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Article history: In this investigation, comparative study of tensile and impact properties of multi-pass SMAW Armox
Received 29 October 2017 500T steel joints fabricated by austenitic stainless steel (ASS) and low hydrogen ferritic steel (LHF)
Received in revised form consumables vis-a-vis base metal was carried out. The tensile tests were conducted on computer
11 January 2018
controlled Walter þ Bai Ag UTM at a nominal strain rate of 103 s1. Subsequently, charpy impact tests
Accepted 18 January 2018
Available online 31 January 2018
were carried out on an instrumented Zwick-Roell test setup to obtain load vs. displacement and
maximum energy absorbed vs. displacement of the specimen. It was observed that, the joint efficiency of
weldment processed by LHF consumable was 41.7% and weldment processed by ASS was 30.6% of its base
Keywords:
Armox500T
metal indicating the influence of electrode consumable on tensile properties of the joints. On the con-
Multi-pass SMA welding trary, impact toughness of weldment processed by ASS was 20% more and weldment processed by LHF
ASS and LHF welding consumables was 12% less than that of base metal. Microstructural studies also revealed that, ASS can be considered as
Mechanical properties a candidate welding consumable for good strain hardening and toughness of the welding joint in impact
Microstructural characterization applications. However, LHF steel consumable is recommended for welding joints that requires higher
joint efficiency under tensile loading conditions.
© 2018 Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://
creativecommons.org/licenses/by-nc-nd/4.0/).
https://doi.org/10.1016/j.dt.2018.01.005
2214-9147/© 2018 Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
A. Saxena et al. / Defence Technology 14 (2018) 188e195 189
offered a higher resistance to hydrogen induced cracking. Datta impact test samples is as shown in Fig. 1 (e). Weldments produced
et al. [10,11] presented the weldability properties of ASTM A 537 C l. by low hydrogen ferrite (LHF) and austenitic stainless steel (ASS)
1 pressure-vessel quality steel and 20 mm thick O SA 517 Gr. F steel consumable electrodes are referred to as weldment-1 and
plates using single pass and multi-pass SMAW process respectively weldment-2 respectively. In order to ensure the repeatability and
with AWS A5.5 E11018 M (LHF) consumables. Results from previous consistency, three samples were tested for tension and impact as
investigations reveal that, single pass welded joint was found to described in the following sections.
possess adequate strength, impact toughness and meet the MSTS
requirements for ASTM A 537 C l. 1 steel and the impact toughness 2.2. Tension test
of the parent material was superior to that of multi-pass weld zone
and heat affected zone (HAZ) at all test temperatures. Reddy et al. The tensile test samples as described under section 2.1 were
[12,13] revealed in their investigation that, SMAW joint efficiency of pulled to fracture at a nominal strain rate of 103 s1 on a computer
ASS filler metal deposits was found to be around 72% of its coun- controlled Walter þ Bai Ag UTM. The load-extension data was
terpart high-strength low-alloy steel base metal. In addition, the converted to engineering stress-strain andtrue stress-true plastic
weld deposits exhibited good toughness and better ballistic per- strain (s-ε) data.
formance. Lakshminarayanan et al. [14] studied the effect of SMAW,
GMAW and GTAW processes on tensile and impact properties of 2.3. Charpy impact test
AISI 409 M grade steel using duplex stainless steel consumables.
They have observed that, GTAW ferritic stainless steel joints have The Charpy impact test was performed on an instrumented
superior tensile and impact properties compared to SMAW and Zwick-Roell test setup. The experimental setup consists of anvils on
GMAW joints. Bott and Teixeira [15] investigated the influence of which the standard notched specimen (Fig. 1 (e)) prepared as per
multiple post weld heat treatment (PWHT) on mechanical prop- ASTM, E23 [16] is freely supported and a pendulum with a mass of
erties of quenched and tempered BS7191 Grade 450EM steel 30kg attached to a rotating arm pinned at the machine body. The
(0.10 wt%C-1.08 wt%Mn) and its ferritic multipass SMA weldments span length between the anvils was kept at 40mm.The released
prepared by AWS E-9018 M type electrode. Results revealed that, pendulum hammer follows a circular trajectory and hits the test
the base metal was affected by PWHTs and presented a brittle mode specimen at the middle span at a striking velocity of 5.23 m/s thus
of fracture and this tendency tends to increase with increasing transferring kinetic energy to it. Energy losses due to bearing fric-
numbers of cycles. Further, the weld metal Charpy V-notch tion and air resistance have been ignored while calculating the
toughness showed lesser reduction than the base metal after energy absorbed by the specimen. The impact test data was ob-
extended PWHT. tained in terms of load vs. displacement as well as the maximum
From the above discussions, it is clear that, welding consum- energy absorbed vs. displacement of the specimen.
ables and welding processes have considerable effect on the per-
formance of quenched and tempered steel joints that are specially 2.4. Microstructural characterization
used in military applications. Further, the data on tensile and
impact properties of multi-pass SMAW Armox 500T joints fabri- The standard metallographic technique was used to prepare the
cated by ASS and LHF welding consumables is seldom available in sample for microstructural characterization of test samples. Solu-
the literature. In order to fill up this knowledge gap albeit partially tion made of 1 gm picric acid, 5ml HCl and 100ml ethanol was used
and in view of importance of this data in the design of structures, for etching of base metal for 15s and weldments for 25s. Optical
the present investigation is oriented towards understanding the microstructures were taken from semi-automatic microscope
effect of these consumables on transverse tensile and impact (Make: Leica Microsystems) and back scattered SEM images (20kV
properties of multi-pass SMAW Armox 500T steel joints in com- electron high tension) have been taken from Gemini SEM Sigma
parison with its base metal. Further, microstructural characteriza- (Make: Zeiss).
tion and fractographic analysis of test materials is also carried out
and feasibility of using LHF over ASS welding consumables for 3. Results and discussion
joining of Armox 500T structures is suggested.
3.1. Microstructural observations
2. Experimental details
The back scattered SEM image and optical micrograph of the
2.1. Welding of Armox500T plates e sample preparation base metal, weldment-1 and weldment-2 are shown in Fig. 2(aeb),
Fig. 3(aeb) and Fig. 4(aeb) respectively. The chemical composition
As received Armox500T steel was water quenched from 1273 K (wt. %) determined by EDX method is given in Table 2. The detailed
and tempered in the range of temperatures 473e773 K. Prior to microstructural observations from SEM and optical microscope are
quenching and tempering the steel was hot rolled at 1523 K. Test given in the following sections.
plates measuring 150 200 25 mm were carefully machined and
butt-welded by shielded metal arc welding (SMAW) with five 3.1.1. Armox500T steel (base metal)
welding passes using two different electrodes i.e. austenitic stain- Back scattered SEM image of Armox500T steel (Fig. 2 (a)) in-
less steel (ASS) consumable and low hydrogen ferrite (LHF)as dicates tempered martensite lath in acicular form with coarse and
shown in Fig. 1 (a). The welding process parameter details are given fine precipitate along with some grain boundaries. On the other
in Table 1. Tensile test and charpy impact test samples were wire cut hand, the optical micrograph of Armox500T (Fig. 2 (b)) shows the
from Armox500T steel plate in rolling direction (hereafter referred presence of columnar laths and blocks of laths. Pandey et al. [17]
to as base metal) and fusion zone of two weldments in the and Li et al. [18] have highlighted that, mechanical properties are
configuration shown in Fig. 1(b). The smooth (un-notched) tensile structure sensitive and they vary with the amount and distribution
specimens as shown in Fig. 1(c) were prepared to evaluate yield of phases like retained austenite with martensite. Therefore, in the
strength, UTS and ductility of joints. Notched tensile specimens as present work, micrographs with higher magnification were used
shown in Fig. 1 (d) were prepared to evaluate notch tensile strength for closer identification of precipitation. Amount of retained
and notch strength ratio of the joints. The geometry of charpy austenite will reduce the tendency of cracking. Further, the retained
190 A. Saxena et al. / Defence Technology 14 (2018) 188e195
Fig. 1. (a) Schematic of SMAW Joint, (b) Test Samples wire cut from Fusion zone, (c) Tensile test sample, (d) Notched tensile test sample, (e) Charpy impact test sample (All di-
mensions are in mm).
Table 1
SMAW welding process parameters.
Weldment-1: Low hydrogen ferrite (LHF) consumable electrode -AWS A5.1 E7018
No. of passes Filler material diameter/mm Current/A Voltage/V Welding speed/(mm$min1) Heat input/(kJ$mm1)
Weldment-2: Austenitic stainless steel (ASS) consumable electrode -AWS A5.4 E308-16
austenite may get transformed to bainite or martensite, which was oriented laths is undesirable in welding because it offers little
clearly observed in micrographs of parent materials. Further, opti- resistance to crack propagation [22e25]. Presence of low carbon
cal micrograph is showing white etching wedge-shaped widman- martensite clearly distorted by presence of C content i.e. the axial
statten ferrite plates in a matrix quenched to martensite. These ratio of its unit cell is almost unity. Under this condition, the system
plates are coarse (notice the scale) and etch clearly because they tries to reduce its energy to the maximum level and hence the
contain very little substructure. It is evident through strain hard- phase separation occurs at the interfaces having similar atomic
ening and uniformity in strain distribution as seen in Fig. 5. spacing. Since, these phases cannot migrate to the grain bound-
aries; they get separated inside the grains. In addition, the acicular
3.1.2. Weldment-1 (processed using LHF consumable electrode) ferrite microstructure (Fig. 3 (a)) also consists of small particles of
Back scattered SEM image and optical micrograph of weldment- intergranular nucleated ferrite without any particular orientation.
1 (Fig. 3 (aeb)) indicatessound and clear welding jointwith no voids Thus, the resulting small effective grain size and lack of orientation
and micro-cracks. Nucleation and growth tendencies are influenced makes acicular ferrite a desirable weld microstructure with excel-
by chilling action of the parent metal and gives variable grain size lent mechanical properties compared to weldment-2 as described
(dendritic size) within the weld. The microstructure of weldment-1 in the following section.
is mainly acicular ferrite associated with second phase containing
widmanstallen and bainite phase without martensite [10,19e21]. 3.1.3. Weldment-2 (processed using ASS consumable electrode)
This type of microstructure containing large colony size and Back scattered SEM image and optical micrograph of weldment-
A. Saxena et al. / Defence Technology 14 (2018) 188e195 191
Fig. 2. Armox500T base metal (a) Back scattered SEM, (b) Optical micrograph.
Table 2
Chemical composition (wt. %) of test samples under investigation.
Material C Si Mn P S Cr Ni Mo N B Fe
Base metal 0.31 0.265 0.86 0.019 0.007 0.60 0.82 0.24 e 0.005 Balance
Weldment-1 0.06 0.58 0.85 0.017 0.012 0.04 0.03 0.015 0.018 e Balance
Weldment-2 0.05 0.51 1.18 0.018 0.06 18.03 9.45 0.04 e Balance
192 A. Saxena et al. / Defence Technology 14 (2018) 188e195
Fig. 5. (a) Engineering stress-strain and (b) True stress- True Plastic strain.
2 (Fig. 4 (aeb)) mainly composed of martensite and partially d- transverse tensile properties of the joints compared to ASS
ferrite phase. In general, coarse grained or mixed grain size struc- consumable.
ture obtained by fast heating and cooling in the weld region causes The microstructure of fusion zone of weldment-1 (Fig. 3 (a)) is
the properties of the weld region to be completely different from mainly acicular ferrite associated with second phase containing
the properties of the parent metal.In addition, residual stresses are widmanstallen and bainite phase without martensite [10,19e21].
developed in the weld region due to high hardness martensite Small interweaving ferrite plates formed within austenite grains
formation resulting from rapid cooling of the weld zone. The grain transforms during the cooling of low alloy steel weld deposits re-
size changes from coarse to fine with decrease in temperature. sults in a good combination of strength and toughness. Therefore,
Therefore, it is recommended to do annealing for stress-relieving this is considered to be desirable structure in low carbon steels in
and recrystallization to increase the life of weld region view of its commercial importance [28]. Weldment-1 with acicular
[11,22,26,27]. The amount of delta-ferrite was estimated using Cr ferrite in which each lath is divided by high boundary angle dis-
and Ni equivalents [26] of weld metal chemical composition. Cr and playing fine grain size (typically 1e3 mm) [29] usually possesses
Ni equivalents are found to be 22 and 10.5 respectively and based high tensile strength compared to weldment-2 as given in Table 3.
on the Schaeffler diagram, about 20 (vol. %) ferrite was expected to The microstructure of fusion zone of weldment-2 (Fig. 3 (b)) shows
exist in the austenitic matrix. skeletal d-ferrite in a plain austenitic matrix. Presence of high Ni
(9.45%)in weldment-2 balances the austenitic structure against the
3.2. Effect of welding consumables on tensile and impact properties formation of martensite [30].
The load-displacement curves obtained from the instrumented
Tensile tests were carried out for base metal and weldments as charpy impact test are not smooth because of serrated oscillations
described under section 2.2. The load vs. elongation data was present in the data points. Therefore, data points were smoothened
converted to engineering stress-strain and subsequently true stress by method of moving averages [31]. Load vs. displacement andE-
vs. true plastic strain (s-ε) data as shown in Fig. 5 (a) and (b). The nergy vs. displacement curves are plotted as shown in Fig. 6 (a) &
strain hardening index, n was estimated using a relation s ¼ Kεn, (b) respectively. Results indicated that, in case of weldment-2, the
where K is strength coefficient, s and ε are the flow stress and true crack initiation at notch occurred before general yielding and in
plastic strain respectively. The tensile properties such as yield case of base metal and weldment-1, the same occurred at the peak
strength, ultimate tensile strength, n, K, % elongation, notch tensile load without general yielding. It is known that, Ni content in-
strength, notch strength ratio and joint efficiency of base metal and fluences the formation of austenitic phase (high impact toughness)
weldments are presented in Table 3. The UTS or in other words joint and reduction of the ferrite content (increased brittleness) in the
efficiency of weldment-1 and weldment-2 was observed to be 41.7 fusion zone compared toweldment-1 possessing very small content
and 30.6% of its base metal respectively indicating the influence of of Ni (0.03%). It is evident from Table 3 that, impact toughness of
electrode consumable used in SMAW welding process on tensile weldment-2 (9.45% Ni) is 20% more than its counterpart base metal
properties of the test materials. During tensile test, all the speci- (0.82% Ni); on the other hand, impact toughness of weldments-1
mens (joints) were found to fracture in the weld region only. Thus, (0.03% Ni) is 12% less than that of base metal.
it may be assumed that, the UTS data presented in Table 3 are
primarily the ultimate tensile strength of the welded joint. From 3.3. Fractrography
the comparison of results, it is noted that, the use of LHF steel
consumable for welding of test materials has enhanced the SEM Fractrography images of Armox 500T base metal,
Table 3
Tensile and Impact properties of test samples under investigation.
Material Yield strength/MPa UTS/MPa K/MPa n Elongation Notch tensile strength/MPa Notch strength ratio Joint efficiency Internal energy/J
/% /%
Fig. 6. (a) Load vs. Displacement and (b) Energy vs. Displacement.
weldment-1 and weldment-2 are shown in Fig. 7(aeb), Fig. 8(aeb) distributed dimples was observed in case of weldments-2.
and Fig. 9(aeb) respectively. Fractrographic analysis of base metal
indicates that, the zone under the notch and the sphere along the 4. Feasibility of LHF over ASS consumables for joining of
edges of the test specimen, only ductile dimple fracture mostly of Armox 500T steels
shear character was present. This type of failure mechanism in the
base metal is considered as trans-crystalline ductile. On the other The weldment-2 produced by ASS consumable has a duplex
hand, fractrograph of weldment-1 shows mainly ductile fracture microstructure consisting of delta ferrite in a plain austenitic ma-
with bimodal morphology (combination of coarse and fine dim- trix (Fig. 4(aeb)) and weldment-1 fabricated by LHF consumable
ples) with pores and voids, whereas ductile fracture with uniformly produces an acicular ferrite structure (Fig. 3(aeb)). This acicular
194 A. Saxena et al. / Defence Technology 14 (2018) 188e195
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