FARABI Y

YANBU PETROCHEMIC
CALS
COMPANY

FARA
ABI NORMAAL PARAFFIIN AND DERRIVATIVES
C
COMPLEX, Y
YANBU, KINNGDOM OF SAUDI
ARABIAA
G446-0828-2810-Q
QA-0100-006
65

PICKLING
P & PASSIVAT
TION PROCE
EDURE

EMPLOYER R : FARABI Y
YANBU PET TROCHEMICCALS COMP PANY
PROJECT : FARABI N
NORMAL PA ARAFFIN ANND DERIVAATIVES COM
MPLEX
EPC CONTR RACTOR : L&T HYDRROCARBON N ENGINEERING
LTHE JOB NO : G446
PR NO : G446-2810
0-MR-0100-0005
VENDOR
V NAME : ION EXCHHANGE IND
DIA LIMITED
D
ITEM DESCCRIPTION : DEMINERRALIZATIONN PACKAGEE (810-ME-01)
ITEM TAG : 810-ME-01
1
DOCUMENT
CATEGOORY AL CODES / REVIEW
APPROVA APP
PROVAL COODES / REVIIEW
(USE TICK MARK) ST
TATUS- LTH
HE STA
ATUS- PMC / EMPLOYEER

[CODE 1] REEJECTED [CODE 11] REJECTEED

R
Revise and Resubmit.
R Revise a
and Resubmit.
A
[CODE 2] COOMMENTS A AS NOTED [CODE 22] COMMEN NTS AS NOT TED
W
Work may prroceed subje
ect to Work maay proceed subject
s to
c
compliance w and inco
with orporation off nce with and incorporatio
complian on of
R c
comments. comments.

[CODE 3] NOO COMMENNTS [CODE 3

3] NO COMM MENTS
W
Work may prroceed. Work ma
ay proceed.
I
[CODE 4] INFORMATIO ON ONLY [CODE 44] INFORMA ATION ONLY Y
A
Accepted forr information only. Accepted
d for informa
ation only.
LTHE APPROVAL EMPLOYER App
proval
DISCIPLINE
PREPARED BY DISCIPLINE
REVIEWED BY SIGNATURE
APPROVED BY
DATE ( dd-m
mm-yy)
Date ( dd-mm-yy)
CODE
Code
This approvval does not abso olve the CONTRA ACTOR
This review / apprroval does not re
T elieve the vendor from meetinng their contractuual obligation of delivering
d a
/ manufacturer of the full responsibility as to design
n complete, sa afe and efficiently operating unit/ffacilities
mensions & comp
correctness of dim pliance with all meeting all rrequirement of thhe contract
a
applicable regulattions and with the
e requirements
m
made in purchaseer specifications.

02 15-Jun
n-18 Issu
ued for Review
w GP NT
T M
MR SG RS

01 13-Ap
pr-18 Issu
ued for Review
w GP NT
T M
MR SG RS

PREPAR
RED REVIEWWED APPR
ROVED VIEWED
REV AP
PPROVED
Rev Datte DE
ESCRIPTION
BY BYY B
BY BY BY

ALL RIGHTS
R RESERVED
THIS DOCUMENT AND ANY
A DATA AND INNFORMATION CONTA AINED THEREIN AREE CONFIDENTIAL AND
A THE PROPERTYY OF L&T HYDROCAARBON ENGINEERIN
NG (LTHE) AND THE
E
YRIGHT THEREIN IS VESTED IN LTC NO PART OF THIS DOCU
COPY UMENT, DATA, OR IN
NFORMATION SHALLL BE DISCLOSED TO
O OTHERS OR REPRO
ODUCED IN ANY MA
ANNER OR USED FOR
R
ANY PURPOSE WHATSOE EVER, EXCEPT WITH
H THE PRIOR WRITTEN
N PERMISSION OF LT
TC.

1
 FARABI Y
YANBU PETROCHEMIC
CALS
COMPANY

FARA
ABI NORMAAL PARAFFIIN AND DERRIVATIVES
C
COMPLEX, Y
YANBU, KINNGDOM OF SAUDI
ARABIAA
G446-0828-2810-Q
QA-0100-006
65

PICKLING
P & PASSIVAT
TION PROCE
EDURE

REVISION HISTORY
Y SHEET

S. Rev. Page Clause /

No. Noo. Line No. Brief Description / Reason
R of R
Revision Remarkss
No.
1  01
1  1‐7  -   Initial sub
bmission
2  02
2  1‐7  -   Client Commments inco
orporated an
nd issued forr 
Review 

2
 FARABI Y
YANBU PETROCHEMIC
CALS
COMPANY

FARA
ABI NORMAAL PARAFFIIN AND DERRIVATIVES
C
COMPLEX, Y
YANBU, KINNGDOM OF SAUDI
ARABIAA
G446-0828-2810-Q
QA-0100-006
65

PICKLING
P & PASSIVAT
TION PROCE
EDURE

CO
ONTENT
T

1. Purpose…………………
……………………
……………………
……………………
…….…………Pa
age 04 of 07

2. Referen
nces……………
……………………
……………………
……………………
…….…………Pa
age 04 of 07
7

3. Pre-cleaning of sta
ainless steel…………………
……………………
……….………..P
Page 04 of 07
0

4. Acid Cleaning………….………………
……………………
……………………
……….……...P
Page 05 of 07
0

5. Final cleaning or Passivation..

P …………………
……………………
…….…………..P
Page 05 of 07
0

6. Inspecttion after Clleaning………

……………………
……………………
….…………… Pa
age 06 of 07

7. Protecttion of Clean
ned surface...…………………
……………………
……………… Pa
age 06 of 07

8. Sample
e Report Forrmat …………
……………………
……………………
……..…..…….P
Page 07 Of 07
0

3
 FARABI Y
YANBU PETROCHEMIC
CALS
COMPANY

FARA
ABI NORMAAL PARAFFIIN AND DERRIVATIVES
C
COMPLEX, Y
YANBU, KINNGDOM OF SAUDI
ARABIAA
G446-0828-2810-Q
QA-0100-006
65

PICKLING
P & PASSIVAT
TION PROCE
EDURE

1. PURPOS
SE:

Thee purpose off this procedu ure is to remoove surface contaminants

c s that may immpair the normal corrosion
res
sistance, or re
esult in the la
ater contamin eel or cause product conttamination. All
nation of the stainless ste A the
asssociated Carttridge filters, tanks and thhe interconneecting skid piiping are acid
d cleaned, pickled and pa
assivated
from
m Outside su urfaces and wherever
w acc
cessible insid
de surfaces.

RANCES:
2. REFER

AS
STM A380:- Standard
S pracctice for clea
aning, Descalling & passiv
vation of stain
nless steel pa
arts, Equipment &
sy
ystems

AS
STM A967:- Std.
S Spec for Chemical Pa
assivation Trreatments forr Stainless Steel Parts

Note: Pickling & Passivation

n shall be carrried out in acid solution which
w shall b
be based upo
on a mixture of
HF
F/HNO3. Acid d concentratio
on shall be controlled
c as per manufaccturer’s recommmendationss.

AFETY ASPE
SA ECT:

1] Chemical
C application is done by specialized perso onnel wearing g special protective clothiing.
2] A suitable airr supply and venting system shall be m maintained.
3] Keep
K away all
a equipmentt from the nearby area of application of o chemicals.
I all instances, the supplier,, Instructions shall be
4] In e carefully followed.
5] No
N other worrk can be carrried out in thhe same vicinnity/location to
t be pickled during the trreatment.
6] Strict
S personnel access control
c must be
b maintaine ed in designa ated area.
7] In
I case of coontamination, immediately y take a wash h with rinsed water for miinimum 15 minutes,
m rinse
e eyes
pro
operly. Inform
m the incidentt to the safetty departmennt for further treatment.
t

3. PRE – CLEANING
C OF
O STAINLE
ESS STEEL

Oxxidation may be removed by mechanic cal means. T The surface shall be polish hed with a grrinder
andd a smooth trransition to th
he unpolishe
ed base mate erial surface shall
s be mad de. Never usee grinding whheels,
sannding materia
als or wire brrushes made e of iron, iron oxide, steel,, zinc or othe
er undesirablee materials th
hat may
cauuse contamin
nation of the stainless steeel.

Griinding wheels, sanding wheels

w and wire brushes that
t have bee
en previouslyy used on another materia
al shall not
be used on staiinless steel.

Never use steel shot, grit orr abrasive tho

ose have bee
en used to bllast other ma
aterial.

ux or slag from
Flu m welding to
o be removed
d by chipping
g and brushin
ng with S. S. Wire brush or
o
Griinding with iro
on-free wheeel.

4
 FARABI Y
YANBU PETROCHEMIC
CALS
COMPANY

FARA
ABI NORMAAL PARAFFIIN AND DERRIVATIVES
C
COMPLEX, Y
YANBU, KINNGDOM OF SAUDI
ARABIAA
G446-0828-2810-Q
QA-0100-006
65

PICKLING
P & PASSIVAT
TION PROCE
EDURE

4 . ACID CLEA ANING

Aciid Cleaning iss a process in
i which a soolution of a m
mineral or org
ganic acid in water,
w somettimes in com
mbination
with a wetting agent
a or dete
ergent or both
h, is employeed to remove iron and oth her metallic contamination
c n, light oxide
ms, shop soil,, and similar contaminantts. Suggested
film d solutions, contact
c timess, and solutio
on temperatu
ures for
varrious alloys are
a as per Ta able A2.1

WAATER RINSE E AFTER PICKLING :

After acid clean
ning the surfaaces must be e thoroughly rinsed with clean
c water to
o remove all traces of the
e acid and
oroughly dried
tho d after the fin
nal water rins
se.

5. FINAL
F CLEA
ANING OR PASSIVATIO
P ON

The e passivated d parts shall exhibit

e a chem
mically clean
n surface and
d shall, on vissual inspectio
on, show no etching,
pittting, or frostin
ng resulting from
f the passivation proccedures.

WAATER RINSE E AFTER PA ASSIVATION—

Imm
mediately aftter removal frrom the pass
sivating soluttion, the partss shall be tho
oroughly rins
sed, with clea
an water.

5
 FARABI Y
YANBU PETROCHEMIC
CALS
COMPANY

FARA
ABI NORMAAL PARAFFIIN AND DERRIVATIVES
C
COMPLEX, Y
YANBU, KINNGDOM OF SAUDI
ARABIAA
G446-0828-2810-Q
QA-0100-006
65

PICKLING
P & PASSIVAT
TION PROCE
EDURE

6 INSPECTION
I N AFTER CL
LEANING

6.1 Visual—
Item
ms cleaned in accordancce with this prractice should be free of paint,
p oil, gre
ease, weldingg flux, slag, heat-treating
h
andd hot-formingg scale (tightly adherent scale
s resultin
ng from weldiing may be permissible
p on some surfa aces), dirt,
trassh, metal andd abrasive paarticles and chips,
c and otther gross coontamination..
Some deposited d atmospherric dust will normally be present on ex xterior surface es but should
d not be pressent on
inte
erior surfacess.
After pickling cleaning, treatted surface shall
s be exam mined and de eclared, free of any visiblee deposits off oils,
greease, or other contaminan nts. If any of them are preesent, picklin
ng cleaning shall be re-pe erformed.

6.2
2 Wipe Tests s—
Rubbing of a su urface with a clean, lint-free, white cottton cloth, co
ommercial paaper product, or filter pape
er
mooistened (but not saturated) with high-purity solven nt acetone, ke etone or anyy precision ag
gent , may bee used for
evaaluating the cleanness
c off surfaces. ( After
A Visual Inspection thiis test may b
be perform if any smudge present on
ated surface.)
trea

7 PROTECTIO
P ONS OF CLE
EANED SURF
FACES

Pla
astic wrapping will be donne to protect cleaned surffaces as sooon as final cle
eaning is com
mpleted, and should be
maaintained duriing all subsequent shipping, inspectio
on, storage, and
a installatio on.

6
 FARABI Y
YANBU PETROCHEMIC
CALS
COMPANY

FARA
ABI NORMAAL PARAFFIIN AND DERRIVATIVES
C
COMPLEX, Y
YANBU, KINNGDOM OF SAUDI
ARABIAA
G446-0828-2810-Q
QA-0100-006
65

PICKLING
P & PASSIVAT
TION PROCE
EDURE

8 SAMPL
LE REPORT
T FORMAT.

PIC
CKLING AND
D PASSIVATIION REPORT
T

REPORT
T REF : DAT
TE OF TEST :

1. GENERA
AL DETAILS:
EMPLOYER :
PROJECT :
EPC CONTRA
ACTOR :
(IEIL) JOB NO. :
(IEIL) P.O. REF.
R NO. :
SUB SUPPLIER :

2. ITEMS DESCRIPTION:
D :
EQUIPMENT
T NAME :
TAG NO. :
MATERIAL GRADE
G :

3. REFERE
ENCE DOCUME
ENTS:
DOCU
UMENT TITLE LTHE DO
OC. NO. IEIL DOC.N
NO. REV.
INSPECTION
N AND TEST PL
LAN :
PICKILING PROCEDURE NO.
N :
G.A.DRAWIN
NG NO. :

4. PRE-CLE
EANING :

5. PICKLIN
NG SOLUTION DETAILS:

6. TEMPER
RATURE:

7. PASSIVA
ATION DETAIILS:

8. REMARK
KS:

ASSIVATION
PICKLING & PA
SUB SUPPLIER CLIENT
AUTHORITY