F.

Tools And Materials

a. Tools
1. Pipettes 10 pieces
2. Test tube 12 pieces
3. Erlenmeyer 250 ml 2 pieces
4. Erlenmeyer 100 ml 1 piece
5. Spatula 1 piece
6. Reflux 1 piece
7. Vial 21 pieces
8. Analytical balance 1 pieces
9. Beaker glass 100 ml 1 piece
10. Beaker glass 250 ml 2 pieces
11. Stative and clamps 1 piece
12. Plastic pipe sufficiently
13. Stopwatch 1 piece
14. Thermometer 1 piece
15. Mold 3 pieces
16. Burrete 50 ml 1 piece
17. Brown burrete 50 ml 1 piece
18. Hot plate 1 piece
19. Measured glass 10 ml 1 piece
20. Tripod 1 piece
21. Gauze 1 piece
22. Rack 1 piece
23. Clamp 1 piece
24. Bunsen 1 piece
b. Materials
1. NaOH solid 3,2 grams
2. Aquades sufficiently
3. Coconut oil 17 grams
4. Palm oil 17 grams
5. Bulk oil 17 grams
6. Stearic acid solid 3 grams
 7. Alcohol 36 grams
8. Glycerin 12 grams
9. Olive oil 3 ml
10. Dye sufficiently
11. Fragrance sufficiently
12. Ethanol 75 ml
13. PP indicator sufficiently
14. KOH standar 0,1 N sufficiently
15. KOH alcoholic 0,5 N 75 ml
16. HCl standar 0,5 N Sufficienty
G. Lanes Work
1. Making Soap
a. Make NaOH solution

1,4 grams of NaOH

1. Dissolved in 3,3 mL of
water
NaOH Solution

b. Making soap with coconut oil

10 grams of Coconut Oil

1. + 1 gram of tearic acid

2. Heat until 70°C and all of stearic acid melts
3. let this mixture until 50°C
4. + NaOH solution
5. stir it
6. + 12 grams of alcohol
7. + 4 grams of gliceryn
8. Heat and stir it, unil the solution become colorless
9. let this mixture become cooler
10. + 1 mL of olive oil
11. Pour into the mold

Soap
 c. Making soap with palm oil
10 grams of Palm Oil

1. + 1 gram of tearic acid

2. Heat until 70°C and all of stearic acid melts
3. let this mixture until 50°C
4. + NaOH solution
5. stir it
6. + 12 grams of alcohol
7. + 4 grams of gliceryn
8. Heat and stir it, unil the solution become colorless
9. let this mixture become cooler
10. + 1 mL of olive oil
11. Pour into the mold

Soap

d. Making soap with bulk oil

10 grams of Bulk Oil

1. + 1 gram of tearic acid

2. Heat until 70°C and all of stearic acid melts
3. let this mixture until 50°C
4. + NaOH solution
5. stir it
6. + 12 grams of alcohol
7. + 4 grams of gliceryn
8. Heat and stir it, unil the solution become colorless
9. let this mixture become cooler
10. + 1 mL of olive oil
11. Pour into the mold

Soap

2. Emulsion Properties of Soap

a. Coconut Oil
 3 mL of aquades
1. + 5 drops of coconut oil
2. + 2 mL of soap solution
1 mL (0,1 – 0,2 g soap
which dissolved in 6-8
mL of hot water)
3. Shake it strongly
4. Wait a minute
5. Record the time
Solution become 2
layers
b. Palm Oil
3 mL of aquades
1. + 5 drops of palm oil
2. + 2 mL of soap solution
1 mL (0,1 – 0,2 g soap
which dissolved in 6-8
mL of hot water)
3. Shake it strongly
4. Wait a minute
5. Record the time
Solution become 2
layers
c. Bulk Oil
3 mL of aquades
1. + 5 drops of Bulk oil
2. + 2 mL of soap solution
1 mL (0,1 – 0,2 g soap
which dissolved in 6-8
mL of hot water)
3. Shake it strongly
4. Wait a minute
5. Record the time
Solution become 2
layers
3 mL of aquades
1. + 5 drops of
coconut oil
2. Shake it strongly
4. Wait a minute
5. Record the time
Solution become 2
layers
3 mL of aquades
1. + 5 drops of
palm oil
2. Shake it strongly
4. Wait a minute
5. Record the time
Solution become 2
layers
3 mL of aquades
1. + 5 drops of
Bulk oil
2. Shake it strongly
4. Wait a minute
5. Record the time
Solution become 2
layers
3. Acid Number
a. Coconut Oil

5 grams of coconut oil

1. + 25 mL ethanol
2. + 5 drops of indicator PP
3. Titration with KOH 0,1 N
as a standart solution
4. Repeat it 3 times

Volume of KOH
5. counted the number of acid
Acid Number

b. Palm Oil

5 grams of palm oil

1. + 25 mL ethanol
2. + 5 drops of indicator PP
3. Titration with KOH 0,1 N
as a standart solution
4. Repeat it 3 times

Volume of KOH
5. counted the number of acid
Acid Number

c. Bulk Oil

5 grams of bulk oil

1. + 25 mL ethanol
2. + 5 drops of indicator PP
3. Titration with KOH 0,1 N
as a standart solution
4. Repeat it 3 times

Volume of KOH
5. counted the number of acid
Acid Number
4. Saponification Number
a. Coconut Oil

10 grams of Coconut Oil

1. + 25 mL KOH alcoholic
0,5 N
2. Refluxed for 30 minutes
3. Cooled & + 5 drops
indicator PP
4. Titration with standart
solution HCl 0,5 N
5. Repeat it 3 times
6. Counted the saponification
number

Saponification Number

b. Palm Oil

10 grams of Palm Oil

1. + 25 mL KOH alcoholic
0,5 N
2. Refluxed for 30 minutes
3. Cooled & + 5 drops
indicator PP
4. Titration with standart
solution HCl 0,5 N
5. Repeat it 3 times
6. Counted the saponification
number

Saponification Number
c. Bulk Oil

10 grams of Bulk Oil

1. + 25 mL KOH alcoholic
0,5 N
2. Refluxed for 30 minutes
3. Cooled & + 5 drops
indicator PP
4. Titration with standart
solution HCl 0,5 N
5. Repeat it 3 times
6. Counted the saponification
number

Saponification Number