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Indian Standard
HIGH DENSITY POLYETHYLENE PIPES FOR
SEWERAGE - SPECIFICATION
C) DIS 19ge
( Page 1, clause 3.1 ) - Add the following new clause at the end and renumber subsequent clauses:
'3.2 Grade of Material
3.1.1 Pipes shall be classified according to the grade of materials given in Table I.
3.2.2 The maximum allowable hydrostatic design stress ( r ) of a pipe is obtained by applying the design
coefficient of 1.25 (Min) to the MRS value of the material, taking into consideration the temperature at which
the pipe is to be designed for.
3.1.3 The material grading shall be given by the raw material supplier and in case of master batch, by the pipe
manufacturer. '
( Page I, clause 3.3 ) - Substitute the following for the existing clause and renumber the subsequent
clause:
3.3 Pressure Rating
Pipes shall be classified by pressure rating ( PN ) corresponding to the maximum permissible working pressure
at 30°C, as follows:
Pressure Rating of Pipe Maximum Permissible
Working Pressure
PN 2.5 O.25MPa
PN 4 O.40MPa
PN 6 O.60MPa
PN 8 O.80MPa
PN 10 1.OOMPa
PN J2.5 1.2SMPa
PN 16 1.60MPa
( Page It C/aule 5.1.1 ) - Delete the clause and renumber the subsequent clauses.
Prlee Group I
1
Amendment No.1 to IS 14333: 1996
( Page 2, clause 6.1 ) - Substitute to Table 2' for 'Table I '.
( Page 2, Table I, Title) - Substitute 'Table 2' for 'Table I'.
( Page 2. clause 6.2 ) - Substitute the following for the existing clause:
to6.2 Wall Thickness
The minimum and maximum wall thickness of pipes for all the three grades of materials namely, PE 63. PE 80
'I
and PE )00 shall be as given in Tables 3. 4 and 5 respectively ( see A-3 ). 'I
16 to 75 2
90to 125 3
140to 180 4
200 to 280 5
Above 280 7
2
AmendmeDt No. 1 to IS 14333 : 1996
Tatile 3 Wall Thickness of Pipes for Material Grade PE 63
( Clause 6.2 )
All dimensions in millimetres.
01.
ON
. PN 2.S
Min
...
Max
, .
Min
PN.... 4
Max Min
PN 6
,..----.."'o-~
Max Min
PN.... 8
Max Min
PN... 10 ,
Max Min
PN 12.5
,..----.."'0--
Max Min
PN 16
,..----.."'0-----.,
Max
(1) (2) (3) (4) (S) (6) (7) (8) (9) (10) (II) (12) (13 ) (14 ) ( 15)
63 4.0 4.6 S.8 6.6 7.S 8.S 9.0 10.1 10.9 12.2 I ~.3 14.9
7S 3.0 3.S 4.7 S.4 6.9 7.8 8.9 10.0 10.8 12.1 13.0 14.S 1~.8 17.6
90 3.6 4.2 5.7 6.5 8.2 9.3 10.6 11.9 12.9 14.4 15.6 17.4 19.0 21.1
110 4.4 5.1 6.9 7.8 10.0 11.2 13.0 14.5 15.8 17.6 19.0 21.1 23.2 25.8
125 5.0 5.7 7.9 8.9 11.4 12.8 14.8 16.5 17.9 19.9 21.6 24.0 26.4 29.3
140 5.6 6.4 8.8 9.9 12.8 14.3 16.5 18.4 20.0 22.2 24.2 26.9 29.5 32.7
160 6.4 7.3 10.0 11.2 14.6 16.3 18.9 21.0 22.9 25.4 27.6 30.6 33.7 37.3
180 7.2 8.2 11.3 12.7 16.4 18.3 21.2 23.6 25.8 28.6 31.1 34.5 37.9 41.9
200 8.0 9.0 12.5 14.0 18.2 20.3 23.6 26.2 28.6 31.7 34.S 38.2 42.2 46.7
225 9.0 10.1 14.1 IS.8 20.5 22.8 26.5 29.4 32.2 35.7 38.8 42.9 47.4 52.4
250 10.0 11.2 15.7 17.S 22.8 25.3 29.5 32.7 3S.8 39.6 43.2 47.8 52.7 58.2
280 11.2 12.6 17.5 19.5 25.5 28.3 33.0 36.5 40.0 44.2 48.3 53.4
315 12.6 14.1 19.7 21.9 28.7 31.8 37.1 41.1 4S.0 49.7 S4.4 60.1
355 14.2 15.9 22.2 24.7 32.3 35.8. 41.8 46.2 50.8 56.1
400 16.0 18.6 25.0 29.0 36.4 42.1 47.1 54.4 57.2 66.0
3
A.endaent No. I to IS 14333: 1996
Table 5 Wall Thtckneu 01Pipes for Material Grade PE 100
( Clause 6.2 )
All dimensions in millimetres.
ON MI" MtD Min Mai Min Ma; Min Max Min Max
(I) (2) (3) (4) (S) (6) (7) (8) (9) (10) ( II )
63 3.6 4.2 4.7 ~.4 5.8 6.6 7.0 7.9 8.7 9.8
75 4.3 5.0 ~.6 6.4 6.9 7.8 8.4 9.~ 10.4 11.7
90 5.1 5.9 6.7 7.6 8.2 9.3 10.0 11.2 12.S 14.0
110 6.3 7.2 8.2 9.3 10.0 11.2 12.3 IJ.8 1~.2 17.0
125 7.1 8.1 9.3 IO.~ 11.4 12.8 13.9 15.5 17.3 19.3
140 8.0 9.0 !O.4 11.7 12.8 14.3 15.6 17.4 19.4 21.6
160 9.1 10.3 11.9 13.3 14.6 16.3 17.8 19.8 22.1 24.6
110 10.2 11.5 13.4 15.0 16.4 18.3 20.0 22.2 24.9 27.6
200 11.4 12.8 14.9 16.6 '1.2 20.3 22.3 24.1 27.6 30.6
225 12.8 14.3 16.7 18.6 20.S 22.8 25.0 27.7 31.1 34.S
2S0 14.2 IS.9 18.6 20.7 22.8 .: 2S.3 27.8 30.8 34.S 38.2
210 15.9 17.7 20.8 23.1 25.2 28.3 31.2 34.6 38.7 42.8
315 17.9 19.9 23.4 26.0 21.7 31.8 35.0 38.7 43.S 48.1
355 20.1 22.4 26.3 29.2 32.3 3~.8 39.5 43.7 49.0 S4.1
400 22.7 26.4 29.7 34.4 36.4 42.1 44.5 51.4 55.2 63.7
s
Amendment No.1 to IS 14333: 1996
( Page 3, Table 3 ) - Substitute the following table for the existing:
Table 6 Requirement of Pipes for Inte....al Pressure Creep Rupture Test
( Clauses 8_1, 9.1.2 and 8-4.3 )
51 Test Test Tempenture Tnt D.ratlon I.dueed Stress
No. e-c MJ.i .... Holeltw. Time, h in Mr.
PE 63 PE 80 PE 100
(CEDSO)
6
Printed II New India rrinlina Prell. Khurja. India
AMENDMENT NO. 1 SEPTEMBER 1003
TO.
IS 14333: 1996 HIGH DENSITY POLYETHYLENE
PIPES FOR SEWERAGE - SPECIFICAnON
( Page 1, clause 5.1.2, lines 1 and 2 ) - Substitute '940.0 kg/m3 and
958.0 kglm3, for '940.5 kglm3 and 946.4 kglm3•• .
( Page 1, clause 5.1.3, line 2 ) - Substitute '0.20 and 1.10· for '0.41 and
1.10' .
(CEO SO)
Reprography Unit.81S. New Delhi.India
AMENDMENT NO. 3 DECEMBER 2004
TO
IS 14333: 1996 mGH DENSITY
POLYETHYLENE PIPES FOR SEWERAGE -
SPECIFICATION
( Page 1, clause S.I,first para ) - Substitute the following for the existing:
'High density polyethylene (HDPE) used for the manufacture of pipes shall
confonn to designation PEEWA-45-T-003 or PEEWA-45-T-006 or
PEEWA-50-T-003 or PEEWA-SO-T-006 or PEEWA-S7-T-003 or
PEEWA-S7-T-006 of IS 7328. HOPE conforming to designation
PEEWA-4S-T-012 or PEEWA-SG-T-012 or PEEWA-S7-T-012 of IS 7328 may
also be used with the exception that melt flow rating (MFR.) shall be between
0.20 gllO min to 1.10glI0 min (both inclusive). '
[ Page 1, clause 5.1.2, line 2 (see also A~ndment No.2) ]- Substitute
'958.4' for '958.0'.
[ Page 1, clause 5.1.3, line 2 (see also AIMndment No.2) ] - Substitute
'O.20gllOminand 1.10gl10min'for'O.20and 1.10'.
( Page 3, clause 8.4 ) - Substitute the following for the existing:
'When tested from a composite sample of minimum three pipes, as per IS 2530,
at 190°C with nominal load of S kgf, MFR shall be between 0.20 gllO min to
1.10 gllO minutes. The MFR shall also be within 30 percent of the MFR of the
material used in manufacturing pipes tsee 5.1.3). t
[ Page S. AMex ~ clause A-I (see also Amendment No.1) ] - Substitute
the following for the existing:
·With the advancement in technology natural (unpigmented) resin designation
PEEAA-4S-T-003 or PEEAA-4S-T-006 or PEEAA-SQ-T'()()3 or
PEEAA-50-T-006 or PEEAA-57-T-003 or PEBAA-S7-T-006 of IS 7328 and
PEEAA-4S-T-012 or PEEAA-So-T-012 or PEEAA-S7-T-012 of IS 1328 with
the exception that melt flow rating (MFR) shall be between 0.20 gllO min to
1.10 gllO min (both inclusive) duly stabilized with antioxidants (see 5.2) may be
compounded with suitable black master batch or processed directly after physical
mixing with suitable black master batch in the pipe extruder for production of
pipe which shall conform to the performance requirements of the pipes as
specified in this standard (see 8). The material of pipe to be produeed shall
conform to requirements of 5.1. '1
(CEDSO)
Repropaphy Unit. 81S, New Delhi.Iadia'
AMENDMENT NO.4 JANUARY 2009
TO
IS 14333 : 1996 HIGH DENSITY POLYETHYLENE PIPES
FOR SEWERAGE - SPECIFICATION
(Page 2, Table 1, coil to 4) - Insert the following new values at the end:
(CED SO)
Indian Standard
HIGH DENSITY POLYETHYLENE PIPES' FOR
SEWERAGE - SPECIFICATION
1 SCOPE S MATERIALS
This standard lays down the requirements for 5.1 Bllb DeDilty Polyethylene
"high density polyethylene pipes from 63 mm. to
630 mm nominal diameter of pressure ratrng High density polyethylene (HOPE) used for
-from 0·25 MPa to 1·0 MPa for sewerage appli- the manufacture of pipes shall conform to desi-
-cations. gnation PEBWA-4S-T-006 of IS 7328: 1992.
HDPE conforming to designation PEEWA-45-
2 REFERENCES T..012 of IS 7328 : 1992 may also be used with
the exception that melt flow rate ( MFR ) shan
the Indian Standards listed below are necessary not exceed 1·10 g/10 min ( see A-I ).
.adjuncts to this standard:
IS No. Title 5.1.1 The MRS ( Minimum Required Strength)
of the material used should Dot be lower than
2530: 1963 Method of test for polyethylene 6·3 MPa at 20°C at SO years. A conformity
moulding materials and polye- certificate from the manufacturer of the resin
thylene compounds shall be obtained to this effect.
4905 : 1968 Methods for random sampling
5.1.2 The specified base density between 940.5
7328 : 1992 High density polyethylene kg/m l and 946.4 kg/rna (both inclusive) shall
materials for moulding and be determined at 27°C according to procedure
extrusion (first revision) prescribed in Annex A of IS 7328: 1992. The
value of the density shall also not differ from
-3 DESIGNATION the nominal value by more than 3 kl/ml as per
5.2.1.1 of IS 7328 : 1992.
.3.1 Pipes shall be designated acco.rding. to the
pressure rating ( see 3.2 ) and nominal diameter 5.1.3 The MFR of the material shall be between
{ see 3.3)_ For example, PN 10 DN 200 indi- 0-41 and 1·10 (both inclusive) when tested at
-cates a pipe having a pressure rating 1·0 MPa
190°C with nominal load of 5 kgfas determined
and outside nominal diameter 200 mm. by method prescribed in 7 of IS 2530: 1963.
The MFR of the material shall also be within
-3.2 Pressure Ratlol ±20 percent of the value declared by the manu-
facturer.
Pipes shall be classified by pressure rating ( PN )
;88 follows: '
5.1.4 The resin shall be compounded with
Pressure Rating Maximum Permtssibl« carbon black. The carbon black content in the
of Pipe Working Pressure, MPa material shall be within 2-5 ± O· 5 percent and
the dispersion of carbon black shall be satisfac-
PN 2·5 0·25 tory when tested according to the procedure
PN 4 0·40 described in IS 2530: 1963.
PN 6 0-60
PNIO 1-00 5.2 Aatl·Oddlat
3.3 Nominal Diameter ( DN ) The percentage of 8nti..oxidant used shall not
be more than 0-3 percent by mass of finished
The nominal diameter of pipes covered in this resin.
:Itandard are: .-:.
63, 7S t 90, 11).1125. 140. 160, 180, 200, 225, 5.3 Rework•• Material
250,280, 31S, 355, 400, 450, SOO, 560 and 630
mm. The addition of Dot more than 10 perceer of the
manufacturer'. own rework material resultin•
.4 COLOUR from the manufacture of pipes of this standard
is permillJble. No other reworked or recycled
"Th. colour ottbe pipe .hall be blact. material sball be used.
1
-IS 14333 : 19M
2
1814333: 19M
Table 3 Require_eat of Pipes for Internal 8.5 C.rhD Blaek Content and DispersioD
Pre.lure Creep Rupture Telt
When tested from a composite sample of
( Clauses 8.1, 9.1.2 and 8-4,3) minimum three pipes, in accordance with
IS 2530: 1963, the carbon black content shall be
81 Telt Telt Test Duration Induced within l'S ± O'S percent and the dispersion of
Minimum Stresl carbon black shall be satisfactory.
No. Temp
°c Holdlna 01 la MPa . ,
( Time) hours
9 SAMPLING, FREQUENCY OF TESTS
(1) (2) (3) (4) AND CRITERIA FOR CONFORMITY
i) Type test 80 165 3'S
9.1 Type Tests
Ii) Acceptance 80 48 4'1
test
'.1.1 Type tests are intended to prove the
suitability and performance of a new composi-
8.4 Melt Flow Rate ( MFR ) tion, a Dew technique or a new size of a pipe.
Such tests, therefore, need be applied only when
When tested from a composite sample of a change is made in polymer composition or
minimum three pipes as per IS 2530: 1963, at method of manufacture. or when-a new size of
190°C with nominal load of 5 kgf, MFR shall pipe is to be introduced. Even if no change is
be between ,0'4 to .'1 S/IO min and. also shall envisaged. type test shall be done at least once
not differ by more tha':l 30 percent of. the ~FR in ~wo years on each pressure rating of pipe of
of tho material used 10 manufacturlog pipes tho hilhest aize manufactured during the
(til. 5.1.3 ). period.
3
IS 1'":1'"
'.1.2 Three ,ample. of the same size and same 9.2.3 DI",.",iollal and Yt'IIGI R'flllr,m"."
preslure ratiD, selected at random ahall be
tested for compliance with the requirements 'of '9.2.3.1 The number of telt lamples shall be ina
tbe type test, giveD in Table 3. accordance with Table 4.
9.1.3 If all the samples pass the requirements of -'.2.3.2 These pipes shall be selected at random·
the tyre test, the type of the pipe under CODIi· from the lot and in ordor to en.uro the raudom-
deration shall be considered eliaiblc for typo ness of aelection, a random number table Ihall.
approval. be used. For guidance and use of random.
number tables, IS 4905 : 1968 may be referred•.
'.1.4 In case any of the aamples fails in the In the absence of a random number table the:
type test, the testinl authority, at its discretion, following procedure may be adopted.
may call for, fresh samples not exceeding the
original number and subject them to the type Starting from any pipe in the lot count them al~
test again. If in repeat test. no single failure 1,2,3.4.•.••. etc, up to r and so on where r is the
occurs, the type ()f pipe under consideration . integral part of Nln, N being the number or:-
shall be considered eligible for type approval. pipes in the lot and n is the number of pipes in.
If any of tile samples fails in the repeat tests, the samples. Every rth pipe so counted ahall be
the type cf pipe shall Dot be approved. The withdrawn so as to contitute the required,
manufacturer or the supplier may be asked to sample size.
improve the design and resubmit the product
for t) pe approval. 9.2.3.3 The number of pipes given for the first
sample in co) 3 of Table 4 shall be examined.
for dimensional and visual requirements giveD1
9.1.5 A t the end of the validity pericd ( normally in 6.1, 6.1 and 7. A pipe failing to satisfy any
two years) or earlier as may be necessary, the of these requirements shall be considered 8S·
testing authority may call for fresh samples for defective. The lot shall be deemed to have satis-
type test for the purpose of type approval. fied these -requirements. if the number of
defectives found in the first sample are less than
'.2 Acce,taace Tests or equal to the corresponding acceptance number
given in col 5 of Table 4. The lot shall be deemed.
9.2.1 Acceptance tests are carried out on not to have met these requirements if the
samples selected from a lot for the purpose of number of defectives found in the first sample-
acceptance of the Jot. is greater than or equal to the correspcndingi
rejection numbers given in col 6 of Table
4. Jf, however, the number of defeetives-
'.2.2 Lot found in the first sample lies between
the corresponding acceptance and rejection-
All pipes of the same size, and same pressure numbers given in col 4 and S of Table 4, the-
rating and also manufactured essentially under second sample of the size given in col 3
similar conditions of manufacture, sball consti- of Table 4 6baJJ be taken and examined for these
~ lute a lot. For ascertaining conformity of the requirements, The lot shall be considered to have"
Jot to the requirements of this specification, satisfied these requirtments, jf the number or
samples shall be selected in accordance with the defectives found JD the cumulative sample is Jes..
provisions as mentioned here in under and than or equal to the corresponding acceptance
tested for compliance. Dumber given in col 5 of Table 4; otherwise not•.
ID .b.
No. of Pipe I
(1)
Lot
S••ple
No.
(2)
S...ple
Size
(3)
e.mulatl,e
SalDple Size
(4)
AcceptaDce
No.
(5)
ReJectloa
No.
(6),
Up to 150 Firat 13 13 0 2:
Second 13 26 1 2:
151 to 280 Pint 20 20 3:
Secoad 20 40 ~ 4t
281 to 500 Firat 32 32 1 4
Secoad 12 4 ~
501 to 1 200
1 201 to 3 200
Plrat
Secopd
Pi-nt
50
50
80
64
50
100
2
6 ,.
S
7
80 3
Second 80 160 8 9
3 201 to 10 000 Pint 125 125 5 9
Secoad 125 250 12 13
10 001 to 35 000 Firat 200 200 7 11
SecoDd 200 .400 18
'1'
4
'• •4»1:"
".2.4 Hydraulic ChtJl'act.rlstlcs. Reverl/o", donsity (8.~ ),. MFIl ( 8.4), and carbon black
lion T.,t,
.o."8I1y, MFlf. and Carbon Black Conl'lll/ Dllp,r- content/diipersion ( 8.5 ), The lot sball be con-
sidered to ha:vo OIet. the requirements of these
tests. irnone of samples tested (ails.
'9.2.... 1 The lot having sttisfied dimensional and
visual requirements shall be tested (or hydraulic 10 MARKING
characteristics, reversion. density, MFR and
·carbon black content/dispersion requirements. 10.1 Bacb straight length of pipe shall be clearly
marked in indelible ink/paint on either end and
'9.2.4.2 A separate sample size for each of the for coil at both ends or bot embossed on wbite
test. shall be taken as stipulated in Table Sand base every meter throughout the length of pipe'
selected at random from the sample already coil with the following information:
examined for dimensional and visual inspection. a) Manufacturer's name/Trade mark.
All the pipes in each of the sample size shall be
1ested for compliance of the requirements for b) DeSignation of pipe ( see 3.1 ), and
:hydraulic characteristics ( 8.1 ). reversion ( 8.2 )
c) Lot number/Batch number.
Table 5 Scate or SamplfDI fo," Tests for
Hydraulic Characteristics. Reyersion. 10.2 BIS Certification MaridDI
Density. MFR aDd Ca,boD Black
CooteDt/Dlspersioo Each pipe may also be marked with the Standard
Mark.
( Clause 9.2.4.2 )
10.1.1 The use of the Standard Mark is governed
No.orPlpel Sample Size by the proyi.ionl of the Bureau 0/ Indian
(1) (2) Standards Act. 1986 and the Rules and Regula-
tions made thereunder. The details of conditions
Up Co 150 3 under which a licence (or the use of the Stan-
lSI Co 1 200 j dard Mark may be granted to manufacturers or
1 201 to 3' 000 8 producers may be obtained from the Bureau of
Indian Standards.
ANNEX A
( Clauses s.i, 6.1 and 6.2 )
EXPLANATORY NOTES
.~". "
.
..
1814533 al_
A-3.2 Minimum wall thicknoss I. in mm of tbe A-3.3 Maximum wall tbickness haa been OIllcula-·
pipe have been calculated as follows and ted .8 follows: .
rounded off for the next higher 0·1 mm.
a) For pipes with an outside diameter less.
pxd than or equal to 3SS mm, maximum waU':
, == -----
2a + p thickness J .. 1'1 X minimum wall thick-
ness + 0·2 mm), rounded off to .next.
higher L 'J mm.
where
b) For pipes with outside diameter equal to-
p = maximum permissible working pressure or greater than 400 mm, maximum wallt
in MPa; thickness (=- 1'15 x minimum wall thick-·
d = nominal outside diameter in mm; and ness + 0' 2 mm ), rounded off to the next
higher 0·1 mm,
a == maximum allowable hydrostatic design NOTE - Consideriol operational problems, maxi--
stress. that i.'3'O MPa. mum wall thickness of pipes are considered around.
6Omm,
ANNEX B
( Clause 8,1 )
INTERNAL PRESSURE CREEP RUPTURE TEST
B..l GENERAL 8-4.3 The pressure in the pipe shall then be'
increased to the test pressure ( p ) gradually and:
The test. shall be carried out not earlier than 24 without shock preferably within 10 to 30 seconds..
hours after the pipes have been manufactured. in the bath whose temperature has been adjus-
ted in accordance with 8-4.2. The pressure with,
B-1 TEST SPECIMENS a permissible deviation of ± 2'5 percent shalt
be maintained for the period laid down ln.
A sample of pipe having free length between the Table 3.
end fittings equal to ten times the outside diame-
ter but not less than 250 mm and not greater
than 750 mm, shall be taken for testing from The test pressure (p) shall be calculated as
each pipe to be tested. follows from the minimum dimensions given in
the Table 2 and the corresponding inducedt
B-3 APPARATUS stress values given in Table 3.
2at s
Equipment permitting the application of a con- P== (d-s)
trolled internal hydraulic pressure to the
specimen which are immersed in a thermostati-
cally controlled water-bath. where
p == test pressure in MPa;
B·4 PROCEDURE
s .. minimum wall thickness in mm]:
8-4.1 The pipes shall be fitted with the locking
plugs at both ends in such a way that the axial al :=I induced stress in MPa; and
forces comins from the internal pressure are d - outside diameter of pipet in mm ..
transmitted to the pipe, The pipe shall remain
free to move in longitudinal direction,
8-5 ASSESSMENT 011' RESULTS
8-4.2 Through a closable opening in one of the
locking plugs. the pipe shall be filled with water The samples shall not show silns of localized!
at ambient temperature. It shall be then put in swelling or leakage and shall not burst duriD~.
a water bath at the test temperature of sooe the prescribed test duration. The test showiol-.
( permissible deviation ± 1°C) and kept in failure within a distance equivalent to the length
the bath for minimum one hour to adjust the of end cap from the end shall be disregardecl.
temperature. and the test repeated,
.6
18'14333 : 19M
ANNEX C,
( Clause 8.2 )
LONGITUDINAL REVERSION TEST
"Thermostatically controlled at 110 ± 2°C and is C-2.1 Set the oven temperature at 110 ± 2°C.
capable of re-establishing this temperature The glass plate with the test pieces shall then be
·within 15 minutes after the introduction of test placed in the oven heated to test temperature
specimen in the oven. and capable of maintaining continuous forced
air circulation. The test pieces shall be kept in
the oven at the temperatures and for the periods
C-l.2 Tbermometer. graduated to O.5°C specified below:
"C-l.3 Test Specimens Wall Test Period
Thickness. S Temperature 0/ Stressing, ,
Either 3 complete sections of pipe. approxirna- mm ·C min
-tely 200 mm long, shall be taken as test pieces, Up to 8 110± 2 60 ± 1
·or where the pipe diameter is greater than 200 Over 8 up to 16 110 ± 2 120 ± 2
mrn, pieces of pipe of about 200 mm axial length
and with an approximate circumferential arc Over 16 110 ± 2 240 ± 5
~leDgth of 200 mm shall be prepared by cutting.
In such cases, the entire circumference of C-Z.3 Remove the test pieces from the oven and
..approximately 200 mm long section of pipe shall allow to cool in air. without being moved at the
be divided into pieces measuring approximately ambient temperature. Measure the minimum
200 mm square. The direction of the pipe axis distance between the two marks.
· shall be marked on the pieces. All pieces are
required to be tested. A mark shall be scribed C-3 EXPRESSION OF RESULTS
,on the external surface approximately 50 mm
"from each end of the test pieces in the axial C-3.1 For each test piece, calculate the IODl!i-
"direction of pipe (in the case of complete tudinal reversion, T. 88 a percentage, as follows:
. section of pipe, the mark shall be scribed around
·the whole circumference ). The distance between T ~ 10-11 X 100
,the two marks, 10 (reference length). shall be /0
.approximately 100 mm and shall be measured
to the nearest 0'25 mm at ambient temperature. where 10 and
and after the test.
'1 are the distances in mm before
uC.1 PROCEDURE .,
C-3.2 The average value (arithmetic 'Dean) of
·C-1.t Place the test pieces concave side up on a all the test pieces shall be obtained and
;,glass plate previously dusted with talcum, to reported.
ANNEX D
( Foreword)
CHEMICAL RESISTANCE CLASSIFICATION TABLE FOR HDPE PIPES AND FITTINGS
7
.14313',1_
al specified in ISO 8584·1 and or ISO/11t., HS : Relistance Not Satisfactory. Not recom..
8584-2. mended for service applicatioDI under
· any condition.
D-l.3 To aSleSI the tendency of • material ~
toward. environmente] stress eracldDj,.rate· ~ ,Tile" ,pipel~ are· MJio,ully,·' attacked." They'shalll
tests have to be carried out. Other properties Dot be used for eithe~. prc'.\Ire or ' Don-pressure
of the pipe material (. f9~ example. permeabiUty.) app)ications.:', There is' DO point ~n coaductinl·
1
or of the fluid conveyed (for example toxicity, teats. under. pressure 81 the pipeS would be
inflammability, etc, ) should alao be considered certain to fall these tests.
separately.
0-2.Z DescrlptioD of FluId.
0-1.4 The table summarizes the data liven in a
Dumber of chemical resistance tahiti at present D-Z.2.1 Nature 01 CI,emlcals (Co/um,. 2 in the·
in use in varicuseountries, derived from both ,'Table)
practical experience and test results. This evalua-
tion is based on values obtained by immersion The fluids. arc listed by their most common
of high density polyethylene test specimens in names, including trivial and trade names in
the fluid concerned at 20°C or 60°C and atmos- alphabetical order, with some of the chemic~18,.
pheric pressure, followed in certain cases by the synonyms are also listed, in the alphabetical
determination of tensile characteristics. order.
0.1.5 In the preparation of this appendix, In some cases, further information on nature at-
assistance has been derived trom the following: chemical is given, namely:
a) ISO/TR 10358-1993 - Plastics pipes and KSCA : Known Stress-Crack Alent
, fittings - Combined chemical resistance
classification table. SSCA : Suspected Stress-Crack Agent
b) Chemical resistance of 'Sclair' P : Plastlclser
polyethylene
Canada.
resins from Du Pont, o : Oxidiser
Subl. : Sublimes
c) Marlex (Phillips) - Low, medium and
high density polyethylenes: properties dec. : Decomposes
- Processing.
D-2.2.Z Characteristics 01Chemicals ( Columns 3~
B-2 EXPLANATION OF SYMBOLS AND and 4 in the Table)
ABBREVIATIONS
~elting point (m.p. ) and boiling point (b.p.)
10 degree CelSIUS (0 C) are given wherever
0.%.1 Clailification (Lalt Column In the Table)
appropriate. The values refer to fluids' of
The following symbols are used to indicate the technical-grade purity at standard atmospheric.
pressure, unless otherwise stated.
behaviour of HDPE pipes in contact with
chemical agents: D-2.2.3 Concentration of Chemical, ( Column S
In the Table)
S : satisfactory resistance. No indication
that the serviceability would be impaired.
!h~ concentr~tion and/or purity of the fluid is.
indicated, using the following symbols:
The pipes can be used for applications in which
they are not subjected to pressure or other Dil, sol. == Dilute aqueous solution at a'.
stresses; for applications in which they are concentration equal to or Jess thao
exposed to pressure, the final assessment shall 10 percent.
be on the basis of subsequent test under
pressure. Sol, Aqueous solution at a concentratlce
-
hisher . than 10 percent but Dol
L : Limited resistance, depending on condition saturated.
of use. Sat. sol. .. Saturated aqueous solutioa,
prepared at 20°C.
HDPE pipes can be used for applicatioos in CODe. Il:I Concentrated fluid'
which they are Dot subjected to pressure or
other strcss, but a case in which. certain All cone." Behaviour of tluid over entire ranp
amount of corrosion can be accepted. For of concentration' :
.pplicatioDI :,in which tbey aee exposed to
pttuure" th_ final assessment ahall be on the tl - At least t~bDical .... Irade' purity
hui~ of a~ .u~uent telt uncftMt~pres.~re.",
,r r ,,' I
II .. ,. ~ \ ~I
tt, " ""IJ'~ChDicaJ - grade aOJid
~ '" ... . _.. "
..,-1 .. - Ttchnica1 arade. liquid 0-2.2.4 Senlct T~nt~e ( CoIu.." ~ 1ft 1M
It,.. " .• '. 1 .,. .,'t • . '
t : . -
, :~\ 1"~ ~
t ......l .....~.....
, ~. '. .~
Ttlbk) ';. ....
'Worlc.101.- Workin. solution olth. GOnClDtr..- Test temperatures at which chemical resi.tance
. tion usually used in the industry deterained ( 20°C and 60°C ). ," -" . tl
con_ned.
N.2.5 ClollfllNtlon (Ltul colum" In I .
:Su.p. - Suspension of solid in a saturated Table)
sol ulton at 20°C.
The clieIqical resistance of HDPE pipe materials
The concentrations are expressed as a percent••e il ..iven in accordance with the classification
.by ma.s at 20°C, unlels other wise .tated. s)'ltem AI dtlCl'ibod undor o-z.t above.
,.
i
:
t8-1. 20
60 •L
2. Acetic Acid (KSCA) 17 118 Upto 10 20 I
I
60 S
: 10 to 40 20 S
SO 20 8
40 to 60 20 8
60 L
80 20 8
60 L
3. Acetic Acid, .Iacial 17 118 > 96 20 8
(KSCA) 60 L
.
4. Acetic Anh}dride -73 1-40 t8"1 20 N8
(SSCA 66 NS
I
5. Acetone -95 56 tg-I 20 L
60 L
6. Acrylic emulsion Work sol. 20 S
60 S
7. Adipic acid lSI 338 Sat. sol. 20 S
60 S
8. Air t.-. 20 S
60 S
I 9. Allyl alcohol -129 97 t.-l 20 S
• 60 S
, 10. Aluminium chloride 194 181 All cone. 20 S
( S.2 atm.) (Subl. ) 60 S
11. Aluminium fluoride 1040 1276 Suap. 20 S
(..s.bl. ) 60 S
9
·.,_altN
SI No.
12.
Chemical
Aluminium hydroxide
I ••p.
- R.O
·C
I, ~.~. Cone.
%
SUlp.
Tempo-
...turo
20
·C
aa..ll·
cation
S
.'00 60 8
13. AlulDinium nitrate 73 1'0 Sat~ sol. 20 8
dec. 60 8
14. Aluminium oxychloride 226 8ulp. 20 8
. ..
60 8
10
I
Sat sol.
60
20
S
S
I
i 60 S
45. Barium sulphate I 580 Susp. 20 S
60 S
; 46. Barium sulphide 2227 Sat. 101. 20 S
I 60 S
I
47. Beer Work sol. 20 S
I 60 S
u
"JP~J,.W',
°C .
13
IS t.ua :·1'"
60 S ,
14
IS 143)3 ·1·""
•
SI No. Chemical m. p. b. p. CODe. Tempe- Claslifl.
°c °c 0/0 rature cation
°C
(KSCA) 60 S .
125. Bthyl. acetate (SSCA/P ) - 83 77 tg-I 20 L
60 NS
100 20 S
60 . L
I
128. . Ethyl chloride ( P ) - 136
NS
60
I
I 15
IS IGJJ: 1,"
81 No.
-
Chemica! ~~. b.p.
.oC I
I
C.one.
%
I Tempe-
rature
°c
CI...r-
ficatioD
16
,
8.,10.' .,(.hemical
I ....p.
·C
b.p.
°C
Conc.
%
T...... \
rature
C~lfi.
cahon
·C
';"
Sat, 101. 20 S
60 S
60 20 S
60 L
- j
17
IS 14333: 1996
I~'
81. No. Chemical m.p, CODC~ TeiDp. CI.uiS-
oC percent °C cation
18
i' IS 14333: 1996
-
SI No. Chemical
I ~'l'
bp.
°C
Cone.
%
Tempe- CIa.,ift·
rature
°c
cation
Sat. sol. 20 S
60 S
18S. Mayonnaise Work. sol. 20 S
20 8
60 S
219. Phosphorus ( III ) -92 75 tg-I 20 S
chl~ri~e 60 S
220. Photographic solationl .' 20 S
60 S
221. Pickling baths:
Sulphuric acid 20 S
60 S
Hydrochloric acid 20 S
60 S
Sulphuric- Nitric 20 S
60 NS
222. Picric acid ( Subl ) 122 Set. sol. :0 S
223. Plating solutions
(KSCA ):
Brass 20 S
60 S
Cadmium 20 S
60 S
Chromium 20 S
60 S
Copper 20 S
60 S
Gold 20 S
60 S
Indium 20 S
60 S
Lead 20 S
60 S
Nickel 20 S
60 S
Rhodium 20 S
60 S
Silver 20 S
60 S
Tin 20 S
60 S
Zinc I 20
60
S
S
10·20 20 S
60 S
23
• '14313 : .".
SI No,
263.
Chemical
Silicic acid
"
I m. p.
°C
ISO
b. p.
·C
CODO.
, sol.
Tempe-
ratur.
°C
20
CI.-.i..
ficatioli
S
dec. 60 S
26t Silver acetate dec. Sat. 801. 20
60
. S
S
265. Silver cyanide 320 Sat. 101. 20 S
dec. 60 S
266. .Silver nitrate 212 444 Sat..sol. 20 S
60
S
S
S
268. Sodium acetate 324 Sat. 801. 20 S
60 S
269. Sodium anitmonate 280 Sat. sol. 20 S
dec. 61) S
,270. Sodium arsenite Sat. sol. 20 S
60 S
271. Sodium benzoate Sat. sol. , 20 S
60 S
.~. ' .
" ";,1 '",
,),~. , .
',:r:;
i~;
.
'."
, ',\ "
IS J~333 ._: 19K·
-25
SI No. Chemical m.p. b. p. CODe. tempe- Claisl..
°C °C % rature ficatioD
0(:
SINo.
I Chemical m. p.
·e
b. p.
·C
CODe.
0/0
Tempe-
rature
°C
Clalli-
fic.tion
325. Water 20 S
60 S
326. Water. brackish 20. S
60 S
327. Water, distilled 20 S
60 S
27
IS'I.o33 :'19.94
58 ~o 5
60 S
M,mbers
HYDRAULIC ENGINEER Municipal Corporation of Greater Bombay, Bombay
DEPUTY HYDRAULIC ENOINEER ( Alternate )
SHRI P. S. RAJVANSHl Central Public Health & Environmental Eoaineering OrlanizatioD.
Ministry of Works & Housing, New Delhi
SHRI M. S. NARAYANAN ( Alternate )
DR R. PARMASIVAM National Environmental Engineering Research Institute (CSIR)p
Nagpur
. SHRIMATI S. S. DRAOE ( A ltemate )
SHill M. S. IDNANI Oarware Plastics e.t Polyester Ltd, Bombay
SHRI C. P. SATHE ( Alternate)
SHRIS. PRAKASH Delhi Municipal Corporation, Delhi
CHIEP ENOINEI:R ( C ) (Alternat, )
SHRI S. S. BHANDARI Wavin India Ltd, Ghaziabad
SMRI V. K. SHARMA NOelL, Bombay
SHRI N. N. SHAH ( Alternat,)
CHIF ENGINEER ( PPR & D) U.P. Jal Nigam, Lucknow
MATERIALS MANAGER ( Alternate)
LT COL P. K. MASAND Ministry of Defence, New Delhi
SHRI R. N. SINHA, AEE ( Alternate)
ENGtNE~RINO DIRECTOR Tamil Nadu Water Supply & Drainage Board, Madras
CHIEF ENGINEER ( WESTBRN REGION) (Alternate)
DEPUTY CHIEF ENGINEER Public Health Enaineerinl Department, Government of Kerala,
Trivandrum
DR P. S. RANA Housing and Urban Development Corporation Ltd. New Delhi
SHR) K. SUBRAMANIAM ( Alternate)
SCIENTIST Central Building Research Institute ( CSIR ), Roorkee
SHRI SUDHESH KUMAR SHARMA ( Alternate)
SHRf K. L. KHANNA EPC Irrigation Ltd, Bombay
SHRI VINAYAK V. SHEMBEKAR ( Alternate )
SHRI R. B. DOC10R Ahmedabad Municipal Corporation, Ahmedabad
SHRI R. A. PATEL (Alternate)
DR H C. MRUTHYUNJAYA Jain Plastic and Chemicals, Jalgaon
SHRI S. NARAINASWAMY (Alternate)
SHRIMATI SE2MA VAIDYA Graphite Vicarb India Ltd, Nasik
SHRI A. SAMANTA ( Alternate)
DR DHANANJAY RAU Finolex Industries Ltd, Pune
SHRIR.C. CHOUDHRY Office of the Chief E.ngineer, Public Health, Orissa, Bhubanesbwar
SURI GULAM AHMED Public Health Engineering Zone, Government of Karnataka,
Karnataka
SHRf RAJENDRA PRASAD Directorate General of Supplies & Disposals, New Delhi
SHRf JAY KUMAR ( Alternate )
SHRl V. K. JAIN Public Health Engineering Department, Government of Rajasthan
Jaipur "
SHRt M. K. M. Joshi ( Alternate)
CHIEf ENGINEER ( DESIONS ) Central Public Works Department, New Delhi
SUPERINTENDING ENGIN£3R ( S & S ) ( Alternate)
SHRI WILLIAM MENDONCA Supreme Industries Ltd, Bombay
SHRI H. D. V JiDAV ( Alternat« )
SHRf G. K. LALCHANDANI Central Institute of Plastics Engineering and Technology, Madras
DR A. P. DAs ( Alternate)
SHRI D. K. SANYAL Calcutta Municipal Corporation, Calcutta
SaRI A. K. BrswAS ( Alternate )
DR S. M. PATEL Institute of Co-operative Management, Ahmedabad
DR M. K. PANDEY ( Alternate)
SHRI C. K. SHAtMA RITES. New Delhi
DIRECTOR ( MATERIALS MANAGEMBNT ) Delhi Development Authority, New Delhi
SUPERINTENDINO ENOINEBR ( DESIGNS) ( Alternate)
SHRI K. P. NANAVATY Reliance Industries Ltd, Bombay
Dr Y. N. SHARMA ( Alternate)
SHRI O. P. RATRA Buildinl Materials and Technology Promotion Council (Ministry
of Urban Development ), New Delhi
SHRIO. K. SRINIVASAN Vimplex India Pvt Ltd, Madras
DR S. SUNDERANOORTHY Madras Metropolitan Water Supply and Sewerage Board, Madral
SHRI THIMU O. SHBNBAGAWANDAM ( Alternate )
SBRI S. SUNDARAM KWH HeUplastics ( India) Ltd, Bombay
SHIU H. N. PRADNIS ( ~/tl,nate )
S8RI VINOD KUMARr Director General, BIS ( EX-Dfficio M,mber )
DIRECTOR cl Beaa ( Civil Enl. )
S,c"tar,
SRRIR. S. JUNBJA
Joint Director ( ci-n Boal ), BIS
( COllt/II"td "" /MIe 29 )
29
PaDel for Polyethylene Pipes, CBO 50: P4
COllve",r
SRRI KANWAR A. SINOR
R,prel'"
RITES. New Deihl
'I",
Member,
5Hal V. IC. SHARMA socn, Bombay
SHRI M. S. DAn ( ~1/,rnQt. )
SHIU K. L. KHANNA EPC Irriaation Ltd, Bombay
SHRI SH8M 81UR ( AII,r"al, )
V. V.
DR Y. N. SHARMA Reliance IDdultries Ltd, Bombay
SHRI JAGMOHAN BAMRI ( ~11,r1Ul1' )
DR H.C. MRUTHYUNJAYA Jain Plastic & Chemical., Jal ••on
SHRI S. NARAINASWANI ( .411,rll"'. )
SHRIS. SUNDARAM KWH Heliplaitici ( India) Ltd, Bombay
SHRI N. N. PHADNIJ ( Alt,rnal.)
SHRI S. PaAKAIH DWS & SDU. New Delhi
SHRI ANAND PRAKASH ( Allerna/e)
LT COL P. K. MASAND EDlineer-ia-Cbief's DraDeb, Ministry of D.Cooce, New Delhi
SSRI R. N. SINHA ( Alternale )
SHRI O. P. RATRA BMTPC, New Delhi
ENGINBERING DIRECTOR Tamil Nadu Water Supply" Drain_lo Board, Madra
CHIEF ENGINEER ( SPO) CPWD, New Delhi
SUPERINTENDING ENGINEER ( S AS) ( Alternate )
DR KIRTIVAN D. KOTLAN Manity. PlasticheJ:!l" Mysore
SHRI J. B. S. DAKSRI Uniplaa IDdia Ltd, New Delbi
SHRI R. K. KAPUR ( Alternate )
SHRI DILBARIIH BAHADUR IDler-link Services Pvt Ltd. New Delhi
Bureauof IndiaD StlDdard.
BIS is a statutory institution established under the Bureau 01 Indian Standards Act. 1986 to
promote harmonious development of the activities of standardization, marking and quality
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any form without the prior permission in writing of BIS. This does not preclude the free use, in
the course of implementing the standard, of necessary details, such' as symbols and sizes, type or
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Review of Indian Standards
Amendments are issued to standards as the need arises on the basis of comments. Standards are
also reviewed periodically; a standard along with amendments is reaffirmed when such review
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