Procedure

1. The stirrer was set up in the MDI beaker.

2. Polymeg-bitanediol mixture was added while continuous stirring in the MDI. The power of the
stirrer was increased as the viscosity rises.
3. The temperature was recoded and measured every 15 second.
4. The agitation was stopped after 4 minutes or when 2 consecutive temperature reading are the
same.
5. The stirrer was remove and poured into a pre-coated aluminum pan.
6. The polymer was spread to a thin layer and cooled quickly in ice water.
7. The polyurethane was weighed and recorded.
8. The structure of polyurethane structure was observed using a microscope.