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Mechanism of reaction series, Parallel and consecutive reaction autocatalytic reactions, chain reaction polymerization reaction. Interpretation of kinetic data, Integral and differential method of analysis, variable volume reactions, total pressure method of kinetic analysis. Unit-II Classification of Reactors: Concept of ideality, Development of design equations for batch, semi batch, tubular and stirred tank reactor, Design of Isothermal and non-isothermal batch, CSTR, PFR, reactors. Combination of reactors, Reactors with recycle, yield and selectivity in multiple reactions. Multiple Reactions in Batch, continuous stirred tank and plug flow reactors uniqueness of steady state in continuous stirred tank reactor, optimum temperature progression, thermal characteristics of reactors. Non-ideal reaction, RTD dispersion model, Tank and series model, recycle model, segregated flow in mixed models, evaluation of RTD characteristics.
Unit-III
Unit-IV
Suggested Readings: 1. O. Levenspiel Chemical Reaction Engineering 2nd Ed. Willey Eastern, Singapore. 2. Houghen Watson & Ragatz Chemical Process Principles Part III (Kinetics & Catalysis) 2nd Ed. Asian Publishing House Bombay. nd 3. Fogler, H.S. Elements of Chemical Reaction Engineering 2 Ed. Prentice Hall of India Pvt. Ltd. New Delhi 1999. rd 4. J.M. Smith Chemical Engineering Kinetics 3 Ed. McGraw Hill. nd 5. K.G. Denbigh & K.G. Turner Chemical Reaction Theory an Introduction 2 Ed. United Press and ELBS 1972. 6. G. Copper & GVJ Jefferys Chemical Kinetics and Reactor Engineering Prentice Hall 1972
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Unit-II
Unit-III
Humidification: General Theory, psychometric chart, fundamental concepts in humidification & dehumidification, wet bulb temperature, adiabatic saturation temperature, measurement of humidification calculation of humidification operation, cooling towers and related equipments. Drying : Equilibrium mechanism theory of drying, drying rate curve. Batch and continuous drying for tray driers, Drum dryers, spray and tunnel dryers. Unit-IV Leaching and Extraction: Leaching: solid liquid equilibrium, Equipment, principles of leaching, concurrent and counter current systems and calculation of number of stage required. Liquid-Liquid extraction: Liquid equilibrium & Ponchon Savarit method, packed & spray column, conjugate curve and tie line data, plait point, ternary liquid-liquid extraction, operation and design of extraction towers analytical & graphical solution of single and multistage operation in extraction, Co-current, counter current and parallel current system.
Unit-V
Suggested Readings: 1. McCabe, W.L. Smith J.M. Unit Operation in Chemical Engg. 5th edition Tat McGraw Hill-Hogakucha, Tokyo, New Delhi. 2. Coulson J.M. Richardson J.F. Chemical Engg. Vil-2 Edition-2, Butserworth Heinmann, Oxford, New Delhi. 3. Treybal R.E. Mass Transfer Operation- 3rd edition, McGraw Hill ok Co. New York.
Convection: Fundamentals of convection, basic concepts and definitions. Natural and forced convection, hydrodynamic and thermal boundary layers, laminar and turbulent heat transfer inside and outside tubes. Heat transfer in boundary layer and in films, co/counter/cross current contacting for heat transfer, individual and overall heat transfer coefficient, fouling factor. Unit V Heat Transfer with Phase change: Condensation of pure and mixed vapours, filmwise and dropwise condensation, loading in condensers and basic calculation on condensers, heat transfer in boiling liquids, boiling heat transfer coefficients. Suggested Readings: 1. Donald Q. Kern Process Heat Transfer Tata McGraw Hill. 2. Alan J. Chapman Heat Transfer IV Ed. Collier Mcmillan. 3. Heat Transfer by Y.V.C. Rao. 4. J.P. Hallman 5. Vinay K. Dutta PHI (Heat Transfer).
1. P. Harriot, "Process Control" , Tata McGraw Hill, New Delhi, 1984. 2. D.P. Eckman, "Industrial Instrumentation", Wiley Eastern Ltd., New York 1990.
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To determine the equivalent thermal conductivity of composite wall. To determine heat transfer coefficient in force convection. 4. To determine heat transfer coefficient in Natural convection. 5. To determine heat transfer coefficient with the help of Steafan Boltzman Apparatus. 6. To calculate emmissivity of the test plate by emissivity measurement apparatus. 7. To determine heat transfer coefficient in double pipe heat exchanger. 8. To study the heat transfer characteristics of a shell and tube heat exchanger (heating/cooling) of water. 9. To determine heat transfer coefficient in parallel and counter flow heat exchanger. 10. To measure the rate of evaporation using an open pan evaporator. 11. To measure the rate of condensation of pure water vapour and to determine the heat transfer coefficient. 12. Demonstrate the film-wise drop-wise condensation and determination of the heat transfer coefficient. 13. To study the single effect evaporator and find out the transfer corfficient.
MECHANICAL OPERATIONS LAB (CH-342) 1. Sphericity factor on friction losses. 2. Agitated vessel 3. Settling studies 4. Drag studies 5. Filtration (constant rate) 6. Filtration (constant pressure) 7. Screening 8. Elutriation Clarification, cyclone separator 9. Jaw crusher 10.Ballmill 11. Particle size distribution 12. Storage of Solids 13. Cyclone studies, Multiple cyclone, mixer screw type ribbon type