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Defence Technology xxx (2018) 1e13

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Defence Technology
journal homepage: www.elsevier.com/locate/dt

Ballistic impact properties of woven bamboo- woven E-glass-


unsaturated polyester hybrid composites
Aidy Ali a, *, Rabiatun Adawiyah a, Kannan Rassiah b, Wei Kuan Ng a, Faiz Arifin a,
Faiz Othman a, Muhammad Shauqi Hazin a, M.K. Faidzi a, M.F. Abdullah a,
M.M.H. Megat Ahmad a
a
Department of Mechanical Engineering, Faculty of Engineering, Universiti Pertahanan Nasional Malaysia (UPNM) National Defense University of Malaysia
(NDUM), Kem Sg. Besi, 57000, Kuala Lumpur, Malaysia
b
Department of Mechanical Engineering, Politeknik Port Dickson (PPD), KM 14, Jalan Pantai, Si Rusa, Negeri Sembilan, Malaysia

a r t i c l e i n f o a b s t r a c t

Article history: In this study, a laminated woven bamboo/woven E glass/unsaturated polyester composite is developed to
Received 16 July 2018 combat a ballistic impact from bullet under shooting test. The aim of this study is to understand the
Received in revised form fundamental effects of the woven bamboo arrangement towards increasing ballistic resistance proper-
28 August 2018
ties. The work focusses on the ballistic limit test known as NIJ V50, which qualifies materials to be
Accepted 4 September 2018
Available online xxx
registered for use in combat armor panels. The results show that the composites withstood 482.5 m/s ± 5
limit of bullet velocity, satisfying the NIJ test at level II. The findings give a strong sound basis decision to
engineers whether or not green composites are qualified to replace synthetic composites in certain
Keywords:
Woven bamboo
engineering applications.
E glass © 2018 Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://
Hybrid composites creativecommons.org/licenses/by-nc-nd/4.0/).
Ballistic limit velocity
Energy absorption

1. Introduction America, the role of bamboo in construction industrial and


component has been stimulated by widespread availability in the
Natural fibers are generally obtained from animal, plant, or tropical and subtropical climate regions. Fast growth and combi-
mineral sources. The development of fiber composites using plants nations with other raw material have developed composites with
has attracted interest. Bamboo is especially of interest as the fiber is high mechanical strength and low specific weight. The replacement
ecofriendly and helps in fixing carbon dioxide. These characteristics of natural fibre composites for synthetic fibre reinforced plastics
have made bamboo an important plant fiber, with a high growth has grown significantly due to lower cost and improved sustain-
rate and availability. About 1000 species of bamboo grow abun- ability, which includes both advantages and disadvantages [2]. The
dantly in South America and Asia [1]. Sustainable and recyclable structural community has great interest in natural-based rein-
composite materials from the utilization of bamboo are obviously forced composites, as they offer good mechanical properties,
in high demand from consumers and industry due to excellent recyclability, and environmentally-sustainable production and use.
performance. Since 2015, bamboo composites have become new green ma-
Bamboo is a fast-growing, perennial, abundant bio-resource terials that are widely used and explored by researchers. A review
belonging to Barbusse, a genus under Gramineae. Researchers on thermomechanical behavior of bamboo is detailed in
have increasingly developed their expertise by applying many Refs. [3e8]. In 2014, Kannan et al. [7] successfully mapped the
types of different materials from bamboo fibers to generate high mechanical properties of bamboo in 3 dimensional views that
end quality sustainable industrial product. In Asia and South allowed researchers to evaluate the most maximum performance
of bamboo parts in term of mechanical properties. Later, the
research explores on developing bamboo in form of strips then
make them into woven to produce a layer of bamboo [9e12].
* Corresponding author.
Moreover, Kannan and Aidy et al. [13] successfully study the per-
E-mail address: saidynaidy@gmail.com (A. Ali).
Peer review under responsibility of China Ordnance Society formance of these bamboo composites in dynamic properties that

https://doi.org/10.1016/j.dt.2018.09.001
2214-9147/© 2018 Published by Elsevier Ltd. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

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2 A. Ali et al. / Defence Technology xxx (2018) 1e13

is call fatigue and fracture of the bamboo. Such information is vital viscosity of 450e600 cps, a volumetric shrinkage of 8%, and an acid
to allow engineers to decide whether or not to apply bamboo value of 29e34 mg KOH/g for the solid resin. This type of resin is a
composites in their engineering components, especially as a new rigid, minimally reactive, and thixotropic general-purpose
construction material. orthophthalic unsaturated polyester resin. It is easily pre-
There has been tremendous improvement in the design of bal- promoted for an ambient temperature cure with the addition of
listic protective materials, which have been in use from time im- methyl ethyl ketone peroxide (MEKP) as the catalyst. Additionally,
memorial. Developments in the technology of manufacturing high it is conveniently workable in hand lay-up applications and offers
performance fibers and production processes have enabled the easy air release.
production of light weight body armor with improved protection
levels. Such composites and fabrics have been a good replacement
2.2. Bamboo
for modern armor material in place of high-density metals and
alloys. Body armor is designed to protect the human torso by pre-
The bamboo species used in these tests was Gigantochloa
venting penetrating threats and internal damage. The actual per- Scortechinii (Buluh Semantan), collected from Kampung Bukit Lar-
formance of armor is measured in terms of the interaction between
ang in Malacca, Malaysia. Bamboo plants were cut into lumber strip
the armor and human torso. The effectiveness of armor against fiber parts using a cleaver and a hand saw. The strips were cut by
non-penetrating threats also should be considered in this case.
knife to thicknesses of 1.5 mm, then woven into a fabric (see Fig. 1).
Modern body armor can be classified as either hard body armor The reason for using 1.5 mm thicknesses was previously described
or soft body armor. Categories of body armor can be differentiated
in Ref. [9].
in terms of material. Hard body armor has greater protection level
compared to soft body armor. A hybrid system consists of layers of
ceramics and fabrics bonded together and serves the specific pur- 3. Fabrication of composites
pose of preventing projectile penetration. Hard body armor mostly
used by law enforcement officers and military personnel as it offers The materials, including woven bamboo (WB), woven E-glass
high level of threat protection. However, soft body armor is greatly (WEG) and unsaturated polyester (UP), were used to fabricate
preferred as it provides adequate protection and is more flexible woven Bamboo/woven E-glass hybrid composites. Two different
when moving [14]. Designing a ballistics materials from composites layer configurations of Bamboo/E-glass/UP hybrid composite were
are now becoming more popular because of its promising results fabricated. Table 1 shows the configurations and properties of the
and achievements [27]. Very limited work on ballistic was reported developed composites.
and the recent study by Renato Batista da Cruz et al. [28] success- The layering process of WB, WEG and UP was divided into three
fully developed and characterized a giant bamboo fiber reinforced stages. First, woven bamboo was dry in a MEMMERT BASIC Uni-
epoxy composite for multilayer ballistic armor. It was reported the versal Oven-UFB 400e500 at 60  C for 6 h to reduce moisture to
performance increase 22% compared with aramid fabric. strengthen the adhesion between unsaturated polyester resin. Af-
In this study, woven bamboo has been combined with woven E ter 6 h of heating, the average moisture content of strips of woven
glass fiber to combat the ballistic impact of bullets. The aim of this bamboo reached about 20%.
study is to understand the correlation and fundamental effects of Then, WB and WEG were subjected to the hand lay-up process
the woven bamboo arrangement towards increasing the ballistic to form laminate. WEG was laminated with its respective layers
limit of a green bamboo composites. The work is focusses on the according to the specified configuration, followed by lamination of
ballistic limit test known as V50 and NIJ that qualifies materials for WB with its respective layers. Before lamination, WB and WEG
use in combat armor panels or materials. The measurement and were cut squares with dimensions of 300 mm  300 mm. Then, 6
testing of ballistic limit on other natural woven can be studied in WB and 9 EG were weighted separately to obtain their respective
Ref. [15]. There has been numerous work on ballistic properties of weights. The weights of 6 WB and 18 WEG are shown in Table 2.
hybrid composites of synthetic fibers. However, there are limited After obtaining the weight of fibers, the amount of unsaturated
work reported on measurement of ballistic limit on natural fibers. polyester (UP) needed to produce Woven Bamboo/Woven E-glass/
However, none of the reported work has performed measurements UP hybrid composites can be determined. Total weight of UP
of the ballistic limits of woven bamboo composite. This study needed are sum of 200% of total weight of woven bamboo and 60%
provides the ballistic limits of hybrid woven bamboo/woven E of total weight of Woven E-glass. Hence, for each configuration of
Glass. The failures modes of the shooting damage are also analyzed. Woven Bamboo/Woven E-glass/UP hybrid composites as shown in

2. Materials

The materials used in this study are “unsaturated polyester”


(UP) as the matrix material and “Woven bamboo fiber” (WB) and
‘Woven E-Glass fiber’ (WEG) as the filler fiber. The mechanical
properties of fabrics are strongly influenced by the warp and weft.
Dense fabrics tend to have higher bending, shear and tensile ri-
gidity. In this study, for the woven bamboo using combination of
Weft (30 thread/cm) and Warp (60 thread/cm) and for the E Glass
using combination of Weft (40 thread/cm) and Warp (66 thread/
cm).

2.1. Unsaturated polyester

The matrix system consists of Reversol P-9509 unsaturated


polyester (UP) supplied by the Synthomer (Malaysia) Sdn. Bhd.
Company. Reversol P-9509 has a specific gravity of 1.12 at 25  C, a Fig. 1. Woven-fabric laminated bamboo.

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Table 1
Configurations and properties of bamboo/E-glass/UP composite.

Types of layer arrangement Number of layers of each material Total layers Dimension (length*width*height)/mm
*WB ¼ Woven bamboo
*EG ¼ E-glass

WB/EG 4/18 22 300*300*18


EG/WB/EG 9/4/9 22 300*300*18

Table 2 accordingly to the recorded speed in the NIJ standard as summa-


Weight of fiber. rized in Table 3.
Types of fiber Quantity of layer Total weight/kg

Woven bamboo 4 0.329


4.3. Velocity measurement device
Woven E-glass 18 0.591
To measure the velocity of the bullet, 2  Portable PRO CHRONO
velocity devices were used. The first device was placed at 2.67
Table 2, 1.0126 kg of UP is needed. from the test gun while the second device is then placed at 0.78 m
Then, the PVC film was placed on the flat table. Then, a release from the target in accordance to the standard as shown in Fig. 5. All
agent, Silicon, was used to spray the surface of PVC film in order to setup was performed to ensure that the ballistic limit test is
ease the removal of laminate composite after the lamination pro- perform successfully as shown in Fig. 5. According to the V50
cess is done. UP type Reversol P-9509 is then mixed with methyl standard for armor, the mounting fixtures, frame support and
ethyl ketone peroxide (MEKP) with the weight ratio of 100 UP:1 clamps must be able to retain the sample and withstand the shock
MEKP. They were stirred until the color of mixture changed from resultant due to the ballistic impact of test projectiles. The sample
light white to clear yellow. After that, the mixture was brushed in was capable of being adjusted in the vertical or horizontal di-
one direction onto the PVC film. Then, a piece of woven E-glass was rections to make it easy to locate the point of impact anywhere on
placed immediately on top of the PVC film. The mixture was once the sample.
again brushed in one direction on the woven E-glass. The process
was repeated for several layers of WEG as needed in the configu- 4.4. Shooting test procedure for V50
ration described in Table 2. After lamination of WEG, WB was
placed on top of the piled up laminated layer of woven WEG and The test targets were assembled and measured according to the
brushed with the mixture in one direction. The process was test range configuration in the 0101.06 NIJ Standard (see Fig. 5). A
repeated for the 6 layers of WB. The above process was repeated for test round was fired through the paper behind the frame after
several layers of woven bamboo and WEG. The final step was to replacing the witness plate to determine the exact point of impact.
place a 10-kg load on the composite and store the composite at Additional rounds were fired as required until the proper alignment
room temperature for a period of 24 h to allow gelling and curing to and a stable striking velocity were achieved. A 9 mm bullet was the
progress. After 24 h, the load was removed and the WB/WEG/UP first firing was loaded with certain striking velocity and either
hybrid composites were formed. Fig. 2 (a) to (d) illustrate the complete penetration or partial penetration were established.
fabrication process of WB/WEG/UP hybrid composites with con- After obtaining 6 complete penetrations and 6 partial penetra-
figurations of 6 BW and 18WEG. tions, sample 1 (18 layers of Woven Bamboo and 4 layers of Woven
E-glass) was replaced with Sample 2 (9 layers of E-glass, 4 layers of
Woven Bamboo and 9 layers of Woven E-glass).
4. Ballistic limit testing (V50)
5. NIJ test
The ballistic limit test for laminated WB/WEG/UP hybrid com-
posites was experimentally determined using standard equipment
The NIJ standard impact test was conducted using a single stage
in Kompleks Persenjataan Pusat Sains Dan Teknologi Pertahanan
gas gun to propel the projectile through a long panel 4 m and 9 mm
Bahagian Teknologi Persenjataan, STRIDE Batu Arang. This section
in diameter, as shown in Fig. 6. There are four main parts to the
provides details of the equipment and methods in this testing.
single stage gas gun apparatus, the gun barrel, a pressure reservoir,
the catch chamber and the computer software system. The gun
4.1. Test gun barrel was designed as a long cylindrical vessel of 4 m length,
ensuring that the projectile slides through and shoots the target.
Testing used 9 mm test barrel (PROTOTYPA) test gun as shown The barrel has a very smooth interior surface in order to reduce
in Fig. 3. The purpose of using a test gun rather than a normal friction with projectiles. The gas gun used compressed helium gas
mounted gun is because it gives precise results for shooting. to fire the projectile. The velocity of the projectile was controlled by
the gas pressure. Nine samples for each testing condition were
4.2. Bullet considered to ensure good data repeatability. The gas gun was
connected to a ballistic data acquisition system.
The 9 mm bullet is the commonly-used round fired from pistols The target with dimensions 100  100 mm was placed at square
and sub machine guns. In this ballistic test, the bullets used iron frame with circular hole uphold tightly to be tested. Nuts and
weighed of 7.45 g as depicted in Fig. 4. bolts clamped the frame to prevent the specimen from moving out
According to level IIIA standard of National Institute of Justice of the impacted targets. The impacted signal was calculated to
(NIJ 0101.06), the rifles utilized were 357 Magnum JSP and 9 mm include the velocity of projectiles obtained by means of measuring
FMJ. All jacket materials were mostly made up of copper alloy the time interval for the projectiles passing through reference
consisting of 90% copper and 10% zinc with lead cure that alloyed point. First, the pressure was set to 151 bar, which is considered the
together with hardening material. The projectiles were shoot highest pressure with maximum volume of helium gas in the tank.

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Fig. 2. Laminating process.

Then, the tests were repeated with pressures of 140 and 130 bar 6. Results and discussion
three times to obtain the average velocity. Having performed the
test, the failure of the developed composites can be seen obviously 6.1. V50 ballistic velocity results
using naked eye. To make the image clearer, a stereo microscope
was used to magnify the failure and damage on the specimen. The ballistic limit or V50 is commonly defined as a 50%

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with increments for an expanding number of ballistic tests [19]. It is


a generally utilized rule for surveying the effectiveness of defensive
layer.
The results of the shooting tests were collected to determine the
ballistic limit for 18 layers of Woven Bamboo and 4 layers of Woven
E-glass (4:18 WB:WEG); and 9 layers of E-glass, 4 layers of Woven
Bamboo, and 9 layers of Woven E-glass (9:4:9 WEG:WB:WE-
G),respectively. The results for (4:18 WB: WEG) are tabulated in
Table 4.
Table 4 shows the outcomes of up-and-down firing of V50 bal-
listic limit for 18 layers of Woven Bamboo and 4 layers of Woven E-
glass (18:4 WB:WEG). The amount of propellant for various effect
velocities was resolved through an experimental method by
adjusting the mass of the propellant, which is the explosive mass.
Fig. 3. Test gun for shooting. The propellant fills for the shots and next shot were adjusted until
at least three partial penetrations and three complete penetrations
were achieved [l8]. The first velocity was tested higher than
probability of penetrating a target that given impact velocity. It is an reference velocity of 390 m/s. According to the V50 Ballistic Test for
average from the highest partial penetration and complete pene- body armor [40], the first striking velocity must be above the base
tration of velocities. The amount of propellant for different impact prerequisite. The outcome acquired from the first firing of velocity,
velocities has been determined through an empirical method by 390 m/s, was partial penetration, followed by the second strike,
adjusting the mass of the propellant. As indicated by US MIL-STD- 359 m/s and third of striking velocity, 470 m/s consisting of the
662F, V50 might be ascertained by taking the arithmetic mean of same explosive mass. The sample still produced a partial penetra-
equal number of highest partial and lowest complete penetration of tion result when the velocity was increased to 470 m/s, with a
impact velocities. The ballistic limit velocity (V50) was estimated weight of explosive mass of 0.41 g for the next firing. However, at a
during experimental data on the basis of whether the projectile velocity of 480 m/s with 0.50 g, perforation occurred through the
penetrated the hybrid composite either completely or partially. It is sample. Thus, complete penetration was obtained.
the most broadly perceived apparatus to determine the ballistic The velocity was increased to 488 m/s with diminishing explo-
execution of a material, for instance, precision of the estimation, sive mass to 0.48 g, which indicated partial penetration on the

Fig. 4. Bullet use for Test.

Table 3
NIJ standard 0101.06 PeBFS performance test summary [16e18].

Test variables
Armor type Test round Test bullet Bullet weight Reference velocity/(m$s1)
I 1 .22 Caliber LR 2.6 g 329
LRN 40 gr
2 .380 ACP 6.2 g 322
FMJ RN 95 g
IIA 1 9 mm 8.0 g 341
FMJ RN 124 gr
2 40 S&W 11.7 322
FMJ 180 gr
II 1 9 mm 8.0 g 367
FMJ RN 124 gr
2 .357 Magnum 10.2 g 436
JSP 158 gr
IIIA 1 9 mm 8.2 g 436
FMJ RN 124 gr
2 44 Magnum 15.6 g 436
SJHP 240 gr
III 1 7.62 mm NATO 9.6 g 838
FMJ 148 gr
IV 2 .30 Caliber 10.8 g 869
M2 AP 166 gr

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Fig. 5. Setting up of the sample.

Fig. 6. The gun barrel with high speed camera.

sample. In order to obtain complete penetration again, the velocity (9:4:9 WEG: WB: WEG) configuration was found in the range of
was increased to 498 m/s along with increasing weight of 0.49 g. 414.5 m/s ± 5.
The bullet managed to penetrate the 18 layers of WB and 4 layers of
WEG successfully. By utilizing a similar speed but decreasing mass 6.2. NIJ test results
by just 0.05 g, complete penetration once again occurred. The ve-
locity was decreased to 490 m/s, 486 m/s and 484 m/s along with Impact and absorbed energy are two primary parameters used
the decreasing of weight of 0.483 g, 0.48 g, and 0.47 g, respectively. to evaluate the ballistic impact properties of hybrid composite in
The complete penetration results were recorded all throughout the agreement with the NIJ 0101.06 standard. The test specimens of
sample. For the last shot, the velocity was decreased to 477 m/s and 10  10 cm of laminated hybrid Woven Bamboo/Woven E-glass fi-
finally partial penetration was obtained. ber were subjected to ballistic impact in order to evaluate the
By taking at the velocity of 488 m/s and 477 m/s, the average compressed gas gun impact data measurement capability. The
velocity obtained was 482.5 m/s ± 5 m/s. The average obtained is impact velocity of a projectile highly influences the performance of
the value of limitation for (18:4 WB:EG). This gives the ballistic the protective systems [20]. According to Ridhwan et al. [21], a
limit of this materials. The value obtained is in the range between couple of components influence parameters such as the projectile
the velocities where penetration occurred. Therefore, the limitation and target geometry, the strike velocity and energy and the impact
of (18:4 WB: WEG) can be found at a value of 482.5 m/s ± 5. angle of the projectile toward the target area. Some of these vari-
The results of (9:4:9 WEG: WB: WEG) sample are tabulated in ables are examined in this section. Fig. 10 shows the shooting
Table 5. For the 9 layers of E-glass, 4 layers of Woven Bamboo and 9 experiment in which the bullets hit the target.
layers of Woven E-glass (9:4:9 WEG: WB: WEG) result, only 8 In this test, the 18 layers of E-glass with 4 layers of woven
striking velocities managed to undergo the firing test. This is bamboo (18:4 WB:EG) were utilized and explored to determine
because the sample failed and reached the limitation of integrity. whether or not the composites had the capacity to reach level IIIA
The sample could not withstand the high impact of projectiles. In of NIJ test under high velocity impact test and type of failure form
the first firing at a velocity of 454 m/s with the weight of explosive toward target area. The tests were conducted using hemispherical
mass of 0.41 g, complete penetration occurred. The velocity was bullet which is made of mild steel with different pressure applied.
reduced to 365 m/s, 421 m/s, and 417 m/s and partial penetration The minimum velocity was set at 436 m/s as required for NIJ level
was successfully obtained. However, when the velocity was IIIA [19].
increased to 476 m/s with value of explosive mass at 0.45 g, com-
plete penetration occurred. The striking velocity again was reduced 6.3. Energy absorption
to 441 m/s and 428 m/s with weight values of 0.40 g and 0.39 g,
respectively. The tests resulted in complete penetration. With the For each test, the impact energy was calculated by referring to
similar velocity but lower weight of 428 m/s and 0.385 g, partial the muzzle velocity [22]. Energy absorption in relation to impact
penetration was obtained. velocity is interpreted in terms of striking velocity, or the amount of
The velocity at 421 m/s and 417 m/s were calculated to deter- kinetic energy absorbed by the composite material. Projectiles
mine the approximate average of velocity which valued at 414.5 m/ which pass through the panel are considered to have achieved
s ± 5. The average velocity was determined from the velocity where complete penetration (CP), whereas the others are characterized as
partial penetration has occurred. The ballistic resistant limitation of being partial penetration (PP). The energy absorbed by the fabric is

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Table 4
Result of V50 test for (4:18 WB:WEG).

Location number Velocity/(m$s1) Location Explosive mass/g Type of penetration Front face Back face

1 390 Lot 12A 0.39 Partial penetration

2 359 Lot 13 0.39 Partial penetration

3 420 Lot 19A 0.39 Partial penetration

4 470 Lot 19B 0.41 Partial penetration

5 480 Lot 19B 0.50 Complete penetration

6 488 Lot 19B 0.48 Partial penetration

7 498 Lot 19B 0.49 Complete penetration

8 498 Lot 19B 0.485 Complete penetration

(continued on next page)

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Table 4 (continued )

Location number Velocity/(m$s1) Location Explosive mass/g Type of penetration Front face Back face

9 490 Lot 19B 0.483 Complete penetration

10 486 Lot 19B 0.48 Complete penetration

11 484 Lot 19B 0.47 Complete penetration

12 477 Lot 19B 0.45 Partial penetration

equal to the residual energy amount subtracted from total impact reached was 372 m/s as tabulated in Table 6 the minimum velocity
energy. When bullet found penetrates through the sample, Equa- is only 372 m/s. Thus, for this test, the ability for sample to with-
tion (1) can be expressed as stand the bullet only can reach the level II.
A hemispherical bullet provides higher impact force than the
1  2 2
 other available bullets, including ogival and conical shape bullets
E¼ m Vimp  Vres (1) [22]. Air resistance was neglected while running the experiment.
2
The recording cylinder pressure date represents the applied pres-
If no penetration occurs to completely capture the kinetic en- sure at the projectile end. Consequently, the propellant force can be
ergy of the bullet, the residual velocity will be equal to zero, as estimated according the following equation
expressed in Equation (2) below
Propellant force
1 P applied ¼ (3)
E¼ mV 2 (2) Projectile Cross Section Area
2
The dynamic energy that require to propel the projectile
It was observed that the initial of pressure applied led to
through the long panel of the ballistic gun machine of 4.00 m in
increasing speed of the projectile.
length is clarified in the equation below
Fig. 7 depicts the velocity of the projectile versus the energy
absorption in the sample tests. Cylinder gas pressure represents the
Propellant force ¼ Papplied x Projectile Cross Section Area
applied pressure at the projectile end. Three specimens were tested
repeatedly to estimate the effectiveness of each sample. This clar- (4)
ified the higher levels of energy absorption of the targets shot by
The initiation velocity ðVi ) can be estimated from the propellant
each hemispherical bullet. The data was contrasted with the min-
energy and the mass of the bullet
imum speed toward reaching level IIIA according to NIJ 0101.06
Standard [19]. At impacting velocity of 349 m/s, the energy ab-
1
sorption was only 0.323 which was the lowest among the others. Propelling Energy ¼ mV 2 (5)
Meanwhile, at the velocity of 355 m/s and 372 m/s, the energy 2
absorption is increasing to 0.334 J and 0.368 J respectively. The re- Essentially, pressure affects damage size, causing several types
sults generally exhibit expanding linear energy absorption with an of failure related to projectile speed. The flat end surfaces can in-
increase of impact velocity. According to the NIJ 0101.06 standard, crease projectile resistance against target hardness and reduce
the requirement minimum velocity to reach level IIIA is 436 m/s. projectile deformation as a factor of successful penetration.
During the test, the maximum velocity obtain for projectile can be As indicated by Zainab et al. [22], the hemispherical projectile

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Table 5
Result of V50 Test for (9:4:9 EG:WB:EG).

Location number Velocity/(m$s1) Type of penetration Explosive mass/g Location Front face Back face

1 454 Complete penetration 0.41 Lot 19B

2 365 Partial penetration 0.41 Lot 13

3 421 Partial penetration 0.38 Lot 19A

4 417 Partial penetration 0.38 Lot 19A

5 476 Complete penetration 0.45 Lot 19A

6 441 Complete penetration 0.40 Lot 19A

7 428 Complete penetration 0.39 Lot 19A

8 428 Partial penetration 0.385 Lot 19A

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projectile propelling.
The multi-shot of bullets which propelled to the target area of
the sample resulted penetration at certain velocities. The front face
was observed to experience deformation caused by the failure
mode. The damaged and perforation of bullet can be minimized by
controlling and optimizing the velocity of each projectile. At points
5, 7, 8, 9, 10 and 11, complete penetration occurred. By referring to
Table 5, the front and rear faces have shown effects after shooting.
Increasing velocity as well as mass of the explosives unquestionably
led to more prominent damage and full penetration. This was
supported by previous researchers [25] who found that the damage
area increased as the impact loads increased. The pressure wave
starting from the effect direct moved along the yarn towards the
Fig. 7. Energy absorption versus velocity produced from different applied pressure. edge of the texture, where they were reflected. In woven texture,
each yarn hybrid guide served mostly to transmit and somewhat
reflect the pressure wave [26] including numerous factors
Table 6
Performance of NIJ test of the composites. contributing to instrument failure. Delamination is the partition of
cover layers between the limit layers of the fibers, as shown in
Specimen Pressure/psi Velocity/(m$s1) Energy absorption/J
Fig. 10 and Fig. 11.
1 2190 372 0.368 Low impact velocities below the critical velocity (V50), the ve-
2 1885 349 0.323
locity at which 50% of the projectiles perforate the target, allowed
3 2030 355 0.334
the fabric to absorb more energy because the yarns do not fail
during the initial stress rise and the transverse deflection of the
fabric has time to propagate. High impact velocities greater than
should assimilate more energy than ogival and conical to achieve V50 caused localized damage and the yarns failed before significant
perforation. Sharp angle edges play a role in digging at impact point transverse deflection could develop. Fibers at the impacted surface
and shearing the fabric. The hemispherical shape provides more were observed to have pulled and spears of fibers appeared in
extension due to no sharp edge that is responsible about the dy- between of laminated layers. Amid the infiltration procedure, shots
namic shear stress. Fig. 8 delineate the impact of the front and rear do not break a few yarns, the wedging their way through the
face with different pressure applied using hemispherical bullet opening by pushing aside and slipping past the rest of the yarns
shape. In the perforated panel, energy absorption of each layer [20]. Further investigation related to the influence of laminated
gradually increases from front to back. It was discovered that in the layer bamboo was continued in several experiments [8e13].
perforated panels, the energy absorption efficiency of front layers is It is interesting to note that, there is positive effect of tensile
lower than the rear layers, due to various levels of requirement the strength on the ballistics properties of these composites, Previ-
transverse way given by the texture layers after the present layer ously, in Refs. [8,9,12] the characterization on the mechanical ten-
[23]. sile were extensively done. The highest tensile that reported was
achieved on the Woven Bamboo/Woven E Glass composites, it is
6.4. Failures mode not surprise the ballistic performance of this combination give
superior results compared with Woven Bamboo alone.
The ballistic impact failure has been observed in couple of past Fig. 12 shows the influence of pressure on velocity. In this test,
examination [20,22,24]. In this experiment, the multi-shot tests led different amounts of pressure were used which utilized the
toward the objective territory to characterize the ballistic limit of distinctive effects of velocity. Higher pressure contributes to the
laminated hybrid bamboo/E-glass composite to withstand the higher impellent energy with increasing travelling speed. This was
bullet at specified velocities and different propellant masses. The bolstered by Zainab et al. [22], who showed that pressure is directly
failure mode represents the deformation of the front and rear proportional to velocity. Different levels of pressure applied by high
target face that caused by the projectile energy. The failure mech- speed projectiles led to the failure of the bamboo strips after
anisms can be observed after the target absorbed the ballistic shooting. The findings were reached as well in Kannan Rassiah et al.
impact. The sample dimensions were 29  18  29 cm tested under [8e13], who found that the bamboo strip had poor interfacial
the V50 ballistic limit. Fig. 9 shows the effect of sample after bonding and weak adhesion, causing low mechanical properties in
the laminated layer composite.
In order to observe failure inside the damage, a sample was cut
to highlight the cross-section views across the impact point. Since
the impact energy of high velocity objects is dissipated over a
smaller region, an additional damage mechanism is present at high
velocities known as the shear plug, as shown in Fig. 13. The energy
of the projectiles travelling at ballistic velocities was sufficient to
create a shear plug shear the front face of the composite. The depth
of the shear plug appeared to be dependent on the velocity of
projectile. The shear process continued in successive plies until the
impact energy of the projectile was lowered to the point that the
fibers could provide some resistance to shear [24]. For this spec-
imen, the depth of shear plug only occurred at half of the specimen
thickness.
Delamination is observed between plies throughout the thick-
Fig. 8. The effect of shooting on the front and rear face. ness of the composite as shown in Fig. 14. The delamination was

Please cite this article in press as: Ali A, et al., Ballistic impact properties of woven bamboo- woven E-glass- unsaturated polyester hybrid
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A. Ali et al. / Defence Technology xxx (2018) 1e13 11

Fig. 9. The front and rear face after multi shot in V50 test according to location number.

Fig. 10. The delamination occurred after test.

Fig. 11. Fiber pullout.

found to have occurred due to initial wave created upon impact.


The extent of delamination was found to be reduced and mini-
mized, since the damaged mode was through the creation of the
shear plug. The time for delamination to propagate outwards de-
creases with depth in the composite as no penetration occurs.
However [24], obtained opposite findings, in which the velocity of
the projectile decrease as the bullet penetrates throughout the
graphite fibers during the test.
Fig. 15 shows the fracture region of front layer resulting from
initial impact suffered by the front bamboo fiber composite. The
fibers which carried most of the loads are critical when damage
occurs which caused failure. From the post impact panel, it is
Fig. 12. Velocity versus pressure. clearly seen in the front layers that fiber breakage is clear due to the

Please cite this article in press as: Ali A, et al., Ballistic impact properties of woven bamboo- woven E-glass- unsaturated polyester hybrid
composites, Defence Technology (2018), https://doi.org/10.1016/j.dt.2018.09.001
12 A. Ali et al. / Defence Technology xxx (2018) 1e13

Fig. 13. The shear plug region.


Fig. 16. The matrix cracking.

to the disadvantages of natural fibers. which have poor interfacial


adhesion due to hydrophilic character of cellulose. The phenome-
non leads to poor fiber dispersion and fiber matrix interfacial
adhesion [25]. The cellulose, hemicelluloses, pectin and lignin are
rich in hydroxyl groups, leading to natural fiber hydrophobicity
[26].

7. CONCLUSIONS

1) Shooting tests were successfully performed in order to deter-


mine the ballistic limit (V50) for both samples which are 9:4:9
WEG: WB: WEG and 18:4 WB: WEG. By following the military
standard of ML-STD-6682, it was discovered that 18:4 WB: WEG
was able to withstand the bullet up to 482 m/s, which is more
than the minimum speed to qualify for Level of National Insti-
Fig. 14. Delamination between layers. tute of Justice (NIJ) IIIA standards. In the case of, 9:4:9 WEG:
WB:WEG laminated arrangement, the materials only reached
level II of the NIJ standards at 414 m/s. The multi-shot test shows
evident that failure of the mechanism indicated extensive fibre
pull out and delamination between the limit layers of glass fi-
bers, which are brittle compared to bamboo fibre. This clearly
shows that the e-glass cannot absorb the impact as much as the
bamboo, leading to the separation of layers, in which the layers
were no longer stacked together.
2) The NIJ test showed that the developed composites only reached
the minimum speed of level II, which was 367 m/s. The com-
posite failed to satisfy level III A.
3) The mechanism of failures was recognized when the bullet hit
the target, shear plug failure occurred due to the travelling
projectile, which then caused delamination from the dissipation
of early wave from impact. The front face which is bamboo
resulted in breakage of the fibre at the weakest point at which
the bullet arrested at the impact panel.
Fig. 15. The fiber breakage.
Acknowledgements

high impact of the projectile. Different layers suggest that the fibers The authors acknowledge the Fundamental Research Grant
broke randomly at the weakest point over the length [23]. However, Scheme (FRGS) 1/2013/TK01/UPNM/01/2 and Universiti Perta-
breakage is typically limited to the zone near the impact and is hanan National Malaysia (UPNM) for supporting the research work,
constrained by the object size and energy. The propagation of shock The Mechanical Engineering Department Politeknik port Dickson,
energy is another factor contributing to fiber breaks [23]. The Coordinator of Composite Engineering Laboratory (FKP, UTeM)
In Fig. 16, when the bullet was pushed forward, the matrix for granting permission to use all available equipment.
cracking continued to grow in vertical direction. Ellis [24] also re-
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