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Effect of the addition of wood shavings on


thermal conductivity of sand concretes:
Experimental study and modelling

Article in Construction and Building Materials · March 2007


DOI: 10.1016/j.conbuildmat.2005.12.008

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Construction
and Building

Construction and Building Materials 21 (2007) 662–668


MATERIALS
www.elsevier.com/locate/conbuildmat

Effect of the addition of wood shavings on thermal conductivity


of sand concretes: Experimental study and modelling
M. Bederina a, L. Marmoret b, K. Mezreb b, M.M. Khenfer a, A. Bali c, M. Quéneudec b,*

a
Université Amar Thélidji, Département de Génie Civil, Laghouat, Algeria
b
Laboratoire des Technologies Innovantes, EA 3899 UPV, IUT, Département de Génie Civil, Universite de Picardie Jules Verne,
Avenue des facultés, 80025 Amiens cedex 01, France
c
Ecole Polytechnique, Département de Génie Civil, Alger, Algeria

Received 4 March 2005; received in revised form 13 November 2005; accepted 10 December 2005
Available online 3 February 2006

Abstract

This work aims at the valorisation of local materials and the reuse of various wastes. The main objective of this research is to con-
stitute a structural lightweight sand concrete and to improve its thermal properties while preserving its mechanical performances. The
purpose of this work is to study the effect of addition wood shavings on thermal conductivity of the sand concretes. The shavings, which
stem from waste of woodworking activities, have been incorporated, without any preliminary treatment, into two types of sand con-
cretes. A range of shavings contents, varying from 0 to 100 kg/m3, have been examined herein. The sand concretes, constituting the
matrix, are composed of sand, cement, filler, admixture and water. Results demonstrate that the inclusion of shavings into the sand con-
cretes reduces material density to a considerable extent, while the structure remaining homogeneous and with a strong wood–matrix
adherence; furthermore, thermal conductivity has been improved.
At smaller shavings contents, the dune sand concrete exhibited slightly better thermal conductivities than those of the river sand con-
crete. A modelling application per auto-coherent homogenisation reveals good correspondence with the experimental results.
 2006 Elsevier Ltd. All rights reserved.

Keywords: Lightweight concrete; Sand concrete; Wood shavings; Filler; Thermal conductivity; Microstructure; Modelling

1. Introduction a small enough proportion such that the mass ratio (sand/
gravel) remains higher than 1. If the mix were to contain
The use of local materials in the building industry, gravel, the material would be called ‘‘a loaded sand con-
regardless of their level of underutilisation, has become a crete’’ [4,5].
necessary component to the solution to the economic prob- The reuse of various wastes, which constitutes an envi-
lems of developing countries [1]. This finding was high- ronmental nuisance and generated particularly complicated
lighted given the fact that sand concretes are able to problems, has also been the focus of considerable research
replace the conventional concretes in certain structures, lately. Let us start by noting that waste is perceived as any
along with the conclusion that the use of fillers is essential residue stemming from a process, transformation or use [6].
(for improvement compactness and consequently strength, Moreover, the lignocellulosic material additive within a
enhancing workability, deriving saving on cement in com- cementing provides the topic of numerous studies and
parison with mortars [2,3]). By definition, a sand concrete applications [7,8] due to the thermal and acoustic qualities
either does not comprise any gravel at all or only contains as well as the renewable aspect of the resources employed.
The idea pursued herein of introducing lignocellulosic
waste into sand concrete to improve its thermal perfor-
*
Corresponding author. Tel./fax: +33 3 2253 4016. mances, while preserving its mechanical qualities, was thus
E-mail address: michele.tkint@iut-u-picardie.fr (M. Quéneudec). quite attractive. In previous work [2], local dune sands and

0950-0618/$ - see front matter  2006 Elsevier Ltd. All rights reserved.
doi:10.1016/j.conbuildmat.2005.12.008
M. Bederina et al. / Construction and Building Materials 21 (2007) 662–668 663

Nomenclature

A inclusion of air Rc compressive strength


b wood fraction RS river sand
B wood content (kg/m3) S sand content (kg/m3)
C cement content (kg/m3) W water content (l/m3)
DS dune sand q density (kg/m3)
Eq equivalent homogeneous material k thermal conductivity (W m1 K1)
F filler content (kg/m3)

river sand serve as the primary aggregates, with crushing Table 1


wastes as the filler. The present work therefore is aimed Physical properties of various used sands
at studying the influence of adding wood shavings on the Characteristics q (apparent) (kg/m3) qS (specific) (kg/m3)
thermal conductivity of these sand concretes. DS 1428 2596
RS 1482 2576
2. Used materials

2.1. Sands 2.2. Cement

Two different sands were separately used for this study: The used cement is a Portland cement (type II) of class
45 whose denomination is ‘‘CPJ-CEM II/A’’. The chemical
 a dune sand (DS) from the Northern area of the town of analysis and composition of this cement are given in Table
Laghouat (Algeria), and 2. The physical characteristics are the following: specific
 a river sand (RS) from M’zi oued (also area of density 3078 kg/m3 and specific surface area 289 m2/kg.
Laghouat).
Results from the particle size distribution analysis of the 2.3. Fillers
two sands, established according to standard NF P18-560
[10], are presented in the Fig. 1. Fillers are intended both to supplement the particle size
The dune sand is a fine-graded sand, whose maximum distribution curve of sand over its fine part and to fill the
diameter does not exceed 0.63 mm and features a tight par- intergranular vacuums in the sand. Among the several
ticle size distribution. In contrast, the river sand is coarser, types of filler used, it was confirmed that the limestone fill-
with a maximum diameter reaching 5 mm and a more ers are well adapted to the sand concretes (due to their
widely-spread particle size distribution. An SEM investiga- reactivity with cements) and yield the best mechanical per-
tion has revealed the rounded grain shape. Microscopic formance [3]. The fillers used in this work have been
observation shows a low angularity in the grains. The river obtained by sifting (with a sieve opening of 80 mm) crush-
sand grains are more rounded than those of the dune sand ing waste from a quarry located in the region north of
[9]. The densities of the sands used for purposes of this Laghouat. The chemical analysis conducted shows that
study have been listed in Table 1. these fillers are mainly composed of limestone [9]. The spe-
The X-ray analysis of both dune and river sand demon- cific density (as measured using the pycnometer) is of
strates their essentially siliceous nature [9]. 2900 kg/m3. The specific surface (as measured with Blaine’s
permeability meter according to the standard EN 196-6)
[11] is of 312 m2/kg.
100
90
DS 2.4. Wood shavings
Cumulative passing (%)

80
70
60
RS The shavings consist of fir tree waste produced from
50
woodworking activities; they display an irregular shape,
40 with particle size distribution ranging from 0.1 mm and
30 8 mm. These characteristics however are only given as an
20 indication, since their significance has not been determined
10
0 Table 2
10 100 1000 10000 Composition of the two sand concretes (without shavings)
Grain diameter (µm) SiO2 Al2O3 Fe2O3 CaO MgO SO3 PF
20.66 4.77 2.88 63.31 1.17 2.32 1.06
Fig. 1. Particle size distribution of various sands, (dune and river sand).
664 M. Bederina et al. / Construction and Building Materials 21 (2007) 662–668

Table 3
Chemical analysis of the cement used
Material C (kg/m3) S (kg/m3) F (kg/m3) W (l/m3) SPa (%)
Dune sand 350 1305 200 245 1.5
River sand 350 1460 150 210 1.5
a
The percentage of the admixture is calculated, in mass, compared to
the cement mass.

Table 4
Volume of wood shavings in sand volume and concrete volume
Wood Volume Volume wood/sand ratio (%)
content wood/concrete DS-concrete RS-concrete
(kg/m3) ratio (%)
0 0 0 0
Fig. 2. Particle size distribution of wood shavings. 20 3.76 7.77 6.87
40 7.25 15.54 13.74
60 10.50 23.33 20.61
rigorously due to a lack of rigidity and the geometry of 80 13.50 31.07 27.47
shavings. Fig. 2 shows the corresponding particle size 100 16.34 38.85 34.34
distribution.
Real density of the shavings was taken as the apparent cement and filler were then introduced into a mixer and
density of a solid of wood block. The measurement of this mixed for 3 min at slow speed. Once the mixture has
density was then applied to a massive block dried at a tem- become perfectly homogeneous, water-saturated wood
perature of about 60 C so as not to modify the chemical aggregates were added. Mixing then continued at slow
and physical properties of material. The measured value speed for another 3 min. The shavings were added to the
amounted to approximately 512 kg/m3. The apparent den- dry mixture in a saturated state, for the two following
sity of shavings is on the order of 160 kg/m3. Water reasons:
absorption for the lightweight aggregates is both sizable
and variable. Builders have always considered this absorp-  It was noted that with saturated shavings, dispersion in
tion level to be a major difficulty on construction sites by the dry mixture is better.
virtue of causing wide variations in concrete plasticity  The mixing water, intended to hydrate of cement and
and workability. Water absorption, as measured after total enhance concrete workability, will not be absorbed by
immersion of wood block until weight stabilization and the shavings.
expressed by the ‘‘Water/shaving’’ mass ratio, stands at The mixing water was added gradually. Material homog-
approximate 36%. enisation was guaranteed by mixing at slow speed for 3 min,
then at high speed for one more minute. Following setting
2.5. Admixture of the moulds, the samples are maintained in a wet room
(90% HR and 20 C); after 24 h, they were demoulded
The admixture used is an Algerian superplasticiser of and kept in a dry environment (50% HR and 20 C) to
‘‘MEDAPLAST (SP40)’’ type; it is a brown sulfuric Poly- remain close to local climatic conditions.
napthalene (PNS) solution, with a dry extract of 40% The thermal characteristics are measured on dry half-
(±1%) and a pH of 8.2 (index of acid level). cubic samples of 10 · 10 · 5 cm3 (Fig. 3) using a non-sta-
tionary method, which displays several advantages, in
3. Material fabrication and experimental techniques

The optimal compositions of the studied sand concretes,


without the addition of any shavings, were given in a pre-
vious study [2]. These compositions (Table 3), were taken
as the basic compositions in constituting the matrix of
the studied composites.
The material was lightened by incorporating wood shav-
ings with proportions varying from 0 to 100 kg per cubic
meter of sand concrete. The different used proportions
are given in Table 4. In order to better control the use of
mixing water, which plays an important part in the mate-
rial’s physical and mechanical properties, the raw materials
are dried beforehand. Dry mixing proves essential to a
proper homogenisation of the mixture. The sand, the Fig. 3. Introduction of TPS-element between two half test-tubes.
M. Bederina et al. / Construction and Building Materials 21 (2007) 662–668 665

particular in terms of contact resistance, power and dura- Table 5


tion of the emitted signal. The theoretical bases of this tech- Characteristics of the matrix
nique have been discussed by SE Gustaffson [12,13] as well B (kg/m3) 0 20 40 60 80 100
as by various other authors [14–16]. The experimental k (W m k ) 1 1

device used is composed of Transient Plane Source (TPS) DS-concrete 1.20 0.98 0.86 0.71 0.65 0.55
element, a power supply stabilised in tension, a Wheatstone RS-concrete 1.30 1.10 0.90 0.80 0.69 0.65
bridge, an acquisition power station and a microcomputer Rc (MPa)
for the data control and processing. In order to protect the DS-concrete 20 17.5 13.2 9.4 7.4 5.6
RS-concrete 23.6 21.7 14.3 10.6 9.4 6.2
probe against the damage and to ensure that flow is being
distributed over a more representative surface, two copper
plates of 1 mm thick and of 5 · 5 cm in dimension were
2200
introduced between the TPS sensor and the two same mate-
rial block 10 · 10 · 5 cm3. The surfaces of the two half-
samples were polished beforehand in order to minimise 2000 SD
the influence of contact resistance. A chucking device was
employed to ensure a good contact between the various ele-
SA
ments. The whole assembly was then introduced into an 1800

Density (kg/m 3 )
enclosure to allow controlling the experimental tempera-
ture. Two thermocouples were welded onto the metal
1600
plates to check thermal stability at the samples level. The
probe was standardised on several materials of known ther-
mal characteristics in order to validate both the test condi- 1400
tions and parameters. To obtain reliable results, the
duration of the experiment was extended from 240 to
360 s and the power emitted from the stabilised power sup- 1200
ply was maintained equal to 0.06 W cm2. It should also be
noted that the rise in the temperature during the entire test
1000
period did not exceed 1 C in the studied material [12,14]. 0 20 40 60 80 100
The TPS method uses a conducting pattern with a heat
Wood content (kg/m3)
capacity simultaneously as a heating element and tempera-
ture sensor when measuring thermal conductivity of sample Fig. 4. Evolution of the dry density (at 28 days) according to the wood
surrounding the TPS-element [12,14]. The time-dependent content.
resistance of TPS-element during the transient recording
can be written as [12]: concrete. This figure indicates a correlation with the wood
RðtÞ ¼ R0 ð1 þ aDT ðsÞÞ ð1Þ content that follows a parabolic-type law. For a wood con-
tent of 100 kg/m3, the density is reduced by approximately
where R(t), resistance of the TPS-element at time (t); R0, 30%.
resistance of the TPS-element at time zero; a, temperature Lightening the mix by the addition of shavings repre-
coefficient of resistivity (TCR); DT(s), the mean value of sents a complex phenomenon, which entails both a poros-
temperature rise in the TPS-element. ity specific to the wood aggregates and a complementary
The thermal conductivity has been calculated with a porosity of matrix or wood–matrix interactions. Previous
developed Matlab program [17] using the following results have shown [18] that the porous structure of wood
relation: aggregates is slightly or not at all affected by their introduc-
k ¼ cDðsi Þ=DEðtÞ ð2Þ tion into the matrix. As for all the concretes and mortars,
the porosity of the matrix, and consequently its thermal
where c, constant depending of the different resistances in conductivity, depends on several factors such as: age of
the Wheatstone bridge; D(si), theoretical expression of the composite, proportion of aggregates, quantity of
time-dependent increase [17]; DE, the variation in potential cement, W/C ratio, type of mixture, proportion of fine,
across the TPS sensor. temperature, state of sample moisture, mode of samples
The experimental conductivity values are given in Table preparation, etc. [19]. Let us point out for example that
5. water alone may be a lightening factor, by virtue of creat-
ing pores during the evaporation of water in excess of what
4. Experimental results and analyses is necessary for cement hydration.
As regards the matrix-shaving connection, Fig. 5 reveals
The thermal conductivity of wood is definitely lower that, generally, the shavings adhere well to the (cement–fil-
than that of the concretes. The Fig. 4 shows the effect of ler–sand) matrix. However, defects around the wood
the proportion of shavings on the density of the sand aggregates can also be observed at time, most likely due
666 M. Bederina et al. / Construction and Building Materials 21 (2007) 662–668

Fig. 5. Optical micrograph of the wood sand concrete. (a) Concrete with RS (B = 20 kg/m3), (magnification 150·) and (b) concrete with DS (B = 20 kg/
m3), (magnification 175·).

to the retraction of the aggregates following evaporation of the sand component. This finding can be explained by the
the water absorbed by the shavings. This type of defect was identical mineralogical nature of the two sands.
already noted by Aouadja et al. [20]. Similarly, a typical
additional porosity due to air entrainment is observed at 5. Modelling by auto-coherent homogenisation
the level of the matrix.
This additional porosity may have been generated by the Modelling by auto-coherent homogenisation allows
shavings during mixing or by the admixture [17]. estimating thermal conductivity of heterogeneous materi-
The curves in Fig. 4 make it clear that without any wood als on the basis of knowing the conductivity of each com-
addition (i.e. B = 0), the dune sand DS-concrete is slightly ponent and its concentration. This approach was
less dense and more porous than the river sand RS-con- developed for the mechanical characterisation (elasticity
crete [2,3]. This finding is due to the different particle size and elastoplasticity) of heterogeneous materials and was
distribution of the two sands: a dispersed particle size dis- used by Arnaud et al. [21] on hemp in bulk, hemp con-
tribution for RS with a maximum diameter of 5 mm vs. a cretes and hemp wools. Another application has been
tightened particle size distribution for DS with a maximum recently established for lignocellulosic concretes [22]. This
diameter of 0.63 mm. This difference in density is main- method is based on the following energy condition: the
tained for the various wood contents studied but tends to energy contained in heterogeneous material is equal to
decrease as wood content increases. Fig. 6 shows the evolu- that of the equivalent homogeneous material submitted
tion in thermal conductivity vs. composite density. It may to the same boundary conditions. The homogeneous
be noted that at equal densities, thermal conductivity material is assimilated to an assembly of spherical com-
remains appreciably the same regardless of the origin of posite inclusions of variable sizes. We have considered a
heterogeneity within the required homogeneous material.
1.6 The heterogeneous material could be constituted of either
two or three components.
SD
5.1. Case of a heterogeneous material constituted of two
T he mal co nduc ti v ity (w/ m.k)

1.2 components
SA
Equivalent homogeneous material with properties keq
(conductivity) and qeq (density) are assumed to be consti-
0.8 tuted of a sphere of radius R1 representing component
‘‘1’’ (k1, q1) (in the present case, air contained within the
wood particles). It is furthermore surrounded by a concen-
tric shell of external radius R2 representing component ‘‘2’’
0.4 (k2, q2) (wood block) (Fig. 7a).
The resolution of a system with four equations with
three unknowns, which has a solution if the determinant
is null, leads to the following relation:
0 2 3
1400 1600 1800 2000
Density (kg/m3 ) 6 x 7
keq ¼ k2 6
41 þ  7
5 ð3Þ
1x 1
Fig. 6. Evolution of thermal conductivity according to the density of the 3
þ k1
1
concrete. k
2
M. Bederina et al. / Construction and Building Materials 21 (2007) 662–668 667

1.6
Model (DS)

Thermal conductivity (W/m.k)


1.4
Exp. Points (DS)
((a) , ra) ((1), ra) 1.2 Model (RS)
Exp. Points (RS)
1
((b), rb) ((2), rb)
0.8
((3), rc)
0.6

(a) : case of 2 components (b) case of 3 components 0.4

0.2
Fig. 7. Modelling of different phases. 0
0 20 40 60 80 100
where x is the volume concentration of the intern phase Wood content (kg/m3)
‘‘1’’ definite by x = (R1/R2)3.
Fig. 8. Thermal conductivity according to the content of wood: confron-
For this work, the model with two components allows tation of the experimental results to the results obtained by auto-coherent
deducing the total conductivity of homogeneous material model.
as equivalent to the bulk wood shavings along with the
conductivity of the wood particle (k2) (Table 6). This ther- to apply the model to variable wood contents, the material
mal conductivity will now be applied to 3 component densities were evaluated by means of a parabolic regression
model described below. obtained from the experimental results of material densities
(q) as a function of wood content (B):
5.2. Case of a heterogeneous material constituted of three
 For dune sand concrete:
components
q ¼ 0:00002B2  0:0077B þ 2:0390 ðR2 ¼ 0:999Þ ð5Þ
The preceding explanation may now be extended to a  For river sand concrete:
material made of three components 1, 2 and 3 (Fig. 7b).
The additional shell is the matrix ‘‘3’’ representative of q ¼ 0:00001B2  0:0077B þ 2:0999 ðR2 ¼ 0:998Þ ð6Þ
the concrete made of sand, cement and filler (R3, k3, q3). where B is the mass content of wood shavings and R is the
Equivalent thermal conductivity then becomes: coefficient of correlation.
x
keq =k3 ¼ 1 þ 2 3 ð4Þ
dðk1 =k2  1Þ The experimental measurements of conductivity for the
61  x 1þ 7 two sand concretes containing shavings where then com-
6 3 7
4 3 þ dðk1 =k2  1Þð2k1 =k2 þ 1Þ5 pared to the theoretical approach based on the auto-coher-
3 ent method. Fig. 8 indicates that the theoretical results
correspond well to the values obtained during the experi-
with x = (R2/R3)3; d = 1(R1/R2)3; K = m1/m2. ments, which serves to validate both the model coefficients
The auto-coherent model is applied to the composite and relations.
with 3 components, comprising a spherical cavity of air
‘‘1’’ (vacuum contained in wood and matrix), surrounded 6. Conclusions
by a concentric wood shell ‘‘2’’, and moreover surrounded
by an additional shell of matrix ‘‘3’’ (concrete). The phys- The results presented herein reveal a remarkable
ical characteristics of the matrix have been listed in Table 7. improvement of the thermal conductivity of the composite
The concentrations x and d are directly calculated from thanks to the addition of wood shavings. This new material
the masses of each component (of known density). In order inclusion could therefore provide multiple applications, in
particular for heat insulation and as a filling material, or
Table 6
Physical characteristics of the air and wood
for use in structures with low load-bearing capacities
should the wood content not be high enough. In general
Air Wood shaving Wood block
it was found that:
3
q (kg/m ) 0.001 160 512
k (W m1 K1) 0.026 0.087 0.280  The increase in shavings content reduces the weight of
sand concretes by distinctly decreasing their density;
 The increase in shavings contents decreases the thermal
Table 7
Physical characteristics of the matrix conductivity of sand concrete and thus increases their
insulating capacity,
Matrix
 With small proportions of shavings, river sand concrete
Matrix (with RS) Matrix (with DS)
displays thermal conductivities slightly higher than
3
q (kg/m ) 2040 2100 those of dune sand concrete, but this difference tends
k (W m1 K1) 1.20 1.25
to disappear at higher wood contents,
668 M. Bederina et al. / Construction and Building Materials 21 (2007) 662–668

 The increase in shavings content reduces the mechanical [10] NF EN 18-560, Analyse granulométrique par tamisage, Granulats,
strength of sand concretes. However, with small propor- AFNOR, 1990.
[11] NF EN 196-6, Méthodes d’essais des ciments, PARTIE 6/ Déter-
tions, we can obtain interesting values of strength (Table mination de la finesse (indice de classement) – AFNOR, août 1990. p.
5). 15–476.
 As regard the aspect of this composite, observation by [12] Gustafsson SE. Transient plane source techniques for thermal
means optical microscopy shows in general a homoge- diffusivity measurement of solid materials. Rev Sci Instrum
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 The results obtained by applying the auto-coherent compounds with natural rubber prophylactics waste filler. Eur Polym
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