Pharmaceutical Drug Analysis

Pharmaceutical Drug Analysis
Subject : Pharmaceutical Drug Analysis

GENERAL ASPECTS
Pharmaceutical Chemicals Purity and Management
1. Pharmaceutical Chemicals: Purity and Management - Answer (click here)
2. Pharmaceutical Chemicals: Purity - Answer (click here)
3. Pharmaceutical Chemicals: Management - Answer (click here)
4. Description of the Drug or Finished Product - Pharmaceutical
Chemicals: Management - Answer (click here)
5. Sampling Procedures and Errors - Pharmaceutical Chemicals:
Management - Answer (click here)
6. Bioavailability - Pharmaceutical Chemicals: Management - Answer (click
here)
7. Identification Tests - Pharmaceutical Chemicals: Management - Answer
(click here)
8. Physical Constants - Pharmaceutical Chemicals: Management - Answer
(click here)
9. Limit Tests Vis-A-Vis Quantitative Determinations - Answer (click here)
10. Various Types of Tests for Quantitative Determinations -
Pharmaceutical Chemicals: Management - Answer (click here)
11. Limit Tests for Metallic Impurities - Answer (click here)
12. Limit Tests for Lead - Answer (click here)
13. Limit Test for Arsenic - Answer (click here)
14. Limit Test’s for Acid Radical Impurities - Answer (click here)
15. Limit Tests for Non-Metallic Impurities - Answer (click here)
Theory and Technique of Quantitative Analysis

here)
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16. Theory and Technique of Quantitative Analysis - Answer (click here)
17. Volumetric Analysis - Answer (click here)
18. Volumetric Apparatus - Answer (click here)
19. Volumetric Analysis: General Cosiderations - Answer (click here)
20. Technique of Volumetric Analysis - Answer (click here)
21. Biomedical Analytical Chemistry - Answer (click here)
22. Biomedical Analytical Chemistry: Colorimetric Assays - Answer (click
here)
23. Biomedical Analytical Chemistry: Enzymatic Assays - Answer (click here)
24. Radioimmunoassays (RIAS) - Answer (click here)
25. Automated Methods of Clinical Analysis - Answer (click here)
Errors In Pharmaceutical Analysis and Statistical Validation

here)
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here)
26. Errors in Pharmaceutical Analysis - Answer (click here)
27. Classification of Errors in Pharmaceutical Analysis - Answer (click here)
28. Pharmaceutical Statistical Validation - Answer (click here)
29. Statistical Treatment of Finite Samples - Answer (click here)
30. Distribution of Random Numbers - Answer (click here)
31. Significant Figures - Answer (click here)
32. Comparison of Results - Answer (click here)
33. Method of Least Squares - Answer (click here)
34. Recommendations for Criteria of Rejecting an Observation - Answer (click
here)
35. Sampling Statistics - Answer (click here)
CHEMICAL METHODS
Aqueous Titrations
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here)
here)
36. Aqueous Titrations - Answer (click here)
37. Theory of Acidimetry - Answer (click here)
38. Aqueous Titrations: Assay of Drugs - Answer (click here)
39. Theory of Alkalimetry - Answer (click here)
Non Aqueous Titrations

here)
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40. Non-Aqueous Titrations - Answer (click here)
41. Non-Aqueous Titrations: Theory - Answer (click here)
42. Non-Aqueous Titrations: Methodology - Answer (click here)
43. Assay by Non-Aqueous Titrations - Answer (click here)
44. Acidimetry in Non-Aqueous Titrations - Answer (click here)
45. Alkalimetry in Non-Aqueous Titrations - Answer (click here)
Permanganate Dichromate and Ceric Sulphate Titration Methods

here)
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here)
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46. Permanganate, Dichromate and Ceric Sulphate Titration Methods -
Answer (click here)
47. Theory - Permanganate, Dichromate and Ceric Sulphate Titration
Methods - Answer (click here)
48. Assay Methods - Permanganate, Dichromate and Ceric Sulphate
Titration Methods - Answer (click here)
49. Permanganate Titration Methods - Answer (click here)
50. Dichromate Titration Methods - Answer (click here)
51. Ceric Sulphate Titration Methods - Answer (click here)
Iodimetric and Iodometric Titrations

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Answer (click here)
52. Iodimetric and Iodometric Titrations - Answer (click here)
53. Theory - Iodimetric and Iodometric Titrations - Answer (click here)
54. Assay Methods - Iodimetric and Iodometric Titrations - Answer (click here)
55. Iodimetric Assays - Answer (click here)
56. Iodometric Assays - Answer (click here)
57. Argentometric Precipitation Methods - Answer (click here)
58. Argentometric Precipitation Methods: Theory - Answer (click here)
59. Argentometric Precipitation Methods: Assay Methods - Answer (click here)
Complexometric Analysis
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Answer (click here)
60. Complexometric Analysis - Answer (click here)
61. Complexometric Analysis: Theory - Answer (click here)
62. Complexometric Analysis: Assay Methods - Answer (click here)
Gravimetric Analysis
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Answer (click here)
63. Gravimetric Analysis - Answer (click here)
64. Gravimetric Analysis: Theory - Answer (click here)
65. Gravimetric Analysis: Assay Methods - Answer (click here)
66. Substances Assayed Gravimetrically - Answer (click here)
67. Substances Assayed After Conversion - Gravimetric Analysis - Answer
(click here)
Thermoanalytical Analysis
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Answer (click here)
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68. Thermoanalytical Analysis - Answer (click here)
69. Thermogravimetric Analysis (TGA) - Answer (click here)
70. Differential Thermal Analysis (DTA) - Answer (click here)
71. Thermometric Titrations (TT) - Answer (click here)
Diazotization Sodium Nitrite Titration

here)
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here)
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Answer (click here)
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72. Diazotization (Sodium Nitrite Titration) - Answer (click here)
73. Diazotization (Sodium Nitrite Titration): Assay Methods - Answer (click
here)
Estimation of Phenols and Related Compounds

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Answer (click here)
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here)
74. Estimation of Phenols and Related Compounds - Answer (click here)
75. Estimation of Phenols and Related Compounds: Assay Methods - Answer
(click here)
Karl Fischer Method for Determination of Water

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Answer (click here)
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here)
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76. Karl Fischer Method for Determination of Water - Answer (click here)
77. Instrumentation - Karl Fischer Method for Determination of Water -
Answer (click here)
78. Applications of Karl Fischer Method for Determination of Water in
Pharmaceutical Analysis - Answer (click here)
Tetrazolium Assay of Steroids

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Answer (click here)
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here)
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Answer (click here)
79. Tetrazolium Assay of Steroids - Answer (click here)
80. Tetrazolium Assay of Steroids: Theory - Answer (click here)
81. Assay of Pharmaceutical Substances - Tetrazolium Assay of Steroids -
Answer (click here)
ELECTROCHEMICAL METHODS
Potentiometric Methods
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Answer (click here)
82. Potentiometric Methods - Answer (click here)
83. Potentiometric Methods: Theory - Answer (click here)
84. Potentiometric Methods Instrumentation: Electrodes, Automatic Titrator
- Answer (click here)
85. Applications of Potentiometric Titrations in Pharmaceutical Analysis -
Answer (click here)
Amperometric Methods
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86. Amperometric Methods - Answer (click here)
87. Amperometric Methods: Theory - Answer (click here)
88. Amperometric Methods: Instrumentation - Answer (click here)
89. Applications of Amperometric Titrations in Pharmaceutical Substances -
Answer (click here)
OPTICAL METHODS
Refractometry
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90. Refractometry - Answer (click here)
91. Refractometry: Theory - Answer (click here)
92. Refractometry: Instrumentation - Answer (click here)
93. Determination of Refractive Index of Pharmaceutical Substances -
Answer (click here)
94. Applications of Refractivity - Answer (click here)
Polarimetry
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95. Polarimetry - Answer (click here)
96. Polarimetry: Theory - Answer (click here)
97. Polarimetry: Instrumentation - Answer (click here)
98. Determination of Optical Activity of Pharmaceutical Substances - Answer
(click here)
99. Nephelometry and Turbidimetry - Answer (click here)
100. Nephelometry and Turbidimetry: Theory - Answer (click here)
101. Instruments for Nephelometry and Turbidimetry - Answer (click here)
102. Turbidimetric Assay of Pharmaceutical Substances - Answer (click here)
103. Nephelometric Assay of Pharmaceutical Substances - Answer (click here)
Ultraviolet and Absorption Methods

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104. Ultraviolet and Absorption Methods - Answer (click here)
105. Ultraviolet and Absorption Methods: Theory - Answer (click here)
106. Ultraviolet and Absorption Methods: Instrumentation - Answer (click here)
107. Ultraviolet and Absorption Methods: Assay Methods - Answer (click here)
Infrared Spectrophotometry
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108. Infrared Spectrophotometry - Answer (click here)
109. Infrared Spectrophotometry: Theory - Answer (click here)
110. Infrared Spectrophotometry: Instrumentation - Answer (click here)
111. Applications of IR-Spectroscopy in Pharmaceutical Assays - Answer (click
here)
112. Applications of IR-Spectroscopy in Analytical Chemistry - Answer (click
here)
Nuclear Magnetic Resonance Spectroscopy

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113. Nuclear Magnetic Resonance Spectroscopy - Answer (click here)
114. Nuclear Magnetic Resonance Spectroscopy: Theory - Answer (click here)
115. Interpretation of a NMR-Spectrum - Answer (click here)
116. Nuclear Magnetic Resonance Spectroscopy: Instrumentation - Answer
(click here)
117. Applications of NMR-Spectroscopy in Pharmaceutical Analysis - Answer
(click here)
Emission Spectroscopy
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118. Emission Spectroscopy - Answer (click here)
119. Emission Spectroscopy: Theory - Answer (click here)
120. Emission Spectroscopy: Instrumentation - Answer (click here)
121. Applications of Emission Spectroscopy - Answer (click here)
Flame Spectroscopy
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122. Flame Spectroscopy - Answer (click here)
123. Flame Spectroscopy: Theory - Answer (click here)
124. Flame Spectroscopy: Instrumentation - Answer (click here)
125. Applications of Flame Emission Spectroscopy in Pharmaceutical
Analysis - Answer (click here)
Atomic Absorption Spectroscopy

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126. Atomic Absorption Spectroscopy - Answer (click here)
127. Atomic Absorption Spectroscopy: Theory - Answer (click here)
128. Atomic Absorption Spectroscopy: Instrumentation - Answer (click here)
129. Important Aspects of Atomic Absorption Spectroscopy - Answer (click
here)
130. Application of Atomic Absorption Spectroscopy in Pharmaceutical
ASSAY METHODS BASED ON SEPARATION TECHNIEQUES

Liquid Liquid Extraction
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131. Liquid-Liquid Extraction - Answer (click here)
132. Liquid-Liquid Extraction: Theory - Answer (click here)
133. Factors Influencing Solvent Extraction - Answer (click here)
134. Emulsion Problem Encountered in Extractions - Answer (click here)
135. Assay Methods Based on Liquid-Liquid Extraction - Answer (click here)
Thin Layer Chromatography TLC

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136. Thin Layer Chromatography (TLC) - Answer (click here)
137. Thin Layer Chromatography (TLC): Theory - Answer (click here)
138. Preparation of Thin Layers on Plates - Thin Layer Chromatography
(TLC) - Answer (click here)
139. Choice of Adsorbents - Thin Layer Chromatography (TLC) - Answer
(click here)
140. Choice Of Solvent System in Thin Layer Chromatography (TLC) -
Answer (click here)
141. Activation of Adsorbent - Thin Layer Chromatography (TLC) - Answer
(click here)
142. Purification of Silica Gel-G Layers - Thin Layer Chromatography (TLC)
143. Spotting of the Components - Thin Layer Chromatography (TLC) -
Answer (click here)
144. Development of Thin Layers - Thin Layer Chromatography (TLC) -
Answer (click here)
145. Special Techniques in Thin Layer Chromatography (TLC) - Answer (click
here)
146. Chemical Reactions on Thin Layer Chromatography (TLC) Plates -
Answer (click here)
147. Combination of Thin Layer Chromatography (TLC) With other
Techniques - Answer (click here)
148. Detection of Components - Thin Layer Chromatography (TLC) - Answer
(click here)
149. Evaluation of the Chromatogram - Thin Layer Chromatography (TLC) -
Answer (click here)
150. Applications of TLC in Pharmaceutical Analysis - Answer (click here)
Gas Liquid Chromatography GLC

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151. Gas Liquid Chromatography (GLC) - Answer (click here)
152. Gas Liquid Chromatography (GLC): Theory - Answer (click here)
153. Gas Liquid Chromatography (GLC): Instrumentation - Answer (click here)
154. Working Techniques for Quantitative Analysis - Gas Liquid
Chromatography (GLC) - Answer (click here)
155. Applications of GLC in Pharmaceutical Analysis - Answer (click here)
156. High Performance Liquid Chromatography (HPLC) - Answer (click here)
157. High Performance Liquid Chromatography (HPLC): Theory - Answer
(click here)
158. Instrumentation - High Performance Liquid Chromatography (HPLC) -
Answer (click here)
159. Derivatization - High Performance Liquid Chromatography (HPLC) -
Answer (click here)
160. Applications of High Performance Liquid Chromatography (HPLC) in
Size Exclusion Chromatography

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161. Size Exclusion Chromatography - Answer (click here)
162. Size Exclusion Chromatography: Theory - Answer (click here)
163. Size Exclusion Chromatography: Apparatus - Answer (click here)
164. Applications of Size Exclusion Chromatography in Pharmaceutical
MISCELLANEOUS METHODS
Radioimmunoassay
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161. Size Exclusion Chromatography - Answer (click here)
162. Size Exclusion Chromatography: Theory - Answer (click here)
163. Size Exclusion Chromatography: Apparatus - Answer (click here)
164. Applications of Size Exclusion Chromatography in Pharmaceutical
165. Radioimmunoassay - Answer (click here)
166. Radioimmunoassay: Theory - Answer (click here)
167. Radioimmunoassay: Instrumentation - Answer (click here)
168. Radioimmunoassay: Methodology of the Assay - Answer (click here)
169. Applications of Radioimmunoassay (RIA) in Pharmaceutical Analysis -
Answer (click here)
170. Novel Applications of Radioimmunoassay(RIA)-Techniques - Answer
(click here)

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Subject : Pharmaceutical Drug Analysis

Theory and Technique of Quantitative Analysis

Errors In Pharmaceutical Analysis and Statistical Validation

Non Aqueous Titrations

Permanganate Dichromate and Ceric Sulphate Titration Methods

Iodimetric and Iodometric Titrations

Diazotization Sodium Nitrite Titration

Estimation of Phenols and Related Compounds

Karl Fischer Method for Determination of Water

Tetrazolium Assay of Steroids

Ultraviolet and Absorption Methods

Nuclear Magnetic Resonance Spectroscopy

Atomic Absorption Spectroscopy

ASSAY METHODS BASED ON SEPARATION TECHNIEQUES

Thin Layer Chromatography TLC

Gas Liquid Chromatography GLC

Size Exclusion Chromatography

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