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Composite Structures 184 (2018) 935–949

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Composite Structures
journal homepage: www.elsevier.com/locate/compstruct

Mechanical characterization of innovative 3D multi-cell thermoset MARK


composites produced with weft-knitted spacer fabrics

Sanaz Hassanzadeh , Hossein Hasani, Mohammad Zarrebini
Department of Textile Engineering, Isfahan University of Technology, Isfahan 84156-83111, Iran

A R T I C L E I N F O A B S T R A C T

Keywords: Innovative three-dimensional integrated weft-knitted spacer (3D-IWKS) fabrics due to their unique features and
E-glass 3D composites flexibility in design, have recently gained significant popularity. These newly-designed fabrics could meet the
Weft-knitted spacer fabric requirements of numerous technical applications such as composite manufacturing. This work aims to in-
Thermoset resin impregnation vestigate bending and compression resistance of 3D-IWKS composites with different cross-section geometries.
Mechanical analysis
Using 400Tex E-glass yarns, two types of 3D-IWKS fabric samples as U-shaped single-decker structure (USSD) and
Composite failure theories
V-shaped single-decker structure (VSSD) were knitted on a modern flat knitting machine. The fabric preforms
were then molded via vacuum infusion process (VIP) using epoxy resin in order to produce composite panels in
the form of multi-cell thin-walled configurations. As far as bending strength and stiffness was concerned, VSSD
composites were found to be superior to USSD type. The influence of connecting layers’ orientation against the
applied loads was also evaluated via flatwise compression test. The results pointed to higher strength of USSD
samples with vertical inter-connecting layers in comparison to VSSD samples with angularly inter-connecting
layers. By comparing the edge-wisely compressed specimens, it was found that both types of samples are similar
in load-bearing capacity. The findings totally confirm the high mechanical applicability of these new structures.

1. Introduction lamination effects [3]. In this regard, substituting 2D laminates with 3D


complex-shaped textile-preforms is believed to be highly beneficial for
Growing challenge regarding the use of textile-reinforced compo- improving the mechanical performance of final composite parts. These
sites in technical applications has vastly drawn the attention of nu- textile reinforcements based on their final application, can be produced
merous engineers to the recent development in designing so-called via weaving, knitting, braiding, nonwoven and stitch-bonding tech-
novel low-weighted textile structures with high mechanical perfor- nologies [4–11]. Sandwich structures, as one of the well-known 3D
mances. Thus, research developments in this filed have been shifted textile preforms, generally comprise of two skin layers separated by a
from 2D structures manufacturing to designing 3D complex shapes with honeycomb core [3,10]. Numerous technical advantages such as low
the aim of meeting the requirements of end-uses where multifunctional areal density, low bulk density, comfort, thermo-physiological proper-
properties are paramount [1]. This approach changing is mainly due to ties, improved tensile strength, elastic compressibility and high energy
some limitations of 2D textile-reinforced composites in term of their absorbency, render these novel textiles as the best alternative for those
low design diversity which eventually leads to their functional prop- structures which mainly suffer from core-skin de-lamination effects
erties. As widely accepted, most of 2D laminates generally have inferior [3,4,10,12].
thickness-through mechanical properties in terms of compress-resist- Generally-configured 3D spacer fabrics comprise two separate sur-
ibility, inter-laminar shear strength and fracture toughness. Moreover, face layers which are connected by pile yarns or the fabric layers
due to low drapeability of 2D fibrous multi-plied prepregs, successful [12,13]. It is claimed that 3D spacer structures with fabric-type inter-
forming of composite engineering parts with complex geometrical connections not only exhibit higher mechanical performances but also
shapes could not be possible [1,2]. provide high possibility in designing complex shapes both geome-
It is approved that the commonly used laminating methods of trically and dimensionally. Production of spacer fabrics with pile in-
composite manufacturing such as co-curing, adhesive bonding or me- terconnections via waving and knitting technologies have been widely
chanical fastening yield to create local stress concentration in 2D multi- investigated by numerous researchers but designing of 3D integrated
layered structures which would be followed by the inevitable layers’ de- spacer structures with fabric interconnections is mostly considered


Corresponding author.
E-mail address: s.hassanzadeh@tx.itu.ac.ir (S. Hassanzadeh).

http://dx.doi.org/10.1016/j.compstruct.2017.10.048
Received 4 September 2016; Received in revised form 29 September 2017; Accepted 13 October 2017
Available online 16 October 2017
0263-8223/ © 2017 Elsevier Ltd. All rights reserved.
S. Hassanzadeh et al. Composite Structures 184 (2018) 935–949

Fig. 1. Diversity in geometrical shapes of 3D integrated multi-cell spacer fabrics [19].

Table 1
Material specifications.

Fiber type Density (g/ Mechanical properties


cm3)
Tensile strength Young’s modulus
(MPa) (GPa)

Single Glass 2.50 1831.7 78.6


yarn (SD = 1.14) (SD = 0.05)
Epoxy 1.17 56 6.1

*
A multi-folded yarn comprised of 4 single plies of 100 text glass yarn.

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Fig. 2. Cross-sectional views of the produced 3D-IWKS fabric reinforcements.

Table 2 provided by modern knitting machines have been considered as main


Characteristics of 3D-IWKS Fabrics. advantages in constructing novel 3D composites [14,15]. In addition to
composites manufacturing industries, these knitted fabrics have gained
Sample code Areal density Upper surface Lower surface Fabric
(g/m2) layer layer thickness other technical applications in areas such as automotive, aerospace
(mm) engineering, geotextiles, and environmental protection [16,17].
CPC WPC CPC WPC The inherent low in-plane strength and stiffness as well as low fiber
fraction of the knitted fabrics are considered as the major issues faced
USSD 1788.52 3.33 2.22 3.46 2.25 8
(SD = 82.66) (SD = 0.75)
by most of composite designers. However, the possibility of using high
VSSD 1883.22 3.45 2.17 3.57 2.13 10 performance fibers in fabricating process together with providing ani-
(SD = 92.38) (SD = 1.32) sotropic properties in the final products, have made the knitted per-
forms to gain technical merits in composite manufacturing [3,8]. Re-
USSD: 3D fabric with U-shaped single-decker structure (Fig. 2a).
gardless of yarn type, knitted structures due to their high extensibility
VSSD: 3D fabric with V-shaped single-decker structure (Fig. 2b).
and drapability could be easily formed into numerous complex 3D
shapes [3,14].
through weaving operation; this is while the knitting technology,
Regardless of knitting process type, the produced conventional
especially the weft-knitting methodology, has high potential in forming
spacer patterns are thickness-thoroughly limited to distance between
3D integrated spacers with various geometrical shapes, but is not much
the two needle beds of knitting machine [8,14,18,19]. Increase in these
considered [3–5].
fabrics’ thicknesses, can be easily provided by replacing the connecting
As reported in previous literatures, the loop-like geometry of knitted
pile yarns with the fabric layer. This is the basic rule for constructing
preforms would hinder their uses in composite manufacturing, while
different 3D textile preforms with geometrical diversity which is
the recent developments have considered this feature as a turning point
claimed to be easily achieved via weft knitting process [8,20,21].
regarding 3D configured textile-base composites. This is mainly at-
Technical advancements in weft-knitting machineries as well as emer-
tributed to the recent technological advances in knitting machineries
sion of some new applicable features (e.g. individual needle selection),
which provide high flexibility in designing knitted structures. As a re-
are the main reason behind the successful use of weft-knitting tech-
sult, numerous researchers have been attracted to study the product-
nology in producing innovative 3D multi-cell spacer preforms
ability of newly-designed spacer fabrics named multi-cell thin-walled
[14,19–24]. Geometrical diversity and improved mechanical perfor-
fibrous preforms [12,13]. In spite of inherent dimensional instability
mance, are considered as the main advantages of these innovative
and low mechanical properties of plain knitted fabrics, it is well-noted
textiles [14,19,25,26]. Desired geometry of the final composite as is
that design versatilities together with ease of fabric formability

Fig. 3. Basic components of VIP method used in composite manufacturing.

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Fig. 4. Manufacturing process of 3D-IWKS reinforced composite panels.

Table 3 constructing the simple U-shaped form of 3D-IWKS preforms used as the
Properties of the used epoxy resin. reinforcements of 3D thermoplastic composite panels. They also in-
vestigated tensile strength and stiffness of the final products through
Property Standard test method Value
evaluating the mechanical behavior of plain weft-knitted composite
Viscosity at 25 °C (cps.) ISO 12058-1 8000 layers as the whole structural representative volume element (RVE)
Density at 25 °C (g/cm3) ISO 1675 1.17 [23,24].
Flexural strength (MPa) ASTM D5023-15 70–80 Compared to thermoplastic composites with several advantages, the
Compressive Strength (MPa) ASTM D695-15 72–75
Tensile strength (MPa) ASTM D638-14 50–60
thermoset materials also have their own merits in technical applications
Pot life at 23 °C for 250 g (min) TECAM at 65% RH 150 specially where higher compression and bending strengths are required
Demold time (hrs) — 24 [43] However, a quick reviewing on published works points to a gen-
eral lack of interest among researchers to study the mechanical beha-
vior of the thermoset reinforced composites together with infancy of
shown in Fig. 1, can be either achieved by changing the position of mechanically evaluated reports regarding the 3D-IWKS reinforced
connecting points between the surface layers or by varying the length of composites. Recently, Hamedi et al. [25] studied the bending resistance
knitted constitutive layers [15,26]. of a simple geometrically configured 3D spacer weft-knitted composites
Despite the merits of these 3D integrated weft-knitted spacer (3D- from polyester yarns. Also, they investigated the mechanical sample
IWKS) fabrics for being used as composite reinforcements, the amount behavior under bending using finite element method. Using funda-
of researches conducted on evaluating their mechanical performance is mentals of manufacturing 3D-IWKS reinforced composites, Omrani
rather limited. Some researchers have mostly been involved with fab- et al. [26] did their efforts to produce tubular-shaped configuration of
rication of 3D-IWKS in woven or knitted structures without considering these structures in order to investigate their behavior under external
their mechanical performance [27–33]. Those researches focused on static and internal hydrostatic pressures. They also simulated the
mechanical evaluating of 3D spacer composites are mostly limited to samples behavior using finite element method. For providing a com-
the conventional spacer fabrics (two skin layers with pile-yarn con- plete report regarding the mechanical performance of 3D-IWKS com-
nection) or the sandwich structures (honeycombs surrounded by two posites, this work aim to investigate differences between the mechan-
skin layers). [34–42]. Abounaim et al. [11] were the pioneers in ical performance of the samples varied in their cross-sectional

Fig. 5. 3D-IWKS Composite panels and their specifications.

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Fig. 6. Three-point bending test apparatus and the specimens’ dimensions.

geometries, in terms of their resistance against compression and the used glass yarns in accordance with ASTM D2256 were determined
bending loads. Using E-glass yarn, spacer preforms varied in their cross as given in Table 1. Fig. 2 illustrates the schematic representations and
sections are going to be fabricated and then molded into composite photographs of the produced 3D-IWKS performs after 24-h wet/dry
parts to be mechanically investigated. relaxation. Moreover, specifications of the fabric samples such as loop
density and layers thicknesses are provided in Table 2. The mean CPC
and WPC of the skin layers for both samples were found to be 3.43Loop/
2. Materials and methods
cm and 2.19Loop/cm, respectively.
In order to improve fabric quality prior to commencement of knit-
2.1. Preparation of textile preforms
ting, optimized adjustments such as machine speed and loop length
were carried out as described in [15,44,45]. Because of the glass fibers
Using four-ply twisted of 100Tex E-glass yarns, 3D-IWKS textile
brittleness, the machine carriage speed was limited in range of 0.3m/
preforms with two different cross-sectional profiles were knitted on
s–0.35m/s in order to prevent unwilling yarn breakage during knitting.
Stoll CMS-400, computerized flat knitting machine. Characteristics of

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Fig. 7. Flatwise compression test apparatus and the specimens’ dimensions.

Additionally, the fabric take-down mechanism was adjusted so that no saturation of the glass fibers with resin, yarns were de-sized before resin
excessive pressure could be exerted on the needles and also no breakage impregnation [46].
of yarns could be occurred during loop formation.
Followed by results from Abounaim et al. [8], the product-ability of 2.2. Composite panels reinforced with 3D-IWKS preforms
3D-IWKS fabrics could be achieved only if the proper sequence of
needles from both rear and front beds are being participated in knitting Among various molding techniques of composite manufacturing,
operation. Length of the loops which are particularly transferred to the VIP method due to its individual configuration is mainly suitable for
needles of the opposite bed according to the pre-designed knitting manufacturing composite parts in any geometrical shapes. More detail
pattern, is another critical factor affecting the quality of the final about the VIP method equipment is depicted in Fig. 3.
knitted sample; comparatively longer loops at the position of layers As shown in Fig. 4, composite samples were reinforced with the
connecting point, would guarantees such impeccable loop transferring. USSD and VSSD textile preforms via a 4-step molding process. Before
The preforms underwent dry/wet relaxation, according to ASTM D578 the textile preforms being impregnated with epoxy resin by applying
prior to composite manufacturing process. In order to assure full vacuum with the help of pump of 1-bar negative pressure capability, the

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Fig. 8. Edgewise compression test apparatus and the specimens’ dimensions.

structural free cells must be occupied with especially shaped wooden Based on several reports, Values of Wf for most composites reinforced
inserts in order to remain unchanged after molding. Some of the resin with glass textiles are usually determined via Resin Burning-off method,
specifications are given in Table 3. In this research, the epoxy thermoset through which the applied heat causes the resin component to be
resin EP411 and the hardener H15 with viscosity of 150 mPa.s were completely melted away but the fibers remain unaffected. Following
obtained from DCM Company. Prior to injection, these two components this method, the composite samples were initially heated in an oven at
were mixed in 100pbw:10pbw ratio. Once the infusion was completed, temperature of 250 °C for 10 min; upon burning off the resin compo-
the vacuum pump was stopped and the molded samples were condi- nent, the samples fiber volume fraction was measured. From the test,
tioned at (20 ± 3 °C and 60 ± 5% RH) for 48 h. maximum volume fraction of the samples was approximately de-
In order to enhance mechanical performance of the molded com- termined at 20% which is fairly compatible with the results of Leong
posites, they were post-cured for 3 h in an oven at 80 °C [44,45]. Fig. 5 et.al. [46].
shows the produced composite samples with some of their specifica-
tions. 2.3. Mechanical experiments
It must be considered that maintaining 3D geometries of the per-
forms during molding is solely conditional up on the use of the auxiliary Bending and compression resistances of the two innovative ther-
rod inserts which are shaped according the required geometry of the moset composites groups called as USSD and VSSD, were evaluated.
final composite product [15]. Insertion of these filling inserts into the The composite specimens dimensionally prepared according to the
free spaces of the prepared multi-cellular fabrics is additionally ad- ASTM standards were subjected to bending and compression loads
vantageous in terms of applying a uniform predefined tension to the using a universal tensile tester of 25 KN loading capacity (Tinius Olsen
loops which in turn would affects the mechanical properties of the final H25KS) equipped with axial actuators. The movable head of the testing
composite product [44,45]. Prior to insertion, the rod inserts were in- machine was adjusted so that the specimens could be subjected to the
itially tape-wrapped and then covered with Mirror glaze M0811 wax as normal bending forces at a constant rate of 2mm/min, while for the
a common releasing-agent in order to ease their withdrawing from the compression test (flatwise and edgewise), the rate of cross-head
performs after completion of composite manufacturing process. movement is suggested to be at 0.5mm/min [47–49].
Fibers volume fraction Vf is paramount factor affecting mechanical
performance of the composite materials which is calculated using Eq. 2.3.1. Three-point bending
(1): The standard flexural test method defined for sandwiched materials,
ASTM C 393, was used to investigate mechanical performance of 3D-
Wf / ρf
Vf = IWKS glass/epoxy composites samples under bending loads. From this
Wf / ρf + (1−Wf )/ ρm (1) test, not only the bending stiffness of the whole structure is determined,
but also the core shear strength and modulus together with the com-
where, Wf is fiber weight fraction; ρf and ρm are the fiber and matrix pressive and tensile strength of the skin layers (facings) could be
densities, respectively. Because of the yarns loop-liked configuration measured.
structure of the produced 3D-IWKS preforms, it is expected that the According to the standard, there is no matter if the specimens for
fiber volume fracture of final composite panels to be relatively small. bending tests are prepared as either short beam or long beam; but is

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Fig. 9. Force-displacement behavior of the USSD and VSSD composite under bending loading.

must be noted that the latter is generally preferred if the facings’ moduli compression test as schematically depicted in Fig. 7. Using these
are known. Regardless of the length, composite beam-like specimens parameters, the mechanical performance of the whole structure in term
could be subjected to two different way of loading: single-point loading of the inter-connecting layers failure modes could be investigated. As
with two-point support (i.e. three-point bending) and two-point loading proposed by ASTM C 395 standard test method, the free edges of the
with two-point support (i.e. four-point bending). For testing the struc- samples were resin-infused so that forming a thin layer in between
tures with thin facings and low density cores, applying the concentrated would prevent them to be locally crushed during the test. It is an im-
loads using a wider load rubber-covered pad as simulated as four-point portant point that the test specimens should be in either square or
bending condition, is preferred. This, is due to the fact that such loading circular cross-sectional shape and not have area more than 10.000 mm2
system yields to better load distribution [47]. However, because of [48].
some operational limitations in this research, long samples were tested Same as the bending test, the specimens for flat-wise compression
using three-point loading system. In this regard, for preparing the test test were standardly conditioned (23 ± 3 °C temperature and
specimens is must be taken into account that its span length divided by 50 ± 5% relative humidity).
the total thickness is better to be greater than 20 (L/d > 20), until the
simple beam theory could be valid during the mechanical analysis.
Schematic views of three-point loadings used for evaluating bending 2.3.3. Edgewise compression
behavior of the USSD and VSSD samples are shown in Fig. 6. In ac- Load carrying capacity of 3D-IWKS composite columns in terms of
cordance with ASTM C 393, the width of the test samples is neither less developed facing stresses could be determined through edgewise com-
than twice the total thickness nor greater than half of the span length pression loadings. Core/face column-configured structures regardless of
[47]. Additionally, the samples were conditioned at 23 ± 3 °C tem- their height, are usually subjected to a buckling mode of failure except
perature and 50 ± 5% relative humidity before conducting the test in when facings are considered to be thick [49]. As illustrated in Fig. 8, the
order to eliminate the effect of content moisture. samples were prepared according to ASTM C 364 standard prior to be
subjected to edgewise compression loading.
Similarly, the free edges of the test specimens must be reinforced
2.3.2. Flatwise compression with thin layers of resin in order to prevent unwilling localized end
Compressive strength and modulus of the core elements in 3D-IWKS failure. Additionally, taking care to ensure smooth end surfaces free of
composites could be easily determined via conducting flatwise burrs, is really essential. Without the ends’ lateral supports, the

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Fig. 10. Deformed composite samples in both experimental and test-simulated conditions; (a) USSD type and (b) VSSD type.

specimens would be either confronted by early facings’ failure or might During bending, the composites’ top facings experience compressive
be deviated between the tester cross-heads [49]. tension while the bottoms are subjected to the tensile stresses. ASTM C
393 standard vividly stated that tensile failure is occurred only if either
3. Results and discussions the tensile-experienced facings are thin or they are weaker than the
compression facings [47]. Fig. 9 reveals that failure in the samples is
In the case of 3D-IWKS composites designed in this research, it was mainly due to compression bottom facings followed by large unduly
expected to have lower fiber volume fractions as compared with their deflection and wrinkling of the top facings.
corresponding woven-based composites; this is well attributed to the Using Eqs. (2) and (3), the values of core shear stress τ and facings
inherent character of knitted structures and the curved form of con- bending stress σ could be determined for the composite samples which
stitutive yarns. The void contents of USSD and VSSD composite samples were subjected to the three-point bending test (single-point midspan
were experimentally resulted as 2.92% and 0.72%, respectively. Low load).
values of the samples void percentages confirms the suitability of VIP
P
method used in this work for infusing the resin during 3D-IWKS com- τ=
(d + c ) b (2)
posites molding.
PL
3.1. Bending strength and stiffness σ=
2t (d + c ) b (3)

Fig. 9, shows the force-extension behavior and deformed appear- where P is the applied load (N), d is the sandwich thickness (mm), c is
ances of the both composite groups during the bending test. During the core thickness (mm), b is the specimen width (mm), t is the facing
initial loading stage, it is seen that the force-displacement curve of both thickness (mm), and L is the span length (mm).Considering the fact that
USSD and VSSD composites is linear as far as the point at which the top the core, facings and total thickness of both USSD and VSSD samples are
facing-layer is suddenly crushed. This is mainly attributed to the rela- identical, it is claimed that the resulted difference between their me-
tively thin layers and the created moments at the structural weak point chanical performances could be only attributed to their geometrical
due to the samples lengthening which ultimately exceeds the allowable variations. Differences in their cross-sectional geometry, make the
core shear stress [47]. These results are obviously shown through the midspan-loaded USSD and VSSD beam samples to have different de-
deformed views of samples given in Fig. 9. flections (Δ ) which is derived from Eq. (4) [47].

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Fig. 11. Load distribution on the samples during bending; (a) USSD and (b) VSSD.

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Fig. 12. Force-displacement curves of the composite samples under flatwise compression loading.

PL3 PL (2) USSD samples are more flexible and have higher energy absorption
Δ= +
48D 4U (4) capacity.
where Δ is midspan deflection (mm), D is bending stiffness (N.mm2)
and U is shear rigidity (N) of the test sample. For the sandwich struc- It must be also noted that there would be no matter if the position of
tures with the same facings type, D and U can be determined using applied bending load is either on the facing or on the connecting point;
following equations 5 and 6: three-replicated experimental trials confirmed the irrelevancy of the
point where the load is applied.
E (d3−c 3) b
D=
12 (5) 3.2. Flatwise compression behavior of the samples
G (d + c )2b
U= Mechanical behaviors of 3D composite panels reinforced with USSD
4c (6)
and VSSD textile preforms were also investigated under flatwise com-
where E is the facings modulus (MPa) under bending and G is the core pression loading; this is because flatwise compressive strength and
shear modulus (MPa). Since the core shear modulus is the only differ- modulus are the fundamental mechanical properties for designing
entiating factor in the case of the test samples, the panel shear rigidity is multi-cell core/skin structures. From the force-displacement curves
considered as a pivotal factor affecting the amount of samples deflec- given in Fig. 12, the compressive stress and effective modulus of the
tion under loading. From Fig. 10, the simulated and experimentally core could be computed [48] by employing the Eqs. (7) and (8) as
observed behavior of USSD and VSSD samples could be easily com- following:
pared.
The initial slope of the force-displacement curve represents the P
σ=
stiffness behavior of the test sample. Comparing the curves given in A (7)
Fig. 9, it can be concluded that the USSD samples totally have lower St
bending stiffness while the VSSDs resists more against the applied E=
A (8)
bending load; in other word, the VSSD samples are stiffer than the 2
USSDs which is mainly attributed to way of load distributing. More where P is the ultimate force (N), A is the cross-sectional area (mm ), S
details of load distributionduring the bending test, are provided in the is the slope of initial linear portion of force-displacement curve (N/mm)
Fig. 11. It is observed that the applied single-point midspan bending on and t is the core thickness (mm). Fig. 12 shows that the ultimate force
the VSSD panel is mainly sustained by the core bonding points in which sustained by the USSD samples is approximately twice than that of the
high stress concentration is caused. Additional displacement of the VSSD sample. Moreover, the load-subjected cross-sectional area of the
loading cross-head during the test, leads to the failure of skin layers VSSD samples is larger than that of the USSDs which in turn leads to
which is followed by the facings dimpling into the core. In the case of lower compressive strength for the former. Additionally, compressive
USSD samples, the applied load is uniformly distributed on the total modulus was found to be higher for USSD samples.
surface of the top skin layer which in turn leads to its wrinkling. Further As illustrated in Fig. 13, in flatwise compression test same as
displacement of the testing cross-head, causes the weak points on the bending, the VSSD samples are subjected to a concentrated stress at the
top skin layer to be dimpled into the core. Overall, the following main midspan point while the USSDs are affected by uniformly distributed
outcomes can be derived from Figs. 9 and 10: stresses. From the figure, it is obvious that the value of early-occurred
maximum tension in the USSD samples is approximately triple than that
(1) VSSD samples have the higher bending stiffness and strength. in VSSDs; this, confirms the higher operational strength of the USSD
samples in technical applications than the VSSD samples.

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Fig. 13. Simulated mechanical behavior of 3D multi-cell composites under flatwise compression loading.

Load-bearing capacity of the test 3D spacer composites which were Comparing the values measured as work of rupture, reveals that the
flat-wisely compression loaded, generally deals with mechanical be- USSD samples are highly resistance when subjected to compression
havior of the structural cores. In this regard, the higher compressive loads. On the other hand, by considering the post loading recovery, it
stiffness of the core which plays as the role of connecting element can be stated both the composites enjoy high mechanical performance
would increase strength of the whole structure. It is claimed that ver- as far as low residual thickness reduction is concerned.
tically aligned connecting layers cause the composite structure to show
higher compressive stiffness in comparison to composites with oblique 3.3. Edgewise compression behavior
connections [3]; this, confirms the superior strength of the USSD over
VSSD samples. Load carrying capacity of USSD and VSSD samples in terms of de-
Considering the results of Figs. 12 and 13, buckling deformation of veloped facing stresses and the structural yielding point, can be de-
the USSD samples is stated to be a result of the core layer failure in form duced from their behavior when subjected to edgewise compression
of wrinkling into the structural free cells after applying the compression loading [49]. In the case of core/skin composites columns regardless of
load. However, the connecting layers of the VSSD samples are mainly their height, it is claimed that the structural failure is usually due to
buckled due to the applied shear stresses. buckling deformation unless if the facing layers are significantly thick.

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Fig. 14. Force-displacement curves of the samples under edgewise compression loading.

As expected, the 3D spacer composites designed in this research have reinforcements, has attracted the attention of researchers and engineers
been subjected to the buckling failure during edgewise compression test involved in composite manufacturing. These textile-based composites
since the facings’ thicknesses were about 2 mm. Detailed illustration of are exceptionally advantageous as far as weight to volume ratio and
the samples deformation is shown in Fig. 14. According to the ASTM C high ability in designing especially where complex geometries are
364, the weaker facing layers is wrinkly deformed following which the concerned. Among different available method of textile production, it is
core is subjected to a wavy-shaped deformation; further displacement widely accepted that knitting technology could offer vast range of fi-
of the tester cross-head leads to the sever facings dimpling which brous constructions with rather complex geometries; but the looped
eventually results in the whole structural bending, especially near the configuration of the yarns in these textiles essentially inhibits their use
ends. This type of deformation is mainly due to the core shear failure or as reinforcing elements in composite materials. New design of 3D
the facing-to-core bonds fracture [49]. knitted spacer preforms has been recently admired by 3D composite
Typical force-displacement curves of USSD and VSSD composites manufacturers since they are not associated with disastrous de-lami-
given in Fig. 14 represents that both of the samples exhibit similar nation phenomenon during technical applications. In this study, me-
mechanical performance under edgewise compression. This is due to chanical performances of 3D thermoset composites reinforced by these
the fact that the facing layers of both samples are either materially or innovative 3D integrated multi-cell weft-knitted spacer fabrics (3D-
structurally identical; however, their corresponding mode of failure IWKS) from E-glass fibers, were investigated in terms of bending and
must be accurately investigated. Form the Fig. 14, it is observed that the compression resistance. Because of their geometrical complexity, the
USSD samples fail due to the facings wrinkling as well as ultimate produced 3D textile preforms were molded via VIP molding by which
buckling of the whole structure, while the failure of the VSSD samples is the most suitable resin infusion could be provided.
mainly due to the facing layers dimpling together with subsequent It was concluded that VSSD samples exhibit higher stiffness and
corrugation of the cellular units and structural fracture near the sample modulus in comparison to USSD sample during three-point bending test
ends. which is mainly attributed to differences between the distribution mode
Value of compression stress σ distributed throughout the samples’ of the applied bending loads in both samples. It was also observed that
facing layers could be derived again from Eq. (7). total resistance of the samples depends on the strength of both con-
Pictorial representation of the force-displacement curves reveals necting and skin layers. Investigating the samples fracture mode, re-
similarities between the mechanical behavior of both USSD and VSSD vealed that USSD samples have relatively low core shear strength which
samples during edgewise compression. This confirms that the com- leads to buckling of the inter-connecting layers; this is while the VSSD
pressive strength of the facing layers directly affect the mechanical samples fracture is associated with lower strength of the compression
behavior of composite part which is edge-wisely compressed. top facing layers and not the core shear strength.
In order to verify the accuracy of the experimental results from In the case of flatwise compression test, the applied loads in mainly
edgewise compression testing, a simple simulation was also carried out sustained by the interconnecting layers of the composite samples. Thus,
as depicted in Fig. 15. In this figure, stress distribution throughout the the layer orientation relative to the load direction as well as their
samples as well as their deformed appearance are simply observed. It is stiffness and modulus, significantly affect the mechanical performance
concluded that failure modes and shapes of deformed configurations, of the final composite material. It was observed that both VSSD and
are the main differences between the two composite samples which USSD samples were subjected to the buckling mode of failure when the
were edge-wisely compressed in this study. normal compressive load was applied. Comparing the slope of the force-
displacement curves of both samples approved the higher compressive
4. Conclusions modulus of USSD samples than the other group. Additionally, it was
found that the USSD samples exhibit load bearing capacity three times
Rapid advances in the field of 3D textile products used as composite more than the VSSD samples when subjected to flatwise compression.

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S. Hassanzadeh et al. Composite Structures 184 (2018) 935–949

Fig. 15. Simulated mechanical behavior of 3D multi-cell composites under edgewise compression loading.

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