Emsl Vapor Full Devilerables 491700245njdep Extended Deliverable Package

EMSL Analytical EMSL Order #: 491700245
200 Route 130 North, Cinnaminson, NJ 08077

Phone/Fax: (856)858-4800 / (856)858-4571 Customer ID: RLGE77
http://www.EMSL.com to15lab@EMSL.com Customer PO: Not Available
Attn: Rakesh Ganta Phone: 201-509-8333

RLG Environmental, Inc. Fax: 201-509-8336
32 Bushes Lane
1st Floor
Elmwood Park, NJ 07407 Collected: 2/23/2017
Project: 81 Main Street Received: 2/28/2017
Laboratory Report- Sample Summary

EMSL Sample ID. Client Sample ID. Start Sampling Date Start Sampling Time
491700245-0001 81-WC-1 2/23/2017 11:46 AM
491700245-0002 81-CS-1 2/23/2017 12:20 PM
491700245-0003 81-AA-1 2/23/2017 1:22 PM
491700245-0004 81-K-1 2/23/2017 12:08 PM
491700245-0005 81-WC-2 2/23/2017 11:43 AM
491700245-0006 81-K-2 2/23/2017 12:11 PM
491700245-0007 81-NC-1 2/23/2017 1:01 PM
491700245-0008 81-HS-1 2/23/2017 12:37 PM
491700245-0009 81-MR-1 2/23/2017 12:45 PM
If "Preliminary Report" is displayed in the signature box; this indicates that there are samples that have not yet been analyzed, that are in a preliminary state, or
that analysis is in progress but not completed at the time of report issue.
Report Date: Report Revision Revision Comments

3/10/2017 R0 Initial Report
Marjorie Howley, Laboratory Manager

or other approved signatory
Test results meet all NELAP requirements unless otherwise specified.
491700245-0001_R0 V19 Page 1 of 5

NJDEP Regulatory Format Extended Data Report
General Documents
External Chain of Custody (External documentation and Field Test Data Sheets) 1
Internal Chain of Custody 3
Shipping Documentation- Air bills, Sample Receipt Checklist 5
Copies of Traceability Certificates from Commercial Gas Standard Suppliers 10
Methodology Summary 20
Case Narrative 21
NJDEP- SRP Air Methods Data Summary Tables (Data Sheets in Excel) 23
Method Detection Limit Summary 100
Verified Method Detection Limit Summary 103
QC Summary Data
Reporting Limit Laboratory Control Sample (RLLCS) 107
Method Blank Summary 116
Instrument Performance Check Summary (BFB) 119
Internal Standard Area and Retention Time Summary 123
Sample Data
Sample Lab Data Summary- (with supporting raw data) 128

Standards Data- (with supporting raw data)
Initial Calibration Form Summary 502
Initial Calibration Verification Sample Standard Summary (ICVSS) 527
Continuing and Closing Calibration Verification Summary (CCVS, ECVS) 539
Raw QC Data -(with supporting raw data)
GC/MS Tune Performance Data (BFB) 584
Blank Data (Method and Instrument Blanks) 592
Reporting Limit Laboratory Control Sample Data (RLLCS) 674
Clean Canister Certification Data
Reporting Limit Laboratory Control Sample (RLLCS) 702
Method Blank Summary and Data Report 708
Instrument Performance Check (BFB) 718
Internal Standard Area and Retention Time Summary 722
Clean Canister Data (with supporting raw data). 726
Initial Calibration Summary 756
Initial Calibration Verification Sample Standard Summary (ICVSS) 762
Continuing Calibration Summary(s) including Closing (CCVS, ECVS) 774
Sample Preparation Data
Instrument Run Logs (sample data run logs) 785
Instrument Run Logs (clean canister run logs) 789
Pressure Gauge Readings 793
Canister Dilution Calculation (If Applicable) NA
Screening Data NA
Please visit our website at http://www.emsl.com

© 2012, EMSL Analytical, Inc., All rights reserved. No part of this report may be reproduced or otherwise distributed or used without the express written consent of EMSL.
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32 Bushes Lane
1st Floor
Case Narrative
Method Reference
USEPA: Compendium Method TO-15, “Determination of Volatile Organic Compounds (VOCs) in Air…" Collected in Specially-Prepared Canisters and Analyzed by
Gas Chromatography/Mass Spectrometry (GC/MS), January 1999, (EPA/625/R-96/010b).
Column
Restek RTX-502.2, 60m, 0.25mm ID, 1.4um
Concentrator Traps:
Entech Dual Cold Traps: (1) 1/8” No Packing, (2) 1/8” Tenax.
Gas Standards:
Certified Spectra Gas standards were used for all analyses.
Sample Volumes:
Sample volume aliquots for this procedure are 250cc for indoor/ ambient air and 25cc for soil gas. Other volumes for sample dilutions are reflected on each result
page.
Holding Times:
Standard holding times of 30 days were met for all samples.
Sampling Pressures:
All samples were received at acceptable pressure/vacuum unless listed below.
Sample Dilutions:
Dilutions reported are designated by the sample # with a "DL" suffix resulting from initial analysis having compounds exceeding calibration as reported with an "E"
qualifier.
Ethanol are Isopropanol are not diluted for and may be reported with an "E" qualifier on the final result.
QA/QC criteria outside method specifications are listed below (if applicable).
Initial Calibration
All Initial Calibration criteria met method specification.
Initial Calibration Verification Standard (ICVS)- Second Source

ICVS met method specification with 90% of all compounds within the established recovery range. Individual compounds outside of the established recovery range
may be listed below.
Continuing Calibration Verification Standard (CCVS)

CCVS met method specification with all compounds within 30% deviation.
Ending Calibration Verification Standard (ECVS)

ECVS met method specification with all compounds within 30% deviation.
Method Blanks (MB)

Method Blank met method specification.
Instrument Blanks (IB):

IBIB030217L-B had compound(s)tetrachloroethene reported at 6.4ppbv.
IB030217L-A, IB030217L-C, IB030717L-A, IB030717L-B and IBIB030817L-A were analyzed with no compounds reported.
Reporting Limit Laboratory Control Samples (RLLCS)
RLLCS met method specification with 90% of compounds within the 60-140% recovery range. Individual compounds outside of the recovery range may be listed below.
Manual Integration : -Listed below if applicable. Before and after documentation is included.
L9296, L9297, L9300, L9304 - PCE
491700245-0001_R0 V19 Page 1 of 2

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32 Bushes Lane
1st Floor
Case Narrative
Method 491700245-12
Sample Reference had a small hit for PCE in the initial run (L9299.D). The analyst suspected carryover from 491700245-11. On the reanalysis
(L9303.D) no PCE was detected @>RL, this second analysis was reported. Several samples required muliple dilutions in order to place PCE within
calibration range due to peak saturation. Only the final dilutions are reported in the "results" but all will be presented in the deliverables package.
The following data qualifiers that may have been reported with the data,
ND- Non Detect. This notation would be used in the results column in lieu of a "U" qualifier.
U- Compound was analyzed for but not detected at a listed and appropriately adjusted reporting level.
J- Estimated value reported below adjusted reporting limit for target compounds or estimating a concentration for TICs where a 1:1 response is assumed
B- Compound found in associated method blank as well as in the sample.
E- Estimated value exceeding upper calibration range of instrument. Ethanol and isopropyl alcohol are not specifically targeted to dilute within calibration range.
D- Compound reported from additional diluted analysis.
N- indicates presumptive evidence of a compound based on library search match.
EMSL Analytical, Inc. certifies that this data package is in compliance with the terms and conditions of this contract, both technically and for completeness, for other than the conditions
detailed above. Release of the data contained in this hardcopy data package and in the computer –readable data submitted on diskette has been authorized by the laboratory manager or
his/her designee, as verified by the following signature.
If "Preliminary Report" is displayed in the signature box; this indicates that there are samples that have not yet been analyzed, that are in a preliminary state, or
that analysis is in progress but not completed at the time of report issue.
Report Date: Report Revision Revision Comments

R0 Initial Report
Scott Van Etten, CIH/Jefferson Salvador

or other approved signatory
Test results meet all NELAP requirements unless otherwise specified.
491700245-0001_R0 V19 Page 2 of 2

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Project: 491700245 TARGET/NON TARGET ANALYTES - Sampling Date: 02/23/2017
Field ID Number: 81-WC-1 AIR RESULTS Analysis Date: 03/07/2017
Laboratory ID Number: 03036
CAS Molecular Lab Q Corrected Retention QAS Foot-

Chemical Number Weight Results Results Time Decision notes
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Method TO-15 ppbv ug/m3

Acetone 67-64-1 58.08 51 E 120
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.35 1.1
Bromodichloromethane 75-27-4 163.8 0.20 U 1.3
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 3.0 7.2
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.50 1.0
Carbon disulfide 75-15-0 76.14 0.50 U 1.6
Carbon tetrachloride 56-23-5 153.8 0.20 U 1.3
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
Dibromochloromethane 124-48-1 208.3 0.20 U 1.7
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,2-Dichlorobenzene 95-50-1 147.0 0.20 U 1.2
Dichlorodifluoromethane 75-71-8 120.9 0.20 U 1.0
1,1-Dichloroethane 75-34-3 98.96 0.20 U 0.81
1,1-Dichloroethene 75-35-4 96.94 0.20 U 0.79
1,2-Dichloroethene (cis) 156-59-2 96.94 0.20 U 0.79
1,2-Dichloroethene (trans) 156-60-5 96.94 0.20 U 0.79
1,2-Dichloropropane 78-87-5 113.0 0.20 U 0.92
1,3-Dichloropropene (cis) 10061-01-5 111.0 0.20 U 0.91
1,3-Dichloropropene (trans) 10061-02-6 111.0 0.20 U 0.91
1,2-Dichlorotetrafluoroethane 76-14-2 170.9 0.20 U 1.4
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 39 74
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
1,3-Hexachlorobutadiene 87-68-3 260.8 0.20 U 2.1
n-Hexane 110-54-3 86.17 0.26 0.93
Isopropanol 67-63-0 60.10 2.1 5.1
Methylene chloride 75-09-2 84.94 0.26 0.90
Methyl ethyl ketone 78-93-3 72.10 0.56 1.6
Methyl isobutyl ketone 108-10-1 100.2 0.20 U 0.82
Methyl methacrylate 80-62-6 100.12 0.20 U 0.82
Methyl tert-butyl ether 1634-04-4 88.15 0.20 U 0.72
Styrene 100-42-5 104.1 0.20 U 0.85
Tert-butyl alcohol 75-65-0 74.12 0.20 U 0.61
1,1,2,2-Tetrachloroethane 79-34-5 167.9 0.20 U 1.4
Tetrachloroethene 127-18-4 165.8 0.75 5.1
Tetrahydrofuran 109-99-9 72.11 0.27 0.81
Toluene 108-88-3 92.14 1.0 3.9
1,2,4-Trichlorobenzene 120-82-1 181.5 0.20 U 1.5
1,1,1-Trichloroethane 71-55-6 133.4 0.20 U 1.1
Trichloroethene 79-01-6 131.4 0.26 1.4
Trichlorofluoromethane 75-69-4 137.4 0.24 1.4
1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 187.4 0.20 U 1.5
1,2,4-Trimethylbenzene 95-63-6 120.2 0.20 U 1.0
2,2,4-Trimethylpentane 540-84-1 114.2 0.20 U 0.93
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.40 U 1.7
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Laboratory Name: EMSL Analytical, Inc. Revision March 2007
Laboratory City: Cinnaminson, NJ
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Xylene (o) 95-47-6 106.2 0.20 U 0.87
Volatile Tentatively Identified Compounds (upto 30 compounds)
Difluorochloromethane 000075-45-6 86 8.4 JN 29 4.93
Alkane-Butane, 2-methyl- 000078-78-4 72 3.1 JN 9.2 6.58
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Field ID Number: 81-WC-1DL AIR RESULTS Analysis Date: 03/08/2017

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Acetone 67-64-1 58.08 53 130
Allyl chloride 107-05-1 76.53 0.40 U 1.3
Benzene 71-43-2 78.11 0.40 U 1.3
Bromoform 75-25-2 252.8 0.40 U 4.1
Bromomethane 74-83-9 94.94 0.40 U 1.6
1,3-Butadiene 106-99-0 54.09 0.40 U 0.88
n-Butane 106-97-8 58.12 3.0 7.0
Chlorobenzene 108-90-7 112.6 0.40 U 1.8
Chloroethane 75-00-3 64.52 0.40 U 1.1
Chloroform 67-66-3 119.4 0.40 U 2.0
Chloromethane 74-87-3 50.49 0.50 1.0
2-Chlorotoluene 95-49-8 126.6 0.40 U 2.1
Cyclohexane 110-82-7 84.16 0.40 U 1.4
1,2-Dibromoethane 106-93-4 187.8 0.40 U 3.1
1,4-Dioxane 123-91-1 88.12 1.0 U 3.6
Ethanol 64-17-5 46.07 42 80
Ethylbenzene 100-41-4 106.2 0.40 U 1.7
4-Ethyltoluene 622-96-8 120.2 0.40 U 2.0
n-Heptane 142-82-5 100.2 0.40 U 1.6
n-Hexane 110-54-3 86.17 0.40 U 1.4
Isopropanol 67-63-0 60.10 2.3 5.6
Methylene chloride 75-09-2 84.94 0.40 U 1.4
Styrene 100-42-5 104.1 0.40 U 1.7
Tetrahydrofuran 109-99-9 72.11 0.40 U 1.2
Toluene 108-88-3 92.14 1.0 3.8
Trichloroethene 79-01-6 131.4 0.40 U 2.1
Trichlorofluoromethane 75-69-4 137.4 0.40 U 2.2
Vinyl bromide 593-60-2 106.9 0.40 U 1.7
Vinyl chloride 75-01-4 62.50 0.40 U 1.0
Xylene (m,p) 1330-20-7 106.2 0.80 U 3.5
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Xylene (o) 95-47-6 106.2 0.40 U 1.7
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Field ID Number: 81-CS-1 AIR RESULTS Analysis Date: 03/08/2017

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Acetone 67-64-1 58.08 59 E 140
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.42 1.3
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 6.2 15
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.32 1.6
Chloromethane 74-87-3 50.49 0.55 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,2-Dichloroethane 107-06-2 98.96 0.37 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 23 44
Ethylbenzene 100-41-4 106.2 0.32 1.4
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.75 3.1
n-Hexane 110-54-3 86.17 0.52 1.8
Isopropanol 67-63-0 60.10 7.1 17
Methylene chloride 75-09-2 84.94 4.7 16
Methyl ethyl ketone 78-93-3 72.10 6.1 18
Methyl isobutyl ketone 108-10-1 100.2 0.29 1.2
Styrene 100-42-5 104.1 0.20 U 0.85
Tetrachloroethene 127-18-4 165.8 9.7 66
Tetrahydrofuran 109-99-9 72.11 4.7 14
Toluene 108-88-3 92.14 7.5 28
Trichloroethene 79-01-6 131.4 22 120
2,2,4-Trimethylpentane 540-84-1 114.2 0.25 1.2
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 1.1 4.6
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Xylene (o) 95-47-6 106.2 0.35 1.5
Unknown 92 2.4 JN 9 5.28
Unknown 92 1.1 JN 4.1 10.68
D-Limonene 005989-27-5 136 1.6 JN 9 24.23
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Field ID Number: 81-CS-1DL AIR RESULTS Analysis Date: 03/08/2017

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Acetone 67-64-1 58.08 59 140
Allyl chloride 107-05-1 76.53 0.40 U 1.3
Benzene 71-43-2 78.11 0.44 1.4
Bromoform 75-25-2 252.8 0.40 U 4.1
Bromomethane 74-83-9 94.94 0.40 U 1.6
1,3-Butadiene 106-99-0 54.09 0.40 U 0.88
n-Butane 106-97-8 58.12 6.1 14
Chlorobenzene 108-90-7 112.6 0.40 U 1.8
Chloroethane 75-00-3 64.52 0.40 U 1.1
Chloroform 67-66-3 119.4 0.40 U 2.0
Chloromethane 74-87-3 50.49 0.59 1.2
2-Chlorotoluene 95-49-8 126.6 0.40 U 2.1
Cyclohexane 110-82-7 84.16 0.40 U 1.4
1,2-Dibromoethane 106-93-4 187.8 0.40 U 3.1
1,4-Dioxane 123-91-1 88.12 1.0 U 3.6
Ethanol 64-17-5 46.07 25 46
Ethylbenzene 100-41-4 106.2 0.40 U 1.7
4-Ethyltoluene 622-96-8 120.2 0.40 U 2.0
n-Heptane 142-82-5 100.2 0.80 3.3
n-Hexane 110-54-3 86.17 0.53 1.9
Isopropanol 67-63-0 60.10 7.5 19
Styrene 100-42-5 104.1 0.40 U 1.7
Tetrachloroethene 127-18-4 165.8 10 68
Toluene 108-88-3 92.14 7.7 29
Vinyl bromide 593-60-2 106.9 0.40 U 1.7
Vinyl chloride 75-01-4 62.50 0.40 U 1.0
Xylene (m,p) 1330-20-7 106.2 1.0 4.5
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Xylene (o) 95-47-6 106.2 0.40 U 1.7
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Field ID Number: 81-AA-1 AIR RESULTS Analysis Date: 03/08/2017

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Acetone 67-64-1 58.08 4.4 10
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.44 1.4
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 3.3 7.7
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.21 1.0
Chloromethane 74-87-3 50.49 0.49 1.0
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 5.7 11
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.30 1.1
Isopropanol 67-63-0 60.10 3.5 8.5
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.72 2.7
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.40 U 1.7
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Xylene (o) 95-47-6 106.2 0.20 U 0.87
Unknown 92 1.3 JN 4.9 4.93
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Field ID Number: 81-K-1 AIR RESULTS Analysis Date: 03/08/2017

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Acetone 67-64-1 58.08 14 34
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.60 1.9
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 6.9 16
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.50 2.4
Chloromethane 74-87-3 50.49 0.56 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dichlorobenzene 106-46-7 147.0 0.24 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 150 E 290
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.52 2.1
n-Hexane 110-54-3 86.17 0.38 1.3
Isopropanol 67-63-0 60.10 4.7 12
Styrene 100-42-5 104.1 0.24 1.0
Toluene 108-88-3 92.14 2.4 8.9
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.52 2.3
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Xylene (o) 95-47-6 106.2 0.20 U 0.87
Alkane-Isobutane 000075-28-5 58 2.1 JN 5.0 5.29
Ethyl Acetate 000141-78-6 88 1.2 JN 4.2 11.24
Hexanal 000066-25-1 100 1.0 JN 4.2 17.98
Benzaldehyde 000100-52-7 106 1.5 JN 6.7 23.93
D-Limonene 005989-27-5 136 2.1 JN 12 24.24
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Acetone 67-64-1 58.08 43 E 100
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.37 1.2
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 3.2 7.6
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.54 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 40 75
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.22 0.92
n-Hexane 110-54-3 86.17 0.27 1.0
Isopropanol 67-63-0 60.10 1.9 4.6
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 1.1 4.1
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.42 1.8
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Xylene (o) 95-47-6 106.2 0.20 U 0.87
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Acetone 67-64-1 58.08 43 100
Allyl chloride 107-05-1 76.53 0.40 U 1.3
Benzene 71-43-2 78.11 0.40 U 1.3
Bromoform 75-25-2 252.8 0.40 U 4.1
Bromomethane 74-83-9 94.94 0.40 U 1.6
1,3-Butadiene 106-99-0 54.09 0.40 U 0.88
n-Butane 106-97-8 58.12 3.2 7.6
Chlorobenzene 108-90-7 112.6 0.40 U 1.8
Chloroethane 75-00-3 64.52 0.40 U 1.1
Chloroform 67-66-3 119.4 0.40 U 2.0
Chloromethane 74-87-3 50.49 0.52 1.1
2-Chlorotoluene 95-49-8 126.6 0.40 U 2.1
Cyclohexane 110-82-7 84.16 0.40 U 1.4
1,2-Dibromoethane 106-93-4 187.8 0.40 U 3.1
1,4-Dioxane 123-91-1 88.12 1.0 U 3.6
Ethanol 64-17-5 46.07 44 82
Ethylbenzene 100-41-4 106.2 0.40 U 1.7
4-Ethyltoluene 622-96-8 120.2 0.40 U 2.0
n-Heptane 142-82-5 100.2 0.40 U 1.6
n-Hexane 110-54-3 86.17 0.40 U 1.4
Isopropanol 67-63-0 60.10 2.0 4.9
Styrene 100-42-5 104.1 0.40 U 1.7
Toluene 108-88-3 92.14 1.1 4.1
Vinyl bromide 593-60-2 106.9 0.40 U 1.7
Vinyl chloride 75-01-4 62.50 0.40 U 1.0
Xylene (m,p) 1330-20-7 106.2 0.80 U 3.5
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Xylene (o) 95-47-6 106.2 0.40 U 1.7
Page 22
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Page 23
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Acetone 67-64-1 58.08 8.9 21
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.48 1.5
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 4.6 11
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.43 2.1
Chloromethane 74-87-3 50.49 0.55 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 85 E 160
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.33 1.4
n-Hexane 110-54-3 86.17 0.33 1.2
Isopropanol 67-63-0 60.10 4.5 11
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 1.6 6.1
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.47 2.0
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Xylene (o) 95-47-6 106.2 0.20 U 0.87
D-Limonene 005989-27-5 136 1.1 JN 6.1 24.23
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Page 26
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Field ID Number: 81-NC-1 AIR RESULTS Analysis Date: 03/08/2017

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Acetone 67-64-1 58.08 9.8 23
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.35 1.1
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 3.5 8.4
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 1.0
Chloromethane 74-87-3 50.49 0.52 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 93 E 170
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.23 0.93
n-Hexane 110-54-3 86.17 0.28 1.0
Isopropanol 67-63-0 60.10 4.7 12
Styrene 100-42-5 104.1 0.40 1.7
Toluene 108-88-3 92.14 1.3 4.9
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.44 1.9
Page 27
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Xylene (o) 95-47-6 106.2 0.20 U 0.87
Unknown 92 3.9 JN 15 4.91
D-Limonene 005989-27-5 136 2.3 JN 13 24.23
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Page 29
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Field ID Number: 81-HS-1 AIR RESULTS Analysis Date: 03/08/2017

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Acetone 67-64-1 58.08 28 68
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.52 1.7
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 9.9 23
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.30 1.4
Chloromethane 74-87-3 50.49 0.52 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 16 29
Ethylbenzene 100-41-4 106.2 0.35 1.5
4-Ethyltoluene 622-96-8 120.2 0.23 1.1
n-Heptane 142-82-5 100.2 0.86 3.5
n-Hexane 110-54-3 86.17 0.43 1.5
Isopropanol 67-63-0 60.10 5.4 13
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 7.2 27
1,2,4-Trimethylbenzene 95-63-6 120.2 0.23 1.1
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 1.0 4.4
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Xylene (o) 95-47-6 106.2 0.34 1.5
Unknown 92 4.9 JN 18 4.92
Unknown 92 6.1 JN 23 5.30
Alkane-Pentane, 2-methyl- 000107-83-5 86 1.0 JN 3.6 8.70
Unknown 92 5.6 JN 21 10.68
Ethyl Acetate 000141-78-6 88 2.5 JN 8.9 11.24
Alkane-Hexane, 2-methyl- 000591-76-4 100 1.1 JN 4.3 11.76
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Page 32
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Field ID Number: 81-MR-1 AIR RESULTS Analysis Date: 03/08/2017

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Acetone 67-64-1 58.08 15 35
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.43 1.4
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 5.6 13
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 1.2 5.8
Chloromethane 74-87-3 50.49 0.53 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
Dichlorodifluoromethane 75-71-8 120.9 0.27 1.4
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 180 E 350
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.56 2.3
n-Hexane 110-54-3 86.17 0.44 1.6
Isopropanol 67-63-0 60.10 4.2 10
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 2.5 9.4
Trichloroethene 79-01-6 131.4 1.9 10
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.57 2.5
Page 33
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Xylene (o) 95-47-6 106.2 0.20 U 0.87
Unknown 92 7.0 JN 26 4.92
Unknown 92 2.4 JN 9.1 5.29
Alkane-Butane, 2-methyl- 000078-78-4 72 5.9 JN 17 6.59
Unknown 92 2.1 JN 7.7 10.68
Ethyl Acetate 000141-78-6 88 1.3 JN 4.5 11.24
Hexanal 000066-25-1 100 4.0 JN 17 17.98
D-Limonene 005989-27-5 136 4.6 JN 25 24.23
Nonanal 000124-19-6 142 1.6 JN 9.1 25.37
Unknown 92 1.4 JN 5.3 28.14
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Page 35
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Field ID Number: 81-CS-1SS AIR RESULTS Analysis Date: 03/02/2017

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Acetone 67-64-1 58.08 60 140
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 4.8 15
Bromodichloromethane 75-27-4 163.8 2.0 U 13
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 8.5 41
Chloromethane 74-87-3 50.49 2.0 U 4.1
Carbon disulfide 75-15-0 76.14 5.0 U 16
Carbon tetrachloride 56-23-5 153.8 2.0 U 13
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
Dibromochloromethane 124-48-1 208.3 2.0 U 17
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,2-Dichlorobenzene 95-50-1 147.0 2.0 U 12
Dichlorodifluoromethane 75-71-8 120.9 2.0 U 10
1,2-Dichloroethene (cis) 156-59-2 96.94 1300 E 5200
1,2-Dichloroethene (trans) 156-60-5 96.94 19 77
1,2-Dichlorotetrafluoroethane 76-14-2 170.9 2.0 U 14
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 26 48
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
1,3-Hexachlorobutadiene 87-68-3 260.8 2.0 U 21
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.10 11 28
Styrene 100-42-5 104.1 2.0 U 8.5
1,1,2,2-Tetrachloroethane 79-34-5 167.9 2.0 U 14
Tetrachloroethene 127-18-4 165.8 1100 E 7600
Toluene 108-88-3 92.14 2.0 U 7.5
1,2,4-Trichlorobenzene 120-82-1 181.5 2.0 U 15
1,1,1-Trichloroethane 71-55-6 133.4 2.0 U 11
Trichloroethene 79-01-6 131.4 880 E 4700
Trichlorofluoromethane 75-69-4 137.4 2.0 U 11
1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 187.4 2.0 U 15
1,2,4-Trimethylbenzene 95-63-6 120.2 2.0 U 10
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.50 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
Page 36
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Xylene (o) 95-47-6 106.2 2.0 U 8.7
Page 37
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Page 38
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Field ID Number: 81-CS-1SSDL AIR RESULTS Analysis Date: 03/03/2017

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Acetone 67-64-1 58.08 55 130
Allyl chloride 107-05-1 76.53 12 U 38
Benzene 71-43-2 78.11 12 U 38
Bromodichloromethane 75-27-4 163.8 12 U 80
Bromoform 75-25-2 252.8 12 U 120
Bromomethane 74-83-9 94.94 12 U 47
1,3-Butadiene 106-99-0 54.09 12 U 27
n-Butane 106-97-8 58.12 12 U 29
Chlorobenzene 108-90-7 112.6 12 U 55
Chloroethane 75-00-3 64.52 12 U 32
Chloroform 67-66-3 119.4 12 U 59
Chloromethane 74-87-3 50.49 12 U 25
Carbon disulfide 75-15-0 76.14 30 U 93
Carbon tetrachloride 56-23-5 153.8 12 U 75
2-Chlorotoluene 95-49-8 126.6 12 U 62
Cyclohexane 110-82-7 84.16 12 U 41
Dibromochloromethane 124-48-1 208.3 12 U 100
1,2-Dibromoethane 106-93-4 187.8 12 U 92
1,2-Dichlorobenzene 95-50-1 147.0 12 U 72
Dichlorodifluoromethane 75-71-8 120.9 12 U 59
1,1-Dichloroethane 75-34-3 98.96 12 U 49
1,1-Dichloroethene 75-35-4 96.94 12 U 48
1,2-Dichloroethene (cis) 156-59-2 96.94 1200 4900
1,2-Dichloropropane 78-87-5 113.0 12 U 55
1,3-Dichloropropene (cis) 10061-01-5 111.0 12 U 54
1,3-Dichloropropene (trans) 10061-02-6 111.0 12 U 54
1,2-Dichlorotetrafluoroethane 76-14-2 170.9 12 U 84
1,4-Dioxane 123-91-1 88.12 30 U 110
Ethanol 64-17-5 46.07 33 63
Ethylbenzene 100-41-4 106.2 12 U 52
4-Ethyltoluene 622-96-8 120.2 12 U 59
n-Heptane 142-82-5 100.2 12 U 49
1,3-Hexachlorobutadiene 87-68-3 260.8 12 U 130
n-Hexane 110-54-3 86.17 12 U 42
Isopropanol 67-63-0 60.10 30 U 74
Methylene chloride 75-09-2 84.94 12 U 42
Methyl ethyl ketone 78-93-3 72.10 12 U 35
Methyl isobutyl ketone 108-10-1 100.2 12 U 49
Methyl methacrylate 80-62-6 100.12 12 U 49
Methyl tert-butyl ether 1634-04-4 88.15 12 U 43
Styrene 100-42-5 104.1 12 U 51
Tert-butyl alcohol 75-65-0 74.12 12 U 36
1,1,2,2-Tetrachloroethane 79-34-5 167.9 12 U 82
Tetrahydrofuran 109-99-9 72.11 12 U 35
Toluene 108-88-3 92.14 12 U 45
1,2,4-Trichlorobenzene 120-82-1 181.5 12 U 89
1,1,1-Trichloroethane 71-55-6 133.4 12 U 65
Trichlorofluoromethane 75-69-4 137.4 12 U 67
1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 187.4 12 U 92
1,2,4-Trimethylbenzene 95-63-6 120.2 12 U 59
2,2,4-Trimethylpentane 540-84-1 114.2 12 U 56
Vinyl bromide 593-60-2 106.9 12 U 52
Vinyl chloride 75-01-4 62.50 12 U 31
Xylene (m,p) 1330-20-7 106.2 24 U 100
Page 39
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Xylene (o) 95-47-6 106.2 12 U 52
Page 40
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Page 41
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Field ID Number: 81-MR-1SS AIR RESULTS Analysis Date: 03/02/2017

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Acetone 67-64-1 58.08 170 400
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 2.0 U 6.4
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 3.2 16
Chloromethane 74-87-3 50.49 2.0 U 4.1
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,2-Dichloroethene (cis) 156-59-2 96.94 3.0 12
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 30 57
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.10 6.6 16
Styrene 100-42-5 104.1 2.0 U 8.5
Tert-butyl alcohol 75-65-0 74.12 22 68
Toluene 108-88-3 92.14 2.0 U 7.5
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.50 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
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Xylene (o) 95-47-6 106.2 2.0 U 8.7
Alkane-unknown cyclohexane 92 36 JN 13 21.00
Alkane-unknown 92 38 JN 14 21.26
Page 43
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Page 44
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Field ID Number: 81-MR-1SSDL AIR RESULTS Analysis Date: 03/03/2017

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Acetone 67-64-1 58.08 160 370
Allyl chloride 107-05-1 76.53 12 U 38
Benzene 71-43-2 78.11 12 U 38
Bromoform 75-25-2 252.8 12 U 120
Bromomethane 74-83-9 94.94 12 U 47
1,3-Butadiene 106-99-0 54.09 12 U 27
n-Butane 106-97-8 58.12 12 U 29
Chlorobenzene 108-90-7 112.6 12 U 55
Chloroethane 75-00-3 64.52 12 U 32
Chloroform 67-66-3 119.4 12 U 59
2-Chlorotoluene 95-49-8 126.6 12 U 62
Cyclohexane 110-82-7 84.16 12 U 41
1,2-Dibromoethane 106-93-4 187.8 12 U 92
1,2-Dichloroethene (cis) 156-59-2 96.94 12 U 48
1,2-Dichloroethene (trans) 156-60-5 96.94 12 U 48
1,4-Dioxane 123-91-1 88.12 30 U 110
Ethanol 64-17-5 46.07 38 71
Ethylbenzene 100-41-4 106.2 12 U 52
4-Ethyltoluene 622-96-8 120.2 12 U 59
n-Heptane 142-82-5 100.2 12 U 49
n-Hexane 110-54-3 86.17 12 U 42
Isopropanol 67-63-0 60.10 30 U 74
Styrene 100-42-5 104.1 12 U 51
Toluene 108-88-3 92.14 12 U 45
Vinyl bromide 593-60-2 106.9 12 U 52
Vinyl chloride 75-01-4 62.50 12 U 31
Xylene (m,p) 1330-20-7 106.2 24 U 100
Page 45
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Xylene (o) 95-47-6 106.2 12 U 52
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Page 47
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Field ID Number: 81-MR-1SSDL2 AIR RESULTS Analysis Date: 03/03/2017

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Acetone 67-64-1 58.08 270 U 640
Allyl chloride 107-05-1 76.53 110 U 340
Benzene 71-43-2 78.11 110 U 350
Bromoform 75-25-2 252.8 110 U 1100
Bromomethane 74-83-9 94.94 110 U 420
1,3-Butadiene 106-99-0 54.09 110 U 240
n-Butane 106-97-8 58.12 110 U 260
Chlorobenzene 108-90-7 112.6 110 U 500
Chloroethane 75-00-3 64.52 110 U 280
Chloroform 67-66-3 119.4 110 U 530
Chloromethane 74-87-3 50.49 110 U 220
2-Chlorotoluene 95-49-8 126.6 110 U 560
Cyclohexane 110-82-7 84.16 110 U 370
1,2-Dibromoethane 106-93-4 187.8 110 U 830
1,4-Dioxane 123-91-1 88.12 270 U 1000
Ethanol 64-17-5 46.07 270 U 510
Ethylbenzene 100-41-4 106.2 110 U 470
4-Ethyltoluene 622-96-8 120.2 110 U 530
n-Heptane 142-82-5 100.2 110 U 440
n-Hexane 110-54-3 86.17 110 U 380
Isopropanol 67-63-0 60.10 270 U 660
Styrene 100-42-5 104.1 110 U 460
Toluene 108-88-3 92.14 110 U 410
Trichloroethene 79-01-6 131.4 110 U 580
Vinyl bromide 593-60-2 106.9 110 U 470
Vinyl chloride 75-01-4 62.50 110 U 280
Xylene (m,p) 1330-20-7 106.2 220 U 940
Page 48
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Xylene (o) 95-47-6 106.2 110 U 470
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Page 50
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Field ID Number: 81-WC-2SS AIR RESULTS Analysis Date: 03/03/2017

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Acetone 67-64-1 58.08 29 68
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 2.0 U 6.4
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 2.0 U 10
Chloromethane 74-87-3 50.49 2.0 U 4.1
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 27 51
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.10 5.1 12
Methyl ethyl ketone 78-93-3 72.10 2.0 U 5.9
Styrene 100-42-5 104.1 2.0 U 8.5
Toluene 108-88-3 92.14 2.0 U 7.5
Trichloroethene 79-01-6 131.4 2.0 U 11
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.50 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
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Xylene (o) 95-47-6 106.2 2.0 U 8.7
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Field ID Number: 81-WC-2SSRE AIR RESULTS Analysis Date: 03/03/2017

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Acetone 67-64-1 58.08 28 67
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 2.0 U 6.4
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 2.0 U 10
Chloromethane 74-87-3 50.49 2.0 U 4.1
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 28 54
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.10 5.1 12
Styrene 100-42-5 104.1 2.0 U 8.5
Tetrachloroethene 127-18-4 165.8 2.0 U 14
Toluene 108-88-3 92.14 2.0 U 7.5
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.50 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
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Xylene (o) 95-47-6 106.2 2.0 U 8.7
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Field ID Number: 81-HS-1SS AIR RESULTS Analysis Date: 03/03/2017

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Acetone 67-64-1 58.08 100 240
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 2.0 U 6.4
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 6.5 32
Chloromethane 74-87-3 50.49 2.0 U 4.1
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 38 72
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.10 12 30
Styrene 100-42-5 104.1 2.0 U 8.5
Toluene 108-88-3 92.14 2.0 U 7.5
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.50 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
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Xylene (o) 95-47-6 106.2 2.0 U 8.7
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Field ID Number: 81-HS-1SSDL AIR RESULTS Analysis Date: 03/03/2017

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Acetone 67-64-1 58.08 100 240
Allyl chloride 107-05-1 76.53 12 U 38
Benzene 71-43-2 78.11 12 U 38
Bromoform 75-25-2 252.8 12 U 120
Bromomethane 74-83-9 94.94 12 U 47
1,3-Butadiene 106-99-0 54.09 12 U 27
n-Butane 106-97-8 58.12 12 U 29
Chlorobenzene 108-90-7 112.6 12 U 55
Chloroethane 75-00-3 64.52 12 U 32
Chloroform 67-66-3 119.4 12 U 59
2-Chlorotoluene 95-49-8 126.6 12 U 62
Cyclohexane 110-82-7 84.16 12 U 41
1,2-Dibromoethane 106-93-4 187.8 12 U 92
1,4-Dioxane 123-91-1 88.12 30 U 110
Ethanol 64-17-5 46.07 48 90
Ethylbenzene 100-41-4 106.2 12 U 52
4-Ethyltoluene 622-96-8 120.2 12 U 59
n-Heptane 142-82-5 100.2 12 U 49
n-Hexane 110-54-3 86.17 12 U 42
Isopropanol 67-63-0 60.10 30 U 74
Styrene 100-42-5 104.1 12 U 51
Toluene 108-88-3 92.14 12 U 45
Vinyl bromide 593-60-2 106.9 12 U 52
Vinyl chloride 75-01-4 62.50 12 U 31
Xylene (m,p) 1330-20-7 106.2 24 U 100
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Xylene (o) 95-47-6 106.2 12 U 52
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Field ID Number: 81-HS-1SSDL2 AIR RESULTS Analysis Date: 03/03/2017

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Acetone 67-64-1 58.08 270 U 640
Allyl chloride 107-05-1 76.53 110 U 340
Benzene 71-43-2 78.11 110 U 350
Bromoform 75-25-2 252.8 110 U 1100
Bromomethane 74-83-9 94.94 110 U 420
1,3-Butadiene 106-99-0 54.09 110 U 240
n-Butane 106-97-8 58.12 110 U 260
Chlorobenzene 108-90-7 112.6 110 U 500
Chloroethane 75-00-3 64.52 110 U 280
Chloroform 67-66-3 119.4 110 U 530
Chloromethane 74-87-3 50.49 110 U 220
2-Chlorotoluene 95-49-8 126.6 110 U 560
Cyclohexane 110-82-7 84.16 110 U 370
1,2-Dibromoethane 106-93-4 187.8 110 U 830
1,4-Dioxane 123-91-1 88.12 270 U 1000
Ethanol 64-17-5 46.07 270 U 510
Ethylbenzene 100-41-4 106.2 110 U 470
4-Ethyltoluene 622-96-8 120.2 110 U 530
n-Heptane 142-82-5 100.2 110 U 440
n-Hexane 110-54-3 86.17 110 U 380
Isopropanol 67-63-0 60.10 270 U 660
Styrene 100-42-5 104.1 110 U 460
Toluene 108-88-3 92.14 110 U 410
Vinyl bromide 593-60-2 106.9 110 U 470
Vinyl chloride 75-01-4 62.50 110 U 280
Xylene (m,p) 1330-20-7 106.2 220 U 940
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Xylene (o) 95-47-6 106.2 110 U 470
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Acetone 67-64-1 58.08 300 720
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 2.0 U 6.4
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 570 E 2800
Chloromethane 74-87-3 50.49 2.0 U 4.1
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 44 83
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.10 16 39
Methyl isobutyl ketone 108-10-1 100.2 2.5 10
Styrene 100-42-5 104.1 2.0 U 8.5
Tert-butyl alcohol 75-65-0 74.12 6.7 20
Toluene 108-88-3 92.14 2.0 U 7.5
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.50 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
Page 66
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Xylene (o) 95-47-6 106.2 2.0 U 8.7
1-Hexanol, 2-ethyl- 000104-76-7 130 32 JN 17 24.04
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Page 68
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Field ID Number: 81-WC-1SSDL AIR RESULTS Analysis Date: 03/03/2017

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Acetone 67-64-1 58.08 290 700
Allyl chloride 107-05-1 76.53 12 U 38
Benzene 71-43-2 78.11 12 U 38
Bromoform 75-25-2 252.8 12 U 120
Bromomethane 74-83-9 94.94 12 U 47
1,3-Butadiene 106-99-0 54.09 12 U 27
n-Butane 106-97-8 58.12 12 U 29
Chlorobenzene 108-90-7 112.6 12 U 55
Chloroethane 75-00-3 64.52 12 U 32
Chloroform 67-66-3 119.4 590 2900
2-Chlorotoluene 95-49-8 126.6 12 U 62
Cyclohexane 110-82-7 84.16 12 U 41
1,2-Dibromoethane 106-93-4 187.8 12 U 92
1,4-Dioxane 123-91-1 88.12 30 U 110
Ethanol 64-17-5 46.07 48 90
Ethylbenzene 100-41-4 106.2 12 U 52
4-Ethyltoluene 622-96-8 120.2 12 U 59
n-Heptane 142-82-5 100.2 12 U 49
n-Hexane 110-54-3 86.17 12 U 42
Isopropanol 67-63-0 60.10 30 U 74
Styrene 100-42-5 104.1 12 U 51
Toluene 108-88-3 92.14 12 U 45
Vinyl bromide 593-60-2 106.9 12 U 52
Vinyl chloride 75-01-4 62.50 12 U 31
Xylene (m,p) 1330-20-7 106.2 24 U 100
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Xylene (o) 95-47-6 106.2 12 U 52
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Field ID Number: 81-CS-1SSDL2 AIR RESULTS Analysis Date: 03/03/2017

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Acetone 67-64-1 58.08 270 U 640
Allyl chloride 107-05-1 76.53 110 U 340
Benzene 71-43-2 78.11 110 U 350
Bromoform 75-25-2 252.8 110 U 1100
Bromomethane 74-83-9 94.94 110 U 420
1,3-Butadiene 106-99-0 54.09 110 U 240
n-Butane 106-97-8 58.12 110 U 260
Chlorobenzene 108-90-7 112.6 110 U 500
Chloroethane 75-00-3 64.52 110 U 280
Chloroform 67-66-3 119.4 110 U 530
Chloromethane 74-87-3 50.49 110 U 220
2-Chlorotoluene 95-49-8 126.6 110 U 560
Cyclohexane 110-82-7 84.16 110 U 370
1,2-Dibromoethane 106-93-4 187.8 110 U 830
1,4-Dioxane 123-91-1 88.12 270 U 1000
Ethanol 64-17-5 46.07 270 U 510
Ethylbenzene 100-41-4 106.2 110 U 470
4-Ethyltoluene 622-96-8 120.2 110 U 530
n-Heptane 142-82-5 100.2 110 U 440
n-Hexane 110-54-3 86.17 110 U 380
Isopropanol 67-63-0 60.10 270 U 660
Styrene 100-42-5 104.1 110 U 460
Toluene 108-88-3 92.14 110 U 410
Vinyl bromide 593-60-2 106.9 110 U 470
Vinyl chloride 75-01-4 62.50 110 U 280
Xylene (m,p) 1330-20-7 106.2 220 U 940
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Xylene (o) 95-47-6 106.2 110 U 470
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Acetone 67-64-1 58.08 810 U 1900
Allyl chloride 107-05-1 76.53 320 U 1000
Benzene 71-43-2 78.11 320 U 1000
Bromoform 75-25-2 252.8 320 U 3300
Bromomethane 74-83-9 94.94 320 U 1300
1,3-Butadiene 106-99-0 54.09 320 U 720
n-Butane 106-97-8 58.12 320 U 770
Chlorobenzene 108-90-7 112.6 320 U 1500
Chloroethane 75-00-3 64.52 320 U 850
Chloroform 67-66-3 119.4 320 U 1600
Chloromethane 74-87-3 50.49 320 U 670
2-Chlorotoluene 95-49-8 126.6 320 U 1700
Cyclohexane 110-82-7 84.16 320 U 1100
1,2-Dibromoethane 106-93-4 187.8 320 U 2500
1,4-Dioxane 123-91-1 88.12 810 U 2900
Ethanol 64-17-5 46.07 810 U 1500
Ethylbenzene 100-41-4 106.2 320 U 1400
4-Ethyltoluene 622-96-8 120.2 320 U 1600
n-Heptane 142-82-5 100.2 320 U 1300
n-Hexane 110-54-3 86.17 320 U 1100
Isopropanol 67-63-0 60.10 810 U 2000
Styrene 100-42-5 104.1 320 U 1400
Toluene 108-88-3 92.14 320 U 1200
Vinyl bromide 593-60-2 106.9 320 U 1400
Vinyl chloride 75-01-4 62.50 320 U 830
Xylene (m,p) 1330-20-7 106.2 650 U 2800
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Xylene (o) 95-47-6 106.2 320 U 1400
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EMSL Analytical, Inc. NJDEP Cert. # 03036
Annual MDL Study Summary
EMSL Analytical, Inc. - Cinnaminson, NJ Facility
Method: NJDEP Low Level TO-15 Effective Date: 09/23/2016

Instrument ID: L -core Expiration Date: 9/23/2017
Column ID: RTX- 502.2, 60M x 25um, 1.4um QA Officer Name: William Chamberlain
Analyst: MTH
Matrix: Air QA Officer Signature:
MDL Replicate ID Data Files Analysis Date:
Spike Amount
0.2 L8324 L8325 L8322 L8323 L8320 L8321 L8319 09/23/2016
Replicate Results in (ppbv) Mean TRUE Mean Std. MDL RL True/ MDL
Target Compounds 1 2 3 4 5 6 7 Value Value % Rec. Dev. (ppbv) (ppbv) Ratio
Dichlorodifluoromethane 0.25 0.25 0.25 0.28 0.33 0.26 0.31 0.28 0.20 139 0.034 0.107 0.2 1.9
1,2-Dichlorotetrafluoroethane 0.24 0.23 0.24 0.25 0.28 0.25 0.28 0.25 0.20 126 0.020 0.062 0.2 3.2
Chloromethane 0.29 0.27 0.27 0.27 0.34 0.29 0.37 0.30 0.20 149 0.040 0.125 0.2 1.6
n-Butane 0.24 0.24 0.25 0.25 0.28 0.26 0.27 0.26 0.20 128 0.014 0.045 0.2 4.4
Vinyl chloride 0.23 0.24 0.23 0.23 0.27 0.24 0.27 0.24 0.20 122 0.017 0.055 0.2 3.6
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1,3-Butadiene 0.22 0.33 0.23 0.24 0.26 0.23 0.27 0.26 0.20 128 0.035 0.111 0.2 1.8
Bromomethane 0.25 0.25 0.25 0.25 0.31 0.27 0.31 0.27 0.20 135 0.026 0.081 0.2 2.5
Chloroethane 0.21 0.22 0.22 0.22 0.25 0.21 0.23 0.22 0.20 111 0.014 0.043 0.2 4.7
Ethanol 0.31 0.25 0.23 0.25 0.26 0.24 0.24 0.25 0.20 127 0.025 0.078 0.5 2.6
Vinyl bromide 0.24 0.23 0.23 0.22 0.27 0.24 0.28 0.25 0.20 123 0.021 0.067 0.2 3.0
Trichlorofluoromethane 0.23 0.24 0.24 0.23 0.27 0.24 0.28 0.25 0.20 123 0.018 0.058 0.2 3.5
Isopropanol 0.24 0.20 0.18 0.24 0.20 0.22 0.20 0.21 0.20 105 0.024 0.075 0.5 2.7
1,1,2-Trichloro-1,2,2-trifluoroethane 0.23 0.23 0.23 0.23 0.26 0.24 0.28 0.24 0.20 121 0.019 0.058 0.2 3.4
Acetone 0.21 0.22 0.19 0.20 0.24 0.20 0.25 0.22 0.20 108 0.021 0.067 0.5 3.0
1,1-Dichloroethene 0.23 0.23 0.22 0.22 0.26 0.23 0.28 0.24 0.20 119 0.021 0.065 0.2 3.1
Tert-butyl alcohol 0.23 0.19 0.17 0.23 0.21 0.23 0.24 0.21 0.20 107 0.024 0.077 0.2 2.6
Allyl chloride 0.22 0.21 0.22 0.21 0.24 0.22 0.26 0.23 0.20 113 0.019 0.059 0.2 3.4
Carbon disulfide 0.23 0.23 0.23 0.23 0.27 0.23 0.27 0.24 0.20 120 0.020 0.062 0.5 3.3
Methylene chloride 0.26 0.25 0.25 0.26 0.29 0.26 0.30 0.27 0.20 134 0.020 0.063 0.2 3.2
Methyl tert-butyl ether 0.19 0.20 0.16 0.19 0.21 0.17 0.21 0.19 0.20 95 0.017 0.055 0.2 3.7
1,2-Dichloroethene (trans) 0.22 0.23 0.22 0.23 0.26 0.23 0.27 0.24 0.20 118 0.021 0.065 0.2 3.1
n-Hexane 0.22 0.21 0.21 0.22 0.22 0.22 0.25 0.22 0.20 111 0.015 0.046 0.2 4.4
1,1-Dichloroethane 0.23 0.23 0.22 0.22 0.24 0.23 0.26 0.23 0.20 116 0.014 0.045 0.2 4.4
Page 1 of 3

Analyst: MTH
Spike Amount
0.2 L8324 L8325 L8322 L8323 L8320 L8321 L8319 09/23/2016
Methyl ethyl ketone 0.18 0.19 0.15 0.18 0.20 0.16 0.21 0.18 0.20 91 0.022 0.069 0.2 2.9
1,2-Dichloroethene (cis) 0.22 0.23 0.22 0.22 0.25 0.23 0.27 0.23 0.20 117 0.018 0.055 0.2 3.6
Chloroform 0.22 0.22 0.21 0.22 0.23 0.22 0.25 0.22 0.20 112 0.014 0.044 0.2 4.6
Tetrahydrofuran 0.18 0.18 0.15 0.17 0.17 0.15 0.16 0.17 0.20 83 0.011 0.034 0.2 5.9
1,1,1-Trichloroethane 0.21 0.22 0.22 0.22 0.23 0.22 0.25 0.22 0.20 111 0.012 0.038 0.2 5.2
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Cyclohexane 0.21 0.22 0.21 0.20 0.23 0.22 0.24 0.22 0.20 109 0.013 0.041 0.2 4.9
2,2,4-Trimethylpentane 0.20 0.21 0.20 0.20 0.20 0.20 0.22 0.20 0.20 102 0.009 0.027 0.2 7.3
Carbon tetrachloride 0.21 0.22 0.21 0.22 0.22 0.22 0.24 0.22 0.20 111 0.010 0.033 0.2 6.1
n-Heptane 0.19 0.20 0.18 0.19 0.21 0.19 0.22 0.20 0.20 99 0.014 0.043 0.2 4.7
1,2-Dichloroethane 0.21 0.21 0.21 0.21 0.24 0.22 0.26 0.22 0.20 111 0.019 0.060 0.2 3.4
Benzene 0.21 0.22 0.22 0.22 0.23 0.23 0.25 0.23 0.20 113 0.012 0.037 0.2 5.5
Trichloroethene 0.20 0.22 0.20 0.19 0.34 0.20 0.24 0.23 0.20 113 0.052 0.164 0.2 1.2
1,2-Dichloropropane 0.19 0.21 0.19 0.19 0.32 0.19 0.23 0.22 0.20 108 0.050 0.157 0.2 1.3
Methyl methacrylate 0.16 0.17 0.14 0.15 0.26 0.14 0.18 0.17 0.20 86 0.044 0.139 0.2 1.4
Bromodichloromethane 0.18 0.20 0.18 0.19 0.30 0.18 0.21 0.20 0.20 102 0.043 0.136 0.2 1.5
1,4-Dioxane 0.19 0.14 0.13 0.18 0.20 0.15 0.13 0.16 0.20 80 0.030 0.093 0.5 2.1
Methyl isobutyl ketone 0.19 0.17 0.14 0.18 0.22 0.15 0.15 0.17 0.20 85 0.027 0.085 0.2 2.3
1,3-Dichloropropene (cis) 0.18 0.20 0.18 0.18 0.32 0.18 0.23 0.21 0.20 105 0.050 0.158 0.2 1.3
Toluene 0.18 0.19 0.17 0.18 0.30 0.17 0.22 0.20 0.20 101 0.046 0.145 0.2 1.4
1,3-Dichloropropene (trans) 0.18 0.19 0.17 0.17 0.31 0.17 0.23 0.20 0.20 101 0.051 0.160 0.2 1.3
1,1,2-Trichloroethane 0.19 0.19 0.18 0.18 0.31 0.18 0.21 0.21 0.20 103 0.048 0.150 0.2 1.3
Tetrachloroethene 0.18 0.20 0.18 0.19 0.30 0.18 0.22 0.21 0.20 104 0.042 0.133 0.2 1.5
Dibromochloromethane 0.16 0.18 0.16 0.16 0.28 0.16 0.19 0.19 0.20 93 0.044 0.138 0.2 1.4
1,2-Dibromoethane 0.18 0.20 0.18 0.18 0.32 0.18 0.23 0.21 0.20 106 0.052 0.162 0.2 1.2
Page 2 of 3

Analyst: MTH
Spike Amount
0.2 L8324 L8325 L8322 L8323 L8320 L8321 L8319 09/23/2016
Chlorobenzene 0.19 0.20 0.16 0.18 0.21 0.17 0.21 0.19 0.20 93 0.020 0.064 0.2 3.1
Ethylbenzene 0.17 0.20 0.16 0.17 0.20 0.16 0.21 0.18 0.20 90 0.021 0.066 0.2 3.0
Xylene (m,p) 0.34 0.39 0.31 0.33 0.38 0.30 0.41 0.35 0.40 88 0.041 0.129 0.4 3.1
Xylene (o) 0.17 0.19 0.16 0.17 0.19 0.15 0.20 0.17 0.20 87 0.020 0.062 0.2 3.2
Styrene 0.15 0.18 0.14 0.15 0.17 0.14 0.19 0.16 0.20 80 0.022 0.068 0.2 2.9
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Bromoform 0.15 0.18 0.14 0.16 0.18 0.14 0.19 0.16 0.20 81 0.020 0.062 0.2 3.3
1,1,2,2-Tetrachloroethane 0.17 0.19 0.14 0.17 0.18 0.14 0.19 0.17 0.20 84 0.022 0.069 0.2 2.9
4-Ethyltoluene 0.17 0.19 0.15 0.17 0.18 0.15 0.19 0.17 0.20 87 0.019 0.060 0.2 3.3
1,3,5-Trimethylbenzene 0.18 0.20 0.15 0.17 0.19 0.15 0.20 0.18 0.20 89 0.023 0.072 0.2 2.8
2-Chlorotoluene 0.18 0.20 0.15 0.17 0.20 0.14 0.23 0.18 0.20 92 0.031 0.098 0.2 2.0
1,2,4-Trimethylbenzene 0.18 0.20 0.16 0.18 0.19 0.15 0.19 0.18 0.20 89 0.018 0.056 0.2 3.6
1,3-Dichlorobenzene 0.17 0.19 0.16 0.18 0.18 0.15 0.18 0.17 0.20 86 0.015 0.048 0.2 4.2
1,2,4-Trichlorobenzene 0.20 0.20 0.20 0.21 0.21 0.20 0.18 0.20 0.20 101 0.010 0.032 0.2 6.2
1,3-Hexachlorobutadiene 0.24 0.23 0.22 0.22 0.25 0.25 0.21 0.23 0.20 116 0.015 0.047 0.2 4.3
Naphthalene 0.21 0.20 0.20 0.19 0.22 0.22 0.19 0.20 0.20 102 0.013 0.041 0.2 4.9
Page 3 of 3
Annual MDL Study Verification Summary

Method: NJDEP LLTO-15 Effective Date: 09/27/2016

Column ID: RTX- 502.2, 60M x 25um, 1.4um QA Officer Name: William Chamberlin
Analyst: MTH QA Officer Signature:
Matrix: Air
This MDL verification study validates the MDL performed on this instrument on 09/27/2016.
Analysis Date
09/27/2016 09/27/2016
Data Files
L8345 L8346
Verification Levels (ppbv) MDL MDLV/MDL RL RL/MDLV
Target Compounds CAS # 0.2 0.1 (ppbv) Ratio ppbv Ratio
Dichlorodifluoromethane 75-71-8 0.26 0.14 0.107 1.3 0.2 1.4
1,2-Dichlorotetrafluoroethane 76-14-2 0.20 0.12 0.062 1.9 0.2 1.7
Chloromethane 74-87-3 0.32 0.22 0.125 1.8 0.2 0.9
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n-Butane 106-97-8 0.27 0.17 0.045 3.8 0.2 1.2
Vinyl chloride 75-01-4 0.22 0.12 0.055 2.1 0.2 1.7
1,3-Butadiene 106-99-0 0.21 0.15 0.111 1.3 0.2 1.4
Bromomethane 74-83-9 0.26 0.16 0.081 1.9 0.2 1.3
Chloroethane 75-00-3 0.21 0.09 0.043 2.2 0.2 2.1
Ethanol 64-17-5 0.30 ND 0.078 3.8 0.5 1.7
Vinyl bromide 593-60-2 0.23 0.12 0.067 1.7 0.2 1.7
Trichlorofluoromethane 75-69-4 0.23 0.12 0.058 2.1 0.2 1.6
Isopropanol 67-63-0 0.22 0.08 0.075 1.1 0.5 6.2
1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 0.26 0.12 0.058 2.1 0.2 1.6
Acetone 67-64-1 0.19 0.10 0.067 1.5 0.5 4.9
1,1-Dichloroethene 75-35-4 0.25 0.14 0.065 2.1 0.2 1.5
Tert-butyl alcohol 75-65-0 0.19 0.08 0.077 1.0 0.2 2.6
Allyl chloride 107-05-1 0.28 0.14 0.059 2.4 0.2 1.4
Carbon disulfide 75-15-0 0.26 0.14 0.062 2.3 0.5 3.5
Methylene chloride 75-09-2 0.27 0.16 0.063 2.5 0.5 3.2
Methyl tert-butyl ether 1634-04-4 0.14 0.06 0.055 1.2 0.2 3.1
1,2-Dichloroethene (trans) 156-60-5 0.24 0.12 0.065 1.8 0.2 1.7
n-Hexane 110-54-3 0.22 0.09 0.046 2.0 0.2 2.2
1,1-Dichloroethane 75-34-3 0.23 0.11 0.045 2.4 0.2 1.8
Methyl ethyl ketone 78-93-3 0.15 ND 0.069 2.2 0.2 1.3
Page 1 of 3


Matrix: Air
Analysis Date
09/27/2016 09/27/2016
Data Files
L8345 L8346
1,2-Dichloroethene (cis) 156-59-2 0.23 0.11 0.055 2.0 0.2 1.8
Chloroform 67-66-3 0.22 0.09 0.044 2.1 0.2 2.2
Tetrahydrofuran 109-99-9 0.12 ND 0.034 3.5 0.2 1.7
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1,1,1-Trichloroethane 71-55-6 0.22 0.08 0.038 2.2 0.2 2.4
Cyclohexane 110-82-7 0.22 0.08 0.041 2.0 0.2 2.5
2,2,4-Trimethylpentane 540-84-1 0.20 0.08 0.027 2.8 0.2 2.6
Carbon tetrachloride 56-23-5 0.22 0.09 0.033 2.7 0.2 2.3
n-Heptane 142-82-5 0.19 0.08 0.043 2.0 0.2 2.4
1,2-Dichloroethane 107-06-2 0.22 0.11 0.060 1.9 0.2 1.8
Benzene 71-43-2 0.24 0.10 0.037 2.8 0.2 2.0
Trichloroethene 79-01-6 0.20 0.10 0.164 0.6 0.2 1.9
1,2-Dichloropropane 78-87-5 0.19 0.09 0.157 0.6 0.2 2.2
Methyl methacrylate 80-62-6 0.13 0.00 0.139 0.0 0.2 1.5
Bromodichloromethane 75-27-4 0.18 0.08 0.136 0.6 0.2 2.4
1,4-Dioxane 123-91-1 0.14 ND 0.093 1.5 0.5 3.5
Methyl isobutyl ketone 108-10-1 0.12 0.07 0.085 0.8 0.2 3.0
1,3-Dichloropropene (cis) 10061-01-5 0.19 0.10 0.158 0.6 0.2 2.0
Toluene 108-88-3 0.17 0.08 0.145 0.5 0.2 2.7
1,3-Dichloropropene (trans) 10061-02-6 0.17 0.09 0.160 0.6 0.2 2.3
1,1,2-Trichloroethane 79-00-5 0.16 0.09 0.150 0.6 0.2 2.3
Tetrachloroethene 127-18-4 0.16 0.07 0.133 0.5 0.2 2.8
Dibromochloromethane 124-48-1 0.15 0.07 0.138 0.5 0.2 2.8
1,2-Dibromoethane 106-93-4 0.17 0.09 0.162 0.6 0.2 2.2
Page 2 of 3


Matrix: Air
Analysis Date
09/27/2016 09/27/2016
Data Files
L8345 L8346
Chlorobenzene 108-90-7 0.15 0.07 0.064 1.1 0.2 2.8
Ethylbenzene 100-41-4 0.14 0.07 0.066 1.1 0.2 2.8
Xylene (m,p) 179601-23-1 0.27 0.14 0.129 1.1 0.4 2.9
105 of 794
Xylene (o) 95-47-6 0.12 0.06 0.062 1.0 0.2 3.1
Styrene 100-42-5 0.12 0.06 0.068 0.9 0.2 3.4
Bromoform 75-25-2 0.13 0.07 0.062 1.1 0.2 2.9
1,1,2,2-Tetrachloroethane 79-34-5 0.12 0.05 0.069 0.7 0.2 3.9
4-Ethyltoluene 622-96-8 0.13 0.06 0.060 1.0 0.2 3.2
1,3,5-Trimethylbenzene 108-67-8 0.13 0.06 0.072 0.8 0.2 3.3
2-Chlorotoluene 95-49-8 0.14 0.07 0.098 0.7 0.2 2.9
1,2,4-Trimethylbenzene 95-63-6 0.14 0.06 0.056 1.0 0.2 3.6
1,3-Dichlorobenzene 541-73-1 0.15 0.06 0.048 1.2 0.2 3.5
1,2,4-Trichlorobenzene 120-82-1 0.28 0.12 0.032 3.9 0.2 1.6
1,3-Hexachlorobutadiene 87-68-3 0.17 0.12 0.047 2.5 0.2 1.7
Naphthalene 91-20-3 0.22 0.11 0.041 2.6 0.2 1.9
Page 3 of 3
106 of 794
EMSL Analytical, Inc. EMSL Order: RLLCS
200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample ID: RLLCS030217L-0.2
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030217L-0.5
http://www.EMSL.com TO-15_Lab@emsl.com Report Date: 03/06/2017
Project ID: Reporting Limit Laboratory Control Sample Sampling Date: NA

Canister ID: E12941
Lab Sample ID: RLLCS030217L-0.2 RLLCS030217L-0.5
Lab File ID: L9293.D L9292.D Analysis Date: 03/02/2017
Sample Vol(ml): 50 125 Instrument ID: GC/MS L-C
Dilution Factor: 1 1 Analyst Initials: MTH
Reporting Limit Laboratory Control Sample
NJDEP- SRWM Low Level USEPA Method TO-15 (NJDEP-LLTO-15 -March 2007)
Spike Result % Recovery
Target Compounds CAS# MW ppbv ppbv Rec # Limits (%)
Acetone 67-64-1 58.08 0.5 0.62 124 60-140
Allyl chloride 107-05-1 76.53 0.2 0.23 115 60-140
Benzene 71-43-2 78.11 0.2 0.23 115 60-140
Bromodichloromethane 75-27-4 163.8 0.2 0.21 105 60-140
Bromoform 75-25-2 252.8 0.2 0.20 100 60-140
Bromomethane 74-83-9 94.94 0.2 0.27 135 60-140
1,3-Butadiene 106-99-0 54.09 0.2 0.21 105 60-140
n-Butane 106-97-8 58.12 0.2 0.20 100 60-140
Chlorobenzene 108-90-7 112.6 0.2 0.22 110 60-140
Chloroethane 75-00-3 64.52 0.2 0.21 105 60-140
Chloroform 67-66-3 119.4 0.2 0.22 110 60-140
Chloromethane 74-87-3 50.49 0.2 0.23 115 60-140
Carbon disulfide 75-15-0 76.14 0.5 0.53 106 60-140
Carbon tetrachloride 56-23-5 153.8 0.2 0.22 110 60-140
2-Chlorotoluene 95-49-8 126.6 0.2 0.22 110 60-140
Cyclohexane 110-82-7 84.16 0.2 0.21 105 60-140
Dibromochloromethane 124-48-1 208.3 0.2 0.20 100 60-140
1,2-Dibromoethane 106-93-4 187.8 0.2 0.21 105 60-140
1,2-Dichlorobenzene 95-50-1 147.0 0.2 0.20 100 60-140
Dichlorodifluoromethane 75-71-8 120.9 0.2 0.27 135 60-140
1,1-Dichloroethane 75-34-3 98.96 0.2 0.22 110 60-140
1,2-Dichloroethane 107-06-2 98.96 0.2 0.23 115 60-140
1,1-Dichloroethene 75-35-4 96.94 0.2 0.23 115 60-140
1,2-Dichloroethene (cis) 156-59-2 96.94 0.2 0.23 115 60-140
1,2-Dichloroethene (trans) 156-60-5 96.94 0.2 0.23 115 60-140
1,2-Dichloropropane 78-87-5 113.0 0.2 0.22 110 60-140
1,3-Dichloropropene (cis) 10061-01-5 111.0 0.2 0.21 105 60-140
1,3-Dichloropropene (trans) 10061-02-6 111.0 0.2 0.19 95 60-140
1,2-Dichlorotetrafluoroethane 76-14-2 170.9 0.2 0.22 110 60-140
Master_RLLCS_August_2014_V6 Master_RLLCS_August_2014_V6 Page 1 of 3

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Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030217L-0.5

Canister ID: E12941
Acetone
1,4-Dioxane 123-91-1 88.12 0.5 0.46 92 60-140
Ethanol 64-17-5 46.07 0.5 0.60 120 60-140
Ethylbenzene 100-41-4 106.2 0.2 0.21 105 60-140
4-Ethyltoluene 622-96-8 120.2 0.2 0.21 105 60-140
n-Heptane 142-82-5 100.2 0.2 0.22 110 60-140
1,3-Hexachlorobutadiene 87-68-3 260.8 0.2 0.23 115 60-140
n-Hexane 110-54-3 86.17 0.2 0.22 110 60-140
Isopropanol 67-63-0 60.10 0.5 0.62 124 60-140
Methylene chloride 75-09-2 84.94 0.2 0.25 125 60-140
Methyl ethyl ketone 78-93-3 72.10 0.2 0.21 105 60-140
Methyl isobutyl ketone 108-10-1 100.2 0.2 0.19 95 60-140
Methyl methacrylate 80-62-6 100.12 0.2 0.18 90 60-140
Naphthalene 91-20-3 128.17 0.2 0.17 85 60-140
Methyl tert-butyl ether 1634-04-4 88.15 0.2 0.23 115 60-140
Styrene 100-42-5 104.1 0.2 0.18 90 60-140
Tert-butyl alcohol 75-65-0 74.12 0.2 0.23 115 60-140
1,1,2,2-Tetrachloroethane 79-34-5 167.9 0.2 0.21 105 60-140
Tetrachloroethene 127-18-4 165.8 0.2 0.22 110 60-140
Tetrahydrofuran 109-99-9 72.11 0.2 0.20 100 60-140
Toluene 108-88-3 92.14 0.2 0.21 105 60-140
1,2,4-Trichlorobenzene 120-82-1 181.5 0.2 0.16 80 60-140
1,1,1-Trichloroethane 71-55-6 133.4 0.2 0.23 115 60-140
Trichloroethene 79-01-6 131.4 0.2 0.22 110 60-140
Trichlorofluoromethane 75-69-4 137.4 0.2 0.23 115 60-140
1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 187.4 0.2 0.23 115 60-140
1,2,4-Trimethylbenzene 95-63-6 120.2 0.2 0.22 110 60-140
2,2,4-Trimethylpentane 540-84-1 114.2 0.2 0.23 115 60-140
Vinyl bromide 593-60-2 106.9 0.2 0.23 115 60-140
Vinyl chloride 75-01-4 62.50 0.2 0.21 105 60-140

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Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030217L-0.5

Canister ID: E12941
Acetone(m,p)
Xylene 1330-20-7 106.2 0.4 0.42 105 60-140
Xylene (o) 95-47-6 106.2 0.2 0.22 110 60-140
Surrogate Result Spike Recovery

4-Bromofluorobenzene 9.9 10 99%
# = Compounds outside control limits marked with asterisk (*).

Total Compounds Spiked 64
Total Outside Control Limits 0
% Recoveries within Control Limits 100
Acceptable Criteria: 90% of compounds must be within control limits
NJDEP Certification #: 03036

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Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030717L-0.5

Canister ID: E12941
Acetone 67-64-1 58.08 0.5 0.66 132 60-140
Allyl chloride 107-05-1 76.53 0.2 0.21 105 60-140
Benzene 71-43-2 78.11 0.2 0.23 115 60-140
Bromoform 75-25-2 252.8 0.2 0.23 115 60-140
Bromomethane 74-83-9 94.94 0.2 0.29 145 * 60-140
1,3-Butadiene 106-99-0 54.09 0.2 0.21 105 60-140
n-Butane 106-97-8 58.12 0.2 0.22 110 60-140
Chlorobenzene 108-90-7 112.6 0.2 0.21 105 60-140
Chloroethane 75-00-3 64.52 0.2 0.22 110 60-140
Chloroform 67-66-3 119.4 0.2 0.24 120 60-140
Chloromethane 74-87-3 50.49 0.2 0.21 105 60-140
2-Chlorotoluene 95-49-8 126.6 0.2 0.21 105 60-140
Cyclohexane 110-82-7 84.16 0.2 0.22 110 60-140
1,2-Dibromoethane 106-93-4 187.8 0.2 0.20 100 60-140
Dichlorodifluoromethane 75-71-8 120.9 0.2 0.30 150 * 60-140
1,1-Dichloroethane 75-34-3 98.96 0.2 0.22 110 60-140
1,2-Dichloroethane 107-06-2 98.96 0.2 0.23 115 60-140
1,1-Dichloroethene 75-35-4 96.94 0.2 0.22 110 60-140

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Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030717L-0.5

Canister ID: E12941
Acetone
1,4-Dioxane 123-91-1 88.12 0.5 0.47 94 60-140
Ethanol 64-17-5 46.07 0.5 0.61 122 60-140
Ethylbenzene 100-41-4 106.2 0.2 0.21 105 60-140
4-Ethyltoluene 622-96-8 120.2 0.2 0.21 105 60-140
n-Heptane 142-82-5 100.2 0.2 0.21 105 60-140
1,3-Hexachlorobutadiene 87-68-3 260.8 0.2 0.29 145 * 60-140
n-Hexane 110-54-3 86.17 0.2 0.20 100 60-140
Isopropanol 67-63-0 60.10 0.5 0.62 124 60-140
Naphthalene 91-20-3 128.17 0.2 0.16 80 60-140
Styrene 100-42-5 104.1 0.2 0.17 85 60-140
Toluene 108-88-3 92.14 0.2 0.21 105 60-140
Vinyl bromide 593-60-2 106.9 0.2 0.23 115 60-140
Vinyl chloride 75-01-4 62.50 0.2 0.21 105 60-140

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Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030717L-0.5

Canister ID: E12941
Acetone(m,p)
Xylene 1330-20-7 106.2 0.4 0.41 103 60-140
Xylene (o) 95-47-6 106.2 0.2 0.21 105 60-140

4-Bromofluorobenzene 10 10 100%


112 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030817L-0.5

Canister ID: E12941
Acetone 67-64-1 58.08 0.5 0.62 124 60-140
Allyl chloride 107-05-1 76.53 0.2 0.21 105 60-140
Benzene 71-43-2 78.11 0.2 0.24 120 60-140
Bromoform 75-25-2 252.8 0.2 0.22 110 60-140
Bromomethane 74-83-9 94.94 0.2 0.29 145 * 60-140
1,3-Butadiene 106-99-0 54.09 0.2 0.20 100 60-140
n-Butane 106-97-8 58.12 0.2 0.26 130 60-140
Chlorobenzene 108-90-7 112.6 0.2 0.21 105 60-140
Chloroethane 75-00-3 64.52 0.2 0.21 105 60-140
Chloroform 67-66-3 119.4 0.2 0.24 120 60-140
Chloromethane 74-87-3 50.49 0.2 0.21 105 60-140
2-Chlorotoluene 95-49-8 126.6 0.2 0.23 115 60-140
Cyclohexane 110-82-7 84.16 0.2 0.22 110 60-140
1,2-Dibromoethane 106-93-4 187.8 0.2 0.19 95 60-140
1,1-Dichloroethane 75-34-3 98.96 0.2 0.23 115 60-140
1,2-Dichloroethane 107-06-2 98.96 0.2 0.24 120 60-140
1,1-Dichloroethene 75-35-4 96.94 0.2 0.24 120 60-140
Master_RLLCS_August_2014_V6 RLLCS Page 1 of 3

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Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030817L-0.5

Canister ID: E12941
Acetone
1,4-Dioxane 123-91-1 88.12 0.5 0.41 82 60-140
Ethanol 64-17-5 46.07 0.5 0.54 108 60-140
Ethylbenzene 100-41-4 106.2 0.2 0.21 105 60-140
4-Ethyltoluene 622-96-8 120.2 0.2 0.21 105 60-140
n-Heptane 142-82-5 100.2 0.2 0.22 110 60-140
n-Hexane 110-54-3 86.17 0.2 0.21 105 60-140
Isopropanol 67-63-0 60.10 0.5 0.60 120 60-140
Naphthalene 91-20-3 128.17 0.2 0.17 85 60-140
Styrene 100-42-5 104.1 0.2 0.17 85 60-140
Toluene 108-88-3 92.14 0.2 0.20 100 60-140
Vinyl bromide 593-60-2 106.9 0.2 0.24 120 60-140
Vinyl chloride 75-01-4 62.50 0.2 0.21 105 60-140

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Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030817L-0.5

Canister ID: E12941
Acetone(m,p)
Xylene 1330-20-7 106.2 0.4 0.41 103 60-140
Xylene (o) 95-47-6 106.2 0.2 0.21 105 60-140



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EMSL Analytical, Inc.
EPA TO-15
Method Blank Summary
Instrument ID: 030217L Analysis Date: 03/02/17

Method Blank ID: MB030217L Analysis Time: 19:25
Lab File ID: L9291.D
This Method Blank applies to the following samples, dilutions, and QC:
Lab Sample ID Lab File ID Date Analyzed Time Analyzed
RLLCS030217L-0.5 L9292.D 03/02/17 20:08

RLLCS030217L-0.2 L9293.D 03/02/17 20:52
491700251-1DL L9294.D 03/02/17 21:35
IB030217L-A L9295.D 03/02/17 22:25
491700245-10 L9296.D 03/02/17 23:08
491700245-11 L9297.D 03/02/17 23:52
IB030217L-B L9298.D 03/03/17 00:42
491700245-12 L9299.D 03/03/17 01:26
491700245-13 L9300.D 03/03/17 02:10
491700245-14 L9301.D 03/03/17 07:48
IB030217L-C L9302.D 03/03/17 08:38
491700245-12RE L9303.D 03/03/17 09:21
491700245-10DL L9304.D 03/03/17 10:04
491700245-11DL L9305.D 03/03/17 10:47
491700245-13DL L9306.D 03/03/17 11:30
491700245-14DL L9307.D 03/03/17 12:13
491700245-10DL2 L9308.D 03/03/17 12:56
491700245-11DL2 L9309.D 03/03/17 13:40
491700245-13DL2 L9310.D 03/03/17 14:32
491700245-10DL3 L9311.D 03/03/17 15:15
ECVS030217L-10 L9312.D 03/03/17 15:59
116 of 794
EPA TO-15

RLLCS030717L-0.5 L9317.D 03/07/17 12:01

RLLCS030717L-0.2 L9318.D 03/07/17 12:44
C3434 L9319.D 03/07/17 13:34
491700251-1DL2 L9320.D 03/07/17 14:19
491700264-1 L9321.D 03/07/17 15:09
491700264-2 L9322.D 03/07/17 16:29
491700264-3 L9323.D 03/07/17 17:20
491700264-4 L9324.D 03/07/17 18:10
491700264-5 L9325.D 03/07/17 19:00
491700264-6 L9326.D 03/07/17 19:49
491700264-7 L9327.D 03/07/17 20:40
491700264-7DUP L9328.D 03/07/17 21:30
IB030717L-A L9329.D 03/07/17 22:20
491700245-1 L9330.D 03/07/17 23:10
491700245-2 L9331.D 03/08/17 00:00
491700245-3 L9332.D 03/08/17 00:50
491700245-4 L9333.D 03/08/17 01:40
ECVS030717L-10 L9334.D 03/08/17 02:24
117 of 794
EPA TO-15

RLLCS030817L-0.5 L9339.D 03/08/17 06:57

RLLCS030817L-0.2 L9340.D 03/08/17 07:40
IB030817L-A L9341.D 03/08/17 09:17
491700264-2RE L9342.D 03/08/17 10:07
491700245-5 L9343.D 03/08/17 10:57
491700245-6 L9344.D 03/08/17 11:46
491700245-7 L9345.D 03/08/17 12:36
491700245-8 L9346.D 03/08/17 13:26
491700245-9 L9347.D 03/08/17 14:16
491700245-9DUP L9348.D 03/08/17 15:06
491700245-1DL L9349.D 03/08/17 15:52
491700245-2DL L9350.D 03/08/17 16:37
491700245-5DL L9351.D 03/08/17 17:23
ECVS030817L-10 L9352.D 03/08/17 18:07
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EPA TO-15
Instrument Performance Check Summary
Bromofluorobenzene (BFB)
Instrument Batch ID: 030117L
BFB Check ID: BFB030117L Analysis Date: 03/01/2017
BFB File ID: L9266.D Analysis Time: 17:28
% Relative
m/e Ion Abundance Criteria Abundance
50 8-0 - 40% of mass 95 25.5
75 30.0 - 66.0% of mass 95 51.7
95 Base peak, 100% relative abundance 100.0
96 5.0 - 9.0% of mass 95 6.9
173 Less than 2.0% of mass 174 0.0 (0.0) 1
174 50.0 - 120.0% of mass 95 97.9
175 4.0 - 9.0% of mass 174 7.0 (7.1) 1
176 93.0 - 101.0% of mass 174 93.4 (95.3) 1
177 5.0 - 9.0% of mass 176 6.3 (6.8) 2
1- Value is % mass of 174 2- Value is % mass of 176
This Performance Check applies to the following samples, standards, blanks, and QC.
Laboratory Sample ID Lab File ID Date Analyzed Time Analyzed

IC030117L-40 L9267.D 03/01/2017 18:17
IC030117L-20 L9268.D 03/01/2017 19:03
IC030117L-10 L9269.D 03/01/2017 19:47
IC030117L-2 L9270.D 03/01/2017 20:36
IC030117L-0.5 L9271.D 03/01/2017 21:20
IC030117L-0.2 L9272.D 03/01/2017 22:04
ICVS030117L-10 L9273.D 03/01/2017 22:47
ICVS030117L-10B L9274.D 03/01/2017 23:31
MB030117L_info_run L9275.D 03/02/2017 00:21
MB030117L_B L9276.D 03/02/2017 01:11
RLLCS030117L-0.5 L9277.D 03/02/2017 01:54
RLLCS030117L-0.2 L9278.D 03/02/2017 02:38
491700158-1 L9279.D 03/02/2017 03:28
IB030117L-A L9280.D 03/02/2017 10:04
491700223-2 L9281.D 03/02/2017 11:00
491700223-3 L9282.D 03/02/2017 11:50
491700223-1 L9283.D 03/02/2017 12:33
IB030117L-B L9284.D 03/02/2017 13:23
491700251-1 L9285.D 03/02/2017 14:06
491700251-2 L9286.D 03/02/2017 14:50
ECVS030117L-10 L9287.D 03/02/2017 15:34
ECVS030117L-10B L9288.D 03/02/2017 16:17
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% Relative
50 8-0 - 40% of mass 95 25.1
75 30.0 - 66.0% of mass 95 51.0
96 5.0 - 9.0% of mass 95 6.6
173 Less than 2.0% of mass 174 0.0 (0.0) 1
174 50.0 - 120.0% of mass 95 98.7
175 4.0 - 9.0% of mass 174 7.0 (7.1) 1
176 93.0 - 101.0% of mass 174 94.0 (95.3) 1
177 5.0 - 9.0% of mass 176 6.2 (6.6) 2

CCVS030217L-10 L9290.D 03/02/2017 17:45
MB030217L L9291.D 03/02/2017 19:25
RLLCS030217L-0.5 L9292.D 03/02/2017 20:08
RLLCS030217L-0.2 L9293.D 03/02/2017 20:52
491700251-1DL L9294.D 03/02/2017 21:35
IB030217L-A L9295.D 03/02/2017 22:25
491700245-10 L9296.D 03/02/2017 23:08
491700245-11 L9297.D 03/02/2017 23:52
IB030217L-B L9298.D 03/03/2017 00:42
491700245-12 L9299.D 03/03/2017 01:26
491700245-13 L9300.D 03/03/2017 02:10
491700245-14 L9301.D 03/03/2017 07:48
IB030217L-C L9302.D 03/03/2017 08:38
491700245-12RE L9303.D 03/03/2017 09:21
491700245-10DL L9304.D 03/03/2017 10:04
491700245-11DL L9305.D 03/03/2017 10:47
491700245-13DL L9306.D 03/03/2017 11:30
491700245-14DL L9307.D 03/03/2017 12:13
491700245-10DL2 L9308.D 03/03/2017 12:56
491700245-11DL2 L9309.D 03/03/2017 13:40
491700245-13DL2 L9310.D 03/03/2017 14:32
491700245-10DL3 L9311.D 03/03/2017 15:15
ECVS030217L-10 L9312.D 03/03/2017 15:59
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% Relative
50 8-0 - 40% of mass 95 24.7
75 30.0 - 66.0% of mass 95 51.5
96 5.0 - 9.0% of mass 95 6.6
173 Less than 2.0% of mass 174 0.0 (0.0) 1
174 50.0 - 120.0% of mass 95 101.6
175 4.0 - 9.0% of mass 174 7.5 (7.4) 1
176 93.0 - 101.0% of mass 174 98.5 (96.9) 1
177 5.0 - 9.0% of mass 176 6.6 (6.7) 2

CCVS030717L-10 L9315.D 03/07/2017 09:38
MB030717L L9316.D 03/07/2017 11:18
RLLCS030717L-0.5 L9317.D 03/07/2017 12:01
RLLCS030717L-0.2 L9318.D 03/07/2017 12:44
C3434 L9319.D 03/07/2017 13:34
491700251-1DL2 L9320.D 03/07/2017 14:19
491700264-1 L9321.D 03/07/2017 15:09
491700264-2 L9322.D 03/07/2017 16:29
491700264-3 L9323.D 03/07/2017 17:20
491700264-4 L9324.D 03/07/2017 18:10
491700264-5 L9325.D 03/07/2017 19:00
491700264-6 L9326.D 03/07/2017 19:49
491700264-7 L9327.D 03/07/2017 20:40
491700264-7DUP L9328.D 03/07/2017 21:30
IB030717L-A L9329.D 03/07/2017 22:20
491700245-1 L9330.D 03/07/2017 23:10
491700245-2 L9331.D 03/08/2017 00:00
491700245-3 L9332.D 03/08/2017 00:50
491700245-4 L9333.D 03/08/2017 01:40
ECVS030717L-10 L9334.D 03/08/2017 02:24
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% Relative
50 8-0 - 40% of mass 95 26.0
75 30.0 - 66.0% of mass 95 53.4
96 5.0 - 9.0% of mass 95 6.8
173 Less than 2.0% of mass 174 0.0 (0.0) 1
174 50.0 - 120.0% of mass 95 109.8
175 4.0 - 9.0% of mass 174 7.9 (7.2) 1
176 93.0 - 101.0% of mass 174 106.0 (96.6) 1
177 5.0 - 9.0% of mass 176 7.0 (6.6) 2

CCVS030817L-10 L9337.D 03/08/2017 04:34
MB030817L L9338.D 03/08/2017 06:14
RLLCS030817L-0.5 L9339.D 03/08/2017 06:57
RLLCS030817L-0.2 L9340.D 03/08/2017 07:40
IB030817L-A L9341.D 03/08/2017 09:17
491700264-2RE L9342.D 03/08/2017 10:07
491700245-5 L9343.D 03/08/2017 10:57
491700245-6 L9344.D 03/08/2017 11:46
491700245-7 L9345.D 03/08/2017 12:36
491700245-8 L9346.D 03/08/2017 13:26
491700245-9 L9347.D 03/08/2017 14:16
491700245-9DUP L9348.D 03/08/2017 15:06
491700245-1DL L9349.D 03/08/2017 15:52
491700245-2DL L9350.D 03/08/2017 16:37
491700245-5DL L9351.D 03/08/2017 17:23
ECVS030817L-10 L9352.D 03/08/2017 18:07
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Daily Sequence Evaluation
Internal Standard Area and RT Summary

Lab Standard ID: IC030117L-10 Analysis Date: 03/01/17
Standard File ID: L9269.D Analysis Time: 7:47 PM
Bromochloromethane 1,4-Difluorobenzene Chlorobenzene-d5

Peak R.T. Peak R.T. Peak R.T.
Area # (min) # Area # (min) # Area # (min) #
10 ppbv Std 417460 11.97 1040380 13.66 972788 20.15
Upper Limit 584444 12.30 1456532 13.99 1361903.2 20.48
Lower Limit 250476 11.64 624228 13.33 583672.8 19.82
Lab Sample ID
ICVS030117L-10 391027 11.97 993201 13.67 915732 20.15
ICVS030117L-10B 414933 11.97 1069150 13.67 983288 20.15
MB030117L_info_run 402646 11.96 1028780 13.67 905054 20.15
MB030117L_B 405084 11.97 1030440 13.67 924594 20.14
RLLCS030117L-0.5 410181 11.96 1032080 13.67 911651 20.14
RLLCS030117L-0.2 394819 11.96 1022680 13.66 899463 20.15
491700158-1 393971 11.96 1000120 13.66 920935 20.14
IB030117L-A 417539 11.93 1028780 13.64 939078 20.12
491700223-2 402130 11.94 990840 13.64 883382 20.12
491700223-3 397949 11.94 968363 13.63 871941 20.11
491700223-1 376117 11.93 929806 13.63 848057 20.11
IB030117L-B 391806 11.93 985506 13.64 874592 20.12
491700251-1 386847 11.93 973463 13.63 866297 20.11
491700251-2 379184 11.93 949854 13.62 845890 20.10
ECVS030117L-10 390469 11.92 987052 13.63 932838 20.11
ECVS030117L-10B 401728 11.92 1029480 13.63 956830 20.11
# Column used to flag values outside QC Limits with an asterisk (*).
QC Criteria
Peak Area Upper Limit = +40% of daily 10ppbv calibration level internal standard.
Peak Area Lower Limit = -40% of daily 10ppbv calibration level internal standard.
RT Upper Limit = +0.33 minutes of daily 10ppbv calibration level internal standard.
RT Upper Limit = -0.33 minutes of daily 10ppbv calibration level internal standard.
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Lab Standard ID: CCVS030217L-10 Analysis Date: 03/02/17

10 ppbv Std 416014 11.92 1050300 13.62 979885 20.10
Upper Limit 582420 12.25 1470420 13.95 1371839 20.43
Lower Limit 249608 11.59 630180 13.29 587931 19.77
Lab Sample ID
MB030217L 393763 11.92 986536 13.62 883409 20.10
RLLCS030217L-0.5 388153 11.91 957873 13.61 870686 20.09
RLLCS030217L-0.2 368357 11.91 922466 13.61 845693 20.10
491700251-1DL 357165 11.91 887283 13.61 799199 20.09
IB030217L-A 378091 11.91 946890 13.61 857198 20.09
491700245-10 390563 11.90 979607 13.61 888842 20.10
491700245-11 355873 11.90 914998 13.61 865652 20.10
IB030217L-B 374733 11.91 964747 13.61 870349 20.09
491700245-12 372810 11.90 960498 13.60 839025 20.08
491700245-13 357847 11.90 923723 13.61 865383 20.09
491700245-14 369060 11.89 944664 13.60 862579 20.08
IB030217L-C 352321 11.89 894151 13.60 818748 20.07
491700245-12RE 366410 11.89 927527 13.60 822199 20.08
491700245-10DL 360942 11.90 924574 13.59 860037 20.08
491700245-11DL 353783 11.89 907003 13.60 806885 20.08
491700245-13DL 351247 11.90 886398 13.60 802947 20.08
491700245-14DL 360132 11.90 930183 13.59 823053 20.08
491700245-10DL2 350119 11.90 899023 13.60 806872 20.08
491700245-11DL2 356821 11.89 905795 13.60 807449 20.08
491700245-13DL2 374492 11.89 951699 13.60 834395 20.08
491700245-10DL3 371671 11.90 923761 13.60 853346 20.08
ECVS030217L-10 399903 11.89 1000360 13.59 940213 20.08
QC Criteria
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Standard File ID: L9315.D Analysis Time: 9:38 AM

10 ppbv Std 411521 11.89 1089940 13.59 1046460 20.07
Upper Limit 576129 12.22 1525916 13.92 1465044 20.40
Lower Limit 246913 11.56 653964 13.26 627876 19.74
Lab Sample ID
MB030717L 387874 11.90 1039080 13.60 925073 20.08
RLLCS030717L-0.5 379404 11.90 985866 13.60 920858 20.08
RLLCS030717L-0.2 378343 11.90 1010140 13.61 905252 20.09
C3434 376263 11.91 1008640 13.61 903091 20.09
491700251-1DL2 395996 11.90 1039910 13.61 943566 20.09
491700264-1 374989 11.90 991627 13.61 893215 20.09
491700264-2 374580 11.91 983518 13.61 887117 20.10
491700264-3 363184 11.91 963140 13.61 887533 20.09
491700264-4 365259 11.91 953496 13.61 877672 20.09
491700264-5 360600 11.91 965233 13.61 872510 20.09
491700264-6 363426 11.91 980290 13.61 891292 20.09
491700264-7 367263 11.92 983448 13.61 887934 20.09
491700264-7DUP 363631 11.92 962009 13.62 864323 20.10
IB030717L-A 375412 11.92 996334 13.61 899354 20.09
491700245-1 391258 11.91 1021640 13.62 922452 20.10
491700245-2 373292 11.92 1012170 13.62 899260 20.10
491700245-3 368405 11.92 995050 13.62 894266 20.10
491700245-4 370440 11.92 1000630 13.63 902610 20.11
ECVS030717L-10 387298 11.93 1052860 13.63 990571 20.11
QC Criteria
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10 ppbv Std 421037 11.92 1131180 13.63 1049820 20.11
Upper Limit 589452 12.25 1583652 13.96 1469748 20.44
Lower Limit 252622 11.59 678708 13.30 629892 19.78
Lab Sample ID
MB030817L 382687 11.92 1026620 13.62 914678 20.10
RLLCS030817L-0.5 379273 11.91 1031070 13.62 895732 20.10
RLLCS030817L-0.2 363192 11.91 1001000 13.61 891896 20.10
IB030817L-A 379521 11.91 989194 13.61 902558 20.09
491700264-2RE 382807 11.91 1010960 13.61 889957 20.09
491700245-5 367457 11.92 970705 13.62 875985 20.10
491700245-6 375965 11.91 972232 13.62 876489 20.10
491700245-7 366671 11.91 969410 13.62 870911 20.10
491700245-8 359706 11.92 945353 13.62 846628 20.11
491700245-9 368842 11.92 983775 13.63 893359 20.11
491700245-9DUP 369456 11.92 939148 13.63 881046 20.11
491700245-1DL 348963 11.92 919277 13.63 822079 20.11
491700245-2DL 354057 11.93 922042 13.63 834713 20.11
491700245-5DL 348176 11.93 908513 13.63 822238 20.10
ECVS030817L-10 378233 11.92 1022830 13.63 973538 20.11
QC Criteria
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200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample #: 491700245-0001

32 Bushes Lane Collected: 2/23/2017
1st Floor Received: 2/28/2017
Elmwood Park, NJ 07407
Project: 81 Main Street Sample ID: 81-WC-1
Analysis Analysis Date Analyst Initials Lab File ID Canister ID Sample Vol(ml) Dilution Factor
Initial 03/07/2017 MTH L9330.D E0448 500 1
Target Compound Results Summary

Result Result
Target Compounds CAS# MW ppbv Q ug/m3 Comments
Acetone 67-64-1 58.08 51 E 120
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.35 1.1
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 3.0 7.2
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.50 1.0
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,2-Dichlorobenzene 95-50-1 147 0.20 U 1.2
1,2-Dichloropropane 78-87-5 113 0.20 U 0.92
1,3-Dichloropropene (cis) 10061-01-5 111 0.20 U 0.91
1,3-Dichloropropene (trans) 10061-02-6 111 0.20 U 0.91
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 39 74
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.26 0.93
Isopropanol 67-63-0 60.1 2.1 5.1
Naphthalene 91-20-3 128.17 0.20 U 1.0
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Result Result
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 1.0 3.9
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.5 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87
Total Target Compound Volatiles: 100 220

Qualifier Definitions
J- Estimated value reported below adjusted reporting limit for target compounds.
E- Estimated concentration exceeding upper calibration range. Ethanol and isopropyl alcohol are not specifically targeted to dilute within calibration range.
Method Reference
1) USEPA: Compendium Method TO-15, “Determination of Volatile Organic Compounds (VOCs) in Air…" Collected in Specially-Prepared Canisters and Analyzed by Gas
Chromatography/Mass Spectrometry (GC/MS), January 1999, (EPA/625/R-96/010b).
2)NJDEP- SRWM Low Level USEPA Method TO-15 (NJDEP-LLTO-15 -March 2007) NJDEP Certification #: 03036
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Tentatively Identified Compounds Result Result Retention

Non-Alkane/ Alkene CAS# MW(1) ppbv Q ug/m3 Time Comments
Total Non-Alkane/ Alkene TICs: 8.4 29
(1)- If compound is unknown, MW is assigned as Toluene (92) for ug/m3 conversion purposes.
J- Estimated value for TICs based on a 1:1 response to internal standards assumed.
N- Indicates presumptive evidence of a compound based on library search match.
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Individual Alkanes CAS# MW(1) ppbv Q ug/m3 Time Comments
Total Alkanes TICs: 3.1 9.2

Individual Alkenes CAS# MW(1) ppbv Q ug/m3 Time Comments
No Alkene TICs reported
(1)- If compound is unknown, MW is assigned as equivalent Toluene (92) for ug/m3 conversion purposes.
Method Reference
1) USEPA: Compendium Method TO-15, “Determination of Volatile Organic Compounds (VOCs) in Air…" Collected in Specially-Prepared Canisters and
Analyzed by Gas Chromatography/Mass Spectrometry (GC/MS), January 1999, (EPA/625/R-96/010b).
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200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample #: 491700245-0001DL

Initial 03/08/2017 MTH L9349.D E0448 250 2

Result Result
Acetone 67-64-1 58.08 53 D 130
Allyl chloride 107-05-1 76.53 0.40 U 1.3
Benzene 71-43-2 78.11 0.40 U 1.3
Bromoform 75-25-2 252.8 0.40 U 4.1
Bromomethane 74-83-9 94.94 0.40 U 1.6
1,3-Butadiene 106-99-0 54.09 0.40 U 0.88
n-Butane 106-97-8 58.12 3.0 D 7.0
Chlorobenzene 108-90-7 112.6 0.40 U 1.8
Chloroethane 75-00-3 64.52 0.40 U 1.1
Chloroform 67-66-3 119.4 0.40 U 2.0
Chloromethane 74-87-3 50.49 0.50 D 1.0
2-Chlorotoluene 95-49-8 126.6 0.40 U 2.1
Cyclohexane 110-82-7 84.16 0.40 U 1.4
1,2-Dibromoethane 106-93-4 187.8 0.40 U 3.1
1,4-Dioxane 123-91-1 88.12 1.0 U 3.6
Ethanol 64-17-5 46.07 42 D 80
Ethylbenzene 100-41-4 106.2 0.40 U 1.7
4-Ethyltoluene 622-96-8 120.2 0.40 U 2.0
n-Heptane 142-82-5 100.2 0.40 U 1.6
n-Hexane 110-54-3 86.17 0.40 U 1.4
Isopropanol 67-63-0 60.1 2.3 D 5.6
Methyl ethyl ketone 78-93-3 72.1 0.57 D 1.7
Naphthalene 91-20-3 128.17 0.40 U 2.1
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Result Result
Styrene 100-42-5 104.1 0.40 U 1.7
Tetrachloroethene 127-18-4 165.8 0.76 D 5.2
Toluene 108-88-3 92.14 1.0 D 3.8
Vinyl bromide 593-60-2 106.9 0.40 U 1.7
Vinyl chloride 75-01-4 62.5 0.40 U 1.0
Xylene (m,p) 1330-20-7 106.2 0.80 U 3.5
Xylene (o) 95-47-6 106.2 0.40 U 1.7

Method Reference
491700245-0001DL_R0 V19 Page 2 of 2

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Project: 81 Main Street Sample ID: 81-CS-1
Initial 03/08/2017 MTH L9331.D E12267 500 1

Result Result
Acetone 67-64-1 58.08 59 E 140
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.42 1.3
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 6.2 15
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.32 1.6
Chloromethane 74-87-3 50.49 0.55 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,2-Dichloroethane 107-06-2 98.96 0.37 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 23 44
Ethylbenzene 100-41-4 106.2 0.32 1.4
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.75 3.1
n-Hexane 110-54-3 86.17 0.52 1.8
Isopropanol 67-63-0 60.1 7.1 17
Naphthalene 91-20-3 128.17 0.20 U 1.0
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Result Result
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 7.5 28
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.5 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 1.1 4.6
Xylene (o) 95-47-6 106.2 0.35 1.5

Method Reference
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Unknown 92 2.4 J 9 5.28
Unknown 92 1.1 J 4.1 10.68
D-Limonene 005989-27-5 136 1.6 JN 9 24.23
Total Non-Alkane/ Alkene TICs: 11 44
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Method Reference
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Initial 03/08/2017 MTH L9350.D E12267 250 2

Result Result
Acetone 67-64-1 58.08 59 D 140
Allyl chloride 107-05-1 76.53 0.40 U 1.3
Benzene 71-43-2 78.11 0.44 D 1.4
Bromoform 75-25-2 252.8 0.40 U 4.1
Bromomethane 74-83-9 94.94 0.40 U 1.6
1,3-Butadiene 106-99-0 54.09 0.40 U 0.88
n-Butane 106-97-8 58.12 6.1 D 14
Chlorobenzene 108-90-7 112.6 0.40 U 1.8
Chloroethane 75-00-3 64.52 0.40 U 1.1
Chloroform 67-66-3 119.4 0.40 U 2.0
Chloromethane 74-87-3 50.49 0.59 D 1.2
2-Chlorotoluene 95-49-8 126.6 0.40 U 2.1
Cyclohexane 110-82-7 84.16 0.40 U 1.4
1,2-Dibromoethane 106-93-4 187.8 0.40 U 3.1
1,4-Dioxane 123-91-1 88.12 1.0 U 3.6
Ethanol 64-17-5 46.07 25 D 46
Ethylbenzene 100-41-4 106.2 0.40 U 1.7
4-Ethyltoluene 622-96-8 120.2 0.40 U 2.0
n-Heptane 142-82-5 100.2 0.80 D 3.3
n-Hexane 110-54-3 86.17 0.53 D 1.9
Isopropanol 67-63-0 60.1 7.5 D 19
Methylene chloride 75-09-2 84.94 4.7 D 16
Methyl ethyl ketone 78-93-3 72.1 6.0 D 18
Naphthalene 91-20-3 128.17 0.40 U 2.1
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Result Result
Styrene 100-42-5 104.1 0.40 U 1.7
Tetrachloroethene 127-18-4 165.8 10 D 68
Tetrahydrofuran 109-99-9 72.11 4.6 D 14
Toluene 108-88-3 92.14 7.7 D 29
Trichloroethene 79-01-6 131.4 23 D 130
Vinyl bromide 593-60-2 106.9 0.40 U 1.7
Vinyl chloride 75-01-4 62.5 0.40 U 1.0
Xylene (m,p) 1330-20-7 106.2 1.0 D 4.5
Xylene (o) 95-47-6 106.2 0.40 U 1.7

Method Reference
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Project: 81 Main Street Sample ID: 81-AA-1
Initial 03/08/2017 MTH L9332.D E12292 500 1

Result Result
Acetone 67-64-1 58.08 4.4 10
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.44 1.4
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 3.3 7.7
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.21 1.0
Chloromethane 74-87-3 50.49 0.49 1.0
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 5.7 11
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.30 1.1
Isopropanol 67-63-0 60.1 3.5 8.5
Naphthalene 91-20-3 128.17 0.20 U 1.0
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Result Result
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.72 2.7
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.5 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87

Method Reference
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Unknown 92 1.3 J 4.9 4.93
Total Non-Alkane/ Alkene TICs: 1.3 4.9
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Method Reference
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Project: 81 Main Street Sample ID: 81-K-1
Initial 03/08/2017 MTH L9333.D E15311 500 1

Result Result
Acetone 67-64-1 58.08 14 34
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.60 1.9
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 6.9 16
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.50 2.4
Chloromethane 74-87-3 50.49 0.56 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dichlorobenzene 106-46-7 147 0.24 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 150 E 290
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.52 2.1
n-Hexane 110-54-3 86.17 0.38 1.3
Isopropanol 67-63-0 60.1 4.7 12
Naphthalene 91-20-3 128.17 0.20 U 1.0
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Result Result
Styrene 100-42-5 104.1 0.24 1.0
Toluene 108-88-3 92.14 2.4 8.9
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.5 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.52 2.3
Xylene (o) 95-47-6 106.2 0.20 U 0.87

Method Reference
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Ethyl Acetate 000141-78-6 88 1.2 JN 4.2 11.24
Hexanal 000066-25-1 100 1 JN 4.2 17.98
Benzaldehyde 000100-52-7 106 1.5 JN 6.7 23.93
D-Limonene 005989-27-5 136 2.1 JN 12 24.24
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Alkane-Isobutane 000075-28-5 58 2.1 JN 5 5.29
Alkane-Butane, 2-methyl- 000078-78-4 72 2 JN 5.9 6.59
Total Alkanes TICs: 4.1 11

Method Reference
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Result Result
Acetone 67-64-1 58.08 43 E 100
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.37 1.2
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 3.2 7.6
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.54 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 40 75
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.22 0.92
n-Hexane 110-54-3 86.17 0.27 1.0
Isopropanol 67-63-0 60.1 1.9 4.6
Naphthalene 91-20-3 128.17 0.20 U 1.0
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Result Result
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 1.1 4.1
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.5 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.42 1.8
Xylene (o) 95-47-6 106.2 0.20 U 0.87

Method Reference
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Method Reference
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Initial 03/08/2017 MTH L9351.D E15519 250 2

Result Result
Acetone 67-64-1 58.08 43 D 100
Allyl chloride 107-05-1 76.53 0.40 U 1.3
Benzene 71-43-2 78.11 0.40 U 1.3
Bromoform 75-25-2 252.8 0.40 U 4.1
Bromomethane 74-83-9 94.94 0.40 U 1.6
1,3-Butadiene 106-99-0 54.09 0.40 U 0.88
n-Butane 106-97-8 58.12 3.2 D 7.6
Chlorobenzene 108-90-7 112.6 0.40 U 1.8
Chloroethane 75-00-3 64.52 0.40 U 1.1
Chloroform 67-66-3 119.4 0.40 U 2.0
Chloromethane 74-87-3 50.49 0.52 D 1.1
2-Chlorotoluene 95-49-8 126.6 0.40 U 2.1
Cyclohexane 110-82-7 84.16 0.40 U 1.4
1,2-Dibromoethane 106-93-4 187.8 0.40 U 3.1
1,4-Dioxane 123-91-1 88.12 1.0 U 3.6
Ethanol 64-17-5 46.07 44 D 82
Ethylbenzene 100-41-4 106.2 0.40 U 1.7
4-Ethyltoluene 622-96-8 120.2 0.40 U 2.0
n-Heptane 142-82-5 100.2 0.40 U 1.6
n-Hexane 110-54-3 86.17 0.40 U 1.4
Isopropanol 67-63-0 60.1 2.0 D 4.9
Methyl ethyl ketone 78-93-3 72.1 0.71 D 2.1
Naphthalene 91-20-3 128.17 0.40 U 2.1
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Result Result
Styrene 100-42-5 104.1 0.40 U 1.7
Tetrachloroethene 127-18-4 165.8 0.85 D 5.7
Toluene 108-88-3 92.14 1.1 D 4.1
Vinyl bromide 593-60-2 106.9 0.40 U 1.7
Vinyl chloride 75-01-4 62.5 0.40 U 1.0
Xylene (m,p) 1330-20-7 106.2 0.80 U 3.5
Xylene (o) 95-47-6 106.2 0.40 U 1.7

Method Reference
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Result Result
Acetone 67-64-1 58.08 8.9 21
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.48 1.5
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 4.6 11
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.43 2.1
Chloromethane 74-87-3 50.49 0.55 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 85 E 160
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.33 1.4
n-Hexane 110-54-3 86.17 0.33 1.2
Isopropanol 67-63-0 60.1 4.5 11
Naphthalene 91-20-3 128.17 0.20 U 1.0
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Result Result
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 1.6 6.1
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.5 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.47 2.0
Xylene (o) 95-47-6 106.2 0.20 U 0.87

Method Reference
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D-Limonene 005989-27-5 136 1.1 JN 6.1 24.23
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Method Reference
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Project: 81 Main Street Sample ID: 81-NC-1
Initial 03/08/2017 MTH L9345.D E0420 500 1

Result Result
Acetone 67-64-1 58.08 9.8 23
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.35 1.1
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 3.5 8.4
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 1.0
Chloromethane 74-87-3 50.49 0.52 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 93 E 170
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.23 0.93
n-Hexane 110-54-3 86.17 0.28 1.0
Isopropanol 67-63-0 60.1 4.7 12
Naphthalene 91-20-3 128.17 0.20 U 1.0
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Result Result
Styrene 100-42-5 104.1 0.40 1.7
Toluene 108-88-3 92.14 1.3 4.9
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.5 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.44 1.9
Xylene (o) 95-47-6 106.2 0.20 U 0.87

Method Reference
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Unknown 92 3.9 J 15 4.91
D-Limonene 005989-27-5 136 2.3 JN 13 24.23
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Method Reference
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Project: 81 Main Street Sample ID: 81-HS-1
Initial 03/08/2017 MTH L9346.D E0437 500 1

Result Result
Acetone 67-64-1 58.08 28 68
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.52 1.7
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 9.9 23
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.30 1.4
Chloromethane 74-87-3 50.49 0.52 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 16 29
Ethylbenzene 100-41-4 106.2 0.35 1.5
4-Ethyltoluene 622-96-8 120.2 0.23 1.1
n-Heptane 142-82-5 100.2 0.86 3.5
n-Hexane 110-54-3 86.17 0.43 1.5
Isopropanol 67-63-0 60.1 5.4 13
Naphthalene 91-20-3 128.17 0.20 U 1.0
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Result Result
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 7.2 27
1,2,4-Trimethylbenzene 95-63-6 120.2 0.23 1.1
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.5 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 1.0 4.4
Xylene (o) 95-47-6 106.2 0.34 1.5

Method Reference
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Unknown 92 4.9 J 18 4.92
Unknown 92 6.1 J 23 5.3
Unknown 92 5.6 J 21 10.68
Ethyl Acetate 000141-78-6 88 2.5 JN 8.9 11.24
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Alkane-Pentane, 2-methyl- 000107-83-5 86 1 JN 3.6 8.7

Method Reference
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Project: 81 Main Street Sample ID: 81-MR-1
Initial 03/08/2017 MTH L9347.D E0597 500 1

Result Result
Acetone 67-64-1 58.08 15 35
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.43 1.4
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 5.6 13
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 1.2 5.8
Chloromethane 74-87-3 50.49 0.53 1.1
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
Dichlorodifluoromethane 75-71-8 120.9 0.27 1.4
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 180 E 350
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.56 2.3
n-Hexane 110-54-3 86.17 0.44 1.6
Isopropanol 67-63-0 60.1 4.2 10
Naphthalene 91-20-3 128.17 0.26 1.4
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Result Result
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 2.5 9.4
Trichloroethene 79-01-6 131.4 1.9 10
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.5 0.20 U 0.51
Xylene (m,p) 1330-20-7 106.2 0.57 2.5
Xylene (o) 95-47-6 106.2 0.20 U 0.87

Method Reference
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Unknown 92 7 J 26 4.92
Unknown 92 2.4 J 9.1 5.29
Unknown 92 2.1 J 7.7 10.68
Ethyl Acetate 000141-78-6 88 1.3 JN 4.5 11.24
Hexanal 000066-25-1 100 4 JN 17 17.98
D-Limonene 005989-27-5 136 4.6 JN 25 24.23
Nonanal 000124-19-6 142 1.6 JN 9.1 25.37
Unknown 92 1.4 J 5.3 28.14
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Alkane-Butane, 2-methyl- 000078-78-4 72 5.9 JN 17 6.59

Method Reference
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Project: 81 Main Street Sample ID: 81-CS-1SS
Initial 03/02/2017 MTH L9296.D HD2160 50 10

Result Result
Acetone 67-64-1 58.08 60 140
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 4.8 15
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 8.5 41
Chloromethane 74-87-3 50.49 2.0 U 4.1
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,2-Dichlorobenzene 95-50-1 147 2.0 U 12
1,2-Dichloroethene (cis) 156-59-2 96.94 1300 E 5200
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 26 48
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.1 11 28
Naphthalene 91-20-3 128.17 2.0 U 10
491700245-0010_R0 V18 Page 1 of 4

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Initial 03/02/2017 MTH L9296.D HD2160 50 10

Result Result
Styrene 100-42-5 104.1 2.0 U 8.5
Toluene 108-88-3 92.14 2.0 U 7.5
Trichloroethene 79-01-6 131.4 880 E 4700
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.5 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
Xylene (o) 95-47-6 106.2 2.0 U 8.7

Method Reference
491700245-0010_R0 V18 Page 2 of 4

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No Non-Alkane/ Alkene TICs reported
491700245-0010_R0 V18 Page 3 of 4

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Initial 03/02/2017 MTH L9296.D HD2160 50 10

No Alkane TICs reported

Method Reference
491700245-0010_R0 V18 Page 4 of 4

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392 of 794
393 of 794
394 of 794

Initial 03/03/2017 MTH L9304.D HD2160 25 60

Result Result
Acetone 67-64-1 58.08 55 D 130
Allyl chloride 107-05-1 76.53 12 U 38
Benzene 71-43-2 78.11 12 U 38
Bromoform 75-25-2 252.8 12 U 120
Bromomethane 74-83-9 94.94 12 U 47
1,3-Butadiene 106-99-0 54.09 12 U 27
n-Butane 106-97-8 58.12 12 U 29
Chlorobenzene 108-90-7 112.6 12 U 55
Chloroethane 75-00-3 64.52 12 U 32
Chloroform 67-66-3 119.4 12 U 59
2-Chlorotoluene 95-49-8 126.6 12 U 62
Cyclohexane 110-82-7 84.16 12 U 41
1,2-Dibromoethane 106-93-4 187.8 12 U 92
1,2-Dichlorobenzene 95-50-1 147 12 U 72
1,2-Dichloroethene (cis) 156-59-2 96.94 1200 D 4900
1,2-Dichloroethene (trans) 156-60-5 96.94 16 D 64
1,2-Dichloropropane 78-87-5 113 12 U 55
1,3-Dichloropropene (cis) 10061-01-5 111 12 U 54
1,3-Dichloropropene (trans) 10061-02-6 111 12 U 54
1,4-Dioxane 123-91-1 88.12 30 U 110
Ethanol 64-17-5 46.07 33 D 63
Ethylbenzene 100-41-4 106.2 12 U 52
4-Ethyltoluene 622-96-8 120.2 12 U 59
n-Heptane 142-82-5 100.2 12 U 49
n-Hexane 110-54-3 86.17 12 U 42
Isopropanol 67-63-0 60.1 30 U 74
Naphthalene 91-20-3 128.17 12 U 63
491700245-0010DL_R0 V18 Page 1 of 2

395 of 794

Initial 03/03/2017 MTH L9304.D HD2160 25 60

Result Result
Styrene 100-42-5 104.1 12 U 51
Tetrachloroethene 127-18-4 165.8 5300 DE 36000
Toluene 108-88-3 92.14 12 U 45
Vinyl bromide 593-60-2 106.9 12 U 52
Vinyl chloride 75-01-4 62.5 12 U 31
Xylene (m,p) 1330-20-7 106.2 24 U 100
Xylene (o) 95-47-6 106.2 12 U 52

Method Reference
491700245-0010DL_R0 V18 Page 2 of 2

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200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample #: 491700245-0010DL3

Initial 03/03/2017 MTH L9311.D HD2160 25 1620

Result Result
Acetone 67-64-1 58.08 810 U 1900
Allyl chloride 107-05-1 76.53 320 U 1000
Benzene 71-43-2 78.11 320 U 1000
Bromoform 75-25-2 252.8 320 U 3300
Bromomethane 74-83-9 94.94 320 U 1300
1,3-Butadiene 106-99-0 54.09 320 U 720
n-Butane 106-97-8 58.12 320 U 770
Chlorobenzene 108-90-7 112.6 320 U 1500
Chloroethane 75-00-3 64.52 320 U 850
Chloroform 67-66-3 119.4 320 U 1600
Chloromethane 74-87-3 50.49 320 U 670
2-Chlorotoluene 95-49-8 126.6 320 U 1700
Cyclohexane 110-82-7 84.16 320 U 1100
1,2-Dibromoethane 106-93-4 187.8 320 U 2500
1,2-Dichloroethene (cis) 156-59-2 96.94 1200 D 4800
1,4-Dioxane 123-91-1 88.12 810 U 2900
Ethanol 64-17-5 46.07 810 U 1500
Ethylbenzene 100-41-4 106.2 320 U 1400
4-Ethyltoluene 622-96-8 120.2 320 U 1600
n-Heptane 142-82-5 100.2 320 U 1300
n-Hexane 110-54-3 86.17 320 U 1100
Isopropanol 67-63-0 60.1 810 U 2000
Naphthalene 91-20-3 128.17 320 U 1700
491700245-0010DL3_R0 V19 Page 1 of 2

406 of 794

Initial 03/03/2017 MTH L9311.D HD2160 25 1620

Result Result
Styrene 100-42-5 104.1 320 U 1400
Toluene 108-88-3 92.14 320 U 1200
Vinyl bromide 593-60-2 106.9 320 U 1400
Vinyl chloride 75-01-4 62.5 320 U 830
Xylene (m,p) 1330-20-7 106.2 650 U 2800
Xylene (o) 95-47-6 106.2 320 U 1400

Method Reference
491700245-0010DL3_R0 V19 Page 2 of 2

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Project: 81 Main Street Sample ID: 81-MR-1SS
Initial 03/02/2017 MTH L9297.D HD2161 50 10

Result Result
Acetone 67-64-1 58.08 170 400
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 2.0 U 6.4
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 3.2 16
Chloromethane 74-87-3 50.49 2.0 U 4.1
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,2-Dichloroethene (cis) 156-59-2 96.94 3.0 12
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 30 57
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.1 6.6 16
Naphthalene 91-20-3 128.17 2.2 12
491700245-0011_R0 V18 Page 1 of 4

412 of 794

Initial 03/02/2017 MTH L9297.D HD2161 50 10

Result Result
Styrene 100-42-5 104.1 2.0 U 8.5
Toluene 108-88-3 92.14 2.0 U 7.5
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.5 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
Xylene (o) 95-47-6 106.2 2.0 U 8.7

Method Reference
491700245-0011_R0 V18 Page 2 of 4

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491700245-0011_R0 V18 Page 3 of 4

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Initial 03/02/2017 MTH L9297.D HD2161 50 10

Alkane-unknown cyclohexane 92 36 J 130 21
Alkane-unknown 92 38 J 140 21.26
Alkane-unknown cyclohexane 92 61 J 230 21.71
Alkane-unknown cyclohexane 92 35 J 130 22.58
Total Alkanes TICs: 170 630

Method Reference
491700245-0011_R0 V18 Page 4 of 4

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Initial 03/03/2017 MTH L9309.D HD2161 25 540

Result Result
Acetone 67-64-1 58.08 270 U 640
Allyl chloride 107-05-1 76.53 110 U 340
Benzene 71-43-2 78.11 110 U 350
Bromoform 75-25-2 252.8 110 U 1100
Bromomethane 74-83-9 94.94 110 U 420
1,3-Butadiene 106-99-0 54.09 110 U 240
n-Butane 106-97-8 58.12 110 U 260
Chlorobenzene 108-90-7 112.6 110 U 500
Chloroethane 75-00-3 64.52 110 U 280
Chloroform 67-66-3 119.4 110 U 530
Chloromethane 74-87-3 50.49 110 U 220
2-Chlorotoluene 95-49-8 126.6 110 U 560
Cyclohexane 110-82-7 84.16 110 U 370
1,2-Dibromoethane 106-93-4 187.8 110 U 830
1,4-Dioxane 123-91-1 88.12 270 U 1000
Ethanol 64-17-5 46.07 270 U 510
Ethylbenzene 100-41-4 106.2 110 U 470
4-Ethyltoluene 622-96-8 120.2 110 U 530
n-Heptane 142-82-5 100.2 110 U 440
n-Hexane 110-54-3 86.17 110 U 380
Isopropanol 67-63-0 60.1 270 U 660
Naphthalene 91-20-3 128.17 110 U 570
491700245-0011DL2_R0 V19 Page 1 of 2

431 of 794

Initial 03/03/2017 MTH L9309.D HD2161 25 540

Result Result
Styrene 100-42-5 104.1 110 U 460
Toluene 108-88-3 92.14 110 U 410
Vinyl bromide 593-60-2 106.9 110 U 470
Vinyl chloride 75-01-4 62.5 110 U 280
Xylene (m,p) 1330-20-7 106.2 220 U 940
Xylene (o) 95-47-6 106.2 110 U 470

Method Reference
491700245-0011DL2_R0 V19 Page 2 of 2

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200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample #: 491700245-0012RE

Project: 81 Main Street Sample ID: 81-WC-2SS
Initial 03/03/2017 MTH L9303.D HD2179 50 10

Result Result
Acetone 67-64-1 58.08 28 67
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 2.0 U 6.4
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 2.0 U 10
Chloromethane 74-87-3 50.49 2.0 U 4.1
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 28 54
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.1 5.1 12
Naphthalene 91-20-3 128.17 2.0 U 10
491700245-0012RE_R0 V18 Page 1 of 4

441 of 794

Initial 03/03/2017 MTH L9303.D HD2179 50 10

Result Result
Styrene 100-42-5 104.1 2.0 U 8.5
Tetrachloroethene 127-18-4 165.8 2.0 U 14
Toluene 108-88-3 92.14 2.0 U 7.5
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.5 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
Xylene (o) 95-47-6 106.2 2.0 U 8.7

Method Reference
491700245-0012RE_R0 V18 Page 2 of 4

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Initial 03/03/2017 MTH L9303.D HD2179 50 10

491700245-0012RE_R0 V18 Page 3 of 4

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Initial 03/03/2017 MTH L9303.D HD2179 50 10


Method Reference
491700245-0012RE_R0 V18 Page 4 of 4

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455 of 794

Project: 81 Main Street Sample ID: 81-HS-1SS
Initial 03/03/2017 MTH L9300.D HD2331 50 10

Result Result
Acetone 67-64-1 58.08 100 240
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 2.0 U 6.4
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 6.5 32
Chloromethane 74-87-3 50.49 2.0 U 4.1
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 38 72
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.1 12 30
Naphthalene 91-20-3 128.17 2.0 U 10
491700245-0013_R0 V18 Page 1 of 4

456 of 794

Initial 03/03/2017 MTH L9300.D HD2331 50 10

Result Result
Styrene 100-42-5 104.1 2.0 U 8.5
Toluene 108-88-3 92.14 2.0 U 7.5
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.5 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
Xylene (o) 95-47-6 106.2 2.0 U 8.7

Method Reference
491700245-0013_R0 V18 Page 2 of 4

457 of 794

Initial 03/03/2017 MTH L9300.D HD2331 50 10

491700245-0013_R0 V18 Page 3 of 4

458 of 794

Initial 03/03/2017 MTH L9300.D HD2331 50 10

Total Alkanes TICs: 300 1100

Method Reference
491700245-0013_R0 V18 Page 4 of 4

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476 of 794
477 of 794
478 of 794

Initial 03/03/2017 MTH L9310.D HD2331 25 540

Result Result
Acetone 67-64-1 58.08 270 U 640
Allyl chloride 107-05-1 76.53 110 U 340
Benzene 71-43-2 78.11 110 U 350
Bromoform 75-25-2 252.8 110 U 1100
Bromomethane 74-83-9 94.94 110 U 420
1,3-Butadiene 106-99-0 54.09 110 U 240
n-Butane 106-97-8 58.12 110 U 260
Chlorobenzene 108-90-7 112.6 110 U 500
Chloroethane 75-00-3 64.52 110 U 280
Chloroform 67-66-3 119.4 110 U 530
Chloromethane 74-87-3 50.49 110 U 220
2-Chlorotoluene 95-49-8 126.6 110 U 560
Cyclohexane 110-82-7 84.16 110 U 370
1,2-Dibromoethane 106-93-4 187.8 110 U 830
1,4-Dioxane 123-91-1 88.12 270 U 1000
Ethanol 64-17-5 46.07 270 U 510
Ethylbenzene 100-41-4 106.2 110 U 470
4-Ethyltoluene 622-96-8 120.2 110 U 530
n-Heptane 142-82-5 100.2 110 U 440
n-Hexane 110-54-3 86.17 110 U 380
Isopropanol 67-63-0 60.1 270 U 660
Naphthalene 91-20-3 128.17 110 U 570
491700245-0013DL2_R0 V19 Page 1 of 2

479 of 794

Initial 03/03/2017 MTH L9310.D HD2331 25 540

Result Result
Styrene 100-42-5 104.1 110 U 460
Toluene 108-88-3 92.14 110 U 410
Vinyl bromide 593-60-2 106.9 110 U 470
Vinyl chloride 75-01-4 62.5 110 U 280
Xylene (m,p) 1330-20-7 106.2 220 U 940
Xylene (o) 95-47-6 106.2 110 U 470

Method Reference
491700245-0013DL2_R0 V19 Page 2 of 2

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Initial 03/03/2017 MTH L9301.D HD2749 50 10

Result Result
Acetone 67-64-1 58.08 300 720
Allyl chloride 107-05-1 76.53 2.0 U 6.3
Benzene 71-43-2 78.11 2.0 U 6.4
Bromoform 75-25-2 252.8 2.0 U 21
Bromomethane 74-83-9 94.94 2.0 U 7.8
1,3-Butadiene 106-99-0 54.09 2.0 U 4.4
n-Butane 106-97-8 58.12 2.0 U 4.8
Chlorobenzene 108-90-7 112.6 2.0 U 9.2
Chloroethane 75-00-3 64.52 2.0 U 5.3
Chloroform 67-66-3 119.4 570 E 2800
Chloromethane 74-87-3 50.49 2.0 U 4.1
2-Chlorotoluene 95-49-8 126.6 2.0 U 10
Cyclohexane 110-82-7 84.16 2.0 U 6.9
1,2-Dibromoethane 106-93-4 187.8 2.0 U 15
1,4-Dioxane 123-91-1 88.12 5.0 U 18
Ethanol 64-17-5 46.07 44 83
Ethylbenzene 100-41-4 106.2 2.0 U 8.7
4-Ethyltoluene 622-96-8 120.2 2.0 U 10
n-Heptane 142-82-5 100.2 2.0 U 8.2
n-Hexane 110-54-3 86.17 2.0 U 7.0
Isopropanol 67-63-0 60.1 16 39
Methyl isobutyl ketone 108-10-1 100.2 2.5 10
Naphthalene 91-20-3 128.17 2.0 U 10
491700245-0014_R0 V18 Page 1 of 4

484 of 794

Initial 03/03/2017 MTH L9301.D HD2749 50 10

Result Result
Styrene 100-42-5 104.1 2.0 U 8.5
Tert-butyl alcohol 75-65-0 74.12 6.7 20
Toluene 108-88-3 92.14 2.0 U 7.5
Vinyl bromide 593-60-2 106.9 2.0 U 8.7
Vinyl chloride 75-01-4 62.5 2.0 U 5.1
Xylene (m,p) 1330-20-7 106.2 4.0 U 17
Xylene (o) 95-47-6 106.2 2.0 U 8.7

Method Reference
491700245-0014_R0 V18 Page 2 of 4

485 of 794

Initial 03/03/2017 MTH L9301.D HD2749 50 10

1-Hexanol, 2-ethyl- 000104-76-7 130 32 JN 170 24.04
491700245-0014_R0 V18 Page 3 of 4

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Initial 03/03/2017 MTH L9301.D HD2749 50 10


Method Reference
491700245-0014_R0 V18 Page 4 of 4

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497 of 794

Initial 03/03/2017 MTH L9307.D HD2749 25 60

Result Result
Acetone 67-64-1 58.08 290 D 700
Allyl chloride 107-05-1 76.53 12 U 38
Benzene 71-43-2 78.11 12 U 38
Bromoform 75-25-2 252.8 12 U 120
Bromomethane 74-83-9 94.94 12 U 47
1,3-Butadiene 106-99-0 54.09 12 U 27
n-Butane 106-97-8 58.12 12 U 29
Chlorobenzene 108-90-7 112.6 12 U 55
Chloroethane 75-00-3 64.52 12 U 32
Chloroform 67-66-3 119.4 590 D 2900
2-Chlorotoluene 95-49-8 126.6 12 U 62
Cyclohexane 110-82-7 84.16 12 U 41
1,2-Dibromoethane 106-93-4 187.8 12 U 92
1,4-Dioxane 123-91-1 88.12 30 U 110
Ethanol 64-17-5 46.07 48 D 90
Ethylbenzene 100-41-4 106.2 12 U 52
4-Ethyltoluene 622-96-8 120.2 12 U 59
n-Heptane 142-82-5 100.2 12 U 49
n-Hexane 110-54-3 86.17 12 U 42
Isopropanol 67-63-0 60.1 30 U 74
Naphthalene 91-20-3 128.17 12 U 63
491700245-0014DL_R0 V18 Page 1 of 2

498 of 794

Initial 03/03/2017 MTH L9307.D HD2749 25 60

Result Result
Styrene 100-42-5 104.1 12 U 51
Toluene 108-88-3 92.14 12 U 45
Vinyl bromide 593-60-2 106.9 12 U 52
Vinyl chloride 75-01-4 62.5 12 U 31
Xylene (m,p) 1330-20-7 106.2 24 U 100
Xylene (o) 95-47-6 106.2 12 U 52

Method Reference
491700245-0014DL_R0 V18 Page 2 of 2

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EPA TO-15
Initial Calibration
Internal Standard Area and Retention Time Evaluation
Instrument ID: GC/MS L-C

ICAL ID: Q030117L
Analysis Date 1 Mar 2017

Calibration Cal Peak +/-40% R.T. +/-0.33 Peak +/-40% R.T. +/-0.33 Peak +/-40% R.T. +/-0.33
Level ID Data File Area Mean (min) Mean Area Mean (min) Mean Area Mean (min) Mean
IC030117L-40 L9267.D 427420 Pass 11.97 Pass 1030850 Pass 13.67 Pass 986811 Pass 20.15 Pass
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IC030117L-0.5 L9271.D 389394 Pass 11.96 Pass 990471 Pass 13.67 Pass 901060 Pass 20.14 Pass
Mean Values: 409240 11.97 1018780 13.67 938194 20.15
Criteria: Area response of each calibration level must be within +/-40% of the mean area response for each internal standard.
Retention time shift must be within +/-0.33 minutes of the mean retention time for each internal standard.
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EMSL Analytical, Inc. EMSL Order: ICVS
200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample ID: ICVS030117L-10
Phone/Fax:(856)858-4800/ (856)858-4571 Received Date: NA
Project ID: Initial Calibration Verification Standard Sampling Date: NA

Lab Sample ID: ICVS030117L-10 Canister ID: E0462
Lab File ID: L9273.D Analysis Date: 03/01/2017

Sample Vol(ml): 125 Instrument ID: GC/MS L-C
Dilution Factor: 1 Analyst Initials: MTH
Initial Calibration Verification Standard
Spike Result % Recovery Limits (%)
Target Compounds CAS# MW ppbv ppbv Rec # Lower Upper
Acetone 67-64-1 58.08 10 8.87 89% 71% 125%
Allyl chloride 107-05-1 76.53 10 11.5 115% 86% 118%
Benzene 71-43-2 78.11 10 10.0 100% 86% 114%
Bromodichloromethane 75-27-4 163.8 10 10.0 100% 84% 128%
Bromoform 75-25-2 252.8 10 10.7 107% 68% 142%
Bromomethane 74-83-9 94.94 10 9.28 93% 84% 113%
1,3-Butadiene 106-99-0 54.09 10 9.34 93% 70% 111%
n-Butane 106-97-8 58.12 10 8.50 85% 74% 110%
Chlorobenzene 108-90-7 112.6 10 9.93 99% 72% 125%
Chloroethane 75-00-3 64.52 10 9.16 92% 81% 109%
Chloroform 67-66-3 119.4 10 10.3 103% 89% 119%
Chloromethane 74-87-3 50.49 10 9.11 91% 77% 111%
Carbon disulfide 75-15-0 76.14 10 10.8 108% 100% 129%
Carbon tetrachloride 56-23-5 153.8 10 10.6 106% 89% 120%
2-Chlorotoluene 95-49-8 126.6 10 9.36 94% 64% 130%
Cyclohexane 110-82-7 84.16 10 9.92 99% 85% 118%
Dibromochloromethane 124-48-1 208.3 10 10.3 103% 79% 130%
1,2-Dibromoethane 106-93-4 187.8 10 9.92 99% 75% 125%
1,2-Dichlorobenzene 95-50-1 147.0 10 10.3 103% 60% 132%
Dichlorodifluoromethane 75-71-8 120.9 10 9.55 96% 83% 135%
1,1-Dichloroethane 75-34-3 98.96 10 10.1 101% 87% 115%
1,2-Dichloroethane 107-06-2 98.96 10 10.3 103% 91% 122%
1,1-Dichloroethene 75-35-4 96.94 10 10.7 107% 89% 114%
1,2-Dichloroethene (cis) 156-59-2 96.94 10 9.74 97% 71% 114%
1,2-Dichloroethene (trans) 156-60-5 96.94 10 9.68 97% 89% 116%
1,2-Dichloropropane 78-87-5 113.0 10 9.58 96% 77% 120%
1,3-Dichloropropene (cis) 10061-01-5 111.0 10 10.7 107% 83% 133%
1,3-Dichloropropene (trans) 10061-02-6 111.0 10 10.2 102% 74% 122%
1,2-Dichlorotetrafluoroethane 76-14-2 170.9 10 8.91 89% 69% 107%
LLTO15_Master_ICVSS_LCS_w_Limits_Mar_2016_V2 ICVSS Page 1 of 3

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Acetone
1,4-Dioxane 123-91-1 88.12 10 9.34 93% 56% 115%
Ethanol 64-17-5 46.07 10 7.82 78% 61% 128%
Ethylbenzene 100-41-4 106.2 10 9.72 97% 72% 127%
4-Ethyltoluene 622-96-8 120.2 10 10.2 102% 61% 137%
n-Heptane 142-82-5 100.2 10 9.44 94% 80% 118%
1,3-Hexachlorobutadiene 87-68-3 260.8 10 8.85 89% 50% 132%
n-Hexane 110-54-3 86.17 10 9.87 99% 89% 122%
Isopropanol 67-63-0 60.10 10 7.98 80% 68% 114%
Methylene chloride 75-09-2 84.94 10 10.1 101% 83% 111%
Methyl ethyl ketone 78-93-3 72.10 10 9.64 96% 71% 135%
Methyl isobutyl ketone 108-10-1 100.2 10 9.86 99% 59% 132%
Methyl methacrylate 80-62-6 100.12 10 10.5 105% 68% 135%
Naphthalene 91-20-3 128.17 10 11.3 113% 30% 137%
Methyl tert-butyl ether 1634-04-4 88.15 10 9.62 96% 72% 128%
Styrene 100-42-5 104.1 10 11.2 112% 69% 131%
Tert-butyl alcohol 75-65-0 74.12 10 8.23 82% 66% 104%
1,1,2,2-Tetrachloroethane 79-34-5 167.9 10 9.62 96% 59% 129%
Tetrachloroethene 127-18-4 165.8 10 10.1 101% 80% 125%
Tetrahydrofuran 109-99-9 72.11 10 9.29 93% 64% 124%
Toluene 108-88-3 92.14 10 10.0 100% 76% 124%
1,2,4-Trichlorobenzene 120-82-1 181.5 10 10.5 105% 34% 128%
1,1,1-Trichloroethane 71-55-6 133.4 10 9.92 99% 87% 112%
Trichloroethene 79-01-6 131.4 10 10.0 100% 82% 121%
Trichlorofluoromethane 75-69-4 137.4 10 9.78 98% 86% 113%
1,1,2-Trichloro-1,2,2-trifluoroethane 76-13-1 187.4 10 10.7 107% 85% 115%
1,2,4-Trimethylbenzene 95-63-6 120.2 10 10.6 106% 58% 134%
2,2,4-Trimethylpentane 540-84-1 114.2 10 9.88 99% 84% 122%
Vinyl bromide 593-60-2 106.9 10 9.91 99% 91% 121%
Vinyl chloride 75-01-4 62.50 10 9.44 94% 80% 113%

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Acetone(m,p)
Xylene 1330-20-7 106.2 20 18.9 95% 65% 127%
Xylene (o) 95-47-6 106.2 10 10.0 100% 67% 126%




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200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample ID: ICVS030117L-10B

Lab Sample ID: ICVS030117L-10B Canister ID: E0462

Acetone 67-64-1 58.08 10 9.04 90% 71% 125%
Allyl chloride 107-05-1 76.53 10 11.6 116% 86% 118%
Benzene 71-43-2 78.11 10 10.3 103% 86% 114%
Bromoform 75-25-2 252.8 10 10.4 104% 68% 142%
Bromomethane 74-83-9 94.94 10 9.92 99% 84% 113%
1,3-Butadiene 106-99-0 54.09 10 9.51 95% 70% 111%
n-Butane 106-97-8 58.12 10 8.67 87% 74% 110%
Chlorobenzene 108-90-7 112.6 10 9.93 99% 72% 125%
Chloroethane 75-00-3 64.52 10 10.0 100% 81% 109%
Chloroform 67-66-3 119.4 10 10.2 102% 89% 119%
Chloromethane 74-87-3 50.49 10 9.41 94% 77% 111%
2-Chlorotoluene 95-49-8 126.6 10 9.22 92% 64% 130%
Cyclohexane 110-82-7 84.16 10 9.85 99% 85% 118%
1,2-Dibromoethane 106-93-4 187.8 10 9.81 98% 75% 125%
1,1-Dichloroethane 75-34-3 98.96 10 10.3 103% 87% 115%
1,2-Dichloroethane 107-06-2 98.96 10 10.3 103% 91% 122%
1,1-Dichloroethene 75-35-4 96.94 10 11.0 110% 89% 114%

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Acetone
1,4-Dioxane 123-91-1 88.12 10 9.04 90% 56% 115%
Ethanol 64-17-5 46.07 10 8.37 84% 61% 128%
Ethylbenzene 100-41-4 106.2 10 9.82 98% 72% 127%
4-Ethyltoluene 622-96-8 120.2 10 10.4 104% 61% 137%
n-Heptane 142-82-5 100.2 10 9.82 98% 80% 118%
n-Hexane 110-54-3 86.17 10 10.0 100% 89% 122%
Isopropanol 67-63-0 60.10 10 8.13 81% 68% 114%
Naphthalene 91-20-3 128.17 10 10.9 109% 30% 137%
Styrene 100-42-5 104.1 10 10.8 108% 69% 131%
Toluene 108-88-3 92.14 10 10.0 100% 76% 124%
Vinyl bromide 593-60-2 106.9 10 10.3 103% 91% 121%
Vinyl chloride 75-01-4 62.50 10 9.56 96% 80% 113%

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Acetone(m,p)
Xylene 1330-20-7 106.2 20 19.0 95% 65% 127%
Xylene (o) 95-47-6 106.2 10 9.80 98% 67% 126%




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EMSL Analytical, Inc. EMSL Order: Method Blank
200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample ID: MB030117L_B
Project ID: Method Blank Sampling Date: NA

Lab Sample ID: MB030117L_B Canister ID: E0243

Method Blank- Target Compound Results Summary
Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
Master_Method_Blank_May_2014_V2 Target_Results Page 1 of 3

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Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Tetrachloroethene 127-18-4 165.8 0.20 U 1.4
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

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Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87
Total Target Compounds: 0.0 0.0

E- Estimated value exceeding upper calibration range of instrument. Ethanol and isopropyl alcohol are not specifically targeted to
dilute within calibration range.


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Method Blank- Tentatively Identified Compound Results Summary
Result Result Retention
Tentatively Identified Compounds CAS# MW(1) ppbv Q ug/m3 Time
No Tentatively Identified Compounds (TICs) Reported

Master_Method_Blank_May_2014_V2 TIC_ALL_Results Page 1 of 1

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200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample ID: MB030217L

Lab Sample ID: MB030217L Canister ID: E0243

Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

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Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

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Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



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EMSL Analytical, Inc. EMSL Order: Instrument Blank
200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample ID: IB030217L-A
Project ID: Instrument Blank Sampling Date: NA

Lab Sample ID: IB030217L-A Canister ID: E15294

Instrument Blank- Target Compound Results Summary
Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
Master_Instrument_Blank_May_2014_V2 Target_Results Page 1 of 3

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Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

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Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



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Instrument Blank- Tentatively Identified Compound Results Summary

Master_Instrument_Blank_May_2014_V2 TIC_ALL_Results Page 1 of 1

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200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample ID: IB030217L-B

Lab Sample ID: IB030217L-B Canister ID: E15294

Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

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Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

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Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87
Total Target Compounds: 1 6.4



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200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample ID: IB030217L-C

Lab Sample ID: IB030217L-C Canister ID: E15294

Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

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Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

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Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



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Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

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Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

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Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



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Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

647 of 794


Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

648 of 794


Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



649 of 794




650 of 794
651 of 794
652 of 794
653 of 794
654 of 794
655 of 794


Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

656 of 794


Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

657 of 794


Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



658 of 794




659 of 794
660 of 794
661 of 794
662 of 794
663 of 794
664 of 794


Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

665 of 794


Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

666 of 794


Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



667 of 794




668 of 794
669 of 794
670 of 794
671 of 794
672 of 794
673 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030217L-0.5

Canister ID: E12941
Acetone 67-64-1 58.08 0.5 0.62 124 60-140
Allyl chloride 107-05-1 76.53 0.2 0.23 115 60-140
Benzene 71-43-2 78.11 0.2 0.23 115 60-140
Bromoform 75-25-2 252.8 0.2 0.20 100 60-140
Bromomethane 74-83-9 94.94 0.2 0.27 135 60-140
1,3-Butadiene 106-99-0 54.09 0.2 0.21 105 60-140
n-Butane 106-97-8 58.12 0.2 0.20 100 60-140
Chlorobenzene 108-90-7 112.6 0.2 0.22 110 60-140
Chloroethane 75-00-3 64.52 0.2 0.21 105 60-140
Chloroform 67-66-3 119.4 0.2 0.22 110 60-140
Chloromethane 74-87-3 50.49 0.2 0.23 115 60-140
2-Chlorotoluene 95-49-8 126.6 0.2 0.22 110 60-140
Cyclohexane 110-82-7 84.16 0.2 0.21 105 60-140
1,2-Dibromoethane 106-93-4 187.8 0.2 0.21 105 60-140
1,1-Dichloroethane 75-34-3 98.96 0.2 0.22 110 60-140
1,2-Dichloroethane 107-06-2 98.96 0.2 0.23 115 60-140
1,1-Dichloroethene 75-35-4 96.94 0.2 0.23 115 60-140

674 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030217L-0.5

Canister ID: E12941
Acetone
1,4-Dioxane 123-91-1 88.12 0.5 0.46 92 60-140
Ethanol 64-17-5 46.07 0.5 0.60 120 60-140
Ethylbenzene 100-41-4 106.2 0.2 0.21 105 60-140
4-Ethyltoluene 622-96-8 120.2 0.2 0.21 105 60-140
n-Heptane 142-82-5 100.2 0.2 0.22 110 60-140
n-Hexane 110-54-3 86.17 0.2 0.22 110 60-140
Isopropanol 67-63-0 60.10 0.5 0.62 124 60-140
Naphthalene 91-20-3 128.17 0.2 0.17 85 60-140
Styrene 100-42-5 104.1 0.2 0.18 90 60-140
Toluene 108-88-3 92.14 0.2 0.21 105 60-140
Vinyl bromide 593-60-2 106.9 0.2 0.23 115 60-140
Vinyl chloride 75-01-4 62.50 0.2 0.21 105 60-140

675 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030217L-0.5

Canister ID: E12941
Acetone(m,p)
Xylene 1330-20-7 106.2 0.4 0.42 105 60-140
Xylene (o) 95-47-6 106.2 0.2 0.22 110 60-140



676 of 794
677 of 794
678 of 794
679 of 794
680 of 794
681 of 794
682 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030717L-0.5

Canister ID: E12941
Acetone 67-64-1 58.08 0.5 0.66 132 60-140
Allyl chloride 107-05-1 76.53 0.2 0.21 105 60-140
Benzene 71-43-2 78.11 0.2 0.23 115 60-140
Bromoform 75-25-2 252.8 0.2 0.23 115 60-140
Bromomethane 74-83-9 94.94 0.2 0.29 145 * 60-140
1,3-Butadiene 106-99-0 54.09 0.2 0.21 105 60-140
n-Butane 106-97-8 58.12 0.2 0.22 110 60-140
Chlorobenzene 108-90-7 112.6 0.2 0.21 105 60-140
Chloroethane 75-00-3 64.52 0.2 0.22 110 60-140
Chloroform 67-66-3 119.4 0.2 0.24 120 60-140
Chloromethane 74-87-3 50.49 0.2 0.21 105 60-140
2-Chlorotoluene 95-49-8 126.6 0.2 0.21 105 60-140
Cyclohexane 110-82-7 84.16 0.2 0.22 110 60-140
1,2-Dibromoethane 106-93-4 187.8 0.2 0.20 100 60-140
1,1-Dichloroethane 75-34-3 98.96 0.2 0.22 110 60-140
1,2-Dichloroethane 107-06-2 98.96 0.2 0.23 115 60-140
1,1-Dichloroethene 75-35-4 96.94 0.2 0.22 110 60-140

683 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030717L-0.5

Canister ID: E12941
Acetone
1,4-Dioxane 123-91-1 88.12 0.5 0.47 94 60-140
Ethanol 64-17-5 46.07 0.5 0.61 122 60-140
Ethylbenzene 100-41-4 106.2 0.2 0.21 105 60-140
4-Ethyltoluene 622-96-8 120.2 0.2 0.21 105 60-140
n-Heptane 142-82-5 100.2 0.2 0.21 105 60-140
n-Hexane 110-54-3 86.17 0.2 0.20 100 60-140
Isopropanol 67-63-0 60.10 0.5 0.62 124 60-140
Naphthalene 91-20-3 128.17 0.2 0.16 80 60-140
Styrene 100-42-5 104.1 0.2 0.17 85 60-140
Toluene 108-88-3 92.14 0.2 0.21 105 60-140
Vinyl bromide 593-60-2 106.9 0.2 0.23 115 60-140
Vinyl chloride 75-01-4 62.50 0.2 0.21 105 60-140

684 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030717L-0.5

Canister ID: E12941
Acetone(m,p)
Xylene 1330-20-7 106.2 0.4 0.41 103 60-140
Xylene (o) 95-47-6 106.2 0.2 0.21 105 60-140



685 of 794
686 of 794
687 of 794
688 of 794
689 of 794
690 of 794
691 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030817L-0.5

Canister ID: E12941
Acetone 67-64-1 58.08 0.5 0.62 124 60-140
Allyl chloride 107-05-1 76.53 0.2 0.21 105 60-140
Benzene 71-43-2 78.11 0.2 0.24 120 60-140
Bromoform 75-25-2 252.8 0.2 0.22 110 60-140
Bromomethane 74-83-9 94.94 0.2 0.29 145 * 60-140
1,3-Butadiene 106-99-0 54.09 0.2 0.20 100 60-140
n-Butane 106-97-8 58.12 0.2 0.26 130 60-140
Chlorobenzene 108-90-7 112.6 0.2 0.21 105 60-140
Chloroethane 75-00-3 64.52 0.2 0.21 105 60-140
Chloroform 67-66-3 119.4 0.2 0.24 120 60-140
Chloromethane 74-87-3 50.49 0.2 0.21 105 60-140
2-Chlorotoluene 95-49-8 126.6 0.2 0.23 115 60-140
Cyclohexane 110-82-7 84.16 0.2 0.22 110 60-140
1,2-Dibromoethane 106-93-4 187.8 0.2 0.19 95 60-140
1,1-Dichloroethane 75-34-3 98.96 0.2 0.23 115 60-140
1,2-Dichloroethane 107-06-2 98.96 0.2 0.24 120 60-140
1,1-Dichloroethene 75-35-4 96.94 0.2 0.24 120 60-140

692 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030817L-0.5

Canister ID: E12941
Acetone
1,4-Dioxane 123-91-1 88.12 0.5 0.41 82 60-140
Ethanol 64-17-5 46.07 0.5 0.54 108 60-140
Ethylbenzene 100-41-4 106.2 0.2 0.21 105 60-140
4-Ethyltoluene 622-96-8 120.2 0.2 0.21 105 60-140
n-Heptane 142-82-5 100.2 0.2 0.22 110 60-140
n-Hexane 110-54-3 86.17 0.2 0.21 105 60-140
Isopropanol 67-63-0 60.10 0.5 0.60 120 60-140
Naphthalene 91-20-3 128.17 0.2 0.17 85 60-140
Styrene 100-42-5 104.1 0.2 0.17 85 60-140
Toluene 108-88-3 92.14 0.2 0.20 100 60-140
Vinyl bromide 593-60-2 106.9 0.2 0.24 120 60-140
Vinyl chloride 75-01-4 62.50 0.2 0.21 105 60-140

693 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS030817L-0.5

Canister ID: E12941
Acetone(m,p)
Xylene 1330-20-7 106.2 0.4 0.41 103 60-140
Xylene (o) 95-47-6 106.2 0.2 0.21 105 60-140



694 of 794
695 of 794
696 of 794
697 of 794
698 of 794
699 of 794
700 of 794
701 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS050916L-0.5

Canister ID: E15274
Acetone 67-64-1 58.08 0.5 0.60 120 60-140
Allyl chloride 107-05-1 76.53 0.2 0.22 110 60-140
Benzene 71-43-2 78.11 0.2 0.22 110 60-140
Bromoform 75-25-2 252.8 0.2 0.20 100 60-140
Bromomethane 74-83-9 94.94 0.2 0.19 95 60-140
1,3-Butadiene 106-99-0 54.09 0.2 0.18 90 60-140
n-Butane 106-97-8 58.12 0.2 0.17 85 60-140
Chlorobenzene 108-90-7 112.6 0.2 0.25 125 60-140
Chloroethane 75-00-3 64.52 0.2 0.18 90 60-140
Chloroform 67-66-3 119.4 0.2 0.20 100 60-140
Chloromethane 74-87-3 50.49 0.2 0.18 90 60-140
2-Chlorotoluene 95-49-8 126.6 0.2 0.24 120 60-140
Cyclohexane 110-82-7 84.16 0.2 0.20 100 60-140
1,2-Dibromoethane 106-93-4 187.8 0.2 0.22 110 60-140
1,1-Dichloroethane 75-34-3 98.96 0.2 0.22 110 60-140
1,2-Dichloroethane 107-06-2 98.96 0.2 0.20 100 60-140
1,1-Dichloroethene 75-35-4 96.94 0.2 0.21 105 60-140

702 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS050916L-0.5

Canister ID: E15274
Acetone
1,4-Dioxane 123-91-1 88.12 0.5 0.47 94 60-140
Ethanol 64-17-5 46.07 0.5 1.8 360 * 60-140
Ethylbenzene 100-41-4 106.2 0.2 0.25 125 60-140
4-Ethyltoluene 622-96-8 120.2 0.2 0.23 115 60-140
n-Heptane 142-82-5 100.2 0.2 0.22 110 60-140
n-Hexane 110-54-3 86.17 0.2 0.22 110 60-140
Isopropanol 67-63-0 60.10 0.5 1.7 340 * 60-140
Naphthalene 91-20-3 128.17 0.2 0.12 60 60-140
Styrene 100-42-5 104.1 0.2 0.21 105 60-140
Toluene 108-88-3 92.14 0.2 0.23 115 60-140
1,2,4-Trichlorobenzene 120-82-1 181.5 0.2 0.084 42 * 60-140
Vinyl bromide 593-60-2 106.9 0.2 0.20 100 60-140
Vinyl chloride 75-01-4 62.50 0.2 0.18 90 60-140

703 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS050916L-0.5

Canister ID: E15274
Acetone(m,p)
Xylene 1330-20-7 106.2 0.4 0.47 118 60-140
Xylene (o) 95-47-6 106.2 0.2 0.25 125 60-140



704 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS112216L-0.5

Canister ID: E0443
Acetone 67-64-1 58.08 0.5 0.61 122 60-140
Allyl chloride 107-05-1 76.53 0.2 0.22 110 60-140
Benzene 71-43-2 78.11 0.2 0.22 110 60-140
Bromoform 75-25-2 252.8 0.2 0.20 100 60-140
Bromomethane 74-83-9 94.94 0.2 0.27 135 60-140
1,3-Butadiene 106-99-0 54.09 0.2 0.25 125 60-140
n-Butane 106-97-8 58.12 0.2 0.25 125 60-140
Chlorobenzene 108-90-7 112.6 0.2 0.22 110 60-140
Chloroethane 75-00-3 64.52 0.2 0.21 105 60-140
Chloroform 67-66-3 119.4 0.2 0.22 110 60-140
Chloromethane 74-87-3 50.49 0.2 0.28 140 60-140
2-Chlorotoluene 95-49-8 126.6 0.2 0.24 120 60-140
Cyclohexane 110-82-7 84.16 0.2 0.22 110 60-140
1,2-Dibromoethane 106-93-4 187.8 0.2 0.20 100 60-140
1,1-Dichloroethane 75-34-3 98.96 0.2 0.22 110 60-140
1,2-Dichloroethane 107-06-2 98.96 0.2 0.22 110 60-140
1,1-Dichloroethene 75-35-4 96.94 0.2 0.24 120 60-140

705 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS112216L-0.5

Canister ID: E0443
Acetone
1,4-Dioxane 123-91-1 88.12 0.5 0.48 96 60-140
Ethanol 64-17-5 46.07 0.5 0.73 146 * 60-140
Ethylbenzene 100-41-4 106.2 0.2 0.22 110 60-140
4-Ethyltoluene 622-96-8 120.2 0.2 0.22 110 60-140
n-Heptane 142-82-5 100.2 0.2 0.22 110 60-140
n-Hexane 110-54-3 86.17 0.2 0.21 105 60-140
Isopropanol 67-63-0 60.10 0.5 0.63 126 60-140
Naphthalene 91-20-3 128.17 0.2 0.20 100 60-140
Styrene 100-42-5 104.1 0.2 0.21 105 60-140
Toluene 108-88-3 92.14 0.2 0.22 110 60-140
Vinyl bromide 593-60-2 106.9 0.2 0.23 115 60-140
Vinyl chloride 75-01-4 62.50 0.2 0.21 105 60-140

706 of 794
Phone/Fax:(856)858-4800/ (856)858-4571 RLLCS112216L-0.5

Canister ID: E0443
Acetone(m,p)
Xylene 1330-20-7 106.2 0.4 0.43 108 60-140
Xylene (o) 95-47-6 106.2 0.2 0.22 110 60-140



707 of 794
EPA TO-15

RLLCS050916L-0.5 L8092.D 05/09/16 13:02

RLLCS050916L-0.2 L8093.D 05/09/16 13:46
ICC HD4344 L8094.D 05/09/16 14:51
ICC HD4355 L8095.D 05/09/16 15:41
ICC HD2317 L8096.D 05/09/16 16:31
H0341 L8097.D 05/09/16 17:21
491600507-1 L8098.D 05/09/16 18:11
491600500-1 L8099.D 05/09/16 19:01
491600500-2 L8100.D 05/09/16 19:51
491600500-3 L8101.D 05/09/16 20:41
491600506-1 L8102.D 05/09/16 21:25
491600506-2 L8103.D 05/09/16 22:08
491600506-3 L8104.D 05/09/16 22:52
ECVS050916L-10 L8105.D 05/09/16 23:36
708 of 794


Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

709 of 794


Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

710 of 794


Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



711 of 794




712 of 794
EPA TO-15

RLLCS112216L-0.5 L8568.D 11/22/16 21:00

RLLCS112216L-0.2 L8569.D 11/22/16 21:43
C3380 L8570.D 11/22/16 22:34
491601339-1 L8571.D 11/22/16 23:25
491601339-1DL L8572.D 11/23/16 00:08
491601339-2 L8573.D 11/23/16 00:59
491601339-2DL L8574.D 11/23/16 01:44
491601339-3 L8575.D 11/23/16 02:34
491601339-3DL L8576.D 11/23/16 03:19
491601339-4 L8577.D 11/23/16 04:09
491601339-5 L8578.D 11/23/16 05:00
491601339-6 L8579.D 11/23/16 05:51
491601339-6DL L8580.D 11/23/16 06:34
491601348-1 L8581.D 11/23/16 07:25
491601348-2 L8582.D 11/23/16 08:15
491601348-3 L8583.D 11/23/16 09:06
491601348-4 L8584.D 11/23/16 09:57
491601348-1DL L8585.D 11/23/16 10:43
491601348-2DL L8586.D 11/23/16 11:27
491601348-3DL L8587.D 11/23/16 12:10
C3389 L8588.D 11/23/16 13:01
C3390 L8589.D 11/23/16 13:51
ECVS112216L-10 L8590.D 11/23/16 14:35
713 of 794


Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

714 of 794


Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.50 U 1.8
Ethanol 64-17-5 46.07 0.50 U 0.94
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.50 U 1.2
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

715 of 794


Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



716 of 794




717 of 794
EPA TO-15

BFB Check ID: BFB040116 Analysis Date: 04/01/2016
% Relative
50 8-0 - 40% of mass 95 23.3
75 30.0 - 66.0% of mass 95 49.1
96 5.0 - 9.0% of mass 95 6.8
173 Less than 2.0% of mass 174 0.0 (0.0) 1
174 50.0 - 120.0% of mass 95 93.6
175 4.0 - 9.0% of mass 174 6.9 (7.3) 1
176 93.0 - 101.0% of mass 174 91.1 (97.3) 1
177 5.0 - 9.0% of mass 176 6.2 (6.8) 2

IC040116L-40 L7957.D 04/01/2016 15:39
IC040116L-20 L7958.D 04/01/2016 16:26
IC040116L-10 L7959.D 04/01/2016 17:10
IC040116L-2 L7960.D 04/01/2016 18:01
IC040116L-0.5 L7961.D 04/01/2016 18:45
IC040116L-0.2 L7962.D 04/01/2016 19:29
ICVS040116L-10 L7963.D 04/01/2016 20:13
ICVS040116L-10B L7964.D 04/01/2016 20:58
MB040116L L7965.D 04/01/2016 23:30
RLLCS040116L-0.5 L7966.D 04/02/2016 00:14
RLLCS040116L-0.2 L7967.D 04/02/2016 00:58
491600351-6 L7968.D 04/02/2016 01:48
491600351-7 L7969.D 04/02/2016 02:39
491600351-8 L7970.D 04/02/2016 03:30
IB040116L-A L7971.D 04/02/2016 04:21
491600351-1 L7972.D 04/02/2016 05:04
491600351-2 L7973.D 04/02/2016 05:48
491600351-3 L7974.D 04/02/2016 06:31
IB040116L-B L7975.D 04/02/2016 07:23
C3260 L7976.D 04/02/2016 08:13
C3261 L7977.D 04/02/2016 09:03
ECVS040116L-10 L7978.D 04/02/2016 09:48
718 of 794
EPA TO-15

% Relative
50 8-0 - 40% of mass 95 24.1
75 30.0 - 66.0% of mass 95 51.3
96 5.0 - 9.0% of mass 95 6.6
173 Less than 2.0% of mass 174 0.0 (0.0) 1
174 50.0 - 120.0% of mass 95 95.0
175 4.0 - 9.0% of mass 174 7.0 (7.3) 1
176 93.0 - 101.0% of mass 174 92.6 (97.5) 1
177 5.0 - 9.0% of mass 176 6.2 (6.7) 2

CCVS050916L-10 L8090.D 05/09/2016 10:40
MB050916L L8091.D 05/09/2016 12:19
RLLCS050916L-0.5 L8092.D 05/09/2016 13:02
RLLCS050916L-0.2 L8093.D 05/09/2016 13:46
ICC HD4344 L8094.D 05/09/2016 14:51
ICC HD4355 L8095.D 05/09/2016 15:41
ICC HD2317 L8096.D 05/09/2016 16:31
H0341 L8097.D 05/09/2016 17:21
491600507-1 L8098.D 05/09/2016 18:11
491600500-1 L8099.D 05/09/2016 19:01
491600500-2 L8100.D 05/09/2016 19:51
491600500-3 L8101.D 05/09/2016 20:41
491600506-1 L8102.D 05/09/2016 21:25
491600506-2 L8103.D 05/09/2016 22:08
491600506-3 L8104.D 05/09/2016 22:52
ECVS050916L-10 L8105.D 05/09/2016 23:36
719 of 794
EPA TO-15
% Relative
50 8-0 - 40% of mass 95 26.6
75 30.0 - 66.0% of mass 95 57.6
96 5.0 - 9.0% of mass 95 6.7
173 Less than 2.0% of mass 174 0.0 (0.0) 1
174 50.0 - 120.0% of mass 95 104.2
175 4.0 - 9.0% of mass 174 7.6 (7.3) 1
176 93.0 - 101.0% of mass 174 99.5 (95.5) 1
177 5.0 - 9.0% of mass 176 6.8 (6.8) 2

IC112116L-40 L8547.D 11/21/2016 18:16
IC112116L-20 L8548.D 11/21/2016 19:02
IC112116L-10 L8549.D 11/21/2016 19:47
IC112116L-2 L8550.D 11/21/2016 20:37
IC112116L-0.5 L8551.D 11/21/2016 21:21
IC112116L-0.2 L8552.D 11/21/2016 22:04
ICVS112116L-10 L8553.D 11/21/2016 22:48
ICVS112116L-10B L8554.D 11/21/2016 23:32
MB112116L L8555.D 11/22/2016 01:13
RLLCS112116L-0.5 L8556.D 11/22/2016 01:57
RLLCS112116L-0.2 L8557.D 11/22/2016 02:41
C3390 L8558.D 11/22/2016 12:13
491601365-1 L8559.D 11/22/2016 13:04
491601365-1DL L8560.D 11/22/2016 13:50
491601374-1 L8561.D 11/22/2016 14:40
491601374-1DL L8562.D 11/22/2016 15:37
ECVS112116L-10 L8563.D 11/22/2016 16:21
720 of 794
EPA TO-15

% Relative
50 8-0 - 40% of mass 95 27.1
75 30.0 - 66.0% of mass 95 59.2
96 5.0 - 9.0% of mass 95 6.7
173 Less than 2.0% of mass 174 0.0 (0.0) 1
174 50.0 - 120.0% of mass 95 106.4
175 4.0 - 9.0% of mass 174 7.8 (7.3) 1
176 93.0 - 101.0% of mass 174 102.6 (96.5) 1
177 5.0 - 9.0% of mass 176 7.0 (6.8) 2

CCVS112216L-10 L8566.D 11/22/2016 18:33
MB112216L L8567.D 11/22/2016 20:15
RLLCS112216L-0.5 L8568.D 11/22/2016 21:00
RLLCS112216L-0.2 L8569.D 11/22/2016 21:43
C3380 L8570.D 11/22/2016 22:34
491601339-1 L8571.D 11/22/2016 23:25
491601339-1DL L8572.D 11/23/2016 00:08
491601339-2 L8573.D 11/23/2016 00:59
491601339-2DL L8574.D 11/23/2016 01:44
491601339-3 L8575.D 11/23/2016 02:34
491601339-3DL L8576.D 11/23/2016 03:19
491601339-4 L8577.D 11/23/2016 04:09
491601339-5 L8578.D 11/23/2016 05:00
491601339-6 L8579.D 11/23/2016 05:51
491601339-6DL L8580.D 11/23/2016 06:34
491601348-1 L8581.D 11/23/2016 07:25
491601348-2 L8582.D 11/23/2016 08:15
491601348-3 L8583.D 11/23/2016 09:06
491601348-4 L8584.D 11/23/2016 09:57
491601348-1DL L8585.D 11/23/2016 10:43
491601348-2DL L8586.D 11/23/2016 11:27
491601348-3DL L8587.D 11/23/2016 12:10
C3389 L8588.D 11/23/2016 13:01
C3390 L8589.D 11/23/2016 13:51
ECVS112216L-10 L8590.D 11/23/2016 14:35
721 of 794
EPA TO-15


10 ppbv Std 450423 11.99 1031230 13.69 1020760 20.18
Upper Limit 630592 12.32 1443722 14.02 1429064 20.51
Lower Limit 270254 11.66 618738 13.36 612456 19.85
Lab Sample ID
IC040116L-20 438826 11.98 1027670 13.69 990057 20.18
IC040116L-10 416222 11.98 955449 13.69 926933 20.17
IC040116L-2 401206 11.98 897673 13.68 844688 20.17
IC040116L-0.5 393484 11.97 859556 13.68 808950 20.17
IC040116L-0.2 377655 11.98 813433 13.69 763177 20.17
ICVS040116L-10 392636 11.98 862359 13.68 839602 20.17
ICVS040116L-10B 400901 11.98 892129 13.68 866304 20.16
MB040116L 433094 11.97 896972 13.68 799961 20.17
RLLCS040116L-0.5 433257 11.97 937139 13.67 861907 20.16
RLLCS040116L-0.2 385596 11.97 811359 13.68 766553 20.17
491600351-6 372501 11.98 730378 13.67 685377 20.16
491600351-7 359242 11.98 701303 13.68 644390 20.16
491600351-8 356788 11.98 682933 13.68 631710 20.17
IB040116L-A 383600 11.98 794940 13.68 754377 20.17
491600351-1 385225 11.97 733778 13.68 658973 20.17
491600351-2 367067 11.97 709224 13.68 656796 20.17
491600351-3 361093 11.97 710429 13.67 677792 20.16
IB040116L-B 381608 11.97 792011 13.68 753292 20.17
C3260 431532 11.97 930768 13.68 877233 20.17
C3261 451894 11.97 983509 13.68 911238 20.16
ECVS040116L-10 450423 11.98 961129 13.68 937575 20.17
ECVS040116L-10B 413912 11.98 877411 13.68 863790 20.17
QC Criteria
722 of 794
EPA TO-15


10 ppbv Std 473252 11.93 972449 13.64 956454 20.13
Upper Limit 662553 12.26 1361428.6 13.97 1339035.6 20.46
Lower Limit 283951 11.60 583469.4 13.31 573872.4 19.80
Lab Sample ID
MB050916L 499878 11.93 1089030 13.63 1008650 20.12
RLLCS050916L-0.5 468494 11.92 931003 13.63 873038 20.12
RLLCS050916L-0.2 437424 11.92 843975 13.62 775579 20.12
ICC HD4344 479170 11.93 1043020 13.63 973523 20.12
ICC HD4355 499378 11.94 1097470 13.64 1028570 20.12
ICC HD2317 501037 11.93 1110830 13.64 1044200 20.13
H0341 493194 11.94 1119400 13.64 1030260 20.12
491600507-1 464382 11.94 976229 13.64 877069 20.12
491600500-1 427157 11.94 884053 13.63 800307 20.12
491600500-2 417716 11.93 854602 13.63 771302 20.12
491600500-3 412861 11.92 846623 13.63 771957 20.12
491600506-1 411403 11.93 858839 13.63 777462 20.12
491600506-2 411137 11.93 873898 13.63 796676 20.11
491600506-3 405518 11.93 850302 13.63 781601 20.11
ECVS050916L-10 421034 11.92 938700 13.63 905347 20.12
QC Criteria
723 of 794
EPA TO-15


10 ppbv Std 377215 11.94 1022190 13.64 912684 20.13
Upper Limit 528101 12.27 1431066 13.97 1277757.6 20.46
Lower Limit 226329 11.61 613314 13.31 547610.4 19.80
Lab Sample ID
ICVS112116L-10 336863 11.94 927565 13.64 834156 20.12
ICVS112116L-10B 347473 11.94 949872 13.63 847245 20.12
MB112116L 326670 11.93 896234 13.64 757200 20.12
RLLCS112116L-0.5 326864 11.93 880100 13.63 766925 20.12
RLLCS112116L-0.2 316542 11.93 870121 13.63 758285 20.11
C3390 382027 11.91 981938 13.63 865066 20.10
491601365-1 364726 11.92 948015 13.62 824710 20.10
491601365-1DL 337003 11.92 909123 13.62 773683 20.11
491601374-1 337264 11.92 896266 13.62 788008 20.11
491601374-1DL 346294 11.91 916568 13.62 782544 20.10
ECVS112116L-10 346090 11.91 947610 13.61 840999 20.10
QC Criteria
724 of 794
EPA TO-15


10 ppbv Std 367930 11.91 978999 13.62 888098 20.09
Upper Limit 515102 12.24 1370598.6 13.95 1243337.2 20.42
Lower Limit 220758 11.58 587399.4 13.29 532858.8 19.76
Lab Sample ID
MB112216L 330529 11.91 896249 13.61 766898 20.10
RLLCS112216L-0.5 325379 11.91 871929 13.61 768846 20.09
RLLCS112216L-0.2 316959 11.90 863107 13.61 745213 20.09
C3380 330751 11.90 891142 13.61 768747 20.09
491601339-1 347461 11.90 940134 13.61 811082 20.09
491601339-1DL 321972 11.90 874060 13.61 753507 20.09
491601339-2 316145 11.91 860267 13.60 749997 20.09
491601339-2DL 310095 11.90 831626 13.61 729409 20.08
491601339-3 308978 11.90 837808 13.60 725967 20.09
491601339-3DL 298783 11.90 812422 13.61 700134 20.09
491601339-4 303709 11.90 826234 13.61 717781 20.09
491601339-5 309226 11.90 827543 13.61 722890 20.08
491601339-6 341354 11.90 916642 13.61 782136 20.08
491601339-6DL 319991 11.90 851436 13.60 750926 20.09
491601348-1 309618 11.90 833718 13.60 737164 20.09
491601348-2 315154 11.90 831730 13.60 725921 20.09
491601348-3 311673 11.89 841431 13.60 729613 20.08
491601348-4 311671 11.90 835700 13.60 716864 20.09
491601348-1DL 297438 11.89 811690 13.60 694735 20.08
491601348-2DL 299442 11.90 823122 13.60 699700 20.09
491601348-3DL 282986 11.89 780734 13.60 685047 20.08
C3389 326857 11.90 879318 13.61 759135 20.09
C3390 378935 11.90 1005970 13.60 863123 20.09
ECVS112216L-10 359852 11.90 1002790 13.61 893653 20.09
QC Criteria
725 of 794
EMSL Analytical, Inc. EMSL Order: Canister Certification
200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample ID: H0341
Project ID: Canister Certification Sampling Date: NA

Lab Sample ID: H0341 Canister ID: HD2136

Canister Certification- Target Compound Results Summary
Result Result
Acetone 67-64-1 58.08 0.20 U 0.48
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5
Master_Canister_Certification_March_2016_V5 Target_Results Page 1 of 3

726 of 794


Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.20 U 0.72
Ethanol 64-17-5 46.07 0.20 U 0.38
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.20 U 0.49
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

727 of 794


Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



728 of 794


Canister Certification- Tentatively Identified Compound Results Summary

Master_Canister_Certification_March_2016_V5 TIC_ALL_Results Page 1 of 1

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200 Route 130 North, Cinnaminson, NJ 08077 EMSL Sample ID: C3389

Lab Sample ID: C3389 Canister ID: E0448

Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

736 of 794


Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.20 U 0.72
Ethanol 64-17-5 46.07 0.20 U 0.38
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.20 U 0.49
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

737 of 794


Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



738 of 794




739 of 794
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Result Result
Acetone 67-64-1 58.08 0.50 U 1.2
Allyl chloride 107-05-1 76.53 0.20 U 0.63
Benzene 71-43-2 78.11 0.20 U 0.64
Bromoform 75-25-2 252.8 0.20 U 2.1
Bromomethane 74-83-9 94.94 0.20 U 0.78
1,3-Butadiene 106-99-0 54.09 0.20 U 0.44
n-Butane 106-97-8 58.12 0.20 U 0.48
Chlorobenzene 108-90-7 112.6 0.20 U 0.92
Chloroethane 75-00-3 64.52 0.20 U 0.53
Chloroform 67-66-3 119.4 0.20 U 1.0
Chloromethane 74-87-3 50.49 0.20 U 0.41
2-Chlorotoluene 95-49-8 126.6 0.20 U 1.0
Cyclohexane 110-82-7 84.16 0.20 U 0.69
1,2-Dibromoethane 106-93-4 187.8 0.20 U 1.5

746 of 794


Result Result
Acetone
1,4-Dioxane 123-91-1 88.12 0.20 U 0.72
Ethanol 64-17-5 46.07 0.20 U 0.38
Ethylbenzene 100-41-4 106.2 0.20 U 0.87
4-Ethyltoluene 622-96-8 120.2 0.20 U 1.0
n-Heptane 142-82-5 100.2 0.20 U 0.82
n-Hexane 110-54-3 86.17 0.20 U 0.70
Isopropanol 67-63-0 60.10 0.20 U 0.49
Naphthalene 91-20-3 128.17 0.20 U 1.0
Styrene 100-42-5 104.1 0.20 U 0.85
Toluene 108-88-3 92.14 0.20 U 0.75
Vinyl bromide 593-60-2 106.9 0.20 U 0.87
Vinyl chloride 75-01-4 62.50 0.20 U 0.51

747 of 794


Result Result
Acetone(m,p)
Xylene 1330-20-7 106.2 0.40 U 1.7
Xylene (o) 95-47-6 106.2 0.20 U 0.87



748 of 794




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757 of 794
EPA TO-15
Initial Calibration

ICAL ID: Q040116L
Analysis Date 1 Apr 2016

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Mean Values: 412969 11.98 930835 13.69 892428 20.17
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EPA TO-15
Initial Calibration

ICAL ID: Q112116L
Analysis Date 21 Nov 2016

761 of 794
Mean Values: 375111 11.94 994316 13.64 889532 20.12


Acetone 67-64-1 58.08 10 8.00 80% 70% 130%
Allyl chloride 107-05-1 76.53 10 9.21 92% 70% 130%
Benzene 71-43-2 78.11 10 8.52 85% 70% 130%
Bromoform 75-25-2 252.8 10 9.73 97% 70% 130%
Bromomethane 74-83-9 94.94 10 8.79 88% 70% 130%
1,3-Butadiene 106-99-0 54.09 10 8.72 87% 70% 130%
n-Butane 106-97-8 58.12 10 8.27 83% 70% 130%
Chlorobenzene 108-90-7 112.6 10 8.44 84% 70% 130%
Chloroethane 75-00-3 64.52 10 8.92 89% 70% 130%
Chloroform 67-66-3 119.4 10 8.83 88% 70% 130%
Chloromethane 74-87-3 50.49 10 8.50 85% 70% 130%
2-Chlorotoluene 95-49-8 126.6 10 8.49 85% 70% 130%
Cyclohexane 110-82-7 84.16 10 8.80 88% 70% 130%
1,2-Dibromoethane 106-93-4 187.8 10 9.13 91% 70% 130%
1,1-Dichloroethane 75-34-3 98.96 10 8.71 87% 70% 130%
1,2-Dichloroethane 107-06-2 98.96 10 8.74 87% 70% 130%
1,1-Dichloroethene 75-35-4 96.94 10 8.67 87% 70% 130%
Master_ICVSS_LCS_70_130_July_2014_V1 ICVSS Page 1 of 3

762 of 794


Acetone
1,4-Dioxane 123-91-1 88.12 10 11.3 113% 70% 130%
Ethanol 64-17-5 46.07 10 8.72 87% 70% 130%
Ethylbenzene 100-41-4 106.2 10 8.51 85% 70% 130%
4-Ethyltoluene 622-96-8 120.2 10 8.90 89% 70% 130%
n-Heptane 142-82-5 100.2 10 8.95 90% 70% 130%
n-Hexane 110-54-3 86.17 10 8.83 88% 70% 130%
Isopropanol 67-63-0 60.10 10 8.97 90% 70% 130%
Naphthalene 91-20-3 128.17 10 7.84 78% 70% 130%
Styrene 100-42-5 104.1 10 8.92 89% 70% 130%
Toluene 108-88-3 92.14 10 8.85 89% 70% 130%
Vinyl bromide 593-60-2 106.9 10 8.54 85% 70% 130%
Vinyl chloride 75-01-4 62.50 10 8.87 89% 70% 130%

763 of 794


Acetone(m,p)
Xylene 1330-20-7 106.2 20 17.4 87% 70% 130%
Xylene (o) 95-47-6 106.2 10 8.51 85% 70% 130%




764 of 794


Acetone 67-64-1 58.08 10 7.83 78% 70% 130%
Allyl chloride 107-05-1 76.53 10 9.31 93% 70% 130%
Benzene 71-43-2 78.11 10 8.66 87% 70% 130%
Bromoform 75-25-2 252.8 10 10.0 100% 70% 130%
Bromomethane 74-83-9 94.94 10 9.30 93% 70% 130%
1,3-Butadiene 106-99-0 54.09 10 8.83 88% 70% 130%
n-Butane 106-97-8 58.12 10 8.32 83% 70% 130%
Chlorobenzene 108-90-7 112.6 10 8.68 87% 70% 130%
Chloroethane 75-00-3 64.52 10 9.30 93% 70% 130%
Chloroform 67-66-3 119.4 10 8.95 90% 70% 130%
Chloromethane 74-87-3 50.49 10 8.55 86% 70% 130%
2-Chlorotoluene 95-49-8 126.6 10 8.69 87% 70% 130%
Cyclohexane 110-82-7 84.16 10 8.98 90% 70% 130%
1,2-Dibromoethane 106-93-4 187.8 10 9.23 92% 70% 130%
1,1-Dichloroethane 75-34-3 98.96 10 8.90 89% 70% 130%
1,2-Dichloroethane 107-06-2 98.96 10 8.75 88% 70% 130%
1,1-Dichloroethene 75-35-4 96.94 10 8.84 88% 70% 130%

765 of 794


Acetone
1,4-Dioxane 123-91-1 88.12 10 10.8 108% 70% 130%
Ethanol 64-17-5 46.07 10 8.72 87% 70% 130%
Ethylbenzene 100-41-4 106.2 10 8.75 88% 70% 130%
4-Ethyltoluene 622-96-8 120.2 10 8.84 88% 70% 130%
n-Heptane 142-82-5 100.2 10 9.16 92% 70% 130%
n-Hexane 110-54-3 86.17 10 8.82 88% 70% 130%
Isopropanol 67-63-0 60.10 10 8.55 86% 70% 130%
Naphthalene 91-20-3 128.17 10 8.16 82% 70% 130%
Styrene 100-42-5 104.1 10 9.15 92% 70% 130%
Toluene 108-88-3 92.14 10 9.04 90% 70% 130%
Vinyl bromide 593-60-2 106.9 10 8.74 87% 70% 130%
Vinyl chloride 75-01-4 62.50 10 9.07 91% 70% 130%

766 of 794


Acetone(m,p)
Xylene 1330-20-7 106.2 20 17.7 89% 70% 130%
Xylene (o) 95-47-6 106.2 10 8.78 88% 70% 130%




767 of 794


Acetone 67-64-1 58.08 10 8.93 89% 71% 125%
Allyl chloride 107-05-1 76.53 10 10.5 105% 86% 118%
Benzene 71-43-2 78.11 10 9.63 96% 86% 114%
Bromoform 75-25-2 252.8 10 9.95 100% 68% 142%
Bromomethane 74-83-9 94.94 10 9.04 90% 84% 113%
1,3-Butadiene 106-99-0 54.09 10 8.88 89% 70% 111%
n-Butane 106-97-8 58.12 10 8.47 85% 74% 110%
Chlorobenzene 108-90-7 112.6 10 9.15 92% 72% 125%
Chloroethane 75-00-3 64.52 10 9.01 90% 81% 109%
Chloroform 67-66-3 119.4 10 10.1 101% 89% 119%
Chloromethane 74-87-3 50.49 10 7.91 79% 77% 111%
2-Chlorotoluene 95-49-8 126.6 10 8.73 87% 64% 130%
Cyclohexane 110-82-7 84.16 10 9.49 95% 85% 118%
1,2-Dibromoethane 106-93-4 187.8 10 9.50 95% 75% 125%
1,1-Dichloroethane 75-34-3 98.96 10 9.76 98% 87% 115%
1,2-Dichloroethane 107-06-2 98.96 10 10.2 102% 91% 122%
1,1-Dichloroethene 75-35-4 96.94 10 10.3 103% 89% 114%

768 of 794


Acetone
1,4-Dioxane 123-91-1 88.12 10 8.73 87% 56% 115%
Ethanol 64-17-5 46.07 10 7.82 78% 61% 128%
Ethylbenzene 100-41-4 106.2 10 9.29 93% 72% 127%
4-Ethyltoluene 622-96-8 120.2 10 9.29 93% 61% 137%
n-Heptane 142-82-5 100.2 10 9.11 91% 80% 118%
n-Hexane 110-54-3 86.17 10 9.46 95% 89% 122%
Isopropanol 67-63-0 60.10 10 7.97 80% 68% 114%
Naphthalene 91-20-3 128.17 10 9.37 94% 30% 137%
Styrene 100-42-5 104.1 10 9.35 94% 69% 131%
Toluene 108-88-3 92.14 10 9.33 93% 76% 124%
Vinyl bromide 593-60-2 106.9 10 9.55 96% 91% 121%
Vinyl chloride 75-01-4 62.50 10 8.98 90% 80% 113%

769 of 794


Acetone(m,p)
Xylene 1330-20-7 106.2 20 17.3 87% 65% 127%
Xylene (o) 95-47-6 106.2 10 9.07 91% 67% 126%




770 of 794


Acetone 67-64-1 58.08 10 8.95 90% 71% 125%
Allyl chloride 107-05-1 76.53 10 10.5 105% 86% 118%
Benzene 71-43-2 78.11 10 9.56 96% 86% 114%
Bromoform 75-25-2 252.8 10 10.0 100% 68% 142%
Bromomethane 74-83-9 94.94 10 9.09 91% 84% 113%
1,3-Butadiene 106-99-0 54.09 10 8.78 88% 70% 111%
n-Butane 106-97-8 58.12 10 8.64 86% 74% 110%
Chlorobenzene 108-90-7 112.6 10 9.40 94% 72% 125%
Chloroethane 75-00-3 64.52 10 9.07 91% 81% 109%
Chloroform 67-66-3 119.4 10 10.0 100% 89% 119%
Chloromethane 74-87-3 50.49 10 8.08 81% 77% 111%
2-Chlorotoluene 95-49-8 126.6 10 9.02 90% 64% 130%
Cyclohexane 110-82-7 84.16 10 9.57 96% 85% 118%
1,2-Dibromoethane 106-93-4 187.8 10 9.59 96% 75% 125%
1,1-Dichloroethane 75-34-3 98.96 10 9.74 97% 87% 115%
1,2-Dichloroethane 107-06-2 98.96 10 10.1 101% 91% 122%
1,1-Dichloroethene 75-35-4 96.94 10 10.1 101% 89% 114%

771 of 794


Acetone
1,4-Dioxane 123-91-1 88.12 10 8.74 87% 56% 115%
Ethanol 64-17-5 46.07 10 7.87 79% 61% 128%
Ethylbenzene 100-41-4 106.2 10 9.42 94% 72% 127%
4-Ethyltoluene 622-96-8 120.2 10 9.31 93% 61% 137%
n-Heptane 142-82-5 100.2 10 9.24 92% 80% 118%
n-Hexane 110-54-3 86.17 10 9.38 94% 89% 122%
Isopropanol 67-63-0 60.10 10 7.93 79% 68% 114%
Naphthalene 91-20-3 128.17 10 9.38 94% 30% 137%
Styrene 100-42-5 104.1 10 9.52 95% 69% 131%
Toluene 108-88-3 92.14 10 9.41 94% 76% 124%
Vinyl bromide 593-60-2 106.9 10 9.44 94% 91% 121%
Vinyl chloride 75-01-4 62.50 10 9.25 93% 80% 113%

772 of 794


Acetone(m,p)
Xylene 1330-20-7 106.2 20 17.5 88% 65% 127%
Xylene (o) 95-47-6 106.2 10 9.29 93% 67% 126%




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Phone/Fax: (856) 858-4800/ (856) 858-4571
http://www.EMSL.com to15lab@EMSL.com
Instrument Batch Analysis Log

Instrument Batch ID: 030117L Batch Start Date: 03/01/2017
Instrument ID: GC/MS L-C Batch Start Time: 05:28 PM
Batch Stop Date: 03/02/2017
Analyst Initials: MTH Batch Stop Time: 04:17 PM
Instrument Sample Dilution

Run # Data File EMSL Sample ID Analysis Date Analysis Time Canister ID Volume Factor Comment
1 L9266.D BFB030117L 03/01/2017 05:28 PM S1023 100 cc 1 Tune Standard

2 L9267.D IC030117L-40 03/01/2017 06:17 PM E12284 500 cc 1
3 L9268.D IC030117L-20 03/01/2017 07:03 PM E12284 250 cc 1
4 L9269.D IC030117L-10 03/01/2017 07:47 PM E12284 125 cc 1
5 L9270.D IC030117L-2 03/01/2017 08:36 PM E12941 500 cc 1
6 L9271.D IC030117L-0.5 03/01/2017 09:20 PM E12941 125 cc 1
7 L9272.D IC030117L-0.2 03/01/2017 10:04 PM E12941 50 cc 1
8 L9273.D ICVS030117L-10 03/01/2017 10:47 PM E0462 125 cc 1 Initial Cal Verification Std.
9 L9274.D ICVS030117L-10B 03/01/2017 11:31 PM E0462 125 cc 1 Initial Cal Verification Std.
10 L9275.D MB030117L_info_run 03/02/2017 12:21 AM E0243 500 cc 1 Method Blank
11 L9276.D MB030117L_B 03/02/2017 01:11 AM E0243 500 cc 1 Method Blank
12 L9277.D RLLCS030117L-0.5 03/02/2017 01:54 AM E12941 125 cc 1 Reporting Limit Standard
14 L9279.D 491700158-1 03/02/2017 03:28 AM E0387 500 cc 1
15 L9280.D IB030117L-A 03/02/2017 10:04 AM E15294 500 cc 1 Instrument Blank
16 L9281.D 491700223-2 03/02/2017 11:00 AM E0271 850 cc 1
17 L9282.D 491700223-3 03/02/2017 11:50 AM E0510 500 cc 1
18 L9283.D 491700223-1 03/02/2017 12:33 PM HD2223 50 cc 10
19 L9284.D IB030117L-B 03/02/2017 01:23 PM E15294 500 cc 1 Instrument Blank
20 L9285.D 491700251-1 03/02/2017 02:06 PM E12270 50 cc 10
21 L9286.D 491700251-2 03/02/2017 02:50 PM E12293 50 cc 10
22 L9287.D ECVS030117L-10 03/02/2017 03:34 PM E12284 125 cc 1 Ending Calibration Check
23 L9288.D ECVS030117L-10B 03/02/2017 04:17 PM E12284 125 cc 1 Ending Calibration Check
Additional Comments:
Marge Howley , Analyst
Master_TO15_Instrument_Log_V61 1"of "1
785 of 794
Phone/Fax: (856) 858-4800/ (856) 858-4571


1 L9289.D BFB030217L 03/02/2017 05:01 PM S1023 100 cc 1 Tune Standard

2 L9290.D CCVS030217L-10 03/02/2017 05:45 PM E12284 125 cc 1 Calibration Check Standard
3 L9291.D MB030217L 03/02/2017 07:25 PM E0243 500 cc 1 Method Blank
4 L9292.D RLLCS030217L-0.5 03/02/2017 08:08 PM E12941 125 cc 1 Reporting Limit Standard
6 L9294.D 491700251-1DL 03/02/2017 09:35 PM E12270 25 cc 20 Sample Dilution
7 L9295.D IB030217L-A 03/02/2017 10:25 PM E15294 500 cc 1 Instrument Blank
8 L9296.D 491700245-10 03/02/2017 11:08 PM HD2160 50 cc 10
9 L9297.D 491700245-11 03/02/2017 11:52 PM HD2161 50 cc 10
10 L9298.D IB030217L-B 03/03/2017 12:42 AM E15294 500 cc 1 Instrument Blank
11 L9299.D 491700245-12 03/03/2017 01:26 AM HD2179 50 cc 10
12 L9300.D 491700245-13 03/03/2017 02:10 AM HD2331 50 cc 10
13 L9301.D 491700245-14 03/03/2017 07:48 AM HD2749 50 cc 10
14 L9302.D IB030217L-C 03/03/2017 08:38 AM E15294 500 cc 1 Instrument Blank
15 L9303.D 491700245-12RE 03/03/2017 09:21 AM HD2179 50 cc 10 Reanalysis
16 L9304.D 491700245-10DL 03/03/2017 10:04 AM HD2160 25 cc 60 Sample Dilution
19 L9307.D 491700245-14DL 03/03/2017 12:13 PM HD2749 25 cc 60 Sample Dilution
20 L9308.D 491700245-10DL2 03/03/2017 12:56 PM HD2160 25 cc 540 Sample Dilution
23 L9311.D 491700245-10DL3 03/03/2017 03:15 PM HD2160 25 cc 1620
786 of 794
Phone/Fax: (856) 858-4800/ (856) 858-4571

Instrument ID: GC/MS L-C Batch Start Time: 08:55 AM
Analyst Initials: MTH Batch Stop Time: 02:24 AM

1 L9314.D BFB030717L 03/07/2017 08:55 AM S1023 100 cc 1 Tune Standard

2 L9315.D CCVS030717L-10 03/07/2017 09:38 AM E12284 125 cc 1 Calibration Check Standard
3 L9316.D MB030717L 03/07/2017 11:18 AM E0243 500 cc 1 Method Blank
6 L9319.D C3434 03/07/2017 01:34 PM E0254 500 cc 1
7 L9320.D 491700251-1DL2 03/07/2017 02:19 PM E12270 25 cc 40 Sample Dilution
8 L9321.D 491700264-1 03/07/2017 03:09 PM E0666 500 cc 1
9 L9322.D 491700264-2 03/07/2017 04:29 PM E12282 500 cc 1
10 L9323.D 491700264-3 03/07/2017 05:20 PM E15532 565 cc 1
11 L9324.D 491700264-4 03/07/2017 06:10 PM E15614 500 cc 1
12 L9325.D 491700264-5 03/07/2017 07:00 PM E0366 500 cc 1
13 L9326.D 491700264-6 03/07/2017 07:49 PM E0640 500 cc 1
14 L9327.D 491700264-7 03/07/2017 08:40 PM E0415 540 cc 1
15 L9328.D 491700264-7DUP 03/07/2017 09:30 PM E0415 540 cc 1 Sample Duplicate
16 L9329.D IB030717L-A 03/07/2017 10:20 PM E15294 500 cc 1 Instrument Blank
17 L9330.D 491700245-1 03/07/2017 11:10 PM E0448 500 cc 1
18 L9331.D 491700245-2 03/08/2017 12:00 AM E12267 500 cc 1
19 L9332.D 491700245-3 03/08/2017 12:50 AM E12292 500 cc 1
20 L9333.D 491700245-4 03/08/2017 01:40 AM E15311 500 cc 1
21 L9334.D ECVS030717L-10 03/08/2017 02:24 AM E12284 125 cc 1 Ending Calibration Check
787 of 794
Phone/Fax: (856) 858-4800/ (856) 858-4571

Instrument ID: GC/MS L-C Batch Start Time: 03:51 AM

1 L9336.D BFB030817L 03/08/2017 03:51 AM S1023 100 cc 1 Tune Standard

2 L9337.D CCVS030817L-10 03/08/2017 04:34 AM E12284 125 cc 1 Calibration Check Standard
6 L9341.D IB030817L-A 03/08/2017 09:17 AM E15294 500 cc 1 Instrument Blank
7 L9342.D 491700264-2RE 03/08/2017 10:07 AM E12282 500 cc 1 Reanalysis
8 L9343.D 491700245-5 03/08/2017 10:57 AM E15519 500 cc 1
9 L9344.D 491700245-6 03/08/2017 11:46 AM E0384 500 cc 1
10 L9345.D 491700245-7 03/08/2017 12:36 PM E0420 500 cc 1
11 L9346.D 491700245-8 03/08/2017 01:26 PM E0437 500 cc 1
12 L9347.D 491700245-9 03/08/2017 02:16 PM E0597 500 cc 1
13 L9348.D 491700245-9DUP 03/08/2017 03:06 PM E0597 500 cc 1 Sample Duplicate
17 L9352.D ECVS030817L-10 03/08/2017 06:07 PM E12284 125 cc 1
18
19
20
21
22
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Phone/Fax: (856) 858-4800/ (856) 858-4571

Instrument Batch ID: 112116 Batch Start Date: 11/21/2016

1 L8546.D BFB112116 11/21/2016 05:26 PM T1042R 100 cc 1 Tune Standard

2 L8547.D IC112116L-40 11/21/2016 06:16 PM E0375 500 cc 1
3 L8548.D IC112116L-20 11/21/2016 07:02 PM E0375 250 cc 1
4 L8549.D IC112116L-10 11/21/2016 07:47 PM E0375 125 cc 1
5 L8550.D IC112116L-2 11/21/2016 08:37 PM E0443 500 cc 1
6 L8551.D IC112116L-0.5 11/21/2016 09:21 PM E0443 125 cc 1
7 L8552.D IC112116L-0.2 11/21/2016 10:04 PM E0443 50 cc 1
8 L8553.D ICVS112116L-10 11/21/2016 10:48 PM E0462 125 cc 1 Initial Cal Verification Std.
9 L8554.D ICVS112116L-10B 11/21/2016 11:32 PM E0462 125 cc 1 Initial Cal Verification Std.
13 L8558.D C3390 11/22/2016 12:13 PM E0290 500 cc 1 Reclean
14 L8559.D 491601365-1 11/22/2016 01:04 PM E0543 500 cc 1
16 L8561.D 491601374-1 11/22/2016 02:40 PM E0301 500 cc 1
19
20
21
22
23
24
25
26
27
28
29
30
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Phone/Fax: (856) 858-4800/ (856) 858-4571

Instrument Batch ID: 112216 Batch Start Date: 11/22/2016

1 L8565.D BFB112216 11/22/2016 05:49 PM T1042R 100 cc 1 Tune Standard

2 L8566.D CCVS112216L-10 11/22/2016 06:33 PM E0375 125 cc 1 Calibration Check Standard
3 L8567.D MB112216L 11/22/2016 08:15 PM E0243 500 cc 1 Method Blank
6 L8570.D C3380 11/22/2016 10:34 PM E0654 500 cc 1 Rerun on J
7 L8571.D 491601339-1 11/22/2016 11:25 PM E0312 500 cc 1
8 L8572.D 491601339-1DL 11/23/2016 12:08 AM E0312 50 cc 10 Sample Dilution
9 L8573.D 491601339-2 11/23/2016 12:59 AM E0572 500 cc 1
11 L8575.D 491601339-3 11/23/2016 02:34 AM E0639 500 cc 1
13 L8577.D 491601339-4 11/23/2016 04:09 AM E0656 500 cc 1
14 L8578.D 491601339-5 11/23/2016 05:00 AM E15531 500 cc 1
15 L8579.D 491601339-6 11/23/2016 05:51 AM E0316 500 cc 1
17 L8581.D 491601348-1 11/23/2016 07:25 AM E0327 500 cc 1
18 L8582.D 491601348-2 11/23/2016 08:15 AM E0342 500 cc 1
19 L8583.D 491601348-3 11/23/2016 09:06 AM E0405 500 cc 1
20 L8584.D 491601348-4 11/23/2016 09:57 AM E0410 500 cc 1
24 L8588.D C3389 11/23/2016 01:01 PM E0448 500 cc 1
25 L8589.D C3390 11/23/2016 01:51 PM E0290 500 cc 1
27
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30
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EMSL Analytical EMSL Order #: 491700245

200 Route 130 North, Cinnaminson, NJ 08077

Attn: Rakesh Ganta Phone: 201-509-8333

Laboratory Report- Sample Summary

Report Date: Report Revision Revision Comments

Marjorie Howley, Laboratory Manager

Test results meet all NELAP requirements unless otherwise specified.

491700245-0001_R0 V19 Page 1 of 5

Internal Chain of Custody 3

Shipping Documentation- Air bills, Sample Receipt Checklist 5

Copies of Traceability Certificates from Commercial Gas Standard Suppliers 10

Method Detection Limit Summary 100

Verified Method Detection Limit Summary 103

Reporting Limit Laboratory Control Sample (RLLCS) 107

Method Blank Summary 116

Instrument Performance Check Summary (BFB) 119

Internal Standard Area and Retention Time Summary 123

Sample Lab Data Summary- (with supporting raw data) 128

Initial Calibration Form Summary 502

Initial Calibration Verification Sample Standard Summary (ICVSS) 527

Continuing and Closing Calibration Verification Summary (CCVS, ECVS) 539

Raw QC Data -(with supporting raw data)

GC/MS Tune Performance Data (BFB) 584

Blank Data (Method and Instrument Blanks) 592

Reporting Limit Laboratory Control Sample Data (RLLCS) 674

Clean Canister Certification Data

Reporting Limit Laboratory Control Sample (RLLCS) 702

Method Blank Summary and Data Report 708

Instrument Performance Check (BFB) 718

Internal Standard Area and Retention Time Summary 722

Clean Canister Data (with supporting raw data). 726

Initial Calibration Summary 756

Initial Calibration Verification Sample Standard Summary (ICVSS) 762

Continuing Calibration Summary(s) including Closing (CCVS, ECVS) 774

Sample Preparation Data

Instrument Run Logs (sample data run logs) 785

Instrument Run Logs (clean canister run logs) 789

Pressure Gauge Readings 793

Canister Dilution Calculation (If Applicable) NA

Please visit our website at http://www.emsl.com

Attn: Rakesh Ganta Phone: 201-509-8333

Initial Calibration Verification Standard (ICVS)- Second Source

Continuing Calibration Verification Standard (CCVS)

Ending Calibration Verification Standard (ECVS)

Method Blanks (MB)

Instrument Blanks (IB):

491700245-0001_R0 V19 Page 1 of 2

Attn: Rakesh Ganta Phone: 201-509-8333

Report Date: Report Revision Revision Comments

Scott Van Etten, CIH/Jefferson Salvador

Test results meet all NELAP requirements unless otherwise specified.

491700245-0001_R0 V19 Page 2 of 2

CAS Molecular Lab Q Corrected Retention QAS Foot-

Method TO-15 ppbv ug/m3

CAS Molecular Lab Q Corrected Retention QAS Foot-

Method TO-15 ppbv ug/m3

CAS Molecular Lab Q Corrected Retention QAS Foot-

Method TO-15 ppbv ug/m3

CAS Molecular Lab Q Corrected Retention QAS Foot-

Method TO-15 ppbv ug/m3

CAS Molecular Lab Q Corrected Retention QAS Foot-

Method TO-15 ppbv ug/m3

CAS Molecular Lab Q Corrected Retention QAS Foot-

Method TO-15 ppbv ug/m3