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Thin-Walled Structures
journal homepage: www.elsevier.com/locate/tws
Compression strength of natural fibre composite plates and sections of flax, MARK
jute and hemp
M.R. Bambach
School of Civil Engineering, The University of Sydney, NSW 2006, Australia
A R T I C L E I N F O A B S T R A C T
Keywords: Natural fibres such as flax, jute and hemp have been utilised for thousands of years, however have only recently
Natural fibre composites been considered for fibre-resin composites. A major motivation for such an application is their superior sus-
Flax tainability attributes compared with traditional building materials. Population rise continues to place increasing
Jute demands for new infrastructure. Meanwhile, public concerns about the environment, climate change, energy
Hemp
consumption and greenhouse gas emissions, place increasing demands for the use of sustainable materials in
Plates
infrastructure.
Channels
Compression While there is a wealth of knowledge in the materials aspects of natural fibre composites, relatively few
Design studies have investigated their potential for structural applications. This paper presents an experimental and
analytical study of natural fibre composite plates and channel sections consisting of flax, jute and hemp fibres
and subjected to pure compression. The intrinsic mechanical properties are shown to be relatively modest.
However, the buckling and post-buckling responses are shown to be stable, the ultimate condition is reached in a
stable and predictable manner, and failure ensues in a gradual and ductile process. These characteristics show
promise for the use of natural fibre composite sections in light structural applications such as in the residential
and light commercial markets. Additionally, the analytical effective width mechanics model shows promise for
use as a design technique for estimating their compression strength.
http://dx.doi.org/10.1016/j.tws.2017.05.034
Received 23 November 2016; Received in revised form 29 May 2017; Accepted 31 May 2017
0263-8231/ © 2017 Elsevier Ltd. All rights reserved.
M.R. Bambach Thin-Walled Structures 119 (2017) 103–113
Table 1
Composite plate specimens and test results (subscript P refers to predicted values).
Fibre Layers Fibre weight Width Thickness EC fuC Fbuckle Fultimate λ FbuckleP Fbuckle/FbuckleP
(g/m2) (mm) (mm) (MPa) (MPa) (N) (N) (N)
Flax 2 800 152.8 1.6 4199 38.5 306 2294 5.55 435 0.70
Flax 2 800 152.7 1.6 4199 38.5 218 2231 6.57 435 0.50
Flax 3 1200 154.0 2.5 4199 38.5 1300 5275 3.34 1547 0.84
Flax 3 1200 153.2 2.5 4199 38.5 1293 5081 3.34 1556 0.83
Flax 4 1600 153.8 3.4 4199 38.5 2612 8800 2.78 4141 0.63
Flax 4 1600 154.2 3.4 4199 38.5 2906 9181 2.64 4129 0.70
Jute 2 800 153.2 1.6 3523 40.2 175 1825 7.50 364 0.48
Jute 2 800 153.1 1.6 3523 40.2 187 1995 7.26 364 0.51
Jute 3 1200 152.8 2.5 3523 40.2 1081 4238 3.77 1391 0.78
Jute 3 1200 153.0 2.5 3523 40.2 1218 3863 3.55 1389 0.88
Jute 4 1600 152.9 3.5 3523 40.2 3025 9394 2.65 3652 0.83
Jute 4 1600 152.5 3.5 3523 40.2 2975 8656 2.67 3662 0.81
Hemp 3 861 152.4 2.0 2649 33.9 313 3688 5.67 498 0.63
Hemp 3 861 152.7 2.0 2649 33.9 401 3138 5.02 497 0.81
Hemp 4 1148 153.6 2.7 2649 33.9 1031 6319 3.66 1238 0.83
Hemp 4 1148 152.6 2.7 2649 33.9 987 6313 3.73 1247 0.79
Hemp 6 1722 152.7 3.6 2649 33.9 2656 10,400 2.65 3125 0.85
Hemp 6 1722 153.4 3.6 2649 33.9 2962 10,063 2.51 3109 0.95
Mean: 0.74
2. Methods fabrication, the mass of composite after fabrication, and the constituent
densities.
2.1. General
2.3. Plate specimens
Plate tests consisted of flat plates simply supported on all four sides,
subjected to uni-directional compression. Section tests consisted of Flax, jute and hemp fibre-resin composite plates were fabricated
plain channel sections, being a simple combination of flat stiffened with nominal geometries of 150 mm width and 450 mm length. A
(web) and unstiffened (flange) plate elements, subjected to pure com- length of three times the width was chosen since stiffened plates are
pression. Thin plate buckling involves the development of membrane known to nominally buckle in square half-wavelengths, and having
strains in the two principle orthogonal directions, longitudinal and three half-wavelengths of buckle minimises end effects in plate tests
transverse, thus at a minimum fibres are required in these two principle [25]. Three different plate thicknesses were fabricated for each of the
directions. In this study the simplest fibre orientation appropriate for different fibre types; for the flax and jute composites 2, 3 and 4 fibre
such load consisting of multiple layers of biaxial [0/90] woven fabric layers were fabricated. Since the hemp fabric had a lower aerial mass,
was chosen. A standard bulk commercial laminating epoxy resin with a and in order to create hemp composites with approximately the same
room temperature cure was selected, and the hand layup technique mass of fibre as the flax and jute composites for comparison purposes,
with vacuum bag curing was used for fabrication. This study therefore the hemp plates were fabricated with 3, 4 and 6 layers.
attempted to characterise the compression strength of natural fibre The plates were fabricated with a hand layup technique whereby
composite structures in their simplest form, and no attempt was made each layer of fabric was wetted out with resin using a paint brush and
to optimise these basic characteristics, such as could be achieved with; roller. The fabrics were laid flat and a full vacuum (approximately
complex fibre layouts, different matrix types, automated fibre layups, 100kPa) was then set over the plate and held during a cure time of a
autoclave fabrication, complex plate element stiffener arrangements, minimum of 15 h in a constant temperature room at 23 °C. The plates
etc. were fabricated with approximate dimensions of 250 mm width and
1200 mm length, then following curing were trimmed to size and cut
2.2. Materials into two specimens using a guillotine. The measured plate geometries
are summarised in Table 1. Exemplar plate specimens are shown in
Three different natural fibres were investigated in the present study; Fig. 1.
flax, jute and hemp. The flax and jute fabrics were commercially pro-
duced for fibre-resin composite fabrications by Composites Evolution; 2.4. Plate test rig
Biotex Flax 400 g/m2 2 × 2 Twill weave and Biotex Jute 400 g/m2 2 ×
2 Twill weave. Nominal density, tensile strength and modulus values The plates were tested with simple supports on all four sides (stif-
for the flax were; 1.5 g/cm3, 500 MPa and 50 GPa, and for the jute fened plates). The ends of the plates were seated in circular steel rods
were; 1.46 g/cm3, 400 MPa and 40 GPa. The hemp fabric was not with a 6 mm groove to accommodate plates up to 6 mm in thickness.
produced specifically for fibre-resin composite applications, however Shim plates were used to firmly seat the plates with thickness less than
was recommended as the most appropriate fabric for working with 6 mm. The grooved plate-seat rod was housed in a split needle bearing,
resins by the manufacturer, and was a plain weave 287 g/m2 pure allowing the rod to rotate freely in the solid steel bearing block (Fig. 2).
unbleached hemp fabric with density 1.48 g/cm3. The commercial bulk Each bearing block was 60 mm in width, and each grooved plate-seat
laminating epoxy resin Kinetix R240 with H160 (medium) hardener rod was 20 mm in width, allowing differential rotation across the plate
was used for all composite fabrications, with density 1.1 g/cm3. width. The upper bearings were fixed to the loading platen of the test
Compression and tension material tests of the neat epoxy resin and machine, and the lower bearings were fixed to the rigid base of the
fabricated fibre-resin composites were undertaken in accordance with machine. The plate end bearings have been used and validated pre-
ISO 604 [23] and ISO 527 [24], respectively. The fibre-resin composite viously by the author, and further details are provided in [26]. Simple
material specimens were cut from the fabricated plate specimens. Fibre supports along the plate longitudinal edges were achieved with Teflon
volume fractions were calculated using the mass of fabric prior to half-rounds that were lightly clamped to each side of the plate edge
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M.R. Bambach Thin-Walled Structures 119 (2017) 103–113
the plate specimens; 2, 3 and 4 fibre layers for the flax and jute chan-
nels, and 3, 4 and 6 fibre layers for the hemp channels.
The channels were fabricated with a hand layup technique whereby
each layer of fabric was wetted out with resin using a paint brush and
roller. The fabrics were laid over a mandrel, being a steel square hollow
section of outside dimension 100 mm and corner radius of 8 mm,
thereby all channels had an internal web depth of 100 mm. A full va-
cuum was then set over the channel and held during a cure time of a
minimum of 15 h in a constant temperature room at 23 °C. The chan-
nels were fabricated with approximate dimensions of flange width
70 mm and length 850 mm, then following curing were trimmed to size
and cut into two specimens using a water jet cutter. The measured
channel geometries are summarised in Table 2. Exemplar channel
specimens are shown in Fig. 3.
3. Results
3.1. Materials
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M.R. Bambach Thin-Walled Structures 119 (2017) 103–113
Table 2
Composite channel specimens and test results (dimensions refer to outside dimensions, subscript P refers to predicted values).
Fibre Layers Fibre weight Web Flanges Thick-ness EC fuC Fbuckle Fultimate λ FbuckleP Fbuckle/FbuckleP FultimateP Fultimate/FultimateP
(g/m2) (mm) (mm) (mm) (MPa) (MPa) (N) (N) (N) (N)
Flax 2 800 104.1 39.8 1.7 4199 38.5 949 2683 3.45 1527 0.62 3807 0.70
Flax 2 800 104.0 39.8 1.7 4199 38.5 982 2922 3.39 1526 0.64 3808 0.77
Flax 3 1200 105.5 41.2 2.5 4199 38.5 3898 6898 2.06 4439 0.88 7377 0.94
Flax 3 1200 105.9 41.4 2.5 4199 38.5 3667 6381 2.13 4402 0.83 7370 0.87
Flax 4 1600 107.5 41.3 3.3 4199 38.5 8933 11,023 1.58 11,406 0.78 12,950 0.85
Flax 4 1600 107.4 41.2 3.3 4199 38.5 9287 11,655 1.55 11,463 0.81 12,954 0.90
Jute 2 800 104.0 41.2 1.8 3523 40.2 825 2996 3.86 1299 0.64 3864 0.78
Jute 2 800 104.1 41.1 1.8 3523 40.2 1027 2967 3.46 1306 0.79 3864 0.77
Jute 3 1200 106.1 42.0 2.8 3523 40.2 4414 7678 2.10 5142 0.86 8731 0.88
Jute 3 1200 105.9 42.0 2.8 3523 40.2 4253 7611 2.14 5136 0.83 8733 0.87
Jute 4 1600 107.1 41.7 3.5 3523 40.2 7655 9555 1.79 11,259 0.68 13,791 0.69
Jute 4 1600 107.3 41.8 3.5 3523 40.2 7514 10,078 1.81 11,211 0.67 13,785 0.73
Hemp 3 861 104.8 41.8 2.2 2649 33.9 1031 1985 3.53 1799 0.57 4489 0.44
Hemp 3 861 104.6 42.1 2.2 2649 33.9 985 2207 3.62 1769 0.56 4487 0.49
Hemp 4 1148 106.2 41.2 2.7 2649 33.9 3205 4663 2.24 3812 0.84 6807 0.69
Hemp 4 1148 106.0 41.0 2.7 2649 33.9 2748 4903 2.41 3849 0.71 6812 0.72
Hemp 6 1722 109.0 41.5 3.9 2649 33.9 10,780 11,879 1.47 12,231 0.88 13,611 0.87
Hemp 6 1722 108.9 41.7 3.9 2649 33.9 11,687 13,262 1.41 12,088 0.97 13,607 0.97
Mean 0.75 Mean: 0.77
Table 3
Material properties of the composites and the epoxy resin (neat).
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M.R. Bambach Thin-Walled Structures 119 (2017) 103–113
Fig. 5. Exemplar composite plate test results; (a) flax, (b) jute, (c) hemp.
developed in the different plate specimens, the five transducers were 3.3. Channel tests
not necessarily located in the position of maximum out-of-plane dis-
placement in the plate, therefore these values provide upper bounds to The channel test results are summarised in Table 2. The channels
the buckling loads. typically demonstrated a similar response to the plates, including a
linear-elastic response followed by buckling, stable post-buckling, at-
tainment of the ultimate load and then stable unloading. The post-
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M.R. Bambach Thin-Walled Structures 119 (2017) 103–113
Fig. 8. Exemplar composite channel test results; (a) flax, (b) jute, (c) hemp.
buckling and ultimate load responses were both very stable, and in no transducers were used in the channel tests (one per flange and three in
cases was an unstable brittle fracture mode characterised by sudden the web), and since the flange transducer was frequently not in the
failure and loss of load carrying capacity evident. Exemplar axial force – position of maximum out-of-plane displacement (since many channels
axial displacement plots are provided in Fig. 8, while a plot with photos buckled in two half-waves rather than three), the buckling behaviour
of the deformed shape at different load levels is shown in Fig. 9. The was less well characterised by the transducers than with the plate
channels tests were continued until the load reduced to at least 80% of specimens. The channel buckling loads were therefore quantified using
the ultimate value, and the response demonstrated a very stable, gra- the change in section stiffness methodology, whereby the point of linear
dual unloading mechanism. elastic axial stiffness bifurcation was identified and the corresponding
The buckling modes consisted of two or three half-waves of buck- load taken as the section buckling load. Previous work on steel channel
ling, with no discernible relationship between material or dimensions sections by the author has indicated the validity of this methodology in
and the number of half-waves. The particular buckled shape was likely comparison with using the buckling deformation values [30]. Since the
a response to the geometric and/or material imperfections of the in- stiffness reduction occurs following buckling, these values provide
dividual specimen. Buckling occurred with approximately the same upper bounds to the section buckling loads.
half-wavelength in both the web and the flanges. Exemplar deformed
shapes at the ultimate condition for the three different fibres and their
thinnest and thickest specimens are shown in Fig. 10. Since fewer
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M.R. Bambach Thin-Walled Structures 119 (2017) 103–113
3.4. Failure mechanisms membrane strains in the two principle orthogonal directions, and
without significant shear stresses nor shear buckling, an isotropic
In both the composite plates and channels failure was precipitated theory was considered potentially appropriate [32]. Additionally, in-
by the localisation of the buckling into one of the half-waves, thereby dividual specimens had the same amount of fibre in the 0 and 90 di-
reaching large out-of-plane displacements in that half-wave, resulting rections, and since the elements were thin the through-thickness
in matrix failures along the critical fold lines. Exemplar failure me- properties were not especially important. The in-plane compression
chanisms are shown in Fig. 11, where the mechanisms in the plate and buckling and strength theory used for thin steel structures prone to out-
the channel web resemble the classic flipped disk mechanism, while of-plane buckling was assessed for the potential to be used for the de-
that in the channel flange resembles the inclined yield line mechanism. sign of natural fibre composite plates and channel sections.
It is interesting to note the similarities between these mechanisms and
yield lines that form in the plastic collapse mechanisms commonly
4.2. Buckling
observed in thin steel plates and channels [31].
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M.R. Bambach Thin-Walled Structures 119 (2017) 103–113
plates contain geometric and material imperfections while the theory (fuC).
assumes perfect plate properties. Similar results were found for the
channels (25%), as shown in Table 2 and Fig. 12b, where the lower of fuC
λ=
the theoretical buckling stresses calculated for the web and flanges was fcr (2)
taken as the buckling stress for the section.
0 . 22
Aeffective 1−
kπ 2E t 2 ρ= = λ
fcr = ⎛ ⎞ A λ (3)
12(1 − υ2) ⎝ b ⎠ (1)
These formulae are based on the effective width principle, which
states that the post-buckling strength is obtained when the unbuckled
4.3. Strength portions of the plate elements reach the ultimate stress of the material,
while the buckled portions are assumed ineffective in carrying load
The Winter strength formulae [34] used for the design of thin steel [34]. This mechanics model is a reasonable assumption for the com-
sections in several international cold-formed steel design codes [35,36] posite plates in the present study. The theory is based on two calcula-
are given by Eqs. (2) and (3), where λ is the plate or section slenderness, tions: first, the buckling stress must be established, and from this value
fuC is the material ultimate stress in compression, ρ is the plate or sec- the slenderness is calculated; second, the post-buckling strength is es-
tion effectiveness ratio (the ratio of the effective area to the gross area tablished from the known value of slenderness using the Winter equa-
of the plate or section) and A is the plate or section area. For steel the tion. While the basic form of the Winter equation is given by Eq. (3), it
ultimate stress is taken as the tensile yield stress, however for the is well known that this strength curve typically needs to be empirically
purposes of the present composite materials the ultimate compression adjusted according to the specific material and/or geometric and/or
stress was used (Table 3). The plate or section strength is then calcu- loading conditions at hand. For this purpose plate experiments are ty-
lated as the effective area multiplied by the ultimate compression stress pically employed [37]. In the present study, the experimental buckling
Fig. 12. Comparisons of experimental and theoretical buckling stresses; (a) composite plates, (b) composite channels.
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M.R. Bambach Thin-Walled Structures 119 (2017) 103–113
Fig. 13. Comparisons of experimental and theoretical strengths; (a) composite plates, (b) composite channels.
stresses in the plate tests were used to calculate the experimental plate strengths between 35.3 MPa and 52.1 MPa and tensile moduli between
slenderness values, and these values were plotted against the effec- 3.8 GPa and 6.0 GPa. In the literature a wide variety of mechanical
tiveness ratio (Aeffective/A) established from the experimental plate properties for natural fibre composites have been documented, the
strength. In this calculation it was assumed that 5 mm of plate width on values of which may vary due to the broad range of possible fibre
either side of the Teflon half-round longitudinal supports did not treatments, fabric types, resin types, fibre laying processes, fabrication
buckle. The results are shown in Fig. 13a, where it is evident that the and curing techniques, etc. For example Pickering et al. [5] reviewed
traditional Winter Eq. (3) over-estimates many plate strengths. A re- many published values of various fibres, resins and fibre volume frac-
duced Winter effective width Eq. (4) was established simply by making tions, reporting that unidirectional hemp composites had (tensile
empirical adjustments to the Winter equation until an approximate strength, tensile moduli) values between (77 MPa, 10 GPa) and
lower bound to the test results was achieved (Fig. 13a) [37]. (165 MPa, 17 GPa), while unidirectional flax composites had values
1.5
between (40 MPa, 7 GPa) and (321 MPa, 29 GPa). They also noted
0 . 22
⎛1 − λ ⎞ biaxial hemp values of (62 MPa, 7 GPa) and woven jute values of
ρ=⎜ ⎟
λ (50 MPa, 8 GPa). Costa and D’Almeida [9] tested unidirectional jute
⎝ ⎠ (4)
epoxy resin composites with fibre volume fractions of 10%, noting
The empirical strength Eq. (4) derived from the plate tests was then values of (50.3 MPa, 4.02 GPa). Hargitai et al. [10] tested unidirec-
compared with the channel sections for validation. As with the plates, tional hemp polypropylene composites with fibre mass fractions of
the experimental channel buckling stresses were used to calculate the 40%, finding values of (56 MPa, 5.9 GPa). Oksman [11] tested uni-
experimental channel slenderness values, and these values were plotted directional flax epoxy resin composites with fibre volume fractions of
against the effectiveness ratio established from the experimental 32%, noting values of (132 MPa, 15 GPa), and high performance Artic
channel strengths. The results are shown in Fig. 13b, where it is evident flax with fibre volume fractions of 42% with values of (280 MPa,
that in accordance with the plate tests, the traditional Winter equation 35 GPa). Van de Weyenberg et al. [12] tested unidirectional flax epoxy
over-predicted the strengths of the channels, while the empirical Eq. (4) resin composites with fibre volume fractions of 40%, finding values of
provides a more realistic estimate. (133 MPa, 28 GPa). Weclawski et al. [8] tested unidirectional hemp
Having established an appropriate strength equation for the natural polyester resin composites with fibre volume fractions of 30%, finding
fibre composite channel sections, this equation was used to calculate tension values of (128.9 MPa, 8.9 GPa) and compression values of
design values for the channel compression strengths. In the design (53 MPa, 3.83 GPa). In comparison with unidirectional composites,
procedure the buckling stresses of the web and flanges are those the- woven biaxial composites will have material properties much less than
oretical values calculated from Eq. (1), from which the slenderness the unidirectional values (for the same volume of fibres), since half of
values of the web and flanges are derived from Eq. (2), and following the fibres contribute little to the unidirectional strength, and the weave
which the strength of the channel section is established from Eq. (4). further reduces the fibre effectiveness compared with unidirectional
These values are compared with the test strengths in Table 2, where layers. Notwithstanding this, the mechanical properties of the compo-
they over-predict the test strengths on average by 23%. This stems from sites fabricated in the present study are towards the lower end of pre-
the fact that the theoretical buckling stress values over-predict the ex- viously published values.
perimental values on average by 25% (Table 2). As demonstrated in Importantly, while the mechanical properties of natural fibre com-
Fig. 13b, when the experimental buckling stress values are used the posites are relatively low, the buckling and post-buckling responses
modified strength Eq. (4) predicts the strength reasonably well, and were shown to be stable, the ultimate condition was reached in a stable
when these values are employed in place of the theoretical values from and predictable manner, and the failure ensued in a gradual and ductile
Eq. (1) the over-prediction of the section strength reduces to 7%. process. These stable compression characteristics imply an inherent
However, in a design situation these values would not be known a- suitability for structural applications. The relatively modest compres-
priori, therefore improvements to the prediction of the buckling stresses sion strengths lend themselves to light structural applications, poten-
are required in order to improve the theoretical strength predictions. tially in the residential and light commercial markets. For comparison
purposes, design compression loads for Australian domestic stud wall
columns were extracted from AS1720 [38], using standard conditions
5. Discussion
(moderate wind loads, factored dead and live loads, 2.7 m wall height,
sheet roof, plasterboard claddings, etc). For 0.6 m stud spacings, one
In the present study the intrinsic mechanical properties of the nat-
and two storey house loads are 4.5 kN and 9 kN respectively, while for
ural fibre composites were shown to be relatively low, with tensile
111
M.R. Bambach Thin-Walled Structures 119 (2017) 103–113
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M.R. Bambach Thin-Walled Structures 119 (2017) 103–113
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