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B.F. Dyson
B.F. Dyson
Résumé.- Les méthodes modernes ayant pour but l’amélioration du dimensionnement des pièces travaillant à
haute température, nécessitent la prévision du comportement des materiaux dans des conditions proches de
celles en service. Ce besoin a palarisé l’attention des ingénieurs sur le compréhension des phénomènes
d’accumulation de dommage dans les alliages. La microstructure des métaux peut se dégrader par plusieurs
mécanismes qui dépendent; (i) de la température; (ii) souvent de l’état de constrainte; et (iii) parfois de la
composition chimque de l’environnement. Dans ce papier, quelques récents développements dans la
modèlisation des processus d’endommagement sont rappelés. En particulier, l’emploi d’une seule variable d’état
est évalué et on souligne le bénéfice potentiel d’utiliser deux variables d’état. Un système deux-barres a été
utilisé pour quantifier certaines caractéristiques du fluage associées à la cavitation aux joints de grains, et a
permis de démontrer le bon accord entre la théorie et les expériences. Un modèle pour l’endommagement de
fluage associé à l’évolution des sous-structures de dislocations dans un super-alliage base-nickel a ensuite été
développé et verifié expérimentalement.
Abstract.- Modern methodologies that aim to reduce conservatism in the design of components operating at
high temperatures rely on accurate predictions of materials’ behaviour in conditions relevant to those
experienced in service. This requirement has focussed the attention of materials engineers on developing a
quantitative understanding of damage-accumulation in engineering alloys. The microstructure of metallic
materials can degrade by several mechanisms at rates that depend; (i) on temperature; (ii) often on stress level
or state; and (iii) sometimes on the chemistry of the surrounding fluid environment. In this paper, some
recent developments in the modelling of damage processes have been reviewed; in particular, the single state
variable approach has been assessed and the potential benefits of using two state variables outlined. Also, a
two-bar mechanical analogue has been used to quantify certain features of creep deformation associated with
grain boundary cavitation and the close agreement between theory and experiment is demonstrated. A model
for the creep damage associated with the evolution of the dislocation substructure in nickel-base superalloys has
been developed further and experimental support for an unusual feature of the model has been demonstrated.
periods of tertiary creep is due to the intrinsic instability of macroscopically uniform, which is the usual or (ii)
more
the dislocation substructure to deformation. The physical concentrated in a region contiguous with the external
basis of the model summarised in Table 1 is given in section environment: this being prima facie evidence that the
4: for present purposes, it suffices to know that the cavities are a consequence of attack by a chemical
parameter C characterises the importance of this mechanism. component(s) of the environment. In both cases, cavities are
Attempts have been made to model creep rate when an distnbuted non uniformly on the scale of the grain size;
initial second-phase microstructure is gradually replaced by a being on those grain boundaries predominantly perpendicular
more stable one - for example, one set of particles by to the applied maximum principal tensile stress. The gradual
another (9, 13) - so giving rise to sigmoidal curves when accumulation of cavities contributes directly to fracture, but
lifetime is plotted against stress: this case is not included in also causes an increase in the rate of creep. The minimum
Table 1.
acceleration is when growth is "unconstrained" (10) - the
holes simply increase the applied stress in proportion to thcir
Damage due to loss of internal section. area fraction: while the maximum acceleration occurs when
It is now well established that intergranular fractures are
growth is "constrained" and the effective area fraction of
caused by the nucleation and growth of holes (cavities) on holes can then become equal to the area fraction occupied by
grain boundaries. Two types of cavity distribution can be transverse boundaries in a uniaxially loaded system. A more
identified and are illustrated in Fig 1. These are (i) detailed account of this concept is given in Section 3.
Thirdly, the damage parameter for environmental attack, For loss of internal section by environmental attack, the
2x/R, is an approximation; thus loss of internal or external equivalent equations are (11,15):
section can be calculated only when w 1 and so values
of Cm, 6f and X at w f = 1 are not included in Table 1.
For loss of external section by environmental attack, Cm and
6f are given, for w 1 by (11):
with stresses
creep rates.
which decays to a stationary state value after time T, Eq. 28,
given by: the failure strain was >6%, whereas the other three
exhibited failure strains of approximately 2%. The transition
between constrained and unconstrained growth of cavities is
characterised by a marked increase in strain to failure: Fig.
8 demonstrates this for a CrMoV steel, heat treated to
During this transient period, the recoverable strain simulate the heat affected zone in a weldment. The
accumulated is given by: transition locus between constrained and unconstrained cavity
growth can be calculated in an approximate manner (23) but
requires more material property data than are available with
this particular data-set.
612
03C3e is the effective stress responsible for climb, viz: In deriving Eq’s 39 - 41, 03B4 was assumed constant: with
03C92 = 0, Eq’s 39 and 40 combine to given the linear strain
softening model (16).
613
The results are plotted in Fig. 9 but, for clarity, only three
values of 03C3/03C3o are presented. For present purposes, the
important point to note is the sigmoidal shape of the creep
curve at uluo = 5: the degree of sigmoidal behaviour
increases with decreasing values of 03C3/03C3o and is simply a
consequence of the decreasing dislocation velocity with
increasing strain. Such behaviour has never been reported
for nickel-base superalloys but Fig. 10 shows some data taken
from NPL files of the creep of Nimonic 80A in torsion: the
data were published in another form by Dyson and McLean
(25). Signs of sigmoidal behaviour can be seen in the 100
MPa test and an unusual linear behaviour can be seen at
large strains in the 150 MPa test: at higher stresses, the
normal continuously increasing strain rate with strain was
10: always observed. Although by no means conclusive, the
Fig Creep strain in torsion as a function of èmt;
results in Fig. 10 add confidence to the view that tertiary
demonstrating the onset of sigmoidal creep at the
lower stress. creep in thèse alloys is a consequence of the mechanism
outlined in this section.
Sigmoidal shapes of creep curve are well known in the
li’terature and a theory along the lines presented here has
If it is assumed that ô =
kp, where k is a constant, then been published for glide-controlled creep by Alexander and
Eq 40 is replaced by: The unusual features of nickel-base superalloys
Haasen (26).
are that creep is climb controlled and that the point of
inflection in the creep curve is at least an order of
magnitude greater than reported for other materials.
When ¿’2 = 0, Eq’s 39 and 42 combine to give the 5. Acknowledgements
exponential strain softening used in a previous publication
(16) and in Table 1. The author expresses his gratitude to Dr Ana Barbosa for
Eq’s 39 - 41 have been integrated numerically to yield the computer program to solve Eq’s 39 - 41 and to
writing
creep strain as a function of the dimensionless parameter Ë it Dr T B Gibbons for constructive comments on the
for various values of normalised stress 03C3/03C3o, using the manuscript.
6. Références
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and D.R. Hayhurst (1978) Creep of 17.
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B.F. Dyson and M. McLean (1983) Acta. Metall,
(1968) Physics
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