100 processing plants, production at an average of one million
milk supply. U.S. dairy farmers produce making the United States the largest dairy mt per year.
two-and-a-half times more milk than any processing country in the world.1
European country and six times as much as On the farm, management techniques,
Australia or New Zealand. Many of these dairy products are used as including expanded use of balanced feed
ingredients in the formulation of other foods. rations have been instrumental in increasing
U.S. food processors with international milk output per cow. Between 1990 and 2004,
recognition use U.S. dairy ingredients, average annual yield per cow increased
including U.S. milk powders, to successfully from 6,600 kg to about 8,600 kg, while cow
develop bakery products, confections, meats, numbers decreased from about 10.8 million
sauces, soups and other dairy foods for both in 1980 to about 9 million in 2004. This type
domestic and export sales. of production efficiency demonstrates the
industrys ability to maximize its resources to
meet the growing demand for dairy products
worldwide. These same practices have led
to improvements in the composition of
milk, which have resulted in an increase
of solids-nonfat (SNF) to meet food
manufacturers demands for more
milk protein.
Advanced U.S. technologies ensure efficient
collection and delivery of the highest quality
milk and milk products. State-of-the-art
milking and milk handling equipment,
including automated milking systems, have
improved the speed of cleaning, sanitizing,
and cooling raw milk. Efficient delivery
systems ensure timely transfer of raw milk
to the processing plants.
Dairy farmers and dairy processors alike
abide by strict U.S. sanitary standards. In
Photo courtesy: Wisconsin Milk Marketing Board addition to self-imposed sanitary guidelines,
dairy farmers are visited regularly by
government regulatory agencies, which
conduct quality assurance and safety
inspections at the farms. These inspectors
confirm herd health, oversee veterinary
practices, monitor sanitation of the facilities
and milking equipment, and verify that the
milk is being rapidly cooled and properly
stored until delivered to processing facilities.
8 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
1 T HE U. S. DA I RY I NDUS T RY AND E X P ORT I N I T I AT I V E S
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 9
1 T HE U. S. DA I RY I NDUS T RY AND E X P ORT I N I T I AT I V E S
DEIP helps U.S. dairy farmers, processors, The kind, type, grade and/or class of U.S.
1.2 DAIRY EXPORT INCENTIVE manufacturers, and exporters gain access to agriculture commodity specified as eligible
PROGRAM (DEIP) foreign markets. As a result, the program for export under the applicable invitation
allows the U.S. dairy industry to demonstrate includes:
The Dairy Export Incentive Program (DEIP), the high quality of its products to interested
was created to stimulate exports of products Nonfat Dry Milk meeting the U.S.
international buyers. Any exporter interested
by offering Commodity Credit Corporation Standards for Grades of Nonfat Dry Milk.
in participating in DEIP must undergo a
(CCC) bonuses. Announced by USDA in qualification process. The information that Dry Whole Milk meeting the U.S. Standards
May 1985, the program was reauthorized the exporter must submit as part of this for Grades of Dry Whole Milk.
by the Food, Agriculture, Conservation process includes:
and Trade Act of 1990, the Uruguay Round Documented experience of selling dairy Countries may be recommended for
Agreements Act of 1995, the Federal products for export within the preceding participation in DEIP by USDA program
Agriculture Improvement and Reform three calendar years. experts, members of the U.S. agriculture
Act of 1996, and the Farm Security and Rural An office and agent for services of legal community, foreign government officials,
Investment Act of 2002. The major objective process in the United States (names and and others.
of the U.S. DEIP program is to develop export addresses). All sales facilitated using DEIP are made
markets for U.S. dairy products where U.S. A description of business structure (how by private sector companies, not the
products are not competitive due to price and where incorporated). government. A prospective buyer must select
subsidies from other global sources. A statement describing participation, if a company from which to purchase dairy
As part of its World Trade Organization any, during the past three years in U.S. products. Prospective buyers should note
commitments resulting from the Uruguay government programs, contracts, or that a company selling under DEIP must
Round Agreement on Agriculture, the agreements. register, or qualify, to participate in DEIP and
United States has established annual export In addition to being qualified for DEIP that registration is not an endorsement by
subsidy ceilings by commodity, with respect participation, exporters are required the U.S. government.
to maximum permitted quantities and to post a performance security before
maximum budgetary expenditures. submitting a request for a bonus. For further information about the Dairy
The program enables U.S. entities to make Export Incentive Program, contact:
competitive sales in eligible countries of not Operations Division, Export Credits
less than 150 thousand metric tones of dairy Foreign Agricultural Service, United States
products annually, including 68,201 mt of Department of Agriculture
nonfat dry milk. DEIP enables exporters 14th and Independence Avenue, S.W.
of U.S. dairy products to meet prevailing Washington, D.C. 20250-1000 U.S.A.
world prices for targeted dairy products Tel: + 1-202-720-6122
and destinations. Fax: + 1-202-720-0938
10 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
THE U.S. MILK P OWDER I NDUSTRY 2
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 11
2 THE U.S. MILK P OWDER I NDUSTRY
The United States is one of the worlds most General Benefits of Milk Powders
OVERVIEW efficient producers of milk, and production
Milk is a complex biological fluid consisting
is year-round. This guarantees product
of fats, proteins, minerals, vitamins, enzymes,
The United States has the largest supply availability at any time of the year, including
lactose and water. Not only is milk a highly
the winter season. Production facilities are
of milk in the world, along with an nutritious food, it is also a functional
state-of-the-art, offering milk powders that
abundance of land and considerable ingredient. However, sometimes it is difficult
retain their flavor and freshness during
to transport, store or even formulate with
investment in research and development. normal storage. U.S. plants have the ability
milk in its fluid form. Therefore, processors
to modify their products to meet specialized
In 2004, about 640 thousand mt of employ technologies to remove the majority
needs, thereby allowing the customer to
nonfat dry milk were produced. of water from fluid milk, which results in milk
respond to new opportunities in a fast
powder. The most common milk powders are
On average, about 17-19 % of the worlds skim time frame.
skim milk powder, whole milk powder and
milk powder production is manufactured at Working in cooperation with the U.S. buttermilk powder.
more than 80 plants in the United States, Department of Agriculture (USDA),
making the United States one of the largest Milk powder contributes nutritionally,
U.S. suppliers can offer a quality product
milk powder producers in the world. These functionally and economically to a variety
at a competitive price. Through the
factors, together with strict sanitary and of foods including baked goods, confections,
assistance of the U.S. Dairy Export Incentive
quality standards, year-round production, dairy products, recombined milk, meat,
Program (DEIP) at USDA, U.S. suppliers
and a growing international focus have nutritional beverages, and prepared foods.
can offer buyers a competitively priced milk
helped the U.S. dairy industry position powder product at prevailing world prices. Milk powders are milk products with an
itself as a premium dairy ingredient supplier Blends based on milk powders, which extended shelf-life. By removing the majority
to the world. Detailed information on the offer functional or nutritional benefits, of moisture from milk, fluid milk is converted
milk powder industry, including extensive are also available. into a shelf-stable, dry powder with a shelf
statistics, is available from the American life of 12 to 18 months, as compared to fresh
Dairy Products Institute (www.adpi.org). On the average, approximately 80% of U.S.
pasteurized fluid milks short shelf-life (less
skim milk powder is used within the United
than 21 days).
States. U.S. food manufacturers, big and
small, depend on U.S. milk powder when The general benefits of milk powders include:
formulating their products. The other 20% is Storage Requires small spaces under
exported, enabling manufacturers worldwide regular storage conditions and retains
the opportunity to formulate with high- high quality.
quality and consistent U.S. milk powders. Economy Because mass and volume are
Suppliers also offer blended products with reduced, transportation costs are less.
differentiated composition and customized Balance Surplus milk powder can be
functionality that are competitively priced. reconstituted when fresh milk supplies
are low.
Whether they are used to extend local milk
Use in Emergencies Can be used under
supply, provide nutritional benefits, give
adverse conditions when fresh milk is
convenience of use, or provide functional or
unavailable.
shelf-life benefits, food manufacturers have
Formulations Suitable for use as an
made U.S. milk powders an integral part of
ingredient in a wide variety of foods
their success. They have come to trust the
and beverages.
quality of U.S. milk powders with good
Fortification Can add additional milk
reason. The United States has one of the
protein, dairy calcium and other vitamins
strictest set of food sanitary standards of any
and minerals to a variety of foods.
country in the world.
The U.S. milk powder industry is one of
the worlds most efficient producers, with
efficiencies continually being developed in
the plant.
Through advances in production, the industry
has been able to increase production output
from 472,000 mt in 1992 to about 640,000 mt
in 2004 (nonfat dry milk).
12 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
PRODUCTION AND MANUFACTURING TECHNOLOGIES 3
Photo courtesy: Dairy Management Inc.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 13
3 PRODUCTION AND MANUFACTURING TECHNOLOGIES
Whether it is used to provide mouthfeel, All milk powder processes begin with liquid Homogenization is not a mandatory step
upgrade visual appearance, enhance milk (skim milk, whole milk or buttermilk), in whole milk or buttermilk processing,
nutrition or perform one of a variety of other which is stored at the processing plant at but is usually applied in order to decrease
functional benefits, food manufactures temperatures below 7C. Raw whole milk has the free fat content. Fat globules depleted of
worldwide have made U.S. milk powders an a variable fat content and cream is separated protective membranes reduce milk powder
integral part of successful food formulations. from the milk to facilitate standardization of solubility and increase its susceptibility
They have come to trust the quality of U.S. the fat content prior to further processing. to oxidative rancidity. Homogenization
milk powders with good reason: The United Centrifugal separators are used to further transforms free fat into fat globules. During
States has some of the strictest food sanitary clarify the milk. homogenization, proteins adhere on globule
requirements. surfaces to surround and stabilize the
The milk is pasteurized (high-temperature,
fat globules.
All U.S. milk powders are made from short-time) by heating to at least 72C,
high quality milk in federally approved and holding at or above this temperature After pasteurization, other optional
manufacturing facilities. Dairy farmers and for at least 15 seconds. (An equivalent ingredients such as vitamins and minerals
dairy processors alike abide by strict U.S. temperature/time combination can be can be added to the milk. The milk then
sanitary standards. In addition to self- used). Heat treatment affects the functional undergoes a two-part moisture-removal
imposed sanitary guidelines, dairy farmers properties of skim milk powder and the process: concentration and drying.
are visited regularly by government regulatory keeping quality of whole milk powder, so the
agencies, which conduct quality assurance temperature and time combinations can vary The first part of concentration involves
and safety inspections at the farms. These widely depending on the required properties. pumping milk to a multiple effect vacuum
inspectors confirm herd health, oversee With skim milk powder, the extent of heat evaporator system where water is boiled off
veterinary practices, monitor sanitation of treatment can be related to the whey protein at relatively low temperatures in a series of
the facilities and milking equipment, and nitrogen index, which is related to the steps until the milk is concentrated to around
verify that the milk is being rapidly cooled amount of soluble whey protein. Additional 40-50% total solids. Omitting evaporation of
and properly stored until delivered to the information on the classification of skim milk the milk prior to drying is not economically
processing facilities. At processing facilities, powder according to heat treatment applied feasible because the demand for energy
each tanker of milk is tested to ensure it is can be found in the Definitions section of would be severely increased. For example,
negative for residual antibiotics prior to this manual. the energy used to remove water in multiple
its unloading; milk then moves through effect evaporators with vapor recompression
For all milk powders, heat treatments are is about 10 times lower than in spray drying.
sanitized pipes, vats and tanks as it is
generally carried out at temperatures higher Omission of evaporation would also result
converted into a variety of dairy foods
than those required for pasteurization. The in inferior quality milk powder particles
including milk powders. Virtually all U.S.
aim is to destroy all pathogenic and most that contain occluded air (which impacts
dairy processing plants employ quality
of the other microorganisms, to inactivate extended shelf-life.)
management programs, such as HACCP or
enzymes, especially lipase which could
ISO, to ensure that the finished products The second part involves drying in either a
cause lipolysis during storage, and to activate
meet the highest attainable standards. spray dryer or on a roller dryer. Additional,
the SH groups of b-lactoglobulin, thus
optional processing steps include
increasing resistance of the powder to
instantizing. After processing, cooled
oxidative changes during storage.
milk powders are sifted and sent to blending
and storage silos. Milk powders are then
sampled, packed, check weighed and
palletized as required for shipping.
14 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
3 PRODUCTION AND MANUFACTURING TECHNOLOGIES
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 15
3 PRODUCTION AND MANUFACTURING TECHNOLOGIES
Agglomeration
Cool
Cool
Sieve
Cool
Sieve
Pack
Sieve
Pack
Pack
16 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
QUA L I T Y CON TROL AND GRADI NG STANDARDS 4
Photo courtesy: Dairy Management Inc.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 17
4 QUA L I T Y CON TROL AND GRADI NG STANDARDS
Milk powder standards are the basis for 5. Personnel practices must be appropriate
4.1 GENERAL QUALITY an effective quality control program. to maximize product safety.
CONTROL AND Major benefits are: 6. All processing equipment must be kept
PLANT SURVEYS Assure Uniformity
sanitary and in excellent working condition
to assure the buyer that the milk powder is
U.S. suppliers offer a range of product Uniform quality of product is assured protected from contamination.
approvals and certifications that guarantee by grade specifications, accepted and
their customers some of the highest quality understood throughout the milk powder Inspection and Grading
powders in the world. industry. Milk powder standards enable The final product is sampled by USDA
both manufacturers and purchasers to inspectors. A computer program is used to
U.S. standards for grades of milk powders specify the grade of product offered for sale select samples randomly and these samples
come from the Dairy Division of the United or required for use. are pulled from storage in the presence of the
States Department of Agriculture. The USDA inspector. The inspector examines
standards are based on inspection and Facilitate Purchase
Buyers and sellers are afforded a common each sample to determine compliance to
grading services and ensure a nationally the grade standard or contract specification
and internationally understood language language whereby a milk powder meeting
specific product requirements is recognized and stamps packages with the official
for efficient orderly trade. The United acceptance stamp or grade mark. They also
States leads the world in the creation and by its grade name. Tests and grades are
based on industry-approved analytical issue certificates for product that complies
development of industry standards for testing with the standard or specifications. After
milk powders. These were first adopted in procedures. This eliminates unnecessary
and detailed tests that vary between inspection, dairy products are packaged
1929 and are updated on an as needed basis. under stringent, U.S. government
The American Dairy Products Institute (ADPI) manufacturing and purchasing organizations.
regulated standards.
is an industry organization that compiles the Reduce Risk
USDA standards and publishes the standards The manufacturer of the milk assumes Laboratory Service
in bulletin #916 for members. Standards can responsibility for delivering the grade of Laboratory service consists of analytical and
be ordered from the Institute (www.adpi.org). product offered. Many elements of risk are quality control tests, including all chemical
eliminated from the purchase since the buyer and bacteriological determinations essential
Industry standards for milk powder, whole
may have each purchase checked by grade for grading.
milk powder and buttermilk powder promote
analysis. Similarly, the manufacturer is
the utilization of milk powders by making Personnel
available a uniform grading system. protected against unreasonable complaints
because the grade standards are succinct and The men and women who perform these
Because the U.S. fluid milk supply, its services are experienced and well trained.
manufacturing facilities and its subsequent based upon specific methods of analysis.
Many inspectors and graders have college
storage facilities, are all in accordance Plant Surveys degrees in dairy manufacturing or food
with some of the strictest procedures and science, and have held responsible jobs in
Each plant survey is conducted by
practices in place in the world, milk powders the dairy industry.
experienced, highly trained USDA dairy
made in the United States meet strict
inspectors who make detailed checks on
grade requirements.
more than 100 items. Only plants that meet
These requirements are not designed to meet these requirements are granted approval
all end-uses. To determine the acceptability status and are eligible for grading and quality
of a milk powder in a specific formulation, control services. Some of the items on a dairy
supplemental tests not included in the inspectors list include:
standards are often necessary. Buyers who 1. The plant surroundings must be clean
use such standards in their purchasing to prevent bacterial contamination and
decisions provide themselves with an maximize product safety.
added safeguard regardless of the 2. Areas such as the raw milk grading room,
particular purpose for which the milk receiving line, manufacturing area and
powder is intended. warehouse supply room must have
adequate lighting.
3. Facilities must be of sound construction.
4. Incoming milk must be regularly analyzed
to ensure high quality and product safety.
18 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
4 QUA L I T Y CON TROL AND GRADI NG STANDARDS
Section 131.125: Nonfat dry milk Section 131.147: Dry whole milk
4.2 FOOD AND DRUG Source: FDA. CFR, Title 21, Volume 2, Section Source: FDA. CFR, Title 21, Volume 2, Section
ADMINISTRATION 131.125. Revised April 1, 2003. 131.147. Revised April 1, 2003.
STANDARDS OF IDENTITY (a) Description. Nonfat dry milk is the (a) Description. Dry whole milk is the product
The Food and Drug Administration, part of product obtained by removal of water obtained by removal of water only from
the United States Department of Health and only from pasteurized skim milk. It pasteurized milk, as defined in 131.110
Human Services, has issued standards of contains not more than 5 percent by (a), which may have been homogenized.
identify for three types of dried milk products. weight of moisture, and not more Alternatively, dry whole milk may be
These standards are part of the United than 1.5 percent by weight of milkfat obtained by blending fluid, condensed, or
States Code of Federal Regulations, Title 21, unless otherwise indicated. dried nonfat milk with liquid or dried
Volume 2. They can be downloaded by the (b) Optional ingredients. Safe and suitable cream or with fluid, condensed, or dried
FDAs website (www.fda.gov). characterizing flavoring ingredients milk, as appropriate, provided the result-
(with or without coloring and nutritive ing dry whole milk is equivalent in com-
carbohydrate sweetener) as follows: Fruit position to that obtained by the method
and fruit juice, including concentrated described in the first sentence of this
fruit and fruit juice, natural and artificial paragraph. It contains the lactose, milk
food flavorings. proteins, milkfat, and milk minerals in the
(c) Methods of analysis. The following same relative proportions as the milk
referenced methods of analysis are from from which it was made. It contains
Official Methods of Analysis, 13th edition not less than 26 percent but less than
(1980). Copies may be obtained from 40 percent by weight of milkfat on an as is
the Association of Official Analytical basis. It contains not more than 5 percent
Chemists International, 481 North by weight of moisture on a milk solids non
Frederick Ave., Suite 500. Gaithersburg, fat basis.
MD 20877-2504. (b) Vitamin addition. Addition of vitamin A
Milk fat content: Fat in dried milk is optional. If added, vitamin A shall be
Official Final Action, sections 16.199.200 present in such quantity that, when
Moisture content: Moisture Official prepared according to label directions,
final action, section 16.192. each quart of the reconstituted
(d) Nomenclature. The name of the food is product shall contain not less than
Nonfat dry milk. If the fat content is over 2,000 International Units thereof. Addition
1.5 percent by weight, the name of the of vitamin D is optional. If added, vitamin
food in the principal display panel or D shall be present in such quantity
panels shall be accompanied by the that, when prepared according to label
Statement Contains % milkfat, the directions, each quart of the reconstituted
blank to be filled with the percentage product shall contain 400 International
to the nearest one tenth of 1 percent Units thereof. The requirements of this
fat contained, within limits of good paragraph will be met if reasonable
manufacturing practice. The name of overages, within limits of good
the food shall include a declaration manufacturing practice, are present
in the presence of any characterizing to ensure that the required levels of
flavoring, as specified in Section 101.22 vitamins are maintained throughout
of this chapter. the expected shelf life of the food under
Note: Section 131.127: Nonfat dry milk fortified with customary conditions of distribution.
Vitamins A and D presents the standard for such a
product that is to contain 200 IU of vitamin A and 400 (c) Optional ingredients. The following safe
IU of Vitamin D. and suitable optional ingredients may
be used: carriers for vitamins A and D,
emulsifiers, stabilizers, anticaking agents,
antioxidants, characterizing flavoring
ingredients (with or without coloring and
nutritive carbohydrate sweetener) as
follows: fruit and fruit juice, including
concentrated fruit and fruit juice and
natural and artificial food flavoring.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 19
4 QUA L I T Y CON TROL AND GRADI NG STANDARDS
(d) Methods of analysis. The following 4. The flavor and odor of the milk powder in
referenced methods of analysis are 4.3 UNITED STATES dry form or after reconstitution must be
from Official Methods of Analysis of DEPARTMENT OF sweet, clean and free from rancid, tallowy,
the Association of Official Analytical AGRICULTURE GRADING fishy, cheesy, soapy or other objectionable
Chemists, 13th Ed. (1980), which is flavors or odors.
incorporated by reference. Copies may U.S. suppliers voluntarily participate in the 5. The milk powder must be packed in
be obtained from the Association of U.S. standards for milk powders grading substantial containers, suitable to protect
Official Analytical Chemists International, system. The standards are issued by the and preserve the contents without
481 North Frederick Ave., Suite 500, United States Department of Agriculture. significant impairment of quality with
Gaithersburg, MD 20877-2504, or may The standards for grades themselves respect to sanitation, contamination and
be examined at the National Archives are summarized in this manual, and the moisture content under various customary
and Records Administration (NARA). documents can be downloaded from the conditions of handling, transportation
For information on the availability of this USDA website (www.usda.gov). and storage.
material at NARA, call 202-741-6030, 6. The presumptive coliform estimate of the
or go to: http://www.archives.gov/federal_ milk powder must not exceed 10 per gram
register/code_of_federal_regulations/ibr_ of milk powder.
locations.html. Milkfat content Fat 7. The milk powder must be free from
in Dried Milk-Official Final Action, extraneous matter as described in Section
sections 16.199-16.200. Moisture content 402(a) of the Federal Food, Drug and
Moisture-Official Final Action, section Cosmetic Act.
16.192. Vitamin D content Vitamin D- Source: American Dairy Products Institute, Bulletin
#916. www.adpi.org
Official Final Action, sections 43.195-
43.208. There are differences in composition,
(e) Nomenclature. The name of the food is appearance, flavor and bacteriological
Dry whole milk. The name of the food standards between products that are
shall appear on the principal display panel General Grading Requirements Extra Grade vs. Standard Grade. The
of the label in type of uniform size, style, 1. All nonfat dry milk, dry whole milk and dry following table on page 21 summarizes
and color. The name of the food shall be buttermilk for human consumption must the grading criteria.
accompanied by a declaration indicating conform in all respects to Federal and
the presence of any characterizing Heat Treatment Classification
State government regulations in force at
flavoring as specified in 101.22 of this the present time or that may subsequently The heat treatment classification is not a
chapter. The following phrases in type be issued from time to time. U.S. grade requirement, except for high-heat
size not less than one-half the height of 2. The milk powder must be made from fresh, milk powder for which a higher solubility
the type size used in such name shall sweet milk to which no preservatives, index is permitted. Product submitted for
accompany the name of the food alkali, neutralizing agent or other chemical grading may be analyzed for heat treatment
wherever it appears on the principal has been added and which has been classification upon request and the results
display panel or panels. The phrase pasteurized in the liquid state, before shown on the grading certificate. Heat
Contains _% milkfat, the blank to be concentration, at a temperature of 72C treatment classification will be made
filled in with the whole number closest for 15 seconds, or its equivalent in available only upon a product graded
to the actual fat content of the food. bacterial destruction. by USDA. See section on definitions for
If vitamins are added, the phrase 3. The milk powder must be reasonably additional information.
vitamin A, or vitamin A added, or uniform in composition. The color shall be
vitamin D, or vitamin D added, or white or cream and free from a brown or
vitamins A and D, or vitamins A yellow color typical of overheated product
and D added, as appropriate. The word and free from unnatural color. It must be
vitamin may be abbreviated vit. substantially free from brown specks.
(f) Label declaration. Each of the ingredients
used in the food shall be declared on
the label as required by the applicable
sections of parts 101 and 130 of
this chapter.
20 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
4 QUA L I T Y CON TROL AND GRADI NG STANDARDS
Specific Grading Requirements for Specifications for U.S. Grades of Nonfat Dry Milk, Spray Process*
Nonfat Dry Milk Characteristic U.S. Extra Grade U.S. Standard Grade
Nonfat dry milk is the product obtained by Flavor Sweet, pleasing desirable flavor Fairly pleasing flavor
the removal of only water from pasteurized Physical appearance Uniform white to light cream White or light cream
skim milk. It conforms to the application May possess slight
provisions of the Code of Federal Regulations unnatural color
(see previous section) issued by the Bacterial estimate <10,000 cfu/g <75,000 cfu/g
Food and Drug Administration. Basic Milk fat <1.25% <1.50%
compositional criteria are presented in Moisture <4.0% <5%
the following table: Scorched particles <15 mg <22.5 mg
Solubility index <1.2 ml <2.0 ml
Spray Dried Roller Dried <2 ml (high heat) <2.5 ml (high heat)
Milkfat <1.5% <1.5% Titratable acidity <0.15% (lactic acid) <0.17% (lactic acid)
Moisture <5.0% <5.0% Flavor Characteristics
Bitter Not permitted Slight
Chalky Slight Definite
Extra Grade Cooked Slight Definite
Extra Grade indicates the highest quality Feed Slight Definite
U.S. nonfat dry milk. It shall be free from Flat Slight Definite
lumps, except those that break up readily Oxidized Not permitted Slight
under slight pressure. Scorched Not permitted Slight
Standard Grade Storage Not permitted Slight
Standard Grade includes all nonfat dry milk Utensil Not permitted Slight
that fails in one or more of the particulars Physical Appearance
to meet the requirements of Extra Grade. Dry product:
It may contain small to moderate lumps, Lumpy Slight Moderate
slight color and reasonably free of visible Unnatural color Not permitted Slight
dark particles. Visible dark particles Practically free Reasonably free
There is no standard grade for instant nonfat *Summary, please refer to USDA Standard for Grade document for additional information.
**If lactose is used as a processing aid, the amount must only be that necessary to produce the desired effect,
dry milk. and it must not exceed 2.0% of the weight of skim milk powder.
Optional Tests
Copper content 1.5 ppm
Iron content 10 ppm
Vitamin A 2,000 IU per
(when fortified) reconstituted quart
Vitamin D 400 IU per
(when fortified) reconstituted quart
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 21
4 QUA L I T Y CON TROL AND GRADI NG STANDARDS
Specific Grading Requirements for Specifications for U.S. Grades of Dry Whole Milk*
Dry Whole Milk Characteristic U.S. Extra Grade U.S. Standard Grade
Dry whole milk, made by the spray or roller Flavor Sweet, pleasing desirable flavor Sweet and pleasing
process is the product obtained by removal Physical appearance Uniform white to light cream White or light cream
of water only from pasteurized milk which May possess slight
may have been homogenized. It contains not unnatural color
more than 5% by weight of moisture on a milk Bacterial estimate <10,000 cfu/g <50,000 cfu/g
solids not fat basis, and not less than 26% Coliform count <10 /g <10 /g
but less than 40% by weight of milk fat. It Milk fat >26%, <40% >26%, <40%
conforms to the applicable provisions of the Moisture <4.5% (weight on <5% (weight on a
Code of Federal Regulations (see previous MSNF basis) MSNF basis)
section). Alternatively, dry whole milk may Scorched particles <15 mg (spray process) <22.5 mg (spray process)
be obtained by blending fluid, condensed or <22.5 mg (roller dried) <32.5 mg (roller dried)
dried nonfat milk with liquid or dried cream Solubility index <1.0 ml (spray process) <1.5 ml (spray process)
or with fluid, condensed or dry milk. <15 ml (roller dried) <15 ml (roller dried)
Titratable acidity <0.15% (lactic acid) <0.17% (lactic acid)
It contains the lactose, milk proteins, Flavor Characteristics
milkfat, and milk minerals in the same Cooked Definite Definite
relative proportions as the milk from which
Feed Slight Definite
it was made.
Bitter None Slight
When either or both vitamin A or D is added, Oxidized None Slight
they shall be present in such quantity that, Scorched None Slight
when prepared according to label directions, Stale None Slight
each quart (0.9 l) of the reconstituted Storage None Slight
products shall contain not less than 2,000 IU Physical Appearance
of vitamin A and 400 IU of vitamin D.
Dry product:
Lumps Slight pressure Moderate pressure
Unnatural color None Slight
Visible dark particles Practically free Reasonably free
Reconstituted product:
Grainy Free Reasonably free
*Summary, please refer to USDA Standard for Grade document for additional information.
22 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
4 QUA L I T Y CON TROL AND GRADI NG STANDARDS
Extra Grade Specifications for U.S. Dry Whole Milk Extra Grade
Extra Grade indicates the highest quality Spray Dried Roller Dried
U.S. dry whole milk. It shall be free from Milkfat 26.040.0% 26.040.0%
lumps, except those that break up readily Moisture 4.5% 4.5%
under slight pressure. Titratable acidity 0.15% 0.15%
Solubility index (max) 1.0 ml max 15.0 ml max
Bacterial estimate 10,000 cfu/g 50,000 cfu/g
Scorched particles Disc B (15.0 mg) Disc C (22.5 mg)
Standard Grade Specifications for U.S. Dry Whole Milk Standard Grade
Standard Grade includes all milk powder Spray Dried Roller Dried
that fails in one or more of the particulars to Milkfat 26.040.0% 26.040.0%
meet the requirements of Extra Grade. Moisture 5.0% 5.0%
Titratable acidity 0.17% max 0.17% max
Solubility index (max) 1.5 ml max 1.5 ml max
Bacterial estimate 50,000 cfu/g 50,000 cfu/g
Scorched particles Disc C (22.5 mg) Disc D (32.5 mg)
Optional Tests
Copper content 1.5 ppm
Iron content 10 ppm
Vitamin A 2,000 IU (min)
(when fortified) per reconstituted
quart (0.9 liter)
Vitamin D 400 IU (min) per
(when fortified) reconstituted quart
(0.9 liter)
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 23
4 QUA L I T Y CON TROL AND GRADI NG STANDARDS
Specific Grading Requirements for Specifications for U.S. Grades of Dry Buttermilk and Buttermilk Product*
Dry Buttermilk Characteristic U.S. Extra Grade U.S. Standard Grade
The United States Department of Agriculture Flavor Sweet and pleasing Fairly pleasing
defines dry buttermilk, and grades for it in Physical appearance Cream to light brown Cream to light brown
its Standard for Grades of Dry Buttermilk Bacterial estimate <20,000 cfu/g <75,000 cfu/g
and Dry Buttermilk Product. It defines dry Milk fat >4.5% <4.5%
buttermilk, made by the spray process or the Moisture <4.0% <5%
atmospheric roller process, as the product Scorched particles <15 mg (spray process) <22.5 mg (spray process)
resulting from drying liquid buttermilk that <22.5 mg (roller dried) <32.5 mg (roller dried)
was derived from the churning of butter Solubility index <1.25 ml (spray process) <2 ml (spray process)
and pasteurized prior to condensing at a <15 ml (roller dried) <15 ml (roller dried)
temperature of 71.6C (161F) for 15 seconds, Titratable acidity >0.10%, <0.18% >0.10%, <0.20%
or its equivalent in bacterial destruction. Dry Protein Content
buttermilk should have a protein content of Dry Buttermilk >30% >30%
not less than 30%. Dry buttermilk cannot be
Dry Buttermilk Product <30% <30%
derived from nonfat dry milk, dry whey, or
Flavor Characteristics
products other than buttermilk, and it cannot
contain any added preservatives, neutralizing Unnatural None Slight
agents or other chemicals. Offensive None None
Physical Appearance
Dry buttermilk product is the product Lumps
resulting from drying liquid buttermilk that Visible dark particles Slight Moderate
was derived from the churning of butter and
was pasteurized prior to condensing at a *Summary, please refer to USDA Standard for Grade document for additional information.
24 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
MAJOR CHARAC T ERIST IC S OF MILK P OWDERS
AND TEST METHODS 5
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 25
5 MAJOR CHARAC T ERIST IC S OF MILK P OWDERS
AND TEST METHODS
26 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
5 MAJOR CHARAC T ERIST IC S OF MILK P OWDERS
AND TEST METHODS
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 27
5 MAJOR CHARAC T ERIST IC S OF MILK P OWDERS
AND TEST METHODS
28 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
5 MAJOR CHARAC T ERIST IC S OF MILK P OWDERS
AND TEST METHODS
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 29
5 MAJOR CHARAC T ERIST IC S OF MILK P OWDERS
AND TEST METHODS
30 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
DEF I N I T IONS , COM P O S I T ION AND A P P L I C AT IONS 6
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 31
6 DEF I N I T IONS , COM P O S I T ION AND A P P L I C AT IONS
32 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
6 DEF I N I T IONS , COM P O S I T ION AND A P P L I C AT IONS
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 33
6 DEF I N I T IONS , COM P O S I T ION AND A P P L I C AT IONS
Recommended Uses
as a Function of Heat Treatment
34 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
6 DEF I N I T IONS , COM P O S I T ION AND A P P L I C AT IONS
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 35
6 DEF I N I T IONS , COM P O S I T ION AND A P P L I C AT IONS
36 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
6 DEF I N I T IONS , COM P O S I T ION AND A P P L I C AT IONS
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 37
6 DEF I N I T IONS , COM P O S I T ION AND A P P L I C AT IONS
38 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
NU TRI T IONA L PROPERT IES OF MILK P OWDERS 7
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 39
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
Milk is a highly nutritious food composed Comparative Typical Composition of Dry Milks*
of essential amino acids, calcium, and Nonfat Dry Dry
Dry Milk Whole Milk Buttermilk
a variety of vitamins and minerals. Protein (%) 36.00 26.50 34.00
Nutrient loss during heat processing Lactose (%) 51.00 38.00 48.00
and spray drying are typically minimal; Fat (%) 0.70 26.75 5.00
however, nutrient levels do vary by milk Moisture (%) 3.00 2.25 3.00
Total Minerals (%*) 8.20 6.00 7.90
source and season. The adjacent chart
Calcium (%) 1.31 0.97 1.30
shows average nutrient values for Phosphorus (%) 1.02 0.75 1.00
skim milk powder, whole milk Vitamin A (I.U./100 g) 36.40 1,091.30 507.10
powder and buttermilk powder. Thiamin/Vitamin B1 (mg/100 g) 0.35 0.26 0.26
Ribofalvin/Vitamin B2 (mg/100 g) 2.03 1.48 3.09
See previous specification pages for
Niacin/Vitamin B3 (mg/100 g) 0.93 0.68 0.99
composition ranges. Niacin Equivalents (mg/100 g) 9.30 6.75 8.95
Pantothenic Acid (mg/100 g) 3.31 2.87 3.09
Pyridoxine/Vitamin B6 (mg/100 g) 0.44 0.33 0.44
Biotin (mg/100 g) 0.04 0.04 0.04
Ascorbic Acid/Vitamin C (mg/100 g) 2.00 2.20 5.00
Choline (mg/100 g) 111.20 88.18 110.20
Energy (calories/100 g) 359.40 498.20 379.80
Source: American Dairy Products Institute.
*Please consult your supplier for detailed information to be used for nutritional
labeling purposes. Compositional ranges should be used for specification
purposes as the product composition may vary.
40 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 41
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
Biological Value
Biological Value (BV) is a measurement
of protein quality expressing the rate of
efficiency with which protein is used for
growth. Egg protein is often the standard by
which all other proteins are judged. Based on
the essential amino acids it provides, egg
protein is second only to mother's milk for
human nutrition.
The Biological Value (BV) is a scale of
measurement used to determine what
percentage of a given nutrient source is
utilized by the body. The scale is most
frequently applied to protein sources,
particularly whey protein. Biological Value
is derived from providing a measure intake of
protein, then determining the nitrogen uptake
versus nitrogen excretion. The theoretical
highest BV of any food source is 100%.
In shortBV refers to how well and how
Note: The tables in this text are presented to help
compare dairy proteins with other proteins. Detailed quickly your body can actually use the
information on protein needs and quality evaluation protein you consume.
methods is available from the Food and Agriculture
Organization (www.fao.org) and the United Nations
University (www.unu.edu/unupress/).
42 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
Protein Efficiency Ratio the protein score. Conversely the processing Health Benefits of Milk Proteins
may negatively affect the availability of An Overview
A protein of high quality is one that supplies
lysine as a result of Maillard reactions
all essential amino acids in quantities Individual milk proteins have been shown
(Fomon 1993).
adequate to meet the individuals need to exhibit a wide range of beneficial
for growth. Net Protein Utilization functions including enhancing calcium
Net Protein Utilization (NPU) is another absorption and immune function. The
Federal regulations have stipulated that the
biological measure of protein quality that is antimicrobial mechanisms of whey
protein efficiency ratio (PER) using a rat
often used, which includes an evaluation of proteins such as immunoglobulins,
growth assay, utilizing casein as a reference
protein digestibility as well as the content lactoferrin, lactoperoxidase, lysozyme
protein (AOAC 1975), be used as a means of
of essential amino acids. and glycomacropeptide are now
evaluating protein quality (Food and Drug
well documented (see table on page 44).
Administration, 1986). A number of other Protein Digestibility Corrected Immunoglobulins from milk and whey
countries have similar regulations. The
Amino Acid Score (PDCAAS) have a prophylactic and therapeutic effect
standard protein casein has a PER of 2.7
Although PDCAAS scoring is considered (clinically established in human adults)
(FAO, USDA, National Dairy Council).
an appropriate test of protein quality, it too against specific micro-organisms causing
Any protein with a PER greater than 2.7 is
has its limitations (Darragh, 1999). There is diarrhea, gastritis and dysenteria. In addition
regarded as an excellent quality protein
(see table on page 42 for a comparison of considerable debate regarding the adequacy to containing minerals that enhance bone
PER values). of the reference proteins, the truncation of growth, whey protein was recently reported
the PDCAAS, the accuracy of scoring amino to contain an active fraction that stimulated
The PER method has been criticized for acid availability and the impact of the the proliferation and differentiation of
its lack of precision, reproducibility and anti-nutritional factors (e.g. heat treatment) cultured osteoblasts (bone-forming cells)
appropriateness for measuring protein on the PDCAAS score. (reviewed by Miller 2000).
quality (McLaughlan et al, 1980, Bender,
Calculating PDCAAS requires an approximate Mature cow's milk contains an average 32g
1982, Sarwar et al 1989). In 1993, the
nitrogen composition, the essential amino of protein per liter, mostly casein (26g/l) and
FDA replaced the PER with the Protein
acid profile and the true digestibility score. whey (6g/l) (Whitney et al. 1976; Jenness,
Digestibility-Corrected Amino Acid Scoring,
Whey proteins have a higher score than 1979; Davies, Law, 1980; Stewart et al., 1987;
or PDCAAS, method (Hopkins, 1982, Fomon,
virtually all other protein sources. Leonil et al., 2001). The caseins have been
1993). It combines a measure of protein
divided into four subclasses, a-s1 casein,
digestibility with an amino acid score based
PDCAAs of Key Protein Sources a-s2 casein, b-casein, k-casein as1. Bovine
on a comparison with a natural or hypothetic
reference protein (Young and Pellett, 1991). If Ingredient PDCAAS
whey protein is constituted by numerous
the PDCAAS score if greater than or equal to soluble proteins including b-lactoglobulin
Milk* 1.23
(3g/l), a-lactalbumin (1g/l), Bovine serum
1.00, the protein is a good source of essential Whey protein* 1.15
albumin (0.4g/l), lactoferrin (0.1g/l)
amino acids. Egg white 1.00 immunoglobulins (<2g/l), lysozyme (0.1 g/l)
Several amino acid scoring systems Soybean protein .94 and other quantitatively minor fractions (i.e.
have been developed to compare the Whole wheat-pea flour (**) .82 lactoperoxidase, lipase, other enzymes and
concentration of a limiting essential Chick peas (garbanzos) .69 proteose peptone fractions).
amino acid in a protein of interest, to the Kidney beans .68
The nutritional quality of a protein can be
concentration of those amino acids in a Peas .67
expressed in various ways. Protein Efficiency
reference protein (Fomon 1993). There are Sausage, pork .63
Ratio (PER), Protein Digestibility (PD),
differences in protein digestibility based Pinto beans .61 Biological Value (BV), Net Protein Utilization
on the proteins configuration, amino acid Rolled oats .57 (NPU) and Protein Digestibility Corrected
bonding, presence of interfering components Black beans .53 Amino Acid Score (PDCAAS) are frequently
of the diet (e.g. fiber, tannins, phytate),
Lentils .52 used to indicate the potency of a food protein
presence of antiphysiologic factors or adverse
Peanut meal .52 as a source of amino acids. By all measures,
effects of processing (Fomon 1993). It should
Whole wheat .40 whey proteins offer excellent protein quality.
be noted that protein quality may be changed
without modifying a specific amino acid. Wheat protein (gluten) .25
This may occur as a result of processing for Source: FAO, except for * European Dairy
example. In processing soy protein, moist Association/ U.S. National Dairy Council (from INRA,
France. Unpublished data).
heat inactivates the trypsin inhibitors that **An example of mutual supplementation. Combining
otherwise interfere with digestion, thus whole wheat and pea flours yields a protein with a
higher PDCAAS than that of either product alone.
protein quality is improved without changing
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 43
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
Physiological Effects of Various Protein Fractions Found in Whey Protein Milk Proteins and Infant Nutrition
Protein Fraction Biological Role or Function While breastfeeding and human milk is the
b-lactoglobulin b-lactoglobulin comprises about 50% of whey protein content. preferred source of nutrition for infants, there
Although the specific biological role of b-lactoglobulin is not exist instances when the use of infant formula
known, b-lactoglobulin binds to minerals (e.g., zinc, calcium, etc), is needed. Milk powders are not an adequate
fat soluble vitamins (e.g., Vitamin A & E), and lipids and is therefore source of nutrition for infants, and simple
important for a number of physiological processes [Horton, 1995,
Nakajima et al., 1997]. Contains a high concentration of BCAA. milk powder-based formula is not to be
a-lactalbumin a-lactalbumin comprises about 25% of whey protein and has
fed to infants. Formula specifically designed
been reported to have anticancer [Svensson, 1999], antimicrobial to meet the nutritional needs of infants,
effects [Horton, 1995, Pellegrini, 2003], and immuno-enhancing with medical supervision and prepared in
properties [Horton, 1995, Montagne et al. 1999]. Research hygienic conditions are the only adequate
has also suggested that a-lactalbumin increased serotonin source of nutrition when breastfeeding is
production in the brain, improved mood, and decreased cortisol
levels [Markus, 2000].
not possible and human milk not available
as an alternative.
Peptides Whey derived peptides are believed to reduce cholesterol [Poullain
et al., 1989], blood pressure [Korhonen, 2003, Shah, 2000, Protein sources in the diets of normal
Abubakur et al., 1998], and protect against some forms of cancer
[Tsai, 2000, Bounous, 2000].
children are human milk, cow milk and soy
protein. Infant formula manufacturers are
Albumin About 5% of whey protein consists of bovine serum albumin
(BSA). BSA is believed to have antioxidant [Tong et al., 2000] and increasingly adding whey proteins to cow
antimutagenic properties [Bosselaers et al., 1994]. Binds free fatty milk based formulas to match the high
acids avidly; chelates pro-oxidant transition metals. concentration of whey proteins as found
Immunoglobulins Immunoglobulins (e.g., IgA, IgM, IgE, and IgG) support passive in human milk (see table page 45), and to
immune function. Although most of this research has been formulas for infants with special needs
conducted on infants, research is now examining whether older including fussiness, colic and protein
adults may also benefit from increasing dietary intake of bovine
immunoglobulins.
hypersensitivity (Halken 1993; Odelram,
1996, Ragno, 1993). In a double blinded
Lactoferrin Lactoferrin is a protein that binds to iron and therefore has a
number of potential applications [Layman, 2003]. Additionally, clinical study, it was shown that an
lactoferrin is believed to have anticancer [Tsuda, 2000, Tsuda, extensively hydrolyzed whey protein
2002], antimicrobial [Clare et al., 2003, Valenti et al., 1999, formula is effective in reducing the duration
Cavestro et. al., 2002, Caccavo et al., 2002], antiviral [Florisa of crying (Lucassen, 2000). Traditionally,
et al., 2003], antibacterial [Clare et al., 2003, Cavestro et al., 2002, formulas made with extensively hydrolyzed
Caccavo et al., 2002], and antioxidant properties [Wong et. al.,
1997]. Anti-inflammatory and immune modulation. casein were used to manage infants and
Lactoperoxidase Lactoperoxidase is an enzyme that breaks down hydrogen
children with severe cow milk allergies. In
peroxide and has antibacterial properties. Lactoperoxidase has the 1990s, hydrolyzed whey protein formulas
been used as a preservative and in toothpaste to fight cavities. were found to be highly effective in managing
Lactoperoxidase has also been reported to have antioxidant and infants with cow milk allergies and there
immuno-enhancing properties [Wong et al., 1997]. was a significant cost, taste and odor
advantage of these formulations over their
casein counterparts.
Cow's milk protein (CMP) constitutes an and subsequent metabolism of the absorbed
important part of the protein in diets for amino acids. Caseins are well known for their
young and adult humans, and such proteins good nutritive value and excellent functional
are considered to have a high nutritional properties for food formulation (Friedman,
quality. The nutritional value of dietary 1996). The interest in whey proteins is newer
proteins is usually related to their ability than for caseins, but whey proteins are used
to achieve nitrogen (N) and amino acid increasingly for nutritional purposes because
requirements for tissue growth and they consistently score high in traditional
maintenance (Bos et al., 2000, Tom, 2002, tests of protein quality and are of particular
Tom et al., 2002). This ability depends both interest as a high quality source of rapidly
on the protein content in essential amino available essential amino acids (Bouthegourd
acids and on the digestibility of the protein et al., 2002, Ha, Lien, 2003).
44 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
Protein Composition of Human Milk and Cow Milk 1988, Saarinen et al 1999). However, the
incidence of CMPA rises to 20% in infants
Human Milk (g/dL) Cow Milk (g/dL)
with elevated risk for allergy (Host 1995,
Total proteins 0.89 3.30
1990). Even children with atopic dermatitis
Caseins 0.25 2.60 outgrow their food allergies (Sampson, 1985,
Whey proteins 0.70 0.67 Isolauri et al., 1992, Isolauri & Turjanmaa,
a-Lactalbumin 0.26 (37) 0.19 (18) 1996). Infants with CMPA exhibit various
b-lactoglobulin 0.30 (45) symptoms ranging from loose stools, chronic
Serum albumin 0.05 (7) 0.03 (4) diarrhea or dermatitis seen in 50-60% of
Lactoferrin 0.17 (24) trace cases to respiratory symptoms (wheezing,
Other 0.07 (10) 0.15 (23) sneezing) noted in about 30% of cases
Immunoglobulins 0.105 (15) 0.066 (10) (reviewed by Tome, 2003). Cow milk allergy
Lysozyme 0.05 (7) trace in adults is rare but persists longer. Only 28%
of cow milk allergic adults were symptom-free
Total non-protein nitrogen 0.50 0.28
when milk was reintroduced to their diet after
Data from Hambaeus L: Human milk composition, Nutr Abstr Rev, rev Clin Nutr 54:219-236, 1984. 4 years.
*Values in parentheses are percentages of whey proteins.
Any number of the 20 to 30 protein fractions
Human milk is widely considered the ideal Manufacturers have focused on the amino in cow milk may elicit an allergic reaction in
feeding for newborn infants (AAPCN, 1980). acid requirements of infants primarily humans (Docena et al., 1996, Wal, 1998). The
Since cow milk based formulas are relied because their requirements are higher main allergens in cow milk protein (CMP) are
upon to provide optimal nutritional support during infancy than any other stage in life as believed to be found in the casein fraction
to infants whose mothers have chosen not to reflected in their rapid rate of growth and and in the whey proteins: alpha lactalbumin
breast-feed, infant formula manufacturers development. Amino acids have functions and beta lactoglobulin. Investigators
goal is to minimize the compositional beyond serving as a substrate for protein examining the IgE responses to allergens
differences between human milk and synthesis or as an energy source. They in humans have reported that patients are
cow milk. are also involved in the synthesis of more reactive to caseins than whey proteins.
hormones, host defenses, bile acids and Furthermore, patients diagnosed with
One of the primary compositional differences neurotransmitters. Plasma amino acids persistent CMPA (few years) were reacting
between human milk and cow milk based even affect behavior. Increasing the plasma against caseins (Sicherer and Sampson,
formula is the relative differences in tryptophan concentration by supplementing 1999). A plausible explanation for this is that
concentration of whey proteins (see table infants with increased tryptophan in their patients with persistent versus transient
above). An approach to reducing these feeding will elevate the conversion of CMPA have differential IgE binding
differences in whey proteins has been for tryptophan to serotonin and melatonin (B cell) epitopes (Chatchatee et al., 2001).
manufacturers to increase the concentration in the brain, leading to changes in sleep Characterization of allergenic epitopes in
of a-lactalbumin and lactoferrin in cows milk behavior (Steinberg 1992). Plasma tryptophan patients with CMPA currently underway in
using fractionation technology (Heine, 1996). is just one example of the importance of several laboratories (Nakajima-Adachi et al.,
However, this approach is too costly and not amino acid balance in infants. 1998; Elsayed et al., 2001, Piastra et al., 1994,
feasible for most infant formula markets. Inoue et al., 2001) may result in highly specific
Another approach is to match the plasma Cows Milk Protein Allergy (CMPA) therapies to treat food allergies.
amino acid profile of breastfed infants A food allergy is an adverse reaction to a
as closely as possible. A mathematical food mediated by a dietary antigen. The Milk and cow milk products are of particular
model was developed to yield a value that prevalence of food allergies changes with importance to infants. Infants allergic to
summarizes the closeness of the feeding to age (Madsen, 1997, Crespo, Rogdriguez, 2003, CMP temporarily use substitute formulations
the plasma essential amino acid profile of Tome, 2003) and is highly variable depending such as soy protein formulas or extensively
the breastfed infant (Paule, 1996). A formula on geography. Allergy to cows milk, eggs and hydrolyzed CMP formulations (containing
with a whey to casein ratio of 48:52 yielded fish begin primarily before age 2 while allergy almost no residual antigens). Later, oral
a plasma amino acid profile closer to that of to fruit, legumes or vegetables occurs mainly tolerance to CMP is affected by the infants
human milk than either formula with 60:40 after the 2nd year of life (Crespo et al., 1995). early exposure to some residual cow milk
or a formula with 100% whey protein. The incidence of cow milk protein allergy is antigen. In fact, introducing a partially
approximately 23 % in infants and by age hydrolyzed protein, with relatively high
3 many have outgrown their allergy to cow residual antigenicities, to the infants diet has
milk protein (reviewed by Tome, 2003, Host been shown to not induce an allergic reaction
and Halken, 1990, Hattevig et al., 1993). (sensitization) but to result in oral tolerance
The incidence of CMPA in infants who are (Pahud et al., 1988, Fritsche et al., 1997,
breast-fed ranges from 0.51.5% (Host et al., Fritsche, 1998). Also, the low allergen load in
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 45
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
human milk has been demonstrated to be Key Components of Milk Proteins: Cysteine is the rate-limiting amino acid in
a prerequisite to inducing oral tolerance to Branched Chain Amino Acids glutathione formation (Droege and Holm,
proteins in children at risk for allergies (Host, 1997). Cysteine is also needed to preserve
1994, Kilburn et al., 1998). Factors inducing Whey proteins ability to stimulate muscle muscle mass by regulating protein
oral tolerance are yet unclear. Further protein synthesis is due to its amino acid metabolism (Hack et al., 1997). During
investigation into the mechanism of cow profile being in ratios similar to skeletal periods of metabolic stress, the essential
milk protein tolerance is important to the muscle (Wolfe, 2000, Volpi et al., 2003). Whey metabolism of cysteine by the liver is
management of diets of humans with CMP proteins have a greater concentration of disrupted (Hack et al., 1997). The pathway
allergy, especially infants at risk for allergy. branched chain amino acids than any other of cysteine metabolism by the liver maintains
These infants are dependent on human milk. protein (Walzem et al., 2002, Layman and muscle glutamine stores and glutathione
Baum, 2004). The high concentration of synthesis. Compared to other proteins,
Milk Protein and Body Composition
the branched chain amino acid leucine in whey also has a rich source of cysteine
Dietary whey proteins, which represent 20% whey protein has a key role in muscle DNA which is easily assimilated by the body
of the protein in milk powders, have been transcription pathways of protein synthesis (Walzem, 2002).
shown to be highly effective in preserving (Anthony et al., 2001). The BCAAs leucine,
muscle mass (Renner, 1983, Poullain et al., Milk Proteins and Glutathione Production
isoleucine and valine, are needed for the
1989, Boza, 2000, Bouthegourd et al., 2002, production of muscle glutamine, which Whey protein has a unique capacity to
Belobrajdic et al., 2003), decreasing body fat in turn controls muscle protein synthesis increase glutathione production (Bounous,
and increasing glutathione concentrations (Kimbal and Jefferson, 2002). Glutamine 2000, Bouthegourd et al., 2002). Many
(Lands et al 1999). Increases in muscle mass is also used as a source of energy for the researchers have reported on wheys capacity
with whey protein supplementation requires muscle during periods of metabolic stress to increase glutathione concentrations within
resistance training (Cribb, 2002). However, and in immune function (Walsh et al., 1998). a number of different cells in the body (Lands
whey supplementation (20g/day for Wheys amino acid composition is 26% et al., 1999, Bounous, 2000, Watanabe et al.,
12 weeks) without vigorous exercise branched chain amino acids and 6% 2000, Zemel et al., 2000, Agin et al., 2001,
enhanced glutathione status, improved glutamate (Bucci and Unlu, 2000, Layman Micke et al., 2002, Walzem et al., 2002).
anaerobic athletic performance and reduced and Baum, 2004, see table below) which Glutathione (GSH) is a tripeptide of glycine,
body fat mass (Lands et al., 1999). Compared are exclusively used by muscle to synthesize cysteine and glutamic acid. Since cysteine
to a casein or carbohydrate supplemented glutamine. A diet rich in whey protein results represents the limiting amino acid for GSH
animal, rodents on a whey protein diet had in a greater intake of leucine which due to its synthesis and contains the suphhydryl
lower body fat and more muscle mass during unique regulatory action on muscle protein group for GSH actions, a sufficient supply is
a six week study (Bouthegourd, 2002). The synthesis, insulin signal and glucose-alanine essential. GSH maintains many substances in
percentage of body fat is affected more by pathway results in a desirable glycemic their reduced state and takes part in the cells
muscle mass than by physical fitness level control and increased synthesis of defense against oxygen radicals (Cotgreave et
(Calles-Escandon et al., 1995, Nagy et al., muscle protein. al., 1998, Townsend et al., 2003). Glutathione
1996, Levadoux et al., 2001, Inelmen et al., can directly scavenge free radicals and also
2003). Furthermore, preventing a decline in acts as a cosubstrate in the GSH peroxidase
Leucine and BCAA Content of Foods*
muscle mass thus improves the percentage catalyzed reduction of peroxides, which
of body fat. The consumption of whey protein Leucine BCAA makes it central to defense mechanisms
also leads to a greater level of satiety and Whey protein isolate 14% 26% against intra- and extracellular stress.
lower food intake than a diet consisting Milk protein 10% 21% Glutathione and GSH transferases are major
of other proteins (Anderson and Moore, Egg protein 8.5% 20% components in the metabolism of a variety of
2004). Milk proteins high in BCAAs act via Muscle protein 8% 18% drugs (Lomeastro and Malone, 1995). GSH is
casomorphins which act on gastric receptors also involved in the transport of amino acids
Soy protein isolate 8% 18%
to slow down gastric motility (Daniel, 1990). and in the synthesis of leukotrienes which are
Wheat protein 7% 15%
The physiological responses to a dairy important in the inflammatory response. Low
protein diet are highly desirable in weight loss *Values reflect grams of amino acids/100 g of protein. plasma GSH levels are indicative of muscle
Source: USDA Food Composition Tables.
management. Whey proteins incorporated loss whereas adequate plasma GSH is found
into the diet are a significant health benefit in patients with increased muscle mass.
to the elderly, patients with HIV, cancer,
and athletes.
46 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
Dairy Proteins and HIV/AIDS of HIV-infected patients consuming 45g Dairy Proteins and Sports Nutrition
of whey proteins for 6 months concluded
Patients diagnosed with HIV are at nutritional The beneficial effect of combining dairy
that supplementation with whey proteins
risk at any stage of their illness. Optimal protein supplementation with resistance
persistently increased plasma glutathione
nutritional management is a critical part of training has been a topic of intense
levels in patients with advanced HIV
their medical treatments (Baum et al., 1994, discussion in the scientific community
infections and that the treatment was well
Bartlett, 2003). Side effects of the disease (Fry et al., 2003, Demling and De Santi, 2000,
tolerated (Micke, 2002). Larger, long-term
and/or antiviral treatments include: Cribb et al., 2002, Cribb et al., 2003). A whey
trials are still needed to evaluate how this
hyperglycemia, elevated serum lipids, protein supplement (60g/d) provided to a
positive influence translates into a more
atherosclerosis, central obesity, cohort of overweight men was effective in
favorable course of the disease.
gastrointestinal symptoms and increased decreasing fat mass and increasing fat-free
insulin resistance (Nerad et al., 2003). Dairy Proteins and Elderly Nutrition mass (Demling, 2000). Supplementations
Also, loss of muscle mass or lean body mass Both men and women by age 70-80 have including whey protein with other minerals,
has been shown to be a strong prognostic experienced a 20-40% decline in muscle vitamins and carbohydrates provided even
indicator for the survival of patients with strength (Doherty, 2003). To date 30% of better results than whey protein supplements
HIV (Wheeler et al., 1999, Kotler et al., 1989, those older than 60 years have a condition alone. Many resistance training studies are
Guenter et al., 1993). A whey protein diet is an called sarcopenia or loss of muscle (Doherty, flawed due to the lack of consistency in
ideal complement to the medical treatment 2003). Exercise alone does not seem to training techniques, training intensity and
of HIV patients with its excellent composition halt the age related loss in muscle mass frequency among and between study
of amino acids and role in catabolic and increase of body fat accumulation cohorts. The two best well-controlled
conditions. A diet rich in whey protein, (Feigenbaum, 1999). Significant loss of studies, however, do substantiate that
which has been shown to preserve muscle muscle mass and increased fat mass are positive body composition changes occur
mass by stimulating muscle protein believed to be an underlying cause for with resistance training while on a whey
synthesis, has been recommended in HIV ailments typically associated with the protein isolate containing diet (Cribb et al.,
therapy (Task force on nutrition in AIDS, 1989, elderly such as osteoporosis, diabetes 2002, Cribb et al., 2003). In a ten-week
AIDS Nutrition Services Alliance, 2002). The and decreased resistance to infection resistance training program, athletes
current recommendations state to consume (Evans, 1997, Dutta, 2001, Levadoux et al., provided a whey protein isolate (1.5g/kg/day)
1.01.4g of protein/kg/day to maintain body 2001, Doherty, 2003, Inelman et al., 2003). experienced a weight gain five times greater
weight. Using a highly purified whey protein than the control group. The DEXA (dual
in the diet would enable an HIV patient to In elderly, the post-prandial protein synthesis energy x-ray absorptiometry) body
achieve such a high protein intake (e.g. 84g is reduced compared to healthy young composition assessment revealed that
per day for a 70kg male). individuals (Doherty, 2003, Dorrens and the whey-supplemented group had a
Rennie, 2003). Thus, whey proteins ability to significant decrease in body fat (1kg)
Because of their potential role in the stimulate post-prandial protein synthesis as and increased muscle mass as opposed
stimulation of the immune system, whey demonstrated in elderly patients (Dangin et to the casein-supplemented group (Cribb
proteins have also been used in the nutrition al., 2002) is critical. Further evidence that et al., 2002). In a second study the whey-
of HIV patients. Studies have documented whey protein should be an important supplemented group gained twice as much
the benefits of whey protein isolates element in the diet of the elderly is the fact fat-free mass as the carbohydrate, whey
consumption by HIV patients, resulting in that elderly women who increased their protein isolate and creatine supplemented
substantial reduction in virus activity and dietary intake of protein reduced bone counterparts in this eleven week resistance
increased survival expectancy. HIV infection mineral loss and the risk of fracture (Bell and training program (Cribb et al., 2003). There
is characterized by an enhanced oxidant Whiting, 2002, Hannan et al., 2000). Since are conflicting reports on whether whey
burden and a systemic deficiency of calcium retention is an important issue protein alone, or in conjunction with a
glutathione (GSH), a major antioxidant, and particularly for the elderly, the concern for carbohydrate or casein supplemental mixture
cysteine (Herzenberg et al., 1997, Droge et al., urinary excretion of calcium noted in patients with whey protein, provides the optimum
1993, deQuay et al., 1992). Numerous studies with increased protein intakes is justifiable. dietary support for improving body
have shown that whey proteins help enhance Not only are animal proteins less likely to composition. Better controlled studies
the body's immune system by raising cause an increase in urinary excretion of are needed to better understand the
glutathione levels. Glutathione is a powerful calcium than vegetable proteins but they also composition of whey protein diets on
anti-oxidant with the ability to help the body increase intestinal absorption of calcium strength and body composition in resistance
reduce the risk of infections by improving the at intake levels ranging from 0.7 to 2.1g/kg training athletes.
responsive ability of the immune system (Kerstetter et al., 2003).
(Cotgreave et al., 1998). Individuals with HIV
often have reduced levels of glutathione,
which negatively affects their immune system
(Droge et al., 1994, Buhl et al., 1989). A study
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 47
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
Because of the delayed transit time through dominates and little effect of lactose
7.2 CARBOHYDRATES the digestive system, a part of the sugar is observed. Various mechanisms are
reaches the colon intact and is used as responsible for this, one being that the
Lactose, the principal carbohydrate in milk a substrate for the growth of beneficial metabolism of lactose by intestinal flora
powder, accounts for about 54% of the intestinal flora such as bifidobacteria. increases the concentration of lactic acid
total solids-non-fat content of milk. Minor Growth of bifidobacteria results in an acid in the intestinal tract. Consequently, pH
quantities of oligosaccharides, glucose and environment, which inhibits the growth of decreases, improving the solubility and
galactose are also present in milk powder. E. coli and other putrefying and pathogenic availability of calcium. Lactose is also
Researchers speculate that galactose may organisms. For infants, this is especially capable of forming complexes with calcium,
have a unique role in the rapidly developing important for resistance against intestinal influencing the transport of calcium through
infant brain. Lactose is the first and only infections. In both infants and adults, lactose the intestinal epithelium membranes in a
carbohydrate every newborn mammal in the diet contributes to the maintenance of positive way.
consumes in significant amounts. In infants, stable, healthy intestinal flora.
some lactose enters the colon where it Some individuals have difficulty metabolizing
promotes the growth of beneficial lactic Lactose is recognized for stimulating the lactose because of reduced lactase levels,
acid bacteria which may help combat intestinal absorption of calcium. The effect a condition called lactase nonpersistence.
gastrointestinal disturbances. is independent of the presence of vitamin D Recent research indicates that most
and is exerted on the diffusional component persons with lactase nonpersistence are
Lactose is a natural disaccharide consisting of the intestinal calcium transport system. able to consume the amount of lactose in
of one galactose and one glucose unit. Since lactose acts on passive calcium 250500ml of milk a day if taken with a meal.
It can be hydrolyzed by the enzyme beta- absorption, its effect is dependent on A number of low-lactose and lactose-reduced
galactosidase into its individual sugars. calcium intake levels. At low levels, vitamin milks are also available. Lactose-free milk has
The slow hydrolysis of lactose by the body D-dependent active calcium transport about 99% of its lactose hydrolyzed.
during digestion generates a prolonged
energy supply. Being a carbohydrate, it
provides about 4 calories per gram. Because
digestion of lactose is much slower than of
glucose and fructose, lactose is considered
relatively safe for diabetics. It does not cause
a sharp increase in blood glucose levels like
sweeteners, and therefore has a nutritional
advantage in the diabetic diet.
48 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
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7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
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R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 51
7 NU TRI T IONA L PROPERT IES OF MILK P OWDERS
Dairy Products and Adiposity lipogenesis, increase lipolysis and fat In human intervention studies, the effect of a
oxidation and increase apoptosis. As a 24-week dietary calcium supplementation
Contributed by Dr. M.B. ZEMEL result, increasing dietary calcium to suppress were studied in subjects with a body mass
Department of Nutrition and Medicine,
calcitriol levels is an attractive approach index in the 3039kg/m2 range, and who
The University of Tennessee, Knoxville, TN, USA.
for weight management. Indeed, in studies therefore were classified as obese. The
In the early 1980s, we undertook an conducted in mice, low calcium diets subjects were randomized into a group
intervention study of obese black Americans prevented fat loss, whereas high calcium receiving a calcium-supplemented diet, a
who suffered from hypertension and who diets accelerate it. What makes this research diet supplemented with dairy, and a control
were asked to consume, for a one year period, particularly relevant is that when the calcium group. Although all three groups received
two daily servings of yogurt, in addition to is provided by dairy products, the fat loss equal levels of caloric restriction, the
their diet. The yogurt consumption resulted and attenuation of weight and fat gain is dairy-based diet augmented the loss of
in an extra intake of 4001,000mg of calcium accelerated. It is probable that the increased weight and fat by 70% and 64%, respectively;
daily. In addition to the anticipated effect on effect of dairy vs. supplemental calcium is although the calcium supplements also
blood pressure, the yogurt supplementation due to bioactive compounds found in milk augmented weight and fat loss, they were
resulted in a loss of body fat of 4.9kg that act in synergy with the calcium. only about half as effective as the dairy-rich
over one year. At the time, the possible diet. Additional studies have also shown that
This hypothesis has been tested in animal
mechanism explaining the weight loss was dietary calcium not only accelerates weight
experiments, analyses of population data
not understood. and fat loss, but also results in increased loss
sets and in human intervention studies. The
of fat in the trunk (abdominal region), which
Since then, a number of recent studies studies on animals were conducted with is a more desirable health pattern.
have documented that calcium intake is transgenic mice which exhibit a human-like
inversely related with the risk of obesity, pattern of obesity-related gene expression All the studies conducted to date clearly
and we have developed a plausible and which are susceptible to diet-induced indicate the benefits of a high calcium diet for
mechanism to explain this relationship. obesity. In the studies, mice received feed the management of obesity, with markedly
That mechanism is based on the observation containing 1.2% calcium (the controls diet greater effect for dairy vs. nondairy sources
that a high calcium intake reduces the contained only 0.4% calcium). The calcium of calcium. The additional components of
serum 1,25-dihydroxycholecalciferol diet led to a decrease in lipogenesis of 51%, dairy responsible for the effect are under
(1-25-dihydroxyvitamin D3, 1,25-(OH)2-D, an increase in lipolysis by a factor of 35, investigation, but preliminary data indicated
also referred to here as calcitriol) level. This and substantial reductions in body weight that bioactive components found the
active form of vitamin D stimulates the influx and fat content. Studies on mice were also whey fraction of milk protein may play an
of calcium ions into fat cells, which promotes conducted comparing a high calcium diet important role. It is possible that angiotensin
obesity, as follows. Ca2+ ions are needed by (1.2% of the calcium derived from calcium converting enzyme inhibitors found in the
the adipocytes for the transcription of fatty carbonate), medium dairy diet (1.2% calcium whey proteins (which constitutes 20% of the
acid synthetase, a key enzyme in de novo derived from nonfat dry milk, which also protein in nonfat dry milk), as well as the
lipogenesis; high levels of Ca2+ in the fat replaced 25% of protein) and a high dairy rich concentration of branched chain amino
cell also inhibit lipolysis. Accordingly, the diet (2.4% calcium derived from nonfat dry acids found in whey, may contribute to the
increase in intracellular Ca2+ elicited by milk, which replaced 50% of the protein). antiobesity effect of dairy. This research has
calcitriol cause an increase in lipogenesis, Greater weight reduction, 19, 25 and 29%, important implications for the prevention of
a decrease in lipolysis and a consequent respectively, were observed in the high obesity among children and adults alike, in
expansion of fat storage. In addition, we calcium, medium dairy and high dairy diets. developed as well as developing countries
have also shown that calcitriol acts via a The differences were significant over the where the prevalence of obesity is rising to
Ca2+-independent mechanism to inhibit the control group which was only exposed to alarming levels.
transcription of uncoupling protein 2 (UCP2). energy restriction and where an 11% weight
It is a multifunctional protein which may loss was observed.
increase energy dissipation by the fat cell
The datasets analyzed came from the U.S.
(although this is controversial) and which
National Health and Nutrition Examination
stimulates the clearing away of larger, older
Study (NHANES III) database. These
fat cells via apoptosis (programmed cell
indicated an inverse association between
death). Indeed, we have shown that calcitriol
calcium intake and percentage of body fat
inhibits the destruction of fat cells by
and have now been confirmed in a number
apoptosis and that reduction of calcitriol
of other population studies.
levels by high calcium diets increases fat cell
apoptosis. Accordingly, since dietary calcium
inhibits calcitriol levels, it should reduce
52 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
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References
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These complexes precipitate and of other essential amino acids, as Anderson G.H., Moore S.E., (2004). Dietary proteins in
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without any harm to colon epithelial a placebo or carbohydrates. These humans. J Nutr 134: 974S-979S.
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FUNCTIONAL PROPERTIES AND PERFORMANCE
OF MILK P OWDERS 8
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 57
8 FUNCTIONAL PROPERTIES AND PERFORMANCE
OF MILK P OWDERS
The functional properties may be defined in Functional Properties of Major Milk Powder Components
relation to their performance as powders and Whey Proteins Caseins
to their performance as foods or in use as Whipping/foaming Fat emulsification
ingredients in formulated foods. The functional Gelation Foaming
properties of milk powders are typically Solubility at low pH Solubility at pH >6
dependent upon: powder composition, the Heat denaturation Water binding
influence of processing conditions prior to Lactose Milk fat
drying and drying conditions themselves. Low sweetening power Creaming
Humectant Unique flavor
The major components in milk powder Color development, browning Gloss
(proteins, lactose, milkfat) affect the way Free-flow agent Flavor carrier
in which milk powders perform and their Flavor development Low melting temperature range
suitability for each type of application.
Solubility In the case of whole milk powder and
buttermilk powder, the wettability problem
Dairy protein functionality is dependent
is compounded because of free fat forming
upon ingredients solubility in a solution.
a hydrophobic film on the surface of the dry
In their native state, casein and whey proteins
particles. For this reason, lecithin is often
are highly soluble in food and beverage
added during the drying process to help
systems and, as a result, are frequently
improve the powders ability to dissolve.
used for their emulsifying and whipping/
foaming properties. However, excessive The process of instantizing, which involves
heating results in protein denaturation, a drying process that causes agglomeration,
decreasing solubility. enhances reconstitution properties in cold
liquids by improving one or more of the
Poor solubility (high-solubility index) in milk
following properties: wettability, sinkability,
powders is caused by subjecting the milk to
dispersibility, rate of hydration and solubility.
high temperatures, particularly at high total
solids level during processing. Emulsification
Roller-dried powders, because of the higher The manufacture of food emulsions, typically
temperatures attained, have significantly oil-in-water systems, is a highly energetic and
greater solubility indices (less soluble) than dynamic process in which oil/water interfaces
spray-dried powders. are protected by adsorption of surfactants
and partially lost again by recoalescence
Since milk proteins are sensitive to heat, the of those emulsion droplets that are not
extent of their denaturation reflects the heat protected quickly enough by surfactants.
treatment applied and is used for classifying Recoalescence is an important phenomenon
skim milk powder (high-heat, medium-heat in emulsions stabilized by proteins because
and low-heat). Heat classification provides of the relatively slow development of a
an indication of the suitability of skim stabilizing surface film of proteins around
milk powder for specific applications. By new emulsion droplets.
controlling thermal denaturation, the degree
of solubility can be manipulated. The proteins in milk powders can quite
successfully act at oil/water interfaces to
Milk powders, depending upon their form and stabilize emulsions. Emulsification
composition, generally consist of small, properties can be enhanced by controlled
single particles of high bulk density. denaturation of the protein. In particular,
Non-instant skim milk powder tends to the rate of diffusion to the newly formed
be rather dusty. As a result, reconstitution oil/water interface and the rate of adsorption
is difficult because the skim milk particles and unfolding increase with increasing
tend to clump together on the surface temperature, enhancing the formation and
of the reconstituting liquid and have stabilization of emulsion droplets. The
poor wettability. unfolding of the dairy protein exposes
58 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
8 FUNCTIONAL PROPERTIES AND PERFORMANCE
OF MILK P OWDERS
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 59
8 FUNCTIONAL PROPERTIES AND PERFORMANCE
OF MILK P OWDERS
Functionality of Milk Powders Recombined milk products can be made Water is one of the critical, and most
in Recombining Applications from a combination of skim milk powder important (by volume), ingredients of
and anhydrous milk fat; skim milk powder, recombined milk products. It should be
By Dr. Phil Tong buttermilk powder and anhydrous milk fat; potable and needs to be checked regularly
Professor, whole milk powder and skim milk powder; or from a bacteriological standpoint. Spore
Director Dairy Science, Dairy Products Technology Center, by simply using whole milk powder. Cream contamination of recombined milk products
California Polytechnic University,
powder or emulsifiers are typically added to often finds its source in the water used in
San Luis Obispo, California.
those formulations. manufacture. Preferred methods of water
The production of recombined milk purification include sodium ion exchange
The source of fat can be vegetal in the case of and reverse osmosis. While effective against
products is a major application for milk
filled products. Fortified products, designed some bacteria, chlorination is not effective
powders in international markets and most
to meet the needs of specific population against spores.
countries where milk production is not
targets, can be manufactured with the
sufficient to meet local demand for
addition of whey proteins, calcium, iron, Data available from the scientific literature
dairy products. While the production of
bioactive components and other dairy or suggests that the total hardness of the water,
recombined evaporated (condensed)
non-dairy ingredients. In these cases, the in carbonate equivalent, should not exceed
milk (REM) and recombined sweetened
nutritional content, flavor and functionality 100ppm, with the total dissolved solids less
condensed milk (RSCM) continues to be
of the recombined products is significantly than 350ppm, and not in excess of 500ppm.
an important industry, there has been a
different from that of fresh milk.
large increase in the production of UHT Additives such as gums, carrageenans or
recombined milk products in the past emulsifiers can be added at different steps of
decade. Milk powders are also ingredients the process and processors should contact
in the production of extended shelf-life the suppliers of these ingredients for their
(ESL) milks. recommendations.
It is preferable to heat the water to be used
for reconstitution to 4055C, and when
adding fats, ensure they are added at a
temperature that is higher than their melting
point. This may require, when utilizing AMF in
drums, for example, holding the fat for a day
or two at a temperature of 4550F. The use
of water colder than 30C may result in the
formation of powder lumps, unless advanced
mixing systems are employed.
The powder should be allowed to rehydrate
for about 20 min. to allow for the milk protein
system and minerals to re-equilibrate. In
most operations, the time needed to disperse
the powder in the tank and filter it, allows
sufficient time for this rehydration process to
take place. Recombined liquid milk is not
a shelf-stable product and processors need
to ensure pasteurization or further heat
processing follows rehydration promptly to
improve its original microbiological quality.
If intermediate storage is required during the
process, the temperature of the milk should
be kept below 7C, preferably 4C.
References:
Tong P.S. Recombined and Reconstituted Products.
Encyclopedia of Dairy Sciences, Vol. 4, pp 2401-2405.
Roginski H., Fuguay J. and Fox P., eds. Academic
Press, N.Y.
60 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
8 FUNCTIONAL PROPERTIES AND PERFORMANCE
OF MILK P OWDERS
Gelling Milk components form Bind large quantities of Appeals to the health- Confectionery 77
irreversible gels under water and non-protein conscious by creating
specific conditions. compounds. lower fat products with
Dairy/recombined milk 83
the taste of full-fat. Meat 95
Improves mouthfeel. Helps
lubricate and provide the Prepared foods 103
creamy, smooth texture
of fat.
Water binding Under specific Provides fat-like attributes Reduced-fat products Bakery 71
and viscosity conditions, protein in products, allowing a appeal to health-conscious
building molecules unfold reduction in fat content. consumers, especially
Confectionery 77
and form a gel. The if they can duplicate the Dairy/recombined milk 83
three-dimensional
Retains water, which full-fat mouthfeel.
structure of the gel reduces product costs. Meat 95
binds water.
Reduced ingredient costs
Increases viscosity, which can translate into lower Nutritional beverages 99
has a significant effect on consumer prices or
machinability. Prepared foods 103
increased marketing
Improves product texture, expenditures.
creating moister products. A moister product equates
Increases viscosity in to a fresh product.
rehydrated and fluid
products. Improves product texture,
increasing consumer
appeal.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 61
8 FUNCTIONAL PROPERTIES AND PERFORMANCE
OF MILK P OWDERS
Flavor Lactose reacts with Can provide baked, brown Clean flavor and aroma Bakery 71
enhancement milk proteins leading flavor during baking and with no evidence of
to the production of heating. off-flavors enhances
Confectionery 77
flavorful compounds. customer appeal. Dairy/recombined milk 83
Milk powders have a
Can provide creamy dairy
bland, sweet dairy notes. Homogeneous and Meat 95
flavor. consistent flavor.
Milkfat ensures even flavor Nutritional beverages 99
Milkfat carries fat- distribution.
Prepared foods 103
soluble ingredients
throughout a
formulation.
Milkfats low melting
point ensures
complete flavor
release.
Nutritional Possess high-quality Can improve the nutritional Contributes to a foods Bakery 71
enrichment proteins all of the profile of a food product. healthy image and
amino acids required clean label.
Dairy/recombined milk 83
for a healthy diet
Lactose increases
calcium absorption and Represents a natural
Nutritional beverages 99
in a readily digestible
form. Is high in lactose, stimulates the growth of and good source of Prepared foods 103
a disaccharide that is acid-forming lactobacilli in soluble vitamins.
slowly digested. Milk the intestinal track.
Offers advantages in
powders are high in Provides vitamin enrichment. dietary therapy.
calcium and rich in
thiamin, riboflavin and Provides mineral fortification.
other nutrients.
62 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
MILK POWDERS IN FOOD ASSISTANCE PROGRAMS 9
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 63
9 MILK POWDERS IN FOOD ASSISTANCE PROGRAMS
Successful management strategies for those Dry whole milk is made by removing water 9.1 BENEFITS OF FOOD
with lactose intolerance include, among from pasteurized whole milk. U.S. Extra ASSISTANCE PROGRAMS
others (1) drinking milk in servings of one cup grade DWM contains between 26% and
(230ml) or less (less than 25g of skim milk 40% milkfat with a moisture level of
powder or less than 20g of sweet whey 4.5% (by weight). It has applications
Dry dairy ingredients deliver nutrition and
per serving), (2) drinking milk with a in confections, baked goods, soups functionality that have many benefits
meal or other foods (or consume dairy and some child/infant formula and and make them an important addition for
ingredients in conjunction with other, nutritional preparations. food assisted programs.
non-dairy ingredients), (3) consume other
dairy products such as fermented milks, Milk ingredients have applications in Diverse nutritional benefits:
yogurts or cheese, or use lactose-reduced virtually every food category, including rich in high quality proteins,
or lactose-free milk or ingredients (such as fortified mixes, fermented milks (yogurts, an excellent source of calcium with high
whey protein concentrates or isolates). kefir), lactic cultured products, baked bioavailability,
goods such as flatbreads, beverages, a source of other minerals and vitamins,
According to the World Health Organization, confections, infant formula, dairy foods, presence of bioactive and health-
clinically significant lactose intolerance is meat products, sauces and soups, enhancing compounds that have
unusual in severely malnourished children. nutritional products and nutraceuticals. applications in therapeutic feeding,
In confirmed intolerance cases among In many applications, dairy ingredients are complement proteins, of vegetal origin.
these children, WHO recommends replacing considered critical to the nutritional value
milk partially or completely by yogurt or a of the product as well as its taste, aroma, Versatile:
commercial lactose-free formula. mouthfeel, keeping qualities (shelf-life) can be used for recombination* or
and texture. These diverse applications in fortification purposes,
U.S. dairy ingredients offer a range of are ready to use, do not require further
the food processing sector make SMP and
solutions for food assistance programs. cooking or preparation,
other milk ingredients particularly suitable
New processing technologies to concentrate can also be used as binders, emulsifiers, or
for income-generating activities and
and modify the composition of milk have texture and shelf-life extension agents in a
monetization programs.
made it possible to produce an array variety of food/dairy products,
of ingredients, including many that are As with many dry ingredients, it is critical mixes well and can serve as carriers for
tailor-made for specific food aid applications. that only clean water and other ingredients vitamins, minerals, other nutrients.
U.S. dairy ingredients represent a versatile with the appropriate microbiological,
solution for food assistance programs. sensory and functional attributes be Universal:
They lend themselves to utilization in utilized in recombined and reconstituted a mild flavor is well accepted in many
nutritional preparations, as well as milk products. It is also essential that cultures,
in monetization programs. sanitary/hygenic manufacturing conditions as an ingredient, promotes color and flavor
be established and controlled to insure the development to increase consumer
The most commonly used ingredient is appeal,
safety of the finished product, up to the
nonfat dry milk. It is made by removing water application uses in a wide range of
time of consumption.
from pasteurized fat-free milk. It contains recipes and industrial formulations in
5% or less moisture and 1.5% or less milkfat Packaging: U.S. dairy ingredients such most countries.
(by weight). NFDM is white to light cream in as milk powders and whey are typically
color, with a mild dairy flavor. Major types shipped in 50 lbs. or 25kg multiwall Long shelf-life:
of NFDM include instantized, high heat, poly-lined bags. Plastic-lined corrugated When stored in a dry, cool place, dry dairy
medium heat or low heat. NFDM is often paperboard or other types of tote bins are ingredients have a shelf-life of up to three
recombined for the manufacture of a variety also used. Specialty, high value ingredients years. Additional shelf-life studies and
of dairy products and nutritional beverages. are available in smaller quantities. recommendations for storage under
It is also a common ingredient in child/infant Please consult your U.S. supplier for different conditions are available
formula, baked goods, confections and more information. upon request.
fortified prepared foods such as soups. U.S. dairy ingredients can be used in direct
feeding programs (school lunch, soup
kitchens), in emergency distribution
situations,* and in monetization programs.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 65
9 MILK POWDERS IN FOOD ASSISTANCE PROGRAMS
Studies indicate that intake of calcium-rich Dairy Proteins: How They Compare
9.2 OVERVIEW: NUTRITIONAL foods, such as skim milk powder and
Nutritionally, cows milk protein is
BENEFITS OF DAIRY other whey protein concentrates, during
considered to be high quality because
INGREDIENTS childhood and adolescence is an important
it contains, in optimal amounts, all of the
determinant of achieving peak bone mass
essential amino acids that our bodies
Please refer to the nutrition section of this and minimizing future risk of osteoporosis.
cannot synthesize, in proportions similar to
manual for more information (see Section 7).
During adulthood, intake of dairy foods and human essential amino acid requirements.
The consumption of cows milk and dairy ingredients provides essential nutrients
For many years the standard to determine
ingredients contributes to health throughout needed for body maintenance and protection
protein quality was the Protein Efficiency
life. According to the American Academy against major chronic diseases such as
Ratio, or PER. The standard protein, casein,
of Pediatrics, the nutritional adequacy of osteoporosis, for example. Milk powder and
had a PER of 2.7. Any protein with a PER
diets for children should be achieved by whey protein concentrates furnish a generous
greater than 2.7 is regarded as an excellent
consuming a wide variety of foods, and supply of critical nutrients (easily digestible
quality protein. In 1993, the FDA replaced the
children should be provided with sufficient proteins, calcium) in relation to calories: an
PER with the Protein Digestibility-Corrected
energy to support their growth and important factor when designing nutritional
Amino Acid Scoring, or PDCAAS, method.
development and to reach or maintain rations for pregnant and lactating women as
If the PDCAAS is greater than or equal to
desirable body weight. Dairy ingredients well as seniors and HIV infected individuals.
1.00, the protein is a good source of essential
are nutrient-dense and provide abundant
Experimental studies indicate that cows amino-acids.
amounts of high-quality proteins, vitamins
and minerals necessary for growth milk may help to increase bone strength
The tables in this text are presented to help
and development. and enhance immune function. Furthermore,
compare dairy proteins with other proteins.
several physiological roles have been
Detailed information on protein requirements
Straight cows milk (fresh or dried) is not either defined or suggested for minor whey
and quality evaluation methods is available
recommended for infants during the first 12 proteins or peptides. These components can
from the Food and Agriculture Organization
months of life. Human milk is recommended provide passive protection against infection,
(www.fao.org) and the United Nations
to support infants rapid growth and modulate digestive and metabolic processes,
University (www.unu.edu/unupress/).
development during this period. In and act as growth factors for different cell
circumstances that make breastfeeding types, tissues and organs.
impossible or unadvisable, commercially
prepared iron-fortified cows milk-based
Protein Source BV PER NPU
formulas are used. These formulas contain
dairy ingredients such as whey protein Whey protein concentrate 104 3.2 92
concentrates, lactose and milk powders Whole egg 100 3.8 94
as well as other nutrients, and they are Cows milk 91 3.1 82
formulated to provide adequate nutrition. Beef 80 2.9 73
Casein 77 2.7 76
Soy protein 61 2.12.2 61
BV: Biological value, PER: Protein efficiency ratio, NPU: Net protein utilization.
Sources: FAO, USDA, National Dairy Council.
66 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
9 MILK POWDERS IN FOOD ASSISTANCE PROGRAMS
The Protein Digestibility Corrected Amino Typical Calcium Concentration of Major U.S. Dairy Ingredients
Acid Score (PDCAAS) measures the
Dairy Ingredients Typical Calcium Content in mg/100 g
protein quality, based on the amino-acid
Whey protein concentrate 500700 mg/100 g
requirements of humans. Criteria needed
for PDCAAS are approximate nitrogen Whey protein isolate 600 mg/100 g
composition, essential amino acid profile Sweet whey 700800 mg/100 g
and true digestibility. Whey proteins have Whey permeate 800900 mg
a higher score than virtually all other Mineral-concentrated whey >5,000 mg/100 g
protein sources. Whole milk powder 9501,000 mg/100 g
Skim milk powder 1,300 mg/100 g
PDCAAS of Key Protein Sources Milk minerals 23,00028,000 mg/100 g
Ingredient PDCAAS
Milk* 1.23 Calcium in Dairy Ingredients and Health Enhancing Benefits of
Whey protein* 1.15 Milk Minerals Dairy Ingredients
Egg white 1.00
Milk powders are an excellent source of Individual milk proteins have been shown
Soybean protein .94
calcium and can be used for fortification to exhibit a wide range of beneficial
Whole wheat-pea flour (**) .82
purposes. Milk minerals can be extracted functions including enhancing calcium
Chick peas (garbanzos) .69 from the whey stream, yielding a product that absorption and immune function.
Kidney beans .68 contains about 80% minerals, 10% lactose The antimicrobial mechanisms of whey
Peas .67 and 5% protein. Milk calcium is a product proteins such as immunoglobulins,
Sausage, pork .63 that contains minerals (up to 28% calcium, lactoferrin, lactoperoxidase, lysozyme
Pinto beans .61 13.5% phosphorus, 1.4% magnesium and and glycomacropeptide are now well
Rolled oats .57 0.8% potassium) that are balanced for documented. Immunogloblulins from milk
Black beans .53 optimal bone health and with good and whey have a prophylactic and therapeutic
Lentils .52 bioavailability. Several recent studies have effect (clinically established in human adults)
Peanut meal .52 shown that milk minerals are an optimal against specific micro-organisms causing
Whole wheat .40
form of calcium supplementation because diarrhea, gastritis and dysentery.
they not only provide calcium, but also key
Wheat protein (gluten) .25 Studies have also documented the benefits
minerals (magnesium, potassium, zinc) that
of whey protein isolates for HIV patients.
Source: FAO, except for * European Dairy are critical to bone-building.
Association/ U.S. National Dairy Council (from UNRA, HIV patients who consumed whey protein
France. Unpublished data).
**An example of mutual supplementation. Combining Milk calcium has a protective role against isolates exhibited substantial reduction
whole wheat and pea flours yields a protein with a osteoporosis. Studies have demonstrated in virus activity and increased survival
higher PDCAAS than that of either product alone.
that the calcium absorption efficiency from expectancy. Numerous studies have shown
non-dairy fortified sources was 25% less than that whey proteins help enhance the body's
that from a dairy source. Nutritionists can immune system by raising glutathione levels.
not only use milk calcium as an ingredient Glutathione is a powerful anti-oxidant with
for fortification purposes, but can also take the ability to help the body reduce the risk of
into consideration other mineral-rich dairy infections by improving the responsive ability
ingredients when formulating products of the immune system. Individuals with HIV
and rations. often have reduced levels of glutathione,
which negatively affects their immune
system. These individuals need a boost
to their immune system, which they can
obtain from a diet rich in whey proteins.
The newest research included feeding HIV-
infected patients with 45g of whey proteins
for 6 months in a double blind clinical trial.
The study concluded that supplementation
with whey proteins persistently increased
plasma glutathione levels in patients with
advanced HIV infections and that the
treatment was well tolerated.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 67
9 MILK POWDERS IN FOOD ASSISTANCE PROGRAMS
Extra Grade indicates the highest quality powder. Most of the supply is low heat milk
9.3 U.S. GRADES: WHAT DO milk powder. It should be free from lumps, powder, the rest consists of medium and high
THEY MEAN? except those that break up readily under heat product.
mild pressure. Standard Grade includes
Please refer to the Standards section of this Copies of the United States Standards
all milk powder that fails in one or more of
manual for more information (see Section 4). for Milk Powders are available from
the particulars to meet the requirements
www.usda.gov or the U.S. Dairy Export
of Extra Grade. It may contain small to
U.S. suppliers of milk powders voluntarily Council. A commodity fact sheet for nonfat
moderate lumps.
participate in the U.S. standards for milk dry milk under USDAs food aid programs is
powders grading system. The Commodity Credit Corporation only available at www.fas.usda.gov.
purchases extra grade nonfat dry milk
68 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
9 MILK POWDERS IN FOOD ASSISTANCE PROGRAMS
70 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
BAK ERY A P P L I C AT IONS F OR M I LK P OW DER S 10
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 71
10 B A K E R Y A P P L I C A T I O N S F O R M I L K P O W D E R S
72 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
10 B A K E R Y A P P L I C A T I O N S F O R M I L K P O W D E R S
Procedure:
Procedure:
1. Combine and mix all dry ingredients on
1. Combine flour, whey protein concentrate,
low speed for 3 minutes.
NFDM, baking powder and salt.
2. Add shortening and water, mixing on low
2. Add water and oil.
speed for 2 minutes.
3. Stir quickly with fork, just until dough
3. Mix on medium speed for 11-22 minutes
is mixed.
or until dough passes gluten test
4. Drop dough by spoonfuls on ungreased (when pulled dough stretches with no
baking sheet. rough tearing).
5. Bake in preheated 232C (450F) oven for 4. Proof dough, about 32C (90F), until
10 to 12 minutes, until brown. double in size, about 1 hour.
5. Shape into loaves and place in greased
loaf pans. Allow to full proof until double,
about 30-45 minutes.
6. Bake at 204C (400F) for 20-30 minutes.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 73
10 B A K E R Y A P P L I C A T I O N S F O R M I L K P O W D E R S
74 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
10 B A K E R Y A P P L I C A T I O N S F O R M I L K P O W D E R S
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 75
10 B A K E R Y A P P L I C A T I O N S F O R M I L K P O W D E R S
Pancakes, Buttermilk High Protein Chocolate Chip Cookie Savory Cheese Scone
Ingredients Usage Level (%) Ingredients Usage Level (%) Ingredients Usage Level (%)
Water 50.50 Brown sugar 20.85 Flour, all purpose 37.55
Flour, all-purpose 24.50 Whey protein concentrate-80% 17.85 Water 22.85
Eggs 10.55 Pastry flour 17.85 Cheddar cheese 15.45
Vegetable oil 5.90 Chocolate chips 17.35 Butter 13.10
Buttermilk powder 4.85 Butter 12.65 Whole egg powder 4.60
Sugar, granulated 2.50 Water 9.00 Skim milk powder 2.05
Baking powder 0.90 Eggs 2.50 Baking powder` 1.90
Salt 0.30 Skim milk powder 1.25 Hard grating cheese 1.85
Total 100.00 Vanilla extract 0.30 Salt 0.60
Salt 0.20 Spice 0.05
Sodium bicarbonate 0.20 Total 100.00
Procedure: Total 100.00 Formula courtesy of the Dairy Products Technology
1. Combine all dry ingredients. Center, California Polytechnic State University.
Formula courtesy of the Dairy Products Technology
Center, California Polytechnic State University.
2. Add beaten egg, water and oil. Mix until
homogenous. Procedure:
Procedure: 1. Combine the flour, egg powder, skim milk
3. Pour onto griddle in 43g portions. Flip
1. Cream butter with sugar. powder, baking powder, and salt in a
once to brown on both sides. Pancakes are
mixing bowl.
ready to turn when they bubble and edges 2. Add vanilla and eggs.
look slightly dry. 2. Stir well with a fork to mix and aerate.
3. Add dry ingredients, mix until blended.
3. Add the butter and cut into the flour
4. Add chocolate chips. mixture, using a pastry blender or two
5. Bake at 190C (375F) for 8 to 10 minutes. knives, or work in, using your fingertips,
until the mixture looks like bread crumbs.
4. Add the cheeses and spice, mix lightly.
5. Add the water, mix only until the dry
ingredients are moistened.
6. Gather the dough into a ball and press so
it holds together. Turn the dough out onto
a lightly floured surface. Knead lightly
12 times. Pat the dough into a circle
1.25 cm (1/2 inch) thick.
7. Cut the dough onto pie-shaped pieces,
place 2.5 cm (1 inch) apart on baking
sheet.
8. Bake at 225C (450F) for about 12 minutes
or until the tops are browned. Serve hot.
76 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
CONF EC T IONERY A P P L I C AT IONS F OR M I LK P OW DER S 11
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 77
11 C O N F E C T I O N E R Y A P P L I C A T I O N S F O R M I L K P O W D E R S
Emulsification Flavor/Aroma
11.1 CONFECTIONERY The proteins in milk powders can successfully Milk powders contribute a subtle, pleasant
APPLICATIONS FOR act at oil/water interfaces to form and dairy note and aroma to confections. Very
MILK POWDERS* stabilize emulsions. The lecithin present in little flavor comes from the dairy proteins,
milkfat also assists in stabilizing emulsions. which are quite bland and contribute no
foreign or off-flavors. Most of the flavor
U.S. product developers and manufacturers Gelation comes from the milkfat, which adds richness
benefit from the nutritional, functional and Undenatured dairy proteins are able to form to certain confections. Milkfat also acts as a
economical attributes of high-quality U.S. rigid, heat-induced, irreversible gels that flavor carrier for fat-soluble ingredients and
milk powders on a year-round basis. hold water and fat, and provide structural various flavors. Milkfats low melting point
support to confections. Two types of ensures complete flavor release.
In the United States, 78.6% of all whole aggregates can form: linear or globular. The
milk powder and 14.3% of all buttermilk type of aggregation affects the gels opacity, Also, during the cooking process, the lactose
powder are used directly in confections. an important property in confections. present in milk powders reacts with dairy
Milk powders are a critical ingredient in the proteins leading to the production of
formulation of milk chocolate candy, nougats, Water Binding different flavors.
frosting, and creams. Water-binding capacity refers to the water
held in a gel under a given set of conditions.
Benefits of Milk Powders in This water, enclosed in the gels three-
Confectionery Products dimensional structure, can reduce the cost
Milk powders assist product developers in of food (water is inexpensive) and improve
the formulation of a variety of confectionery sensory perception. The firm, chewy texture
products. Milk powders provide flavor and of several confections is related to the
functionality in confectionery items like binding of water by casein.
caramels and icings. Foaming
U.S. confectioners include high-quality U.S. Formation of foams is very important in
milk powders in formulations because of the confections and is similar to the formation
functional and economical benefits milk of an emulsion. Foaming is defined as the
powders add to confectionery products. creation and stabilization of gas bubbles
In addition, manufacturers are assured of in a liquid. As dairy protein concentration
a consistent, year-round supply of U.S. increases, foams become denser with
milk powders. more uniform air bubbles of a finer texture.
The incorporation of air is important in
confections such as nougat, frosting and
various creams.
Browning/Color
The lactose and protein present in milk
powders contribute, through the Maillard
browning reaction, to the caramelized color
associated with many confections. During
heating, the proteins amine groups react with
lactose and other reducing sugars present in
the formulation, delivering an appealing color
while also contributing to flavor.
78 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
11 C O N F E C T I O N E R Y A P P L I C A T I O N S F O R M I L K P O W D E R S
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 79
11 C O N F E C T I O N E R Y A P P L I C A T I O N S F O R M I L K P O W D E R S
Icing, Fudge
Ingredients Usage Level (%)
Sugar, powdered (10x) 57.36
Water 29.40
Cocoa powder 5.86
Butter 5.05
Skim milk powder 2.20
Salt 0.13
Total 100.00
Procedure:
1. Mix sugar, cocoa, milk and butter with a
paddle blender.
2. Combine water, butter and salt over heat.
Bring to a boil.
3. Beat liquid mixture into solid mixture.
Beat until smooth.
Procedure:
1. Blend dry ingredients on #1 speed in a
mixer fitted with paddle attachment.
2. Add shortening and blend uniformly.
3. Add hot tap water (60C) and vanilla.
Mix on #2 speed to achieve a smooth,
uniform consistency.
80 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
11 C O N F E C T I O N E R Y A P P L I C A T I O N S F O R M I L K P O W D E R S
Frosting, Chocolate
Ingredients Usage Level (%)
Powdered sugar 70.30
Butter 13.00
Boiling water 10.30
Cocoa powder 5.50
Vanilla extract 0.60
Skim milk powder 0.20
Salt 0.10
Total 100.00
Procedure:
1. Mix powdered sugar, skim milk powder,
salt and cocoa powder.
2. Add boiling water, butter and vanilla.
3. Beat with mixer on low until mixed.
4. Beat on medium for 1 minute.
Frosting, Vanilla
Ingredients Usage Level (%)
Powdered sugar 77.00
Butter 10.60
Boiling water 10.25
Skim milk powder 1.15
Vanilla extract 1.00
Total 100.00
Procedure:
1. Mix powdered sugar and skim milk powder.
2. Add boiling water, butter and vanilla.
3. Beat with mixer on low until mixed.
4. Beat on medium for 1 minute.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 81
11 C O N F E C T I O N E R Y A P P L I C A T I O N S F O R M I L K P O W D E R S
82 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
DA I RY AND RECOMB I NED M I LK A P P L I C AT IONS
FOR MILK POWDERS 12
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12 D A I R Y A N D R E C O M B I N E D M I L K A P P L I C A T I O N S
FOR MILK POWDERS
Ingredient Selection Recombined Milk Product It is important to use milk powders that
possess the specific properties that the
The traditional approach to the manufacture Other ingredients used in the formulation of
recombined milk product requires. For
of recombined milk products is to use skim recombined milk products include a countrys
example, fluid milk requires a medium to
milk powder and anhydrous milkfat. However, local milk or cream supply, and, where
low-heat skim milk powder (WPN >3.5)
the fat source could also be frozen, unsalted permitted, vegetable oils such as coconut
because high-heat products may yield an
butter, but this is somewhat inconvenient to or palm. However, vegetable oils, because of
undesirable cooked flavor.
handle. With recent improvements in the their high degree of unsaturated fatty acids,
keeping quality of whole milk powder, it too easily oxidize, creating different types of Reconstituted milk powders need a
can be used in recombined milk products. formulation and storage problems. minimum of 15 to 20 minutes hydration
Whichever powder is chosen, the higher the time in order to minimize any chalky or
Recombination Process
heat treatment used in its manufacture (i.e. powdery mouthfeel. Sometimes prior to
the lower the whey protein nitrogen index), The recombination process begins with further processing, manufactures hold the
the better the oxidative stability will be dispersion of skim milk powder in water reconstituted milk overnight at 4C (39F) to
of the recombined product. This results at 40-50C (104-122F). Water quality is ensure full hydration.
from the formation of sulphydral groups important and should be checked routinely,
during the heat treatment, which act as especially if it is ground water. Chemical, Reconstituted powders are pumped
natural antioxidants. physical, biological and radiological through a duplex filter to separate out
minimum and maximum levels for water any undissolved milk powder particles
In some recombined milk products, 5-12% must be established. and any other extraneous matter. From here
of the skim milk powder is replaced by the process varies according to the product
buttermilk powder to provide a more Powder is fed into the water via a hopper with being made. (See following pages.)
balanced flavor. Buttermilk powder also care taken to avoid air incorporation, which
contains phospholipids, which are not causes foaming. Various techniques are used
present in either skim milk powder or to add the powder to the water. The most
anhydrous milkfat. By using buttermilk common method is to empty the milk
in the manufacture of a recombined powder bags in a dry room with a dust
milk product, it will contain all the major removal system, because a great deal of
components of the real milk product the dust is generated in this step.
recombined product represents. Because
phospholipids contain unsaturated fatty
acids that can auto-oxidize and produce
off-flavors, many product developers prefer
to formulate recombined dairy products
without buttermilk powder.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 85
12 D A I R Y A N D R E C O M B I N E D M I L K A P P L I C A T I O N S
FOR MILK POWDERS
Process
12.2 RECOMBINED FLUID MILK The skim milk powder (and buttermilk
Traditional whole cows milk typically has a powder, if used) is dissolved in water at
slightly higher level of fat than recombined 40-50C (104-122F). Hydration time must be
fluid full-fat milk products. Sometimes the at least 20 minutes; however, overnight
level of solids-nonfat is increased to 10% to hydration at temperatures less than 6C
improve nutrition and flavor. (43F) is recommended. Some form
of de-aeration may be needed before
homogenization. After hydration, the milk
Typical Composition of Recombined
Fluid Full-fat Milk is heated to 60-65C (140-149F) and the
butteroil (or frozen unsalted butter) is added.
Traditional Recombined The product is homogenized at 17 MPa in a
Whole Milk Full-fat Milk
one stage homogenizer or in a two stage
Fat 3.5% 3.0% homogenizer at pressure of between
Solids-nonfat 8.5% 10.0% 14-24 MPa first stage and 2-7 MPa second
Total solids 12.0% 13.0% state. After homogenization, the milk is
pasteurized (72C (161F)/15 sec) and
cooled to 4-6C (39-43F) before blending
Powder Requirements
and packing.
Whey protein nitrogen >3.5 low heat to
A typical heat treatment for sterilized milk
low medium heat
is 120C (248F) for 10 minutes. This kills
Solubility index <0.25 ml clean
dairy flavor
microorganisms and bacterial spores, while
also deactivating enzymes. Unfortunately,
Microbial Good quality
the severe heat treatment does reduce the
Pyruvate test <90 mg/kg powder*
nutritive value of the milk. Its particularly
*The pyruvate test is important in the manufacture detrimental to the water-soluble vitamins and
of UHT milk because proteolytic and lipolytic
enzymes are not destroyed by ultra-high the amino acid lysine. The most noticeable
temperature pasteurization. If pyruvate is present defect for those consumers accustomed to
in large amounts, it will cause bitter flavors
to develop. fresh milk is the strong cooked flavor.
Ultra-high temperature (UHT) pasteurization
Low heat skim milk powder yields a better of milk is typically done at 140C (284F) for
initial flavor in recombined fluid milk than 4 seconds. This kills microorganisms and
powder with a whey protein nitrogen value bacterial spores, while also deactivating
less than 6.0. However, the keeping quality of enzymes. This heat process maintains
long life milk is not as good when low heat desirable nutritive and flavor milk qualities
skim milk powder is used. so that it more closely resembles fresh milk.
The UHT processing equipment and the
aseptic filling unit do not normally run at the
same speed so it is necessary to either have
an aseptic buffet tank or to recycle surplus
milk back into the process.
86 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
12 D A I R Y A N D R E C O M B I N E D M I L K A P P L I C A T I O N S
FOR MILK POWDERS
Process
12.3 RECOMBINED CHEESE After the reconstitution and recombining
AND CULTURED MILK steps explained on the previous pages,
PRODUCTS manufacturing follows traditional cheese
or yogurt making processes. Adjustments
The nature and composition of recombined
need to be made to compensate for the heat
cheese and cultured milk products varies
treatment and homogenization the milk has
considerably according to local tastes. Soft
already received during the recombination
cheeses with high moisture content, bland or
process. For example, in cheesemaking,
acid flavor, tender bodies and open texture
rennet temperatures should be increased in
are more successfully produced using
order to obtain better curd syneresis during
recombined milk than are structured cheese.
draining of the vat. Some manufacturers
Cheeses that have been successfully concentrate the recombined milk using
manufactured using recombined milk include ultrafiltration, thus increasing the dry matter
Feta, Domiati, Kashkaval and Haloumi. content to more closely resemble the dry
Cultured products such as yogurt and For cheese, low heat skim milk powders matter content of the cheese to be produced.
cottage cheese can also be made with provide more ionic calcium than high heat
recombined milk. Flavors and sweeteners powders and minimum interaction of
are selected on the basis of masking the k-casein with b-lactoglobulin. These affect
undesirable cooked flavor that comes from the rate of milk coagulation, curd strength
the high heat skim milk powder typically and syneresis. A rennet coagulum made from
used in recombined yogurt precuts. recombined milk using low heat skim milk
powder has a higher curd tension than a
Powder Requirements coagulum made from high heat skim milk
powder. Some manufacturers use additives
Whey protein nitrogen >4.5 such as calcium chloride or mono-calcium
for cheese preferably >6.0,
low heat
phosphate to improve the use of medium
heat skim milk powder for cheesmaking
Whey protein nitrogen <3.05
for yogurt medium and because low heat powder is often in
high heat short supply.
Rennetability Good
For cultured products such as yogurt,
Fermentation Non-inhibitory viscosity and stability are important finished
substances
product criteria; therefore, powder selection
is based on water-binding capacity. Medium
to high heat milk powders provide the water
binding capabilities required for optimum
body consistency in recombined yogurt.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 87
12 D A I R Y A N D R E C O M B I N E D M I L K A P P L I C A T I O N S
FOR MILK POWDERS
Process
12.4 RECOMBINED The skim milk powder is added via a hopper
EVAPORATED MILK and mixed with water at 40-45C (104-113F).
Foaming needs to be kept to a minimum. The
Just like traditional evaporated milk,
mix is hydrated for 20 minutes or overnight at
recombined evaporated milk has about 15%
4C (39F). The milk is then heated, the fat
less moisture than the fluid milk from which
is added and it is homogenized at 50-70C
it is made. It is typically canned and heat
(122-158F) at pressures of 20 MPa first stage
sterilized in order to extend shelf life.
and 3.5 MPa second stage. Disodium
orthophosphate or monosodium
Typical Composition of Recombined
orthophosphate is normally added to
Evaporated Milk
assist protein stability. After canning, the
Traditional Recombined product is sterilized. Normal sterilization
Whole Milk Full-fat Milk is 120C (248F) for 12 minutes followed by
Fat 7.5% 7.8% cooling to 32-35C (90-95F).
Solids-nonfat 17.7% 17.8%
Total solids 25.2% 25.6%
Sometimes carrageenan is incorporated
into the mix with the skim milk powder.
This reduces fat separation during storage.
Powder Requirements Also the product is often fortified with
vitamins A and D prior to homogenization.
Whey protein nitrogen High heat
Stability* Heat stable
*Refers to the earlier comments on the heat stability
test. This is done with a 20% dispersion of skim milk
powder with and without the addition of disodium
phosphate. The minimum coagulation time is 21
minutes if phosphate has been added.
88 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
12 D A I R Y A N D R E C O M B I N E D M I L K A P P L I C A T I O N S
FOR MILK POWDERS
Process
12.5 RECOMBINED SWEETENED Skim milk powder is dissolved in water using
CONDENSED MILK agitation to the highest possible level of
total solids in order to obtain the best value.
Recombined sweetened condensed milk is
During agitation, the mix is heated to 40-60C
typically made with milkfat; however, in Asia,
(104-140F). Fat and sugar are added. The
it is often made using vegetable oil (filled).
mixture is homogenized at 2-3.5 MPa (for a
Just like traditional sweetened condensed
low viscosity product) or up to 7MPa (for
milk, recombined sweetened condensed milk
higher viscosity), then heated at 80-90C
has about 70% less moisture than the fluid
(176-194F) for 30 seconds to 2 minutes and
milk from which it is made. It is typically
flash-cooled in a vacuum pan to 32C (90F).
canned and heat sterilized in order to extend
Sterile lactose hydrate crystals are added
shelf life.
to promote lactose crystallization, and
the product is cooled further before
canning aseptically.
Powder Requirements
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 89
12 D A I R Y A N D R E C O M B I N E D M I L K A P P L I C A T I O N S
FOR MILK POWDERS
90 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
12 D A I R Y A N D R E C O M B I N E D M I L K A P P L I C A T I O N S
FOR MILK POWDERS
Procedure:
1. Disperse cellulose gel in water using Procedure: Procedure:
high-speed agitation. Completely hydrate, 1. Blend all ingredients into a uniform 1. Blend all ingredients into a uniform
approximately 15 minutes. suspension in a batch tank. suspension in a batch tank.
2. Gradually add skim milk powder, sugar and 2. Test the mix and restandardize 2. Test the mix and restandardize
cocoa. Mix well. (Avoid air incorporation.) if necessary. if necessary.
3. Pasteurize, homogenize and fill packages. 3. Pasteurize milk at 82C (180F) for 3. Pasteurize milk at 82C (180F) for
23 seconds. 23 seconds.
4. Homogenizetwo stage homogenization 4. Homogenizetwo stage homogenization
recommended with 14.1 MPa in the first recommended with 14.1 MPa in the first
stage and 3.5 MPa in the second stage. stage and 3.5 MPa in the second stage.
5. Cool rapidly to 0-4C (32-39F). 5. Cool rapidly to 0-4C (32-39F).
6. Age the mix for at least 4 hours. 6. Age the mix for at least 4 hours.
7. Optionally, completely dispersible 7. Optionally, completely dispersible
flavorings can be added to the mix prior flavorings can be added to the mix prior
to freezing. to freezing.
8. Freeze in two stages. Freeze to 0 to -1C 8. Freeze in two stages. Freeze to 0 to -1C
(32-30F) in the first stage in an ice cream (32-30F) in the first stage in an ice cream
freezer at a rapid rate to a discharge freezer at a rapid rate to a discharge
temperature of -6 to -7C (21-19F). temperature of -6 to -7C (21-19F).
9. Optionally, add particulate materials or 9. Optionally, add particulate materials or
syrups through a fruit feeder. syrups through a fruit feeder.
10. In the second stage, harden the ice cream 10. In the second stage, harden the ice cream
by reducing the temperature of the by reducing the temperature of the
product to at least -18C (0F) in product to at least -18C (0F) in
the center of the packages as quickly the center of the package as quickly
as possible. as possible.
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 91
12 D A I R Y A N D R E C O M B I N E D M I L K A P P L I C A T I O N S
FOR MILK POWDERS
Ice Cream, Low-Fat Ice Cream, Nonfat Ice Cream, Soft-Serve Dry Mix
Ingredients Usage Level (%) Ingredients Usage Level (%) Ingredients Usage Level (%)
Whole milk 55.00 Skim milk 75.30 Skim milk powder 44.82
Water 18.30 Sugar, granulated 10.00 Sugar, granulated 29.88
Sugar, granulated 10.00 Skim milk powder 6.00 Sweetener syrup solids 13.44
Skim milk powder 8.00 Whey protein concentrate-80% 4.00 Butter powder 10.46
Whey protein concentrate-80% 4.00 Sweetener syrup solids 4.00 Carboxymethyl cellulose 0.45
Sweetener syrup solids 4.00 Stabilizer 0.70 Guar gum 0.35
Stabilizer 0.70 Total 100.00 Emulsifier 0.30
Total 100.00 Carrageenan 0.30
Total 100.00
Procedure:
Procedure: 1. Mix dry ingredients into milk with a
1. Mix dry ingredients into milk with a powder horn. Procedure:
powder horn. For mix:
2. Pasteurize milk at 82C (180F) for
1. Combine all ingredients. Store.
2. Pasteurize milk at 82C (180F) for 23 seconds.
23 seconds. For Soft-Serve:
3. Homogenizetwo stage homogenization
2. Mix 3kg of the dry blend into 5.7 liters of
3. Homogenizetwo stage homogenization recommended with 14.1 MPa in the first
cold water using rapid agitation.
recommended with 14.1 MPa in the first stage and 3.5 MPa in the second stage.
stage and 3.5 MPa in the second stage. Final product temperature should be 3. Allow to hydrate for 10-20 minutes. Stir.
Final product temperature should be 5.5C 5.5C (42F).
(42F). 4. Allow to hydrate for 10-20 minutes. Stir.
4. Hold at 0-4C (32-39F) overnight.
4. Hold at 0-4C (32-39F) overnight. 5. Pour into soft-serve machine.
5. Freeze.
5. Freeze. 6. Freeze mix and serve at or below
-10C (14F).
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FOR MILK POWDERS
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12 D A I R Y A N D R E C O M B I N E D M I L K A P P L I C A T I O N S
FOR MILK POWDERS
94 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
ME AT A P P L I C AT IONS F OR M I LK P OW DER S 13
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13 M E A T A P P L I C A T I O N S F O R M I L K P O W D E R S
R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s 97
13 M E A T A P P L I C A T I O N S F O R M I L K P O W D E R S
98 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
NU T R I T IONA L BE V ER AGE A P P L I C AT IONS
FOR MILK POWDERS 14
Procedure:
1. Mix sucrose, fructose and gum blend.
2. Add coffee, mix well.
3. Add the remaining ingredients, except oil,
mix for 5 minutes.
4. Slowly add oil, mix for additional
5 minutes.
5. Rehydration: 40g of dry beverage mix with
240mls (8oz) of water.
Demineralized Whey-based Infant Milk-Based Infant Formula Mix1 Whey Protein Concentrate-Based
Formual Mix1 Infant Formula Mix1
Ingredients Usage Level (%)
Ingredients Usage Level (%) Lactose 38.30 Ingredients Usage Level (%)
Demineralized whey Skim milk powder 34.00 Lactose 37.00
(approximately 1% minerals) 43.00 Fat blend* 27.00
Fat blend* 27.00
Fat blend* 28.00 Whey protein concentrate-34% 18.50
Lecithin 0.50
Skim milk powder 16.00 Skim milk powder 16.00
Vitamins and minerals* 0.20
Lactose 11.30 Vitamins and minerals* 1.00
Water As needed
Vitamins and minerals* 1.20 Lecithin 0.50
Total 100.00
Lecithin 0.50 Water As needed
*Vitamins, minerals and fat content must be adjusted
Water As needed to meet the minimum and maximum limits as Total 100.00
Total 100.00 recommended by national authorities.
The value of breast milk as an ideal food for the infant
1 *Vitamins, minerals and fat content must be adjusted
*Vitamins, minerals and fat content must be adjusted during the first six months of its life cannot be too to meet the minimum and maximum limits as
to meet the minimum and maximum limits as strongly stressed. However, poor health of the recommended by national authorities.
recommended by national authorities. mother and certain social conditions can reduce The value of breast milk as an ideal food for the infant
1
Procedure:
1. Mix half of the water with the starch. Procedure:
Reserve. 1. Mix milk powder, water, chicken base, bay
leaf and pepper. Simmer over low heat.
2. Mix remaining ingredients. Using wire
whisk, whip continuously over low heat. 2. Mix starch with a little of the sherry to
make a smooth paste. Add to simmering
3. When smooth and all cheese is melted,
liquid and bring to boil. Immediately
add starch mixture.
remove from heat and strain.
4. Bring to a boil. Strain through fine mesh.
3. Saut onions in butter until soft. Add
5. Chill. remaining sherry and simmer for 1 minute.
Add to the sauce.
4. Chill.
Iced Coffee Milk (serves 24) Enriched Crackers Enriched Roti-Style Bread
Ingredients Ingredients Usage Level (%) Ingredients Usage Level (%)
Reconstituted milk* 6 quarts Flour 55.10 Flour 58.00
Instant coffee 1/2 cup Skim milk powder 5.10 Skim milk powder 3.30
Sugar 1 cup Salt 1.10 Salt 0.50
*To prepare the milk: Stir 8 cups (19.2 ounces by Water 24.90 Vegetable oil 1.70
weight) of skim milk powder into 5 2/3 cups of Vegetable oil 13.80 Water 36.50
cold water.
Total 100.00 Total 100.00
2. Chill thoroughly. 2. Add water and oil. 2. Add water and oil.
3. Mix well to make a stiff dough. Knead until 3. Mix well for 2 or 3 minutes.
dough is smooth, about 5 minutes.
4. Turn dough out onto a well-floured
Single Serving 4. Roll the dough very thin (about surface. Knead until smooth and pliable,
Ingredients 2-3mm thick). about 10 minutes.
Reconstituted milk* 1 cup 5. Cut into squares and place on 5. Preheat an unoiled skillet. Divide dough
Instant coffee 1 teaspoon parchment-lined baking sheets. into 40g (1.4 ounce) balls.
Sugar 2 teaspoons
6. Bake in preheated 230C (450F) oven for 6. Flatten the balls with the palm of your
*To prepare the milk: Stir 8 cups (19.2 ounces by
weight) of skim milk powder into 5-2/3 cups of
10 to 12 minutes. hand. Roll out each piece into a 18 to 25
cold water. cm (7-10 inch) diameter round.
7. Cook the roti for 1 minute before turning.
Procedure: Cook an additional minute.
1. In a large mixing bowl (or in a blender),
combine the milk, instant coffee and
sugar and stir until the coffee and sugar
are dissolved.
2. Chill Thoroughly.
Variation:
Blend fruit to the mix instead of coffee.
2. Add water and oil. 1. Preheat the oven to 177C (350F) degrees.
Procedure:
3. Stir quickly with fork, just until dough 2. In a mixing bowl, combine the flour, 1. In a large bowl, combine the flour, potato
is mixed. potato flakes, sugar, iodized salt and flakes, sugar, iodized salt and baking soda.
baking powder.
4. Drop dough by spoonfuls on ungreased 2. Stir in the oil, 1/2 cup milk and
baking sheet. 3. Make a well in the center of the dry cream cheese.
ingredients and cut in the shortening.
5. Bake in preheated 230C (450 F) oven for 3. Wrap the dough tightly in plastic wrap and
10 to 12 minutes, until brown. 4. Add the milk and stir with a wooden spoon refrigerate for at least 10 minutes.
until just combined.
4. When you are ready to make the crackers,
5. Turn the dough out onto a lightly floured preheat the oven to 177C (350F).
board and gently knead until the dough
forms a ball. Roll the dough 12mm 5. Roll out the dough on a lightly floured
(1/2 inch) thick. Using a biscuit or cookie surface until it is paper thin and prick it
cutter, cut out 5cm (2-inch) rounds and several times with a fork. Brush the dough
place the biscuits on baking sheets. with the remaining milk and sprinkle with
coarse iodized salt.
6. Bake for 15 minutes or until the biscuits
are barely golden. 6. With a knife or pizza cutter, cut the dough
into random cracker shapes.
7. Place the crackers on a cookie sheet in a
single layer and bake for about 6 minutes
or until golden and crisp.
Potato Bundt Cake (yield one 25cm Procedure: Mexican Spice Cake (yield one 25cm
(10 inch) bundt cake) (10 inch) bundt cake)
1. Preheat the oven to 177C (350F).
Ingredients Grease a 10-inch bundt or tube pan and Ingredients
Bundt Cake set it aside. Potato flakes 1 cup
Potato flakes, standard 1 cup Flour, all purpose 2 cups
2. In a large bowl, mix the potato flakes, flour,
Flour, all purpose 2 cups baking powder and iodized salt together. Reconstituted milk* 1 cup
Baking powder 1 tablespoon Baking powder 1 tablespoon
Salt, iodized 1/4 teaspoon 3. In a separate bowl, beat the butter (or oil) Cocoa powder or
Butter or oil and sugar together for a few minutes, until grated cocoa 1 tablespoon
(at room temperature) 1/2 cup the mixture is fluffy. Cinnamon, ground 1/2 teaspoon
Sugar 1 cup 4. Add the eggs, one at a time, to the sugar Salt, iodized 1/4 teaspoon
Eggs 3 mixture. Add the vanilla. Butter or oil
Vanilla 2 teaspoons (at room temperature) 1/2 cup
Reconstituted milk* 1 cup 5. Fold in half of the flour mixture, then Sugar 1 cup
Optional Icing
the milk and finally the remaining Eggs 3
flour mixture. Vanilla 2 teaspoons
Sugar, confectioners 1 cup
Water 2 tablespoons 6. Pour the batter into the prepared pan. Sugar, confectioners (optional for dusting)
Spinach Mashed Potatoes (serves 20) Carrot Mashed Potatoes (serves 20)
Ingredients Ingredients
Onions, yellow, finely chopped 2 cups Onions, yellow, finely chopped 1 cup
Reconstituted milk* 6 cups Carrots, peeled & chopped 4 cups
Spinach, finely chopped 9 cups Butter (margarine or oil) 1/2 cup
Potato flakes, standard 6 cups Reconstituted milk* 5-1/3 cups
Reconstituted milk, cold* 2-1/4 cups Potato flakes, standard 5-1/3 cups
Salt, iodized 2-1/4 teaspoon Reconstituted milk, cold* 2 cups
Pepper To taste Salt, iodized 2 teaspoon
*To prepare the milk: Stir 3-1/3 cups (8 ounces by
Pepper To taste
weight) of nonfat dry milk into 10-1/3 cups of cold
water. To avoid spoilage, use immediately or cover, *To prepare the milk: Stir 2-2/3 cups (6.4 ounces by
refrigerate and use within 3 to 5 days. weight) of nonfat dry milk into 7-1/2 cups of cold
water. To avoid spoilage, use immediately or cover,
Formula courtesy of USPB; recipe adapted to refrigerate and use within 3 to 5 days.
include NFDM.
Formula courtesy of USPB; recipe adapted to
include NFDM.
Procedure:
1. In a large skillet, heat the butter over Procedure:
medium heat. Add the onions and cook 1. Cook the carrots in boiling water until they
until they become soft and translucent, are completely tender, about 10 minutes.
about 6 to 8 minutes. Add the spinach and Drain the carrots and mash them with a
cook until the spinach has just wilted, fork or potato masher. Keep warm and
about 1 minute more. Remove from heat set aside.
and set aside.
2. In a large saucepan or soup pot, heat the
2. In a large pot, bring the 6 cups of milk and butter over medium heat. Add the onions
2-1/4 teaspoons of iodized salt to a boil and cook until they become soft and
and remove from heat. Add the cold milk. translucent, about 6 to 8 minutes. Add the
Using a spoon, gradually and gently stir in 5-1/3 cups of milk and 2 teaspoons of
the potato flakes. Do not overwork. iodized salt and bring the mixture to a boil.
3. Gently fold the spinach mixture into the 3. Remove from heat and add the cold milk.
potato mixture. Season with iodized salt Using a spoon, gradually and gently stir in
and pepper. Serve warm. the potato flakes. Do not overwork.
It may be necessary to add water (1/8 cup 4. Gently fold the onions and pureed carrots
at a time) to thin the potatoes to the into the potato mixture. Season to taste
desired consistency. Alternatively, add with iodized salt and pepper. Serve warm.
potato flakes (1 tablespoon at a time) to
thicken them. It may be necessary to add water (1/8 cup
at a time) to thin the potatoes to the
desired consistency. Alternatively, add
potato flakes (1 tablespoon at a time) to
thicken them.
Potato Pancakes
(makes 40, 8cm (3-inch) pancakes)
Ingredients
Vegetable oil (for frying) 1/2 cup
Onions, finely chopped 2 medium
Green bell peppers,
finely chopped 2 medium
Tomatoes, finely chopped 2 medium
Potato flakes, standard 5 cups
Flour, all purpose 5 cups
Baking powder 2-1/2 teaspoons
Eggs, well beaten 5
Reconstituted milk* 3-3/4 cups
Sour cream 1 cup
Salt, iodized To taste
Pepper To taste
*To prepare the milk: Stir 1-1/3 cups (3.2 ounces
by weight) of nonfat dry milk into 3-3/4 cups of
cold water.
Formula courtesy of USPB; recipe adapted to
include NFDM.
Procedure:
1. In a small skillet, heat a tablespoon of oil
over medium heat. Add the onions and
bell peppers and cook until they become
soft and translucent, about 5 minutes.
Add the tomatoes and cook for an
additional 5 minutes. Remove from
heat and allow to cool.
2. In a mixing bowl, combine the potato
flakes, flour and baking powder. Gently stir
in the egg, milk, and cooked vegetables.
Season with iodized salt and pepper. Form
the potato mixture into 40 cakes.
3. In a large skillet, heat a few tablespoons of
oil over medium high heat. Cook the cakes
(a few at a time) until they are golden
brown on each side, about 3 minutes
per side.
4. Serve with sour cream.
Since 1995, the U.S. Dairy Export Council has been committed to
USDECUSA USDECMiddle East
developing educational materials on U.S. dairy ingredients based on info@usdec.org amfime@cyberia.net.lb
current scientific research. This manual is an update of the first two editions USDECChina USDECSouth America
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of the Reference Manual for U.S. Milk Powders. We have again attempted
USDECEurope USDECSoutheast Asia
to review the most current technical and scientific information available
usdec.europe@mistral-pr.co.uk usdec@pacrimassociates.com
consultants, researchers, Dairy Management Inc. and USDEC staff have USDECMexico USDECTaiwan
usdecmex@prodigy.net.mx usdec@prcon.com
shared their knowledge and contributed their resources to this new volume.
and other interested groups. We hope this new edition will continue to be a
Vronigue Lagrange
Editor
U.S. Dairy Export Council
2 R e f e r e nce M anu a l f or U. S. M i l k P o w d e r s
REFERENCE MANUAL
FOR U.S. MILK P OWDERS
2005 REVISED EDITION
REF ERENCE MANUA L FOR U.S. MILK P OWDERS 2005 RE V ISED EDI T ION