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  • Wa0023

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    Arjun Jp
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    The document is an X-ray spectroscopy analysis report of a sample containing carbon, silicon, nickel, copper, and tin. It includes an image of the sample at 5000x magnification, a graph of the element peaks detected, and a table listing the elements identified through standardless quantitative analysis along with their estimated mass percentages and error levels. The analysis determined the sample is composed primarily of copper (84.05% by mass) with smaller amounts of nickel (14.6%) and carbon (1.35%).

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    Hibrid.

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    DOC-20190213-WA0023

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    The document is an X-ray spectroscopy analysis report of a sample containing carbon, silicon, nickel, copper, and tin. It includes an image of the sample at 5000x magnification, a graph of the element peaks detected, and a table listing the elements identified through standardless quantitative analysis along with their estimated mass percentages and error levels. The analysis determined the sample is composed primarily of copper (84.05% by mass) with smaller amounts of nickel (14.6%) and carbon (1.35%).

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    © All Rights Reserved
    Download as DOC, PDF, TXT or read online from Scribd
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    12 views1 page

    Wa0023

    Uploaded by

    Arjun Jp
    The document is an X-ray spectroscopy analysis report of a sample containing carbon, silicon, nickel, copper, and tin. It includes an image of the sample at 5000x magnification, a graph of the element peaks detected, and a table listing the elements identified through standardless quantitative analysis along with their estimated mass percentages and error levels. The analysis determined the sample is composed primarily of copper (84.05% by mass) with smaller amounts of nickel (14.6%) and carbon (1.35%).

    Copyright:

    © All Rights Reserved
    Download as DOC, PDF, TXT or read online from Scribd
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    Title : IMG1
    ---------------------------
    Instrument : 6490(LA)
    Volt : 15.00 kV
    Mag. : x 5,000
    Date : 2017/03/13
    Pixel : 256 x 192

    10 µm
    2400
    Acquisition Parameter
    Instrument : 6490(LA)
    2100 Acc. Voltage : 15.0 kV
    Probe Current: 1.00000 nA
    1800 PHA mode : T1
    Real Time : 30.17 sec
    CuLl NiLa CuLa

    Live Time : 30.00 sec


    1500 Dead Time : 0 %
    Counting Rate: 2346 cps
    Counts

    Energy Range : 0 - 20 keV


    1200
    SnLb2

    900
    SnLr2,

    CuKa
    SnLb
    NiLl

    600
    CuKb
    NiKa
    SnLa

    NiKb
    SiKa

    SnLl

    SnLr
    CKa

    300

    0
    0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00

    keV
    ZAF Method Standardless Quantitative Analysis
    Fitting Coefficient : 0.8796
    Element (keV) Mass% Error% Atom% Compound Mass% Cation K
    C K 0.277 1.35 0.43 6.68 0.2964
    Si K
    Ni K 7.471 14.60 4.49 14.77 15.3966
    Cu K 8.040 84.05 6.48 78.56 84.3070
    Sn L
    Total 100.00 100.00

    JED-2300 AnalysisStation

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