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PERMEABILITY OF LIME-TREATED LATERITIC SOIL

By Kolawole J. Osinubi,l Member, ASCE

(Reviewed by the Highway Division)

ABSTRACT: Laboratory investigations were carried out on a. residual lateriti~ soil t~eated with qUic~lime (up
to 8% by weight of dry soil) in order to evaluate the effect of lime conten~, cunng penod~ ~d compactlve ef~ort
on the permeability of lateritic soil-lime mixtures prepared at various maximum dry de":sltles and correspo~ding
optimum moisture contents. The permeability of uncured specimens (standard Proctor) mcreased to a maximum
at 4% lime content and decreased with increasing lime content. Specimens compacted at the energy of the West
African Standard had coefficients of permeability that decreased with increasing lime content. .For the cu~ed
condition, the permeability of all the lime-treated specimens compacted at the two energy levels mcreased With
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curing age up to 14 days and decreased with curing age beyond 14 days.

INTRODUCTION clay particle structure. Many soils compacted drier than OMC
had more random particle orientations and a larger average
Addition of lime to a soil tends to improve its properties as pore size than when compacted wetter than OMC, where ~e
a result of soil-lime reactions. The advantage of this property particles had a more parallel arrangement. The larger the in-
has been utilized mostly for road subgrade stabilization dividual pores for any given total pore area, the greater ~e
("Lime" 1990; Locat et al. 1990; Hammond 1992), although flow would be, since permeability varies as a power functIOn
increasing use is being made of lime stabilization for bulk fill of pore size.
operations, embankments, and cutting slope repai~ ~n~ as a The effect of lime on soil permeability is still not clear.
bearing stratum for lightly loaded foundatIOns. This IS m .ad- Fossberg (1969) reported a decrease of as much as two orders
dition to lime slurry pressure injection, lime columns, and hme of magnitude in the coefficient of permeability with increasing
piles for ground improvement (Rog~rs ~d Bruce 1991; R.og- lime content, and found the decrease to be in direct proportion
ers and Glendinning 1994). Two mam different results of hme to the lime content and curing time. He based his conclusions
action are usually believed to occur in soil-lime mixes. The mainly on the results of consolidometer tests. The samples
first, quick action, occurs immediately on addition of lime and were compacted 1 h after mixing the soil and lime. Townsend
is believed to be due to cation exchange and flocculation. The and Klym (1966), on the other hand, reported a substantial
second reaction, aggregation, which is time-dependent (days
increase in the coefficient of permeability of heavy clay soils
to years), is rather slow. It is attributed to the pozzolanic re- (from 2 X 10- 8 cmls to 4 X 10- 6 cmls). The samples were
actions with formation of cementation compounds (Webb compacted 24 h after mixing the soil and lime and were cured
1992; Rogers and Lee 1994; Narasimha Rao and Rajasekaran as long as 19 weeks, with most of the increase in permeability
1996).
occurring during the first four weeks. The increase in the co-
Lateritic soils, which are defined by the ISSMFE Progress
efficient of permeability was explained in terms of the addi-
Report ("Peculiarities" 1985) as soils belonging to .horizo~ A tional flocculation that occurred during the elapsed time after
or B of well-drained profiles developed under humid trOPiCal mixing prior to compaction. Hunter (1988) explained the in-
climates with clay fraction constituted essentially of the kao-
crease in permeability of lime-treated clay as due to the siltlike
linite group and of iron or aluminium hydrated oxides, can be
mechanical properties imparted on the natural soil.
economically stabilized with lime (Ola 1975). The soil-lime
Lateritic soils are normally utilized as base for road con-
mixture so produced can be used as subbase or base courses
struction and are generally regarded as good foundation ma-
in roads. Moreover, the climate in Nigeria favors this type of
stabilization. terial because they are virtually nonswelling. However, the use
of the material is dependent on the degree of permeability,
One of the most important points taken into consideration
which determines whether the proposed road foundation is
in soil mechanics is the effect of water on the geotechnical
suitable for use. This study offered a good opportunity to in-
properties of soils. Permeability has not been studied as ex-
vestigate the effects of lime content, curing period, and com-
tensively as the other major soil engineering properties like
pactive effort on the coefficient of permeability of lime-treated
strength and compressibility. However, in recent times a sub-
lateritic soil specimens obtained from mixtures prepared at
stantial amount of work has been carried out by various re-
searchers [Ola (1983), Finno et al. (1996), Yin et al. (1996), their maximum dry densities and corresponding optimum
moisture contents.
Nuik and Singh (1997), and others] on permeability.
In his study of the permeability of compacted clay. Mitchell JUSTIFICATION FOR STUDY
(1976) found that the permeability of compacted clay samples
on the dry side of optimum moisture content (OMC) for stan- Quite a large amount of research has been conducted on the
dard compaction was many times higher than on the wet side. effect of lime on the strength properties of soils in the last two
The reason for this phenomenon was explained in terms of decades, but permeability has received far less attention. How-
ever, these researches were mostly carried out on temperate-
'Sr. Lect.. Dept. of Civ. Engrg.• Ahmadu Bello Univ., Zaria, Kaduna zone soils, which are significantly different from tropical re-
State, Nigeria. sidual soils. Unlike the sedimentary soils of temperate zones,
Note. Discussion open until March I, 1999. To extend the closing date the soil deposits generally referred to as lateritic soil have been
one month, a written request must be filed with the ASCE Manager of
Journals. The manuscript for this paper was submitted for review and
known to possess complex macro- and microfabric (Da Fon-
possible publication on September 2, 1997. This paper is part of the toura 1985), texture, and structure (Melfi 1985) due to their
Journal of Transportation Engineering. Vol. 124, No.5, Septemberl morphological features. The response of lateritic soils to sta-
October, 1998. ©ASCE. ISSN 0733-947X198/0005-0465-0469/$8.00 + bilization using different additives also relates significantly to
$.50 per page. Paper No. 16546. the genetic (morphological, physical, chemical, and minera-
JOURNAL OF TRANSPORTATION ENGINEERING 1 SEPTEMBER/OCTOBER 1998/465

J. Transp. Eng. 1998.124:465-469.


logical) characteristics as well as the moisture conditions of TABLE 1. Test Results of Natural Soli
the environment (Gidigasu and Kuma 1987). Property Quantity/description
One of the major problems confronting geotechnical engi- (1 ) (2)
neers in the tropics is the fact that most local soils are not
Natural moisture content (%) 7.1
amenable to standard pretest preparations and testing proce- Liquid limit (%) 44.0
dures, resulting in variations in the test results. These varia- Plastic limit (%) 24.0
bilities have been discussed by Gidigasu (1980) and Gidigasu Plasticity index (%) 20.0
and Yeboa (1972). However, differences in opinion are ex- Linear shrinkage (%) 9.5
pressed over the understanding of the engineering behavior of Percentage passing BS No. 200 sieve 52.0
residual soils. According to Vaughan (1985), the development Group index 7
AASHTO classification A-7-6
of classical concepts of soil mechanics has been based largely USCS classification CL
on the investigation of sedimentary deposits of unweathered Specific gravity 2.62
soils. These concepts have been found to be inappropriate in MOD (standard Proctor) (Mg/m') 1.84
describing the behavior of residual soils and could lead to OMC (standard Proctor) (%) 19.1
significant errors if inadvertently applied. Gidigasu (1988) MOD (West African Standard) (Mg/m') 1.89
concludes that classical soil-mechanics principles have failed OMC (West African Standard) (%) 15.7
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UCS (standard Proctor) (kN/m 2 ) 395


in answering some of the geotechnical problems in certain UCS (West African Standard) (kN/m 2) 590
soils formed under subtropical and tropical environments. pH 6.67
The major part of Nigeria is underlain by basement complex Color Reddish brown
rocks, the weathering of which had produced lateritic materials
spread over most of the area. It is virtually impossible to ex-
ecute any construction work in Nigeria without the use of lat- TABLE 2. Chemical Composition of Lateritic Soli
erite soils. On the basis of the foregoing, a study to determine Concentration
the effect of lime content, curing period, and compactive effort Oxide (% by weight)
on the permeability of lime-treated lateritic soil was con- (1 ) (2)
ducted. CaO 0.28
Si02 35.60
MATERIALS USED AND METHODS OF TESTING AI20, 27.40
Fe20, 2.40
Soil MgO 0.22
Na20 + K20
The soil samples used were obtained from a borrow pit in SO, 0.85
Zaria (latitude 11°15'N and longitude 7°45'E) using the Mn20, 2.0
method of disturbed sampling. A study of the geological and P20,
soil maps of Nigeria after Akintola (1982) and Areola (1982), Loss on ignition 1.46
respectively, shows that the samples taken belong to the group
of ferruginous tropical soils derived from acid igneous and TABLE 3. Oxide Composition of Quicklime
metamorphic rocks. The index properties of the natural soil as
well as its chemical composition are summarized in Tables 1 Concentration
and 2, respectively. The clay mineral present in the soil, which Oxide (% by weight)
was found to be kaolinite with some quartz, was qualitatively (1 ) (2)
assessed by way of differential thermal analysis (DTA) of ma- CaO 53.60
terial passing through a British Standard No. 200 sieve. The Na20 7.12
clay mineralogy was quantitatively assessed by X-ray diffrac- SO, 5.40
Fe20, 4.80
tion (XRD) analysis.
AI20, 4.08
MgO 3.80
Lime K 20 1.20
Loss on ignition 17.68
Hydrated lime was obtained by hydrating quicklime, due to
the nonavailability of the former. Before the quicklime was
hydrated the lumps were ground to particles less than 13 rom was at the foregoing two energy levels because the standard
in size. The quicklime is then able to react readily with water Proctor is easily achieved in the field, while the West African
to produce calcitic hydrated lime in which all the calcium ox- Standard compaction is the conventional energy level com-
ide is converted to calcium hydroxide, with the evolution of monly used in the region.
heat. The chemical analysis of the quicklime used gave the
oxide composition summarized in Table 3. With the proportion Water
of magnesium oxide being less than 5%, the quicklime can be
said to be a high-calcium lime in accordance with O'Flaherty Potable water was used to prepare the specimens at the var-
(1974). ious moisture contents, while distilled water was used as the
permeant in the permeability tests.
Compaction
Preparation of Specimens
Tests involving the moisture-density relationship and un-
confined compression were carried out using soil samples air- The soil-lime mixture used for preparing the permeability
dried for one day. The compactive efforts utilized throughout test specimens was obtained by first thoroughly mixing dry
the tests were the standard Proctor and West African Standard. predetermined quantities of pulverized soil and lime to obtain
If the British Standard (Proctor) compaction mold is utilized, a uniform color. The required quantity of water, which is de-
the compactive effort for the West African Standard consists termined from the moisture-density relation for the soil-lime
of the energy derived from a 4.5 kg rammer falling through mixtures, was then added and the mixing continued. After
45 cm onto five layers, each receiving 10 blows. Compaction compaction, the specimens and molds were placed in trans-
4661 JOURNAL OF TRANSPORTATION ENGINEERING 1 SEPTEMBER/OCTOBER 1998

J. Transp. Eng. 1998.124:465-469.


21
parent cellophane bags. which were sealed and then cured in
the humidity room at 100% relative humidity and a tempera-
ture of 25 ± 2°C. After the curing period had been attained,
the specimens and the molds were removed from the sealed
cellophane bags for permeability testing.

Permeability Tests
The compaction mold with the specimen in it was used as ------ Stan. Proctor
part of the permeameter in order to eliminate disturbance of - + - - West African SIan.
the specimens on extrusion from the molds. The falling head
test was adopted for the investigation. The first step in carrying
out the permeability test was to saturate the specimen in the
mold. The saturation process involved placing the perme-
ameter in a small water container. A transparent plastic hose
12 -1-------\------+-------+------
was connected between the opening at the top of the cell cap
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2 4 6 8
and an electric suction pump. The function of the suction Lime Content, %
pump was to accelerate the saturation of the specimen by elim- FIG. 3. Variation of OMC of li'eated Lateritic 5011 with Lime
inating entrapped air in the voids as much as possible before Content
"sucking" water in order to saturate it. The permeability tests
were performed in accordance with BS 1377 ("Methods" soil. Sodium hexametaphosphate, which is considered most
1990). and the coefficients of permeability reported are the effective as dispersant for these lateritic soils (Gidigasu and
average of five tests per specimen performed on three speci- Kuma 1987) was used in the sedimentation analysis. The over-
mens for any given parameter. all geotechnical index properties of the soil show that it can
be classified under the A-7-6 subgroup of the AASHTO Soil
TEST RESULTS AND ANALYSIS
Classification System (Standard 1986) and CL in the Unified
Identification of Soil Soil Classification System ("Soil" 1993). It is a reddish
brown, well graded soil with a relatively high plasticity of 20%
Table 1 summarizes the geotechnical index properties of the and clay content of not more than 12%.
natural soil. Fig. 1 shows the particle size distribution of the
100 Compaction Characteristics
The effects of lime content on the maximum dry density
80 (MDD) and OMC of lateritic soil for the two compactive ef-
forts are shown in Figs. 2 and 3. respectively. The MDD de-
70
creased with increase in lime content. The decrease in MDD
with increasing lime content conforms with the usual trend
and is in agreement with Ladd et al. (1960) as well as Marks
and Haliburton (1970). The decrease resulted from the floc-
culation and agglomeration of clay particles. caused by the
cation exchange reaction, leading to corresponding decreases
in dry densities (Lees et al. 1982).
The decrease in OMC for the soil-lime mixtures at the en-
10
ergy of the standard Proctor for low lime contents is in agree-
ment with Ladd et al. (1960) as well as Marks and Haliburton
0+-----;-----+----+------1 (1970). When lime dissociates in the presence of water into
0.001 0.01 0.1
Particle size, mm
10 calcium and hydroxyl ions. either of two situations arises. The
calcium ions either replace cations of other elements present
FI,G. 1. Particle Size Distribution of Natural 5011 at the exchange sites in the soil. or the calcium ions are ab-
1.11
sorbed by the soil if there are other unattached anions. apart
from hydroxyl ions. on the soil surface. The decrease in OMC

I
was due to a cation exchange reaction. which caused floccu-
'")1.88
I--~'~
west
-+- Afrtc8n . . .
lation of clay particles. It has been reported (Millard 1993)
that when lime is added to soil the calcium ions replace the
C sodium ions in the clay fraction until the latter becomes sat-
Q
~1.82
urated with calcium and the pH rises to more than 12. The
~
conversion from sodium to calcium ions produced a marked
i reduction in the apparent plasticity of the soil. But the poz-
Q
~1.7s zolanic reaction of lime with clay fraction of the soil is re-
Q ported (Ola 1978) to cause an increase of OMC noticed at
5
E
higher lime contents. At the energy level of the West African
1 1 74
.
Standard. the OMC increased with increasing lime content in
conformity with reported cases.

1.7 Compressive Strength


a 2 4 8 I
Lime Content, % Fig. 4 shows the effect of lime content on the unconfined
FIG. 2. Variation of MOD of Treated lateritic 5011 with Lime compressive strength (UCS) of lateritic soil specimens com-
Content pacted at the two energy levels considered and cured for 7.
JOURNAL OF TRANSPORTATION ENGINEERING / SEPTEMBER/OCTOBER 1998/467

J. Transp. Eng. 1998.124:465-469.


~ 3.50E-QS

~2500 T
..-< 1 P - Standard Proctor ., 3.00E·OS
~
~OOO j
I
WA - West Aflican Standard
"5
f; I ~2.5OE.OS

~ x~x ~

+6~.%===>.-:: i
r / -------- 7 days (P)

---.- 14 days (P) 2.00e-Q5

1!1000V;/~
500
--+-- 28 days (P) '0
--<>--- 7 days ryvA)
1i 1.5OE-Q5
'0

'tl 1./'/
- x - 14 days ryvA)
~ 1.00e-QS
Co)
CIl x
c ------- 28 days ryvA)
'E
8c 500 S.ooe-Qll
::::>
O.OOE+OO
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o j-.'~~~l'-I~~---jl~~~-+-~~- 0 2 4 e e
Lime Content, %
o 2 4 8 8
Lime Content, %
FIG. 5. Variation of Coefficient of Permeability of Uncured
FIG. 4. Variation of UCS of Treated lateritic Soli with Lime Treated lateritic Soli with Lime Content
Content
1.00E+02
P - Standard Proctor

14, and 28 days, respectively. The improvement in strength of WA - West Aflican Standard

lime-treated soil has been attributed to soil-lime reactions,


-------- 2% lime (P)
which result in the formation of cementitious compounds that x1.00E+01
- - - . - 4% lime (P)
bind soil aggregates (Locat et al. 1990; Narasimha Rao and
--+-- 8% lime (P)
Rajesekaran 1996). As expected, the compressive strength in-
creased with age for all the specimens tested. In general, the --<>--- 8% lime (P)

compressive strength increased with increasing lime content - x - 2% lime ryvA)


but decreased for 8% lime-treated specimens cured for 28 days - - 4% lime ryvA)
(standard Proctor) as well as those cured for 14 and 28 days - - 8% lime ryvA)
(West African Standard).
- x - 8% lime ryvA)
The compressive strength for all specimens compacted at
the energy of the standard Proctor varied from 395 to 1,110
kN/m 2, 530 to 1,420 kN/m2, and 600 to 1,525 kN/m2 at the
7-, 14-, and 28-day ages, respectively. Specimens compacted
5 10 15 20 25 30
at the energy of the West African Standard had compressive Curing Period, Days
strengths that varied from 590 to 1,350 kN/m2, 790 to 1,680
kN/m2 , and 900 to 1,940 kN/m2 at the 7-, 14-, and 28-day FIG. 6. Variation of Coefficient of Permeability of Treated lat-
eritic Soli with Curing Period
ages, respectively.
not be unconnected with the closer packing of the soil-lime
Permeability mixture due to the higher compactive effort.
For all the cured specimens prepared at the various lime
Figs. 5 and 6 show the variation of the coefficient of per- contents and the two energy levels considered, the coefficients
meability with lime content for specimens prepared at the of permeability increased with curing age up to 14 days and
MDD and corresponding OMC of the two energy levels con- decreased up to the 28 days considered in the study. Generally,
sidered for the uncured and cured conditions, respectively. For cementation is supposed to increase with increase in lime con-
the uncured specimens compacted at the energy of the standard tent, leading to a decrease in permeability. However, the in-
Proctor, the coefficient of permeability increased to a maxi- crease in permeability for all the treated specimens up to 14
mum at 4% lime content and decreased with further increase days' curing age could be attributed to the complexity of the
in lime content. The increase in the coefficient of permeability lime-soil reaction mechanism, which in general is very depen-
is due to flocculation caused by cation exchange reaction, dent on the amount and type of clay mineral present in the
while the decrease recorded is due to the increase in the pH soil. As lime content increases, the quantity of free silt and
value of the molding water as a result of the partial dissocia- clay particles progressively reduces as coarser particles are
tion of the calcium hydroxide. The calcium ions in turn com- formed. Consequently, larger voids are formed, which allow
bined with the reactive silica or alumina, or both, which were greater flow of fluid.
present in the soil, to form insoluble calcium silicates or alu- The decrease in permeability after 14 days' curing period
minates or both, which obstructed flow through the soil voids. for all the lime-treated specimens is in agreement with the
Furthermore the decrease in coefficient of permeability is hypothesis that when lime hydrates with age it reac~ with ~e
probably due to the excess amount of lime available for long- silica or alumina in the soil, and the gel grows With cunng
term pozzolanic reactions. In effect, 4% lime content can be age, filling the voids. The decrease in the coefficient of per-
said to be the lime-fixation point or lime retention point, in meability could be due to the precipitation of calcium carbon-
agreement with Nandy and Handy (1977). Lime treatment of ate in the voids as the ionized calcium reacted with the dis-
soils in excess of this point is reported to result in lime being solved carbon dioxide in the water.
available for long-term pozzolanic or cementing reactions for
ultimate strength of treated subgrade soils. The coefficient of CONCLUSIONS
permeability values recorded for specimens prepared at the
energy level of the West African Standard showed a decrease The test results recorded from the investigation carried out
with increase in lime content (see Fig. 5). The decrease might on the residual lateritic soil classified as A-7-6 or CL soil in
468/ JOURNAL OF TRANSPORTATION ENGINEERING / SEPTEMBER/OCTOBER 1998

J. Transp. Eng. 1998.124:465-469.


accordance with the AASHTO (Standard 1986) and Unified fraction on some mechanical properties of lime-soil mixtures." J. Inst.
Soil Classification Systems ("Soil" 1993), respectively, Hwy. Engrg., 29(11), 2-9.
"Lime stabilization." (1990). State-of-the-Art-Rep. 5, Transportation Re-
showed that specimens treated with a maximum 8% lime and search Board, National Research Council, Washington, D.C.
compacted at the energy levels of the standard Proctor and Locat, Y., Berube, M. A., and Choquette, M. (1990). "Laboratory inves-
West African Standard yielded seven-day USC values of 1,100 tigations on the lime stabilization of sensitive clays; shear strength
and 1,350 kN/m 2 , respectively. These values are greater than development." Can. Geotech. J., Ottawa, Canada, 27, 294-304.
the conventional 1,034.25 kN/m2 criterion for adequate lime Marks, B. D., and Haliburton, T. A. (1970). "Effects of sodium chloride
and sodium chloride-lime admixtures on cohesive Oklahoma soils."
stabilization. Presented at 49th Annual Meeting, Highway Research Board, Wash-
The coefficient of permeability of uncured specimens com- ington, D.C.
pacted at the energy level of the standard Proctor peaked at Melfi, A. J. (1985). "Characterization and identification of tropical lat-
4% lime content with a value of 3.38 X 10-' cm/s and de- eritic and saprolitic soils for geotechnical purposes." ISSMFE Progress
creased with further increase in lime content. For the speci- Rep. (1982/85), Committee on Tropical Soils, Transportation Research
mens prepared at the energy level of the West African Stan- Laboratory, International Society of Soil Mechanics and Foundations
Engineering, 9-20.
dard, the coefficient of permeability decreased from a value of "Methods of testing soils for civil engineering purposes." (1990). BS
3.38 X 10- 6 cm/s at no lime content to 2.15 X 10- 6 cm/s at /377, British Standards Institute, London, U.K.
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8% lime content. Millard, R. S. (1993). "Cement and lime stabilization." Road building
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Sons, Inc., New York, N.Y.
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energy levels of the standard Proctor and West African Stan- lime construction." Civ. Engrg., ASCE, 60-66.
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respectively. Recorded permeability values increased from formed in lime-stabilized marine clays." J. Geotech. Engrg., ASCE,
3.38 X 10-' and 2.29 X 10- 6 cm/s for uncured specimens to 122(5), 329-336.
Nuik, T. R., and Singh, S. S. (1997). "Permeability of flowable slurry
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