Volume Suhu1 Suhu2

1 170 168
2 176 176
3 180 184
4 186 188
5 190 190
6 194 193
7 198 196
8 200 200
9 202 204
10 204 208
11 207 211
12 213 214
13 216 216
14 220 219
15 224 221
16 226 224
17 229 226
18 231 228
19 235 230
20 238 234
21 240 236
22 242 238
23 244 240
24 246 241
25 249 244
26 250 246
27 252 248
28 254 250
29 255 251
30 257 253
31 258 256
32 260 257
33 262 258
34 264 260
35 265 261
36 266 262
37 269 265
38 269 266
39 270 268
40 272 270
41 274 274
42 276 276
43 276 276
44 276 276
45 278 278
46 280 280
47 281 281
48 282 282
49 284 284
50 285 285
51 286 286
52 286 286
53 286 286
54 287 287
55 288 288
56 290 290
57 291 291
58 292 292
59 294 294
84
60 295 295
80
61 296 296
76
62 298 298
632 299 299
7
68
64
60
 80
76
72
648 300 300
6
65 302 302
64
66 304 304
60
67 306 306
68
56 308 308
Volume % Recovery (mL)

692 308 308

5
70 310 310
48
71 311 311
44
72 314 314
40
73 314 314
746 315 315
3
752 318 318
3
76 320 320
28
77 322 322
24
78 325 325
79
20 327 327
806 330 330
1
81 330 330
12
8
4
0
150 160 170 180 190 200 210 220 230 240 250 260 270 280 290 300 3

Temperatur (C)
 Repeatability 1
Repeatability 2

240 250 260 270 280 290 300 310 320 330 340

peratur (C)
eatability 1
eatability 2
% Sc repeatability
10 1.6 1.660 1.2 2.8
20 0.8 1.330 3.6 4.4
30 1 1.410 2.73 3.73
40 0.6 1.250 2.35 2.95
50 0.8 1.330 1.92 2.72
5
60 0.93 1.380 1.77 2.7
4.5
70 1.03 1.420 1.71 2.74
4

3.5

Sc (oC /%vol)
3

2.5

1.5

0.5

0
0 10 20 3
Perce
 2

Repeatabilit 1.5
y1

Sc (oC / % vol)
1

0.5

0
0 10

0 10 20 30 40 50 60 70 80
Percent Recovered %
 2

1.5
Sc (oC / % vol)

0.5

0
0 10 20 30 40 50 60 70 80
Percent Recovered %
60 70 80
temp percent recovered sc1 sc2 dsc repeatability
10 62 78 1.20 2.80 1.60 1.66
20 72 88 1.00 1.00 0.00 1.00
30 82 112 1.00 2.40 1.40 1.57
40 94 118 1.20 0.60 -0.60 0.75
50 96 136 0.20 1.80 1.60 1.66
60 106 162 1.00 2.60 1.60 1.66
70 120 192 1.40 3.00 1.60 1.66
76 186 196 11.00 0.67 -10.33 -3.02

50 250

200

Temperatur (C)
150

100

50

0
0 10 20 30
Percent Re
 Chart Title
250

200
Temperatur (C)

150
Repeatability 1
Repeatability 2
100

50

0
0 10 20 30 40 50 60 70 80
Percent Recovered (%)