Professional Documents
Culture Documents
Copyright ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States.
1
C 563
mass of graded sand and 2030 sand, both conforming to removed from the moist closet, keep these specimens covered
Specification C 778. with a damp cloth until time of testing. Note and observe
precautions regarding testing and retesting given in the appli-
6. Test Specimens cable sections of Test Method C 109.
6.1 Make six specimens from each batch of mortar. Make
two rounds of three mixtures of mortar as described in 6.3. 9. Calculation
Make both rounds during the same day if possible. Make only 9.1 Calculate and record the strength of specimens as
complete rounds on any given day. described in the section on Calculation in Test Method C 109.
6.2 Preparing Specimen MoldsPrepare molds in accor- 9.1.1 Calculate the indicated optimum SO3 content as fol-
dance with the section on Preparation of Specimen Molds of lows:
Test Method C 109. G 5 @a/~a 2 b!# c 1 d 1 c/2
6.3 Proportioning, Consistency, and Mixing of Mortar
Proportion the dry material for the standard mortar as one part where:
of cement to one part of blended sand by mass. Mix the G 5 optimum percent SO3,
following quantities of dry materials at one time for a 6-cube a 5 average strength both rounds of Mixture No. 2 minus
batch: Mixture No. 1,
b 5 average strength both rounds of Mixture No. 3 minus
Mixture No. 1940 g cement
470 g graded sand Mixture No. 2,
470 g 2030 sand c 5 (percent SO3 in calcium sulfate)/100, and
Mixture No. 2930 g cement d 5 percent SO3 in test cement.
10 g calcium sulfate
470 g graded sand 10. Retest
470 g 2030 sand
Mixture No. 3920 g cement 10.1 Regard the results obtained as suspect and repeat the
20 g calcium sulfate
test under any of the following conditions:
470 g graded sand
470 g 2030 sand 10.1.1 If a and b both are positive and the ratio a/b is less
than 2.00,
6.3.1 Use an amount of mixing water that is 30 % by mass
10.1.2 If a and b both are negative and the ratio a/b is
of cement plus calcium sulfate for all types of hydraulic
greater than 0.500, or
cement, except for Type III cement where the amount shall be
10.1.3 If a is negative and b is positive.
36 %.
6.3.2 Mix mechanically in accordance with the section on 11. Report
Procedure for Mixing Mortars of Practice C 305, except as 11.1 If repeat tests confirm that the ratio of a/b departs from
follows: the limiting values as stated above, report the SO3 content of
6.3.2.1 Add the calcium sulfate to the water; then start the the cement as above optimum or below optimum as the
mixer and mix at slow speed (140 6 5 rpm) for 15 s; then stop data may indicate, but without stating the numerical value of
the mixer and add the cement to the water; then start the mixer optimum SO3.
and mix at slow speed (140 6 5 rpm) for 30 s. 11.2 If the test data indicate that the cement is below
6.4 Molding of Test SpecimensMold specimens in accor- optimum but do not permit a computation of the percentage of
dance with the Procedure Section of Test Method C 109. SO3 required for optimum, an additional series of tests involv-
6.5 Storage of Test SpecimensImmediately upon comple- ing greater substitutions of gypsum for part of the cement
tion of molding, place the test specimens in the moist closet or should yield results that will permit an acceptable calculation
moist room. Keep all test specimens, immediately after mold- of the percentage of SO3 required for optimum. If the test data
ing, in the molds on the base plates in the moist closet or moist indicate that the cement is above optimum but do not permit
room for 20 to 24 h with their upper surfaces exposed to the a computation of the percentage of SO3 required for optimum,
moist air but protected from dripping water. If the specimens in order to establish the required percentage of SO3 for
are removed from the molds before 24 h, keep them on the optimum, it is necessary to make tests of a new sample of
shelves of the moist closet or moist room until they are 24-h similar cement but having an original SO3 content lower than
old. that of the original cement.
7. Temperature and Humidity 12. Precision and Bias
7.1 The temperature and humidity of the moist cabinet or 12.1 PrecisionThe coefficient of variation for this test
moist room shall be as specified in Specification C 511. method, using 6 cubes per batch and testing at 24-h age, is very
7.2 The temperature and humidity of the mixing room shall similar to that for Test Method C 109 compression cubes tested
be as specified in Test Method C 109. at later ages. Refer to Test Method C 109 for suitable values.
12.2 BiasSince there is no accepted reference material
8. Procedure suitable for determining optimum SO3, bias has not been
8.1 Test the specimens at the age of 24 6 14 h from the time determined.
the cement and water made contact during mixing, immedi-
ately after removal from the moist closet in accordance with 13. Keywords
Test Method C 109. If more than one specimen at a time is 13.1 blended hydraulic cement; calcium sulfate; cement;
2
C 563
compressive strength; gypsum; hydraulic cement; optimum cement); sulfate content (of cement)
sulfate content (of cement); portland cement; strength (of
The American Society for Testing and Materials takes no position respecting the validity of any patent rights asserted in connection
with any item mentioned in this standard. Users of this standard are expressly advised that determination of the validity of any such
patent rights, and the risk of infringement of such rights, are entirely their own responsibility.
This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years and
if not revised, either reapproved or withdrawn. Your comments are invited either for revision of this standard or for additional standards
and should be addressed to ASTM Headquarters. Your comments will receive careful consideration at a meeting of the responsible
technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should make your
views known to the ASTM Committee on Standards, 100 Barr Harbor Drive, West Conshohocken, PA 19428.
This standard is copyrighted by ASTM, 100 Barr Harbor Drive, West Conshohocken, PA 19428-2959, United States. Individual
reprints (single or multiple copies) of this standard may be obtained by contacting ASTM at the above address or at 610-832-9585
(phone), 610-832-9555 (fax), or service@astm.org (e-mail); or through the ASTM website (http://www.astm.org).