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ALUMINIUM ALLOY
APRIL 2017
©Indian Institute of Technology Delhi (IITD), New Delhi, 2017
FRICTION STIR WELDING OF 5052
ALUMINIUM ALLOY
by
Submitted
to the
APRIL 2017
CERTIFICATE
This is to certify that the thesis entitled “Friction Stir Welding of 5052 Aluminium Alloy”
being submitted by Mr. Ratnesh Kumar Raj Singh to the Indian Institute of Technology Delhi
is worthy of consideration for the award of the degree of Doctor of Philosophy and is a record
of the original bonafide research work carried out by him. Mr. Ratnesh Kumar Raj Singh has
worked under our supervision for the submission of this thesis, which to our knowledge has
reached the requisite standard. To the best of my knowledge, this work in part or full has not
been presented to any other university or institute for the award of any degree/diploma.
Professor Professor
Hauz Khas, New Delhi – 110016, India Hauz Khas, New Delhi – 110016, India
Date:
i
ACKNOWLEDGEMENTS
I am extremely grateful to the God for the blessings, which of course have been with me always,
and giving me the strength and dedication to complete my work to the best of my ability. I pay
Delhi) and Prof. Sunil Pandey (Department of Mechanical Engineering, IIT Delhi), whose mere
strength. I have been able to complete this work only by virtue of the knowledge that I received
The experiment based research work requires availability of adequate research infrastructure. I
am thankful to my supervisors, who are indeed, my mentors, Prof. Rajesh Prasad and Prof. Sunil
Pandey to help me to get access to all the necessary facilities in IIT Delhi. I am privileged to
work under the supervision of them and owe all thanks to them for supporting, advising and
guiding me from time to time during course of experimentation and throughout my research
studies.
My special thanks are also to Prof. Suhail Ahmad, Department of Applied Mechanics, IIT Delhi
for his constant help and support. Being the chairman of student research committee (SRC), he
always advised me with his valuable suggestions and expert opinions. I acknowledge the help
and support that I received from Prof. Puneet Mahajan, Department of Applied Mechanics, IIT
Delhi, during my research as the member of SRC. I also deeply thank Dr. P.M. Pandey,
Associate Professor, Department of Mechanical Engineering for being the member of my SRC
and for his advices and expert opinions related to my research. I am indebted to Dr. S.
iii
Aravindan, Associate Professor, Department of Mechanical Engineering, for their help, support
I am also thankful to my fellow scholars Dr. Dinesh Rathore, Mrs. Deepti Jaiswal, Mr. Dinesh
Shetti, Mr. Saurabh Shukla, Mr. Gaurav Singh, Mr. Anuj Jindal, Mrs. Shaksi Chauhan, Mrs.
Shanta Mohapatra, Prof. Arshad Noor Siddiquee, Prof. Hariom Choudhary, Dr. Zaheer Khan,
Mr. Abhishek Pandey, Mr. Aryajyoti Goswami, Mr. Mohd. Awol Habib and Mr. Siddharth
Tamang. The support extended by them during the critical stages of this research work is
gratefully acknowledged and I am also thankful for their interest and involvement in the
technical discussions.
The help provided by staff of the Mechanical Engineering and Applied Mechanics Division
Laboratories especially Mr. Ayodhya Prasad, Mr. Anil Kumar, Mr. Tulsiram, Mr. Ramchandar
and Mr. Bhavar Singh is appreciated. The help extended on personal fronts by Mr. Ayodhya
brother. I love them with all of my heart. I am thankful to my parents for the principles they
instilled in me as a young man and for their continued support, guidance, and love for our family.
It would have been impossible to complete this work without my family‟s understanding,
iv
ABSTRACT
Friction Stir Welding (FSW) is a solid state welding process which involves stirring the material
by a non consumable rotating tool to generate frictional heating that soften the base material and
produces the joint. FSW is commonly used for welding of aluminium alloys. Owing to solid state
nature, and reduced dependence on skills, FSW has numerous advantages over fusion welding
processes. Consequently, researchers have shown increasing interest in the application of FSW to
In the present research, friction stir welding of 5052-H32 aluminium alloy has been performed
using conventional robust vertical milling machine (VMM). This VMM has been modified to
work as a FSW machine and fitted with an indigenously developed setup which is capable of
firmly clamping the 6 mm thick 5052 aluminium plates and is also capable for measuring
downward and traverse welding forces. The different attachments have also been fitted with
VMM for measurement of temperature distribution and power consumption during welding. A
tool holder interface has also been developed which is able to effectively clamp the various size
of FSW tool. The hot die steel (H13) tool with a cylindrical threaded pin has been used for the
welding.
Numerous trial experiments have been performed to establish the principal FSW process
parameters. The tool pin and shoulder diameter, tool rotation and welding speed have been
selected as the FSW process parameters and experimentation have been performed in accordance
with the response surface methodology (RSM). Mechanical and metallurgical tests have been
performed for each welded specimen. The weld quality has been analyzed though tensile, impact,
v
fatigue and fracture toughness tests along with microstructural examination. The effect of
individual process parameter on each weld properties has been analyzed in detail.
It has also been found that the external cooling also affects the quality of welds produced by
FSW. To see the effect of external cooling three cooling media such as natural air, water and
liquid nitrogen have been used for welding and welds have been examined based on mechanical
and metallurgical properties. The water has been found a suitable cooling media for batter
mechanical properties.
To achieve best mechanical properties, it is necessary to optimize the process parameters based
on suitable cooling media. So the FSW process parameters have been optimized again for the
best suited cooling media. In this experiment FSW process parameter has been studied through a
separate set of experiments using Taguchi‟s L9 orthogonal array. The effect of process parameter
in cooling media on weld quality characteristics such as strength, elongation, impact strength,
Analysis of results has revealed significant effect of all these FSW parameters and cooling media
on mechanical and metallurgical properties of the weld. The FSW process parameters have also
significantly affected the welding force generated, power consumed and temperature distributed
during welding. The metallurgical test results have revealed occurrence of considerable grain
vi
साय
घषषण घूणन
ष वेल्डिंग (एपएसडब्रू) एक ठोस अवस्था वाऱी वेल्डिंग प्रक्रिमा है लिसभें गैय-उऩबोज्म घूणन
ष
उऩकयण द्वाया घुरनशीर ताऩ उत्ऩन्न कयने के लरए साभग्री को तेिी से घुमाया जाता है , िो आधाय
साभग्री को नयभ कयते हैं औय सिंमुक्त जोड़ फनाता हैं। एपएसडब्रू आभतौय ऩय ए्मूभीननमभ लभश्र
धातओ
ु िं के वेल्डिंग के लरए उऩमोग क्रकमा िाता है । ठोस अवस्था की प्रकृनत औय कौशर ऩय ननबषयता भें
कभी के कायण एपएसडब््मू के फ्मूिन वेल्डिंग प्रक्रिमाओिं से ज्यादा पामदे हैं। नतीितन, शोधकताषओिं
ने फेहतय मािंत्रिक गण
ु ों को प्राप्त कयने के लरए ए्मभ
ू ीननमभ लभश्र धातु को जोड़ने के लऱए एपएसडब््मू
से भिफूत ऊर्धवाषधय लभलरिंग भशीन (वीएभएभ) का उऩमोग क्रकमा गमा है । इस वीएभएभ को एपएसडब्रू
भशीन के रूऩ भें काभ कयने के लरए सिंशोचधत क्रकमा गमा है औय श्वतः ववकलसत सेटअऩ के साथ रगामा
गमा है िो 6 लभभी भोटी 5052 ए्मूभीननमभ प्रेटों को भिफूती से जोड़ने भें सऺभ है औय वे नीिे की
तयप ऱगने वाऱी वेल्डिंग फरों को भाऩने में बी सऺभ है । वेल्डिंग के दौयान ताऩभान ववतयण औय त्रफिरी
की खऩत के भाऩ के लरए ववलबन्न उऩकरण बी वीएभएभ के साथ रगाए गए है । उऩकयण धायक
अंतरपऱक बी ववकलसत क्रकमा गमा है िो क्रक प्रबावी रूऩ से ववलबन्न आकाय के धातु के चादरों को दफाने
भें सऺभ है । वेल्डिंग के लरए गभष भयने वारे स्टीर ( एि 13) से फनी एक फेरनाकाय ऩेचदार वऩन का
प्रमुख एपएसडब््मू प्रक्रिमा भाऩदिं डों को स्थावऩत कयने के लरए कई प्रमोग ऩयीऺण क्रकए गए। उऩकयण
वऩन औय किंधे का व्मास, उऩकयण योटे शन औय वेल्डिंग की गनत का िमन एपएसडब््मू प्रक्रिमा भाऩदिं डों
के रूऩ भें क्रकमा गमा है औय प्रमोग की प्रनतक्रिमा सतह ऩद्धनत (आयएसएभ) के अनुसाय क्रकमा गमा है ।
प्रत्मेक वे्डेड नभूने के लरए यांत्रिक औय धातुववक गुणों के टे स्ट जैसे की तन्मता, प्रबाव, पटीग औय
फ्रैक्िय ऩयीऺणों के साथ-साथ सूक्ष्म-संरचनात्मक ऩयीऺा के साथ वे्ड गुणवत्ता का ववश्रेषण क्रकमा गमा
है । प्रत्मेक वे्ड गुणों ऩय अरग-अरग प्रक्रिमा माऩदं डों के प्रबाव का ववश्रेषण क्रकमा गमा है ।
कयती है । फाहयी शीतरन के प्रबाव को दे खने के लरए प्राकृनतक वामु, िर औय तयर नाइट्रोिन िैसे
शीतरन माध्यमों का इस्तेभार वेल्डिंग के लरए क्रकमा गमा है औय मािंत्रिक औय धातु सिंफिंधी गण
ु ों के
आधाय ऩय वेल्ड की िािंि की गई है । अच्छे यांत्रिक गुणों की वजह से िर को एक उऩमुक्त माध्यम ऩामा
गमा है ।
सवषश्रेष्ठ मािंत्रिक गुण प्राप्त कयने के लरए, उऩमुक्त फाहयी शीतरन ऩय आधारयत प्रक्रिमा भाऩदिं डों को
अनुकूलरत कयना आवश्मक है । इसलरए एपएसडब््मू प्रक्रिमा भाऩदिं डों का अनुकूरतभ शीतरन माध्यम
के लरए क्रपय से अनुकूलरत क्रकमा गमा है । इस प्रमोग भें एपएसडब््मू प्रक्रिमा माऩदं डों का इस्तेभार
तागुची एर 9 ऑथोगोनर सयणी के प्रमोग के एक अरग सेट के भार्धमभ से क्रकमा गमा है । शीतरन
ऩरयणाभों के ववश्रेषण ने इन सबी एपएसडब््मू भाऩदिं डों औय शीतरन माध्यमों के वे्ड के यांत्रिक औय
धातुववक गुणों ऩय भहत्वऩूणष प्रबाव ददखामा है । एपएसडब््मू प्रक्रिमा भाऩदिं डों ने वेल्डिंग के दौयान
उत्ऩन्न वेल्डिंग फर, त्रफिरी का सेवन औय ताऩभान को बी प्रबाववत क्रकमा है । धातुववक गुणों के ऩररछण
के नतीिे ने गनतशीर ऩुनयष िना तिंि के िरते अलस्थय ऺेि भें कापी ग्रेन शोधन की घटना का ऩता िरा है ।
TABLE OF CONTENTS
Certificate i
Acknowledgements iii
Abstract v
Chapter 1 Introduction 1
1.1 Background 3
1.5 References 7
2.1 Introduction 11
vii
2.4 Wrought Aluminium Alloy 15
2.10 References 30
3.1 Introduction 37
3.2 Equipment 39
viii
3.2.2 Work Fixture 39
3.5 Experimentation 44
ix
3.6.8 Selection of orthogonal array 53
3.7 Experimentation 54
3.9.6 Microstructure 68
3.9.7 Fractography 69
x
3.10 References 70
4.1 Introduction 75
xi
4.4.3.2 Effect of shoulder diameter on Charpy impact 100
strength
xii
4.4.6.3 Effect of rotational speed 119
xiii
6.2 Experimental Procedure 148
xiv
6.3.4.1 FCGR Behaviour Along the WNZ 164
xv
welding
xvi
propagets in WNZ
xvii
regions
xviii
8.7 References 275
xix
9.5.2 Microstructure development around the tool pin: 296
study based on broken tool
xx
9.6.2.5 Effect of cooling media 313
Appendices
xxi
LIST OF FIGURES
Fig. 3.3 Force measuring attachment (a) Top view of force measuring attachment, 42
(b) Side view of attachment, (c) Bottom Plate with load cell which is
attached to milling machine and (d) load cell with data acquisition and
storage system
Fig. 3.4 Tool Holder (a) Schematic diagram of tool holder (b) 3 D view of Tool 43
Holder (c) Tool holder with attached tool
Fig. 3.7 Friction Stir welding in (a) Air, (b) Underwater and (c) Under Liquid 57
Nitrogen
xxiii
Fig. 3.10 Dimension (in mm) of subsize tensile samples 61
Fig. 3.13 Stress-Strain diagram for base metal in Parallel and perpendicular to 62
rolling
Fig. 3.15 Fatigue Specimen (a) Dimensions of Fatigue samples, (b)- Sample for 64
FCGR across weld Nugget, (c)- Sample for FCGR along the weld nugget
Fig. 3.16 The FCGR measurement (a) FCGR measurement in base metal by both 65
electronic and COD gauge, (b) FCGR measurement in weld by COD
gauge, (c) FCGR measurement across the weld nugget by COD gauge
Fig. 3.18 Fracture toughness samples (a) Schematic diagram of fracture sample, (b) 67
fracture toughness samples in the centre of weld nugget (c) fracture
toughness sample in HAZ of AS (d) Fracture toughness sample in HAZ of
RS
Fig. 3.19 Fracture toughness testing (a)- Fracture toughness testing machine and (b)- 67
3-point bend fracture toughness testing
Fig. 3.21 Microhardness indentations across the weld nugget and from top to bottom 68
in weld nugget
Fig. 4.1 Engineering Stress-Strain curve for tensile tested samples 79-80
xxiv
Fig. 4.3 Normal Probability vs Studentized Residual plot for UTS 82
Fig. 4.5 Variation of UTS with respect to (a) pin diameter (b) shoulder Diameter (c) 84-85
rotational speed (d) welding speed
Fig. 4.8 Variation of % Elongation with respect to (a) pin Diameter (b) Shoulder 91-92
Diameter (c) Rotational Speed and (d) Welding speed
Fig. 4.10 Normal Probability vs Studentized Residual plot for Charpy Impact 96
Strength
Fig. 4.12 Variation of % Charpy impact strength with respect to (a) pin Diameter (b) 97-98
Shoulder Diameter (c) rotational speed (d) welding speed
Fig. 4.13 Normal Probability vs Studentized Residual plot for FCGR 103
Fig. 4.16 Normal Probability vs Studentized Residual plot CTOD in WNZ 111
Fig. 4.18 Variation of Fracture Toughness in WNZ with respect to (a) pin Diameter 112-113
(b) Shoulder Diameter (c) rotational speed (d) welding speed
xxv
Fig. 4.19 Normal Probability vs Studentized Residual plot for CTOD in HAZ 116
Fig. 4.21 Variation of Fracture Toughness in HAZ with respect to (a) pin Diameter 117-118
(b) Shoulder Diameter (c) rotational speed (d) welding speed
Fig.5.1 Engineering Stress-Strain diagram of welds at (a) Low welding Speed and 130
(b) High welding speed
Fig. 5.2 Charpy impact strength of different welds and their average values (in red 131
mark)
Fig. 5.3 FCGR at different welding condition in the weld nugget 133
Fig. 5.4 Slopes of FCGR curves at different welding condition in the weld nugget 134
Fig. 5.7 Slope of FCGR at different welding condition across the weld nugget 137
Fig. 5.8 FCGR at different welding condition across the weld nugget 137
Fig. 5.9 Fracture toughness properties in weld produced in different cooling media 139
Fig. 6.2 UTS of welds and base along with their average values 151
Fig.6.3 YS of welds and base along with their average values 151
Fig. 6.4 % Elongation of welds and base along with their average values 151
xxvi
Fig. 6.5 Effect of process parameters on UTS 153
Fig. 6.9 FCGR in WNZ of underwater welded samples with 7 mm Pin Diameter 165
Fig. 6.10 FCGR in WNZ of underwater welded samples with 8 mm Pin Diameter 166
Fig. 6.11 FCGR in WNZ of underwater welded samples with 9 mm Pin Diameter 167
Fig. 6.12 Slope of FCGR curve used for calculation of da/dN 168
Fig. 6.13 FCGR variation in WNZ with welding process parameters 171
Fig. 6.14 FCGR in AS and RS HAZ samples with 7 mm Pin Diameter 172
Fig. 6.15 FCGR in AS and RS HAZ samples with 8 mm Pin Diameter 173
Fig. 6.16 FCGR in AS and RS HAZ samples with 9 mm Pin Diameter 174
Fig. 6.17 Slope of FCGR curve in AS and RS used for calculation of da/dN 176
Fig. 6.20 CTOD in weld nugget (Red mark showing average values) 179
Fig. 6.23 Effect of Process Parameter on Fracture Toughness Properties in AS HAZ 186
xxvii
Fig. 6.24 Effect of process parameter on Fracture Toughness Properties in RS HAZ 188
Fig. 7.1 Material flow and top surface roughness correlated by (a) Dark and bright 199
bands in WNZ (taken by Optical Microscope) and (b) shoulder mark on
top surface (taken by SEM)
Fig. 7.2 Weld mid section along the welding direction 201
Fig. 7.3 Showing material flow at (a) location „e‟ and (b) location „f‟ 201
Fig. 7.4 Dark and Bright bands (a) Different in particle size (taken by optical 202
microscope) (b) Different in grain size (taken by SEM)
Fig. 7.5 Optical microstructure of fractured tool pin in transverse direction of weld 202
Fig. 7.6 Optical microstructure taken in (a) Advancing and (b) Retreating side of 203
fractured tool
Fig. 7.7 Optical macrostructure of welds produced at low welding speed in 205
different cooling media
Fig. 7.8 Optical macrostructure of welds produced at high welding speed in 206
different cooling media
Fig. 7.9 Optical macrostructure of weld cross section showing locations for width 208
measurement
Fig. 7.10 Weld width at different location (as shown in Fig. 7.9) 208
Fig. 7.12 Optical microstructure of base metal taken (a) along and (b) across the 209
rolling direction
Fig. 7.13 Optical microstructure of weld produced in different cooling media and 210
welding speed (a) Air@100, (b) Air@400, (c) UW@100, (d) UW@400,
(e) UN@100 and (f) UN@400
xxviii
Fig. 7.14 Optical microstructure of TMAZ in (a)- Advancing and (b)- Retreating 212
Side
Fig. 7.15 Optical microstructure of underwater weld produced at different set of 214-215
process parameters (a)-W71, (b)-W72, (c)- W73, (d)-W81, (e)- W82, (f)-
W83, (g)-W91, (h)-W92, (i)-W93
Fig. 7.16 SEM image of Lazy „S‟ defect found during welding at (a) low 217
magnification and (b) high magnification showing lack of bonding
Fig. 7.17 Nano-indentation results of Lazy „S‟ defect Weld produced at welding 217
parameter (a) Air@100 and (b) UW@100
Fig. 7.18 Hardness distribution across the weld produced in air 219-220
Fig. 7.19 Hardness profile across the weld at (a) low and (b) high welding speed 222
Fig. 7.20 Microhardness profile across the joint for welds of pin diameter (a) 7 mm, 224
(b) 8 mm and (c) 9 mm (the rectangles showed in figures represents the
area affected by tool pin and shoulder)
Fig. 7.21 SEM images of different fracture surfaces of tensile samples showing 229
common type of FSW defects
Fig. 7.22 SEM images of fractured surfaces of tensile samples of Natural Cooled 232
weld at (a) low and (b) high welding speed, Water cooled weld at (c) low
and (d) high welding speed, Nitrogen cooled weld at (e) low and (f) high
welding speed
Fig. 7.24 SEM images of fractured surface of tensile samples produced at different 236
set of process parameters
Fig. 7.26 SEM images of fracture surfaces of fatigue samples at the threshold ∆K 240
xxix
Fig. 7.27 Fracture surfaces of FCGR test samples (i) along weld and (ii) across weld 241
Fig. 7.28 SEM fracture surfaces of FCGR test samples (as shown in Fig. 17) at (a) 241
Low ∆K along the weld, (b) High ∆K along the weld, (c) Low ∆K in
across the weld, (d) High ∆K across weld
Fig. 7.29 SEM images of fractured surfaces of fracture toughness samples 244
Fig. 8.1 Downward forces occurred during welding in air at different process 253-254
parameter
Fig. 8.2 Distribution of forces during FSW in different cooling media at (a) low 256
welding speed (b) high welding speed
Fig. 8.7 Normal % probability vs Studentized residuals plot for power consumption 268
Fig. 8.9 Variation of Power consumption with (a) pin diameter, (b) shoulder 269-270
diameter, (c) rotational speed and (d) welding speed
Fig. 8.10 Power Consumption in different cooling media and welding Speed 272
Fig. 8.11 Power consumption in under water welding with varying process 273
parameter
Fig. 8.12 Effect of process parameter on power consumption in underwater welding 274
xxx
LIST OF TABLES
Table 2.1 Designation system for wrought and cast aluminium alloy 13
Table 2.4 Major alloying elements (Wt. %) of 5xxx Series Aluminium alloy 18
Table 3.4 Upper and lower limit of process parameters selected for welding 47
xxxi
Table 3.9 Welding parameters and their notation 58
Table 4.2 Welding run notation, their actual and coded values 77
Table 4.12 Result of ANOVA table for Fracture toughness in WNZ 109
Table 6.1 Process parameters with their range and levels 149
xxxii
Table 6.2 Welding parameters and weld notation 150
Table 6.5 Response table for signal to noise ratios (Larger is better) for UTS 152
Table 6.7 Response table for Signal to Noise Ratios (Larger is better) for % 156
Elongation
Table 6.10 Response table for Signal to Noise Ratios (Larger is better) for 161
Impact Strength
Table 6.12 FCGR test values for crack propagated in weld nugget 169
Table 6.13 Response table for S/N ratios (Smaller is better) for FCGR in WNZ 170
Table 6.16 Response table for S/N ratios (Smaller is better) for FCGR in AS 175
HAZ
xxxiii
Table 6.18 Response Table for S/N ratios (Smaller is better) for FCGR in RS 176
HAZ
Table 6.21 Response Table for S/N ratios (Larger is better) for CTOD in WNZ 180
Table 6.23 Response table for mean for CTOD in AS HAZ 183
Table 6.24 Response table for S/N ratios (Larger is better) for CTOD in AS 183
HAZ
Table 6.26 Response Table for Means for CTOD in RS HAZ 187
Table 6.27 Response table for S/N ratios (Larger is better) for CTOD in RS HAZ 187
Table 7.2 Surface features of underwater friction stir welded plates 198
Table 7.3 Weld cross-section area for weld produced in different cooling media 207
Table 7.4 Weld cross-section of underwater Friction Stir Welded samples 213
Table 7.5 Fracture location of weld of tensile samples of weld produced in air 228
Table 7.6 Fracture locations of tensile samples of welds produced in different 230
cooling media
xxxiv
Table 7.7 Fracture tensile samples of weld produced in underwater FSW 235-236
Table 7.8 Fracture samples of FCGR test in which crack propagates in WNZ 238
Table 7.9 Fracture samples of FCGR test in which crack propagates across the 239
WNZ
Table 7.10 Fracture Toughness surface of weld produced in different cooling 242
media and fail in Weld Nugget
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LIST OF SYMBOLS
R Shoulder radius
r Pin radius
t Pin height
S Welding Speed
T Total spindle torque
τ Shear flow stress
Ts Torque on shoulder
Tps Torque on the lateral surface of pin
Pt Traverse power
Tpb Torque at pin bottom
Ft Traverse force
F1 Flow force
F2 Frictional force
S Welding speed
N Tool rotational speed
d Pin Diameter
D Shoulder Diameter
υ Poisson‟s ratio
a Original crack length
KI Stress Intensity Factor
vp Plastic component of COD
W Width of sample
B Thickness of sample
S Spam of the sample
δp Plastic part of CTOD
δe Elastic Part of CTOD
δc Total CTOD
𝜎𝑦𝑠 Yield Strength of the material
Qs Heat generation
AS Shoulder contact area
qv Volumetric heat source
FN, FP Normal and traverse forces
T Torque
H Sheet thickness
YS Yield strength of Weld
µ Friction coefficient
UTS Ultimate tensile strength
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