B-Basis T650 3K-135-8H Fabric-7740

Advanced General
Aviation Transport
Experiments
B Basis Design Allowables for

Epoxy Based Prepreg
Fiberite 8-Harness Graphite Fabric
T650 3K-135-8H / 7740
AGATE-WP3.3-033051-102
September 2001
J. Tomblin, J. McKenna, Y. Ng, K. S. Raju

National Institute for Aviation Research
Wichita State University
Wichita, KS 67260-0093
TABLE OF CONTENTS
1.0
INTRODUCTION .....................................................................................................5
1.1 Scope ................................................................................................................................................... 5

1.2 Symbols Used ...................................................................................................................................... 6
1.3 Acronyms and Definitions .................................................................................................................... 7
1.4 References........................................................................................................................................... 8
1.5 Methodology ........................................................................................................................................ 9
1.5.1 Test Matrix..................................................................................................................................... 9
1.5.2 Environmental Conditioning ........................................................................................................ 11
1.5.3 Fluid Sensitivity Screening .......................................................................................................... 11
1.5.4 Normalization Procedures ........................................................................................................... 12
1.5.5 Statistical Analysis....................................................................................................................... 14
1.5.6 Material Performance Envelope and Interpolation...................................................................... 14
1.5.6.1 Interpolation Example........................................................................................................... 16
2.0 FIBERITE T650 3K-135-8H / 7740 PREPREG PROPERTIES................................18

2.1 Prepreg Documentation by Prepreg Lot ............................................................................................ 19
2.2 Process Specification......................................................................................................................... 20
3.0 FIBERITE T650 3K-135-8H / 7740 LAMINATE PROPERTIES...............................21

3.1 Test Results ....................................................................................................................................... 22
3.1.1 Summary ..................................................................................................................................... 23
3.1.2 Individual Test Summaries.......................................................................................................... 24
3.1.2.1 Tension, 1-axis ..................................................................................................................... 25
3.1.2.2 Tension, 2-axis ..................................................................................................................... 26
3.1.2.3 Compression, 1-axis............................................................................................................. 27
3.1.2.5 Shear, 12 axis....................................................................................................................... 29
3.1.2.6 Shear, 13 axis....................................................................................................................... 30
3.1.3 Individual Test Charts ................................................................................................................. 31
3.1.3.1 Tension, 1-axis ..................................................................................................................... 32
3.1.3.2 Tension, 2-axis ..................................................................................................................... 33
3.1.3.5 Shear, 12 axis....................................................................................................................... 36
3.1.3.6 Shear, 13 axis....................................................................................................................... 37
3.2 Raw Data ........................................................................................................................................... 38

3.2.1 Raw Data Spreadsheets and Scatter Charts .............................................................................. 39
3.2.2 Fluid Sensitivity Raw Data Spreadsheets and Scatter Charts .................................................... 82
3.2.3 Representative Shear Stress-Strain Curve ................................................................................. 87
3.3 Statistical Results............................................................................................................................... 89
3.3.1 Plot by Condition ......................................................................................................................... 90
3.3.2 Plot of Pooled Data ................................................................................................................... 101
3.4 Moisture Conditioning History Charts .............................................................................................. 112
3.5 Physical Test Results....................................................................................................................... 117
4.0
TESTING AND REPORTING COMMENTS ........................................................129
APPENDIX A. PHYSICAL TEST DATA SUPPLIED BY MATERIAL VENDOR .........131

APPENDIX B. DATES OF PANEL MANUFACTURE AND COPY OF FAA FORM 81303....................................................................................................................................142
1.0 INTRODUCTION
1.1 Scope
The test methods and results described in this document are intended to provide
basic composite properties essential to most methods of analysis. These properties
are considered to provide the initial base of the building block approach. Additional
coupon level tests and subelement tests may be required to fully substantiate the
full-scale design.
The test methods and results contained in this document are consistent with MILHDBK-17-1E,2D,3E - Military Handbook for Polymer Matrix Composites. All
material, specimens, fixtures and test results contained within this document were
traceable and conformed by the Federal Aviation Administration (FAA). It should be
noted that before application of the basis values presented in this document to
design, demonstration of the ability to consistently produce equivalent material
properties as that evaluated during this program should be substantiated through an
acceptable test program.
1.2 Symbols Used

n12tu
me
E1c
E1t
E2c
E2t
F12su
F13su
F1cu
F1tu
F2cu
F2tu
G12s
major Poissons ratio, tension

micro-strain
compressive modulus, longitudinal
tensile modulus, longitudinal
compressive modulus, transverse
tensile modulus, transverse
in plane shear strength
apparent interlaminar shear strength
compressive strength, longitudinal
tensile strength, longitudinal
compressive strength, transverse
tensile strength, transverse
in plane shear modulus
Superscripts
c
cu
s
su
t
tu
compression
compression ultimate
shear
shear ultimate
tension
tension ultimate
Subscripts
1
2
12
13
1 axis; longitudinal
(parallel to warp direction of reinforcement)
2 axis; transverse
(parallel to fill direction of reinforcement)
in plane shear
interlaminar shear (apparent)
1.3 Acronyms and Definitions

A Basis
AGATE
ASTM
B Basis
C. V.
CTD
CPT
DMA
dry
ETD
ETW
FAR
FAW
Gr/Ep
NASA
RTD
SACMA
SRM
Tg
tply
wet
95% lower confidence limit on the first population percentile

Advanced General Aviation Transport Experiments
American Society for Testing and Materials
95% lower confidence limit on the tenth population percentile
coefficient of variation
cold temperature dry
cured ply thickness
dynamic mechanical analysis
specimen tested with an as fabricated moisture content
elevated temperature dry
elevated temperature wet
Federal Aviation Regulations
fiber areal weight
Graphite/Epoxy
National Aeronautics and Space Administration
room temperature dry
Suppliers of Advanced Composite Materials Association
SACMA Recommended Method
glass transition temperature
cured ply thickness
specimen tested with an equilibrium moisture content per
section 1.5.2
1.4 References
ASTM Standards
D3039-95
D5379-93
D2344-89
D792-91
D2734-94
D3171-90
D695-91
Tensile Properties of Polymer Matrix Composite Materials

Shear Properties of Composite Materials by the V-Notched
Beam Method
Apparent Interlaminar Shear Strength of Parallel Fiber
Composites by Short Beam Method
Density and Specific Gravity (Relative Density) of Plastics by
Displacement
Void Content of Reinforced Plastics
Fiber Content of Resin Matrix Composites by Matrix
Digestion
Compressive Properties of Rigid Plastics
SACMA Standards
SRM 1-94
SRM 8-94
SRM 18-94
Compressive Properties of Oriented Fiber-Resin Composites

Short Beam Shear Strength of Oriented Fiber-Resin
Composites
Glass Transition Temperature (Tg) Determination by DMA of
Oriented Fiber-Resin Composites
Other Documents
FAA Document DOT/FAA/AR-00/47: Material Qualification and Equivalency
for Polymer Matrix Composite Material Systems, J.S. Tomblin, Y.C. Ng and
K.S. Raju, 2001.
MIL-HDBK-17 1E, 2D, 3E Military Handbook for Polymer Matrix Composites
Cessna Aircraft Company, Document # 98-87-005: B-Basis Design
Allowables Test Plan for Preimpregnated Carbon/Epoxy Broadgoods,
Revision B, January 1999.
1.5 Methodology
1.5.1 Test Matrix
Testing was performed according to the test methods delineated in the test matrix, with
modifications as referenced in the AGATE report, Material Qualification and Equivalency
for Polymer Matrix Composite Material Systems. The test matrix for properties included
in this document is listed on the next page, with the following notation cited in each
column:
#x#
where the first # represents the required number of prepreg batches, defined as: Prepreg
containing T650 3K-135 8-Harness Graphite Fabric from one mill roll, impregnated with
one batch of resin in one continuous manufacturing operation with traceability to all
components. The second # represents the required number of replicates per prepreg
batch. For example, 3 x 6 refers to three prepreg batches of material and six
specimens per prepreg batch for a total requirement of 18 test specimens.
Table 1.5.1: Test Matrix and Standards Used

TEST
METHOD
0o (warp) Tension Strength

0o (warp) Tension Modulus,
Strength and Poissons Ratio
90o (fill) Tension Strength
90o (fill) Tension Modulus and
Strength
0o (warp) Compression Strength
0o (warp) Compression Modulus
90o (fill) Compression Strength
90o (fill) Compression Modulus
In-Plane Shear Strength
In-Plane Shear Modulus and
Strength
Short Beam Shear
Fiber Volume
Resin Volume
Void Content
Cured Neat Resin Density
ASTM D3039-95
ASTM D3039-95
Glass Transition Temperature
SACMA SRM 18-94
NO. OF REPLICATES PER

TEST CONDITION
CTD1,5 RTD2,5 ETW3

1x4
3x4
3x4
ETD4,5
3x4
1x2
3x2
3x2
3x2
ASTM D3039-95
ASTM D3039-95
1x4
3x4
3x4
3x4
1x2
3x2
3x2
3x2
SACMA SRM 1-94

SACMA SRM 1-94
SACMA SRM 1-94
SACMA SRM 1-94
ASTM D5379-93
ASTM D5379-93
1x6
1x2
1x6
1x2
1x4
3x6
3x2
3x6
3x2
3x4
3x6
3x2
3x6
3x2
3x4
3x6
3x2
3x6
3x2
3x4
1x2
3x2
3x2
3x2
ASTM D2344-89
ASTM D3171-90
ASTM D3171-90
ASTM D2734-94
---
--3x6
One sample per panel
Supplied by manufacturer for
material
3 dry, 3 wet per prepreg lot
--
Notes :
1
2
3
4
5
CTD: One prepreg lot of material tested (test temperature = -65 5o F, moisture
content = as fabricated, soak time at 65 was 3 min.)
RTD: Three prepreg lots of material tested (test temperature = 70 10o F,
moisture content = as fabricated)
ETW: Three prepreg lots of material tested (test temperature = 180 5o F,
moisture content = equilibrium per section 1.5.2, soak time at 180 was 60 sec.)
ETD: Three prepreg lots of material tested (test temperature = 180 5o F,
moisture content = as fabricated, soak time at 180 was 60 sec.)
Dry specimens are as fabricated specimens that have been maintained at
ambient conditions in an environmentally controlled laboratory.
10
1.5.2 Environmental Conditioning

All wet conditioned samples were exposed to elevated temperature and humidity
conditions to establish moisture saturation of the material. Specimens were exposed to
85 5 % relative humidity and 145 5 F until an equilibrium moisture weight gain of
traveler, or witness coupons (1 x 1 x specimen thickness) was achieved. ASTM D5229
and SACMA SRM 11 were used as guidelines for environmental conditioning and
moisture absorption.
Effective moisture equilibrium was achieved when the average moisture content of the
traveler specimen changed by less than 0.05% for two consecutive readings within a
span of 7 0.5 days and was expressed by:
W i - W i - 1 < 0.0005
Wb
where
W i = weight at current time

W i-1 = weight at previous time
W b = baseline weight prior to conditioning
It is common to see small fluctuations in an unfitted plot of the weight gain vs. time curve.
There were no fluctuations that made significant errors in results or caused rejection in
the moisture equilibrium criteria. Once the traveler coupons passed the criteria for two
consecutive readings, the samples were removed from the environmental chamber and
placed in a sealed bag with a moist paper or cotton towel for a maximum of 14 days until
mechanical testing. Strain gauged specimens were removed from the controlled
environment for a maximum of 2 hours for application of gages in ambient laboratory
conditions.
1.5.3 Fluid Sensitivity Screening

All wet conditioned samples were exposed to elevated temperature and humidity
conditions to establish moisture saturation of the material. Specimens were exposed to
85 5 % relative humidity and 145 5 F until an equilibrium moisture weight gain of
traveler, or witness coupons (1 x 1 x specimen thickness) was achieved. ASTM D5229
and SACMA SRM 11 were used as guidelines for environmental conditioning and
moisture absorption.
Effective moisture equilibrium was achieved when the average moisture content of the
traveler specimen changed by less than 0.05% for two consecutive readings within a
span of 7 0.5 days and was expressed by:
11
W i - W i - 1 < 0.0005
Wb
where
W i = weight at current time

W i-1 = weight at previous time
W b = baseline weight prior to conditioning
It is common to see small fluctuations in an unfitted plot of the weight gain vs. time curve.
There were no fluctuations that made significant errors in results or caused rejection in
the moisture equilibrium criteria. Once the traveler coupons passed the criteria for two
consecutive readings, the samples were removed from the environmental chamber and
placed in a sealed bag with a moist paper or cotton towel for a maximum of 14 days until
mechanical testing. Strain gauged specimens were removed from the controlled
environment for a maximum of 2 hours for application of gages in ambient laboratory
conditions.
1.5.4 Normalization Procedures

The normalization procedure attempts to reduce variability in fiber-dominated material
properties by adjusting raw test values to a specified fiber volume content. Only the
following properties were normalized:
0 (warp) Tensile Strength and Modulus

90 (fill) Tensile Strength and Modulus
0 (warp) Compressive Strength and Modulus
90 (fill) Compressive Strength and Modulus
The normalization procedure was adopted from MIL-HDBK-17-1E, section 2.4.3.3. The
procedure which was used to normalize the data is based on two primary assumptions:
The relationship between fiber volume fraction and ultimate laminate

strength is linear over the entire range of fiber/resin ratios. (It
neglects the effects of resin starvation at high fiber contents.)
Fiber volume is not commonly measured for each test sample, so

this method accounts for the fiber volume variation between
individual test specimens by utilizing a relationship between fiber
volume fraction and laminate cured ply thickness. This relationship
is virtually linear in the 0.45 to 0.65 fiber volume fraction range.
12
Additional information is detailed in FAA Document DOT/FAA/AR-00/47: Material

Qualification and Equivalency for Polymer Matrix Composite Material Systems. For all
normalized data contained in this document, the test values are normalized by cured ply
thickness according to:
Normalized Value = Test Value
CPTspecimen
CPTnormalizing
where:
CPTspecimen =
Average Sample Thickness

# of plies
13
1.5.5 Statistical Analysis

When compared to metallic materials, fiber reinforced composite materials exhibit a high
degree of material property variability. This variability is due to many factors, including
but not limited to: raw material and prepreg manufacture, material handling, part
fabrication techniques, ply stacking sequence, environmental conditions, and testing
techniques. This inherent variability drives up the cost of composite testing and tends to
render smaller data sets than those produced for metallic materials. This necessitates
the usage of statistical techniques for determining reasonable design allowables for
composites.
The analyses and design allowable generation for both A and B basis values were
performed using the procedure detailed in section 5.3 of FAA Document DOT/FAA/AR00/47: Material Qualification and Equivalency for Polymer Matrix Composite Material
Systems.
1.5.6 Material Performance Envelope and Interpolation

Using the B-basis numbers, a material performance envelope may be generated for the
material system by plotting these values as a function of temperature. Figure 1.5.1
shows an example material performance envelope using B-basis values.
14
120
Actual Basis Value
Estimated Value
B-Basis Strength Values (ksi)
100
RTD
CTD
80
ETD
RTW
60
Material
Performance
Envelope
ETW
40
20
-100
-50
50
100
150
200
Temperature (o F)
Figure 1.5.1 Material performance envelope.

Since each specific aircraft application of the qualified material may have different
Material Operational Limits (MOL) than those tested in the material qualification (which is
usually the upper limit), some applications may require a reduced MOL. In this case,
simple linear interpolation may be used to obtain the corresponding basis values at the
new application MOL.
This interpolation may be accomplished using the following simple relationships
assuming TRTD < TMOL < TETD :
For the corresponding MOL dry basis value, the interpolated basis value using the
qualification data is
B MOL = B RTD where
(B RTD - BETD )(TRTD - TMOL )

(TRTD - TETD )
BMOL = new application basis value interpolated to TMOL
15
BRTD = basis RTD strength value

BETD = basis ETD strength value
TRTD = RTD test temperature
TETD = ETD test temperature
TMOL = new application MOL temperature
For the corresponding MOL wet basis value, an estimated Room Temperature Wet
(RTW) value must be calculated. This may be accomplished by the simple relation
BRTW = BRTD - ( BETD - BETW )

The interpolated wet basis value using the qualification data may then be obtained by
BMOL = BRTW -
where:
(BRTW - BETW )(TRTW - TMOL )

(TRTW - TETW )
BMOL = new application basis value interpolated to TMOL

BRTW = estimated basis RTW strength value
BETW = basis ETW strength value
TRTW = RTW (i.e., RTD) test temperature
TETW = ETW test temperature
TMOL = new application MOL temperature
These equations may also be used for interpolated mean strengths as well as A-basis
values with the appropriate substitutions. It should be noted that because unforeseen
material property drop-offs with respect to temperature and environment can occur,
extrapolation to a higher MOL should not be attempted without additional testing and
verification. In addition, the interpolation equations shown above are practical for
materials obeying typical mechanical behavior. In most cases, some minimal amount of
testing may also be required to verify the interpolated values.
1.5.6.1 Interpolation Example
This section provides an example of linear interpolations to a specific application
environment less than the tested upper material limit used in qualification. Assuming a
specific application environment of 150o F, Figure 1.5.2 depicts the linear interpolation of
the B-basis design allowable to this environment. Using the above equations along with
the nominal testing temperatures (see Table 1.5.1), the interpolated basis values at 150o
F become
ETD : BMOL = 75.106 ksi
16
ETW : BMOL = 59.746 ksi

120
Actual Basis Value
Estimated Value
100
CTD
B-Basis Strength Values (ksi)
RTD
80
ETD
RTW
60
ETW
40
20
-100
-50
50
100
150
200
Temperature (o F)
Figure 1.5.2 Example of 150o F interpolation for B-basis values.
17
2.0 FIBERITE T650 3K-135-8H / 7740 PREPREG PROPERTIES
18
2.1 Prepreg Documentation by Prepreg Lot
Prepreg Documentation
Prepreg Batch or Lot #
Batch (Lot) ID as labeled on samples
Date of Manufacture
Expiration Date
Resin Content [%]
Reinforcement Areal Weight & Test Method
Resin Flow & Test Conditions
Gel Time & Test Conditions
Volatile Content
Reinforcement Documentation
Fabric Batch or Lot #, Warp

Sizing weight, %
Fabric Batch or Lot #, Fill
Sizing weight, %
Date of Manufacture
Average Fiber Density per Lot & Test Method
Prepreg Manufacturer & Product ID:

HMF 7740/T650-35-3K-8HS-370-42
Impregnation Method: SOLVENT
310601
310602
310603
11-13-97
11-13-97
11-13-97
11-13-98
11-13-98
11-13-98
37 %
39 %
38 %
371 g/sq m
368 g/sq m
369 g/sq m
20% @
23% @
22% @
100 psi
4 min @ 177 C
3 min @
0.9
1.0
100 psi
177 C
100 psi
3 min @
177 C
0.9
Fiber/Fabric Manufacturer & Product ID: T650/35 3K 309NT

Precursor Type: PAN
Nominal Filament Count: 3K
Finish/Sizing Type and %: UC309, , .931.14%
Nominal tow or yarn count/inch:
Twist: not available
B3S0602, 705, 803, 804, 820 B3S0602, 705, 803, 804, 820
B3S0303
.93, 1.14, .97, 1.03, 1.09 %
.93, 1.14, .97, 1.03, 1.09 %
1.11 %
B3S0803, 804, 820
B3S0803, 804, 820
B3S0303
.97, 1.03, 1.09 %
.97, 1.03, 1.09 %
1.11 %
8-97
8-97
4-3-97
1.775 (warp), 1.776 ( fill ) g/cc
1.775 (warp), 1.776 ( fill ) g/cc
1.761 g/cc
Matrix Documentation
Resin Manufacturer & Product ID:
Matrix Batch or Lot #

Date of Manufacture
Average Neat Resin Density by Lot
& Test Method
310601
310602
310603
11-13-97
11-13-97
11-13-97
1.27 g/ccm
1.27 g/ccm
1.27 g/ccm
19
2.2 Process Specification

This specification does not address issues relating to safety, quality control, bagging
material selection, bagging procedure, tool preparation, or equipment selection.
Although these may affect overall part quality, it is the responsibility of the end user to
develop procedures related to these issues in a manner that produces parts with high
quality and consistency.
The following autoclave cure procedures are excerpts from Cessna process specification
CSAC005. The exception to this specification is the cure cycle and ply orientation
tolerance. The cure cycle for panel fabrication is 250F, 10: for 120 minutes, +60, -0;
45 psi, 5. Individual ply orientation is 2 with respect to the tooled reference edge.
The detailed cure cycle procedure is given below. All test specimens were cured per this
specification by Cessna Aircraft Company. However, the effects of the upper and lower
limits of vacuum, temperature, cure time, heat-up rate and hold temperature on the
mechanical and thermal properties have not been investigated.
(1) Apply 22 in-Hg of vacuum minimum to vacuum bag. Initiate autoclave pressure 3
psi/minute minimum, vent bag at 2010 psig. Final vessel pressure 455 psi.
(2) From 230F to 240F, a minimum heat up rate of 0.3F/minute is acceptable.
(3) All thermocouples shall be at temperature
20
3.0 FIBERITE T650 3K-135-8H / 7740 LAMINATE PROPERTIES
21
3.1 Test Results
22
3.1.1 Summary
M ATERIAL:
Fiberite 7740/T650 3K-135-8H Graphite Fabric
PREPREG:
Fiberite HMF 7740/T650-35-3K-8HS-370-42
FIBER:
Am oco T650/35 3K 309NT
Tg (dry):
229.85 F
PROCESSING:
Tg (wet): 183.22 F
7740/T650 3K-135-8H
Sum m ary
RESIN:
Fiberite HMF 7740
Tg M ETHOD:
DMA (SRM 18-94)
Autoclave cure: 25010F for 120+60,-0 m in. @ 455 psi
Date of fiber m anufacture
Date of testing
4/3/97 8/97
2/4/99 4/21/99
Date of resin m anufacture
11/13/97
Date of data subm ittal
Date of prepreg manufacture
11/13/97
Date of analysis
Date of com posite m anufacture
8/99
2/11/99 4/21/99
3/19/98 4/16/98
LAM INA M ECHANICAL PROPERTY SUM M ARY

Data Reported as:
CTD
M easured
(Normalized by CPT=0.0150 in)
RTD
ETD
ETW
B-Basis
M ean
B-Basis
M ean
B-Basis
M ean
B-Basis
Mean
F1tu
(ksi)
115.71
(116.14)
125.79
(126.05)
121.89
(123.00)
132.52
(133.49)
119.95
(120.00)
130.41
(130.24)
120.76
(121.59)
130.77
(131.45)
E1 t
(M si)
---
10.01
(10.09)
---
9.95
(10.04)
---
9.91
(9.89)
- --
9.78
(9.82)
---
0.060
---
0.050
---
0.030
- --
0.032
n12tu
F2tu
(ksi)
111.78
(112.91)
120.55
(122.30)
116.18
(116.09)
125.30
(125.74)
116.13
(116.25)
125.24
(125.91)
114.91
(114.60)
123.48
(123.65)
E2 t
(M si)
---
10.63
(10.75)
---
9.84
(9.86)
---
9.41
(9.48)
- --
9.36
(9.44)
F 1cu
(ksi)
85.60
(83.49)
103.09
(101.61)
88.03
(86.73)
103.18
(102.55)
68.28
(67.93)
80.03
(80.32)
48.45
(47.89)
56.35
(56.16)
E1 c
(M si)
---
9.61
(9.40)
---
9.43
(9.40)
---
9.53
(9.42)
- --
9.73
(9.63)
F 2cu
(ksi)
97.21
(96.70)
112.73
(112.50)
93.31
(93.61)
105.92
(106.56)
69.12
(68.72)
77.47
(78.23)
44.39
(44.19)
50.10
(50.02)
E2 c
(M si)
---
9.57
(9.28)
---
9.28
(9.29)
---
9.24
(9.23)
- --
9.52
(9.53)
F 12su
(ksi)
20.74
22.99
16.57
18.09
11.97
13.07
8.15
8.86
G 12s
(M si)
---
0.79
---
0.63
---
0.42
- --
0.33
(ksi)
---
- --
9.60
10.39
---
---
- --
---
F13su**
** Apparent interlam inar shear strength
23
3.1.2 Individual Test Summaries
24
3.1.2.1 Tension, 1-axis

Tension, 1-axis
Material:
Resin content:
31 - 38 wt%
Comp. density:
1.52 - 1.54 g/cc
Fiber volume:
53 - 59 vol%
Void content:
1.0 to 3.6 %
Ply thickness:
0.0146 - 0.0156 in.
Ply range:
7 plies
Test method:
D3039-95
Modulus calculation:
linear fit from 1000 - 3000 me
Normalized by:
0.0150 in. ply thickness
G/Ep
[0]7
CTD (B)
RTD (A)
ETD (G)
Test Temperature [F]
-65
75
180
ETW (F)
180
Moisture Conditioning
dry
dry
dry
64 days, .63-.72% wt gain
Equilibrium at T, RH
as fabricated
as fabricated
as fabricated
145 F, 85 %
Source code
BDJXXXXB
BDJXXXXA
BDJXXXXG
BDJXXXXF
Normalized
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
Mean
126.05
125.79
133.49
132.52
130.24
130.41
131.45
130.77
Minimum
111.17
111.90
124.05
122.94
117.61
118.02
125.68
124.30
Maximum
136.47
138.67
142.82
138.64
138.80
141.04
136.24
137.84
C.V.(%)
6.81
6.75
3.69
3.48
5.60
5.76
2.34
2.85
B-value
116.14
115.71
123.00
121.89
120.00
119.95
121.59
120.76
A-value
109.66
109.10
116.13
114.93
113.30
113.10
114.75
113.82
Normalized
Measured
F1tu
(ksi)
E1t
(Msi)
No. Specimens
18
18
18
No. Prepreg Lots
Mean
10.09
10.01
10.04
9.95
9.89
9.91
9.82
Minimum
9.89
9.65
9.86
9.57
9.75
9.56
9.58
9.36
Maximum
10.44
10.18
10.20
10.12
10.25
10.22
10.29
10.29
C.V.(%)
2.09
2.08
1.57
2.06
1.89
2.97
2.67
3.41
No. Specimens
No. Prepreg Lots
Mean
n 12t
30
0.060
0.050
9.78
6
3
0.030
0.032
No. Specimens
No. Prepreg Lots
25

Tension, 2-axis
Material:
Resin content:
32 - 38 wt%
Comp. density:
1.50 - 1.53 g/cc
Fiber volume:
53 - 59 vol%
Void content:
1.4 to 4.1 %
Ply thickness:
0.0144 - 0.0156 in.
Ply range:
7 plies
Test method:
D3039-95
Normalized by:
G/Ep
[0]7
CTD (B)
RTD (A)
ETD (G)
-65
75
180
ETW (F)
180
dry
dry
dry
as fabricated
as fabricated
as fabricated
145 F, 85 %
Source code
BDUXXXXB
BDUXXXXA
BDUXXXXG
BDUXXXXF
Normalized
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
Mean
122.30
120.55
125.74
125.30
125.91
125.24
123.65
123.48
Minimum
113.03
113.68
117.25
117.17
117.09
116.54
105.95
110.00
Maximum
132.98
130.93
135.89
133.73
133.32
132.93
133.65
135.22
C.V.(%)
4.40
4.18
4.58
3.94
3.87
4.00
4.88
4.66
B-value
112.91
111.78
116.09
116.18
116.25
116.13
114.60
114.91
A-value
106.76
106.04
109.77
110.22
109.92
110.17
108.32
108.97
Normalized
Measured
tu
F2
(ksi)
E2t
(Msi)
No. Specimens
18
18
18
No. Prepreg Lots
30
3
Mean
10.75
10.63
9.86
9.84
9.48
9.41
9.44
Minimum
9.90
10.10
9.70
9.55
9.27
9.25
8.94
9.36
8.67
Maximum
11.24
11.33
10.04
10.18
9.60
9.67
9.88
9.70
C.V.(%)
4.42
4.25
1.44
2.58
1.66
1.59
3.39
4.10
No. Specimens
No. Prepreg Lots
26
3.1.2.3 Compression, 1-axis

Compression, 1-axis
Material:
Resin content:
30 - 34 wt%
Comp. density:
1.50 - 1.53 g/cc
Fiber volume:
53 - 60 vol%
Void content:
0.6 to 3.9 %
Ply thickness:
0.0141 - 0.0155 in.
Ply range:
8 plies
Test method:
SRM 1-94, D695-91 (mod)
Normalized by:
G/Ep
[0]8
CTD (B)
RTD (A)
ETD (G)
-65
75
180
180
dry
dry
dry
63-66 days, .71-.78% wt gain
as fabricated
as fabricated
as fabricated
145 F, 85 %
Source code
BDKXXXXB
BDKXXXXA
BDKXXXXG
Mean
ETW (F)
BDKXXXXF
Normalized
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
101.61
103.09
102.55
103.18
80.32
80.03
56.16
56.35
Minimum
93.44
95.00
95.54
96.16
66.85
65.70
43.39
44.15
Maximum
107.85
109.53
111.41
113.08
88.16
88.62
69.43
68.54
C.V.(%)
5.46
5.59
4.57
4.91
6.03
6.16
12.38
11.48
B-value
83.49
85.60
86.73
88.03
67.93
68.28
47.89
48.45
A-value
73.41
75.88
76.31
78.06
59.77
60.55
42.11
42.94
Normalized
Measured
cu
F1
(ksi)
E1
(Msi)
No. Specimens
18
18
No. Prepreg Lots
30
3
Mean
9.40
9.61
9.40
9.43
9.42
9.53
9.63
Minimum
9.35
9.54
8.94
9.05
8.88
8.81
8.83
8.92
Maximum
9.46
9.69
9.86
9.86
10.02
10.69
10.62
10.65
C.V.(%)
0.80
1.12
3.31
3.62
5.01
7.18
6.77
6.75
No. Specimens
No. Prepreg Lots
2
1
6
3
6
3
9.73
6
3
27

Compression, 2-axis
Material:
Resin content:
37 - 39 wt%
Comp. density:
1.52 - 1.53 g/cc
Fiber volume:
52 - 59 vol%
Void content:
1.1 to 3.9 %
Ply thickness:
0.0145 - 0.0154 in.
Ply range:
8 plies
Test method:
SRM 1-94, D695-91 (mod)
Normalized by:

CTD (B)
G/Ep
[0]8
RTD (A)
ETD (G)
ETW (F)
-65
75
180
180
dry
dry
dry
63-66 days, .68-.80% wt gain
as fabricated
as fabricated
as fabricated
145 F, 85 %
Source code
BDWXXXXB
BDWXXXXA
BDWXXXXG
BDWXXXXF
Normalized
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
Mean
112.50
112.73
106.56
105.92
78.23
77.47
50.02
50.10
Minimum
106.44
105.93
97.63
97.57
68.20
67.97
41.59
41.14
Maximum
119.27
119.72
115.82
115.86
88.08
86.42
58.05
58.18
C.V.(%)
5.16
5.55
5.14
4.87
7.02
6.74
8.41
8.31
B-value
96.70
97.21
93.61
93.31
68.72
69.12
44.19
44.39
A-value
87.91
88.58
85.08
85.00
62.46
62.17
40.14
40.41
Normalized
Measured
F2cu
(ksi)
E2c
(Msi)
No. Specimens
18
18
No. Prepreg Lots
29
3
Mean
9.28
9.57
9.29
9.28
9.23
9.24
9.53
Minimum
9.24
9.48
8.96
8.86
8.68
8.78
9.08
9.14
Maximum
9.33
9.65
9.48
9.64
9.62
9.83
10.02
10.27
C.V.(%)
0.62
1.27
2.22
3.07
3.75
4.44
3.57
4.31
No. Specimens
No. Prepreg Lots
2
1
6
3
6
3
9.52
6
3
28
3.1.2.5 Shear, 12 axis

Shear, 12-axis
Material:
Resin content:
31 - 36 wt%
Comp. density:
1.51 - 1.53 g/cc
Fiber volume:
54 - 60 vol%
Void content:
1.7 to 4.0 %
Ply thickness:
0.0143 - 0.0154 in.
Ply range:
9 plies
Test method:
D5379-93
Normalized by:
N/A
G/Ep
[(0/90)2/0/(90/0)2]
CTD (B)
RTD (A)
ETD (G)
-65
75
180
180
dry
dry
dry
as fabricated
as fabricated
as fabricated
145 F, 85 %
Source code
BDNXXXXB
BDNXXXXA
BDNXXXXG
Normalized
Measured
Normalized
Measured
Normalized
ETW (F)
Measured
BDNXXXXF
Normalized
Measured
Mean
22.99
18.09
13.07
Minimum
22.21
17.43
12.23
7.85
Maximum
24.32
19.10
14.38
10.19
C.V.(%)
3.57
2.69
4.14
6.51
B-value
20.74
16.57
11.97
8.15
A-value
19.49
15.57
11.24
7.65
Normalized
Measured
8.86
su
F12
(ksi)
G12
(Msi)
No. Specimens
20
18
30
No. Prepreg Lots
Mean
0.79
0.63
0.42
0.33
Minimum
0.75
0.54
0.38
0.31
Maximum
0.83
0.67
0.49
0.35
C.V.(%)
7.06
7.19
8.75
4.15
No. Specimens
No. Prepreg Lots
2
1
6
3
6
3
6
3
29

Shear, 13-axis
Material:
Resin content:
31 - 39 wt%
Comp. density:
1.52 - 1.53 g/cc
Fiber volume:
52 - 59 vol%
Void content:
1.1 to 2.2 %
Ply thickness:
0.0141 - 0.0169 in.
Ply range:
7 plies
Test method:
D2344-89
N/A
Normalized by:
N/A
CTD (B)
RTD (A)
G/Ep
[0]7
ETD (G)
ETW (F)
75
dry
as fabricated
BDQXXXXA
Source code
Normalized
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
Normalized
Measured
10.39
Mean
Minimum
9.60
Maximum
11.23
C.V.(%)
3.85
B-value
9.60
A-value
9.03
su
F13
(ksi)
No. Specimens
18
No. Prepreg Lots
NOTES: These values represent the apparent interlaminar shear properties and are to be used for quality control purposes only. Do not use
these values for interlaminar shear strength design values.
30
3.1.3 Individual Test Charts
31
0 Tension -- Normalized Strength

160
140
Strength (ksi)
120
100
80
60
40
Conditioning
X Dry
O Wet
20
0
-100
-50
50
100
150
200
Temperature (F)
NOTE: The symbols represent the pooled average of all tests, and the bars represent the upper and lower limit of the
data. The 180 dry and wet data has been staggered for clarity
32
90 Tension -- Normalized Strength

160
140
Strength (ksi)
120
100
80
60
40
Conditioning
X Dry
O Wet
20
0
-100
-50
50
100
150
200
Temperature (F)
data. The 180 dry and wet data has been staggered for clarity.
33
0 Compression -- Normalized Strength

Fiberite 7740/T650 3K-135-8H Graphite
120
Strength (ksi)
100
80
60
40
Conditioning
X Dry
O Wet
20
0
-100
-50
50
100
150
200
Temperature (F)
NOTE: The symbols represent the pooled average of all tests, and the bars represent the upper and lower limit of
the data. The 180 dry and wet data has been staggered for clarity
34
90 Compression -- Normalized Strength

140
120
Strength (ksi)
100
80
60
40
Conditioning
X Dry
O Wet
20
0
-100
-50
50
100
150
200
Temperature (F)
35
In-Plane Shear -- Measured Strength

28
24
Strength (ksi)
20
16
12
8
Conditioning
X Dry
O Wet
4
0
-100
-50
50
100
150
200
Temperature (F)
36
Apparent Interlaminar Shear -- Measured Strength

16
Strength (ksi)
12
Conditioning
X Dry
O Wet
0
-100
-50
50
100
150
200
Temperature (F)
data.
37
3.2 Raw Data

Specimen Naming Convention
Test coupons were identified using an eight-digit specimen code, with the significance of each digit delineated below.
A representative sample ID is shown for reference purposes.
B D J 2
1 2 5 F
1st Character: Fabricator

B designates Cessna
5th Character: Panel Number

The panel(s) fabricated for a specific test method.
2nd Character: Material System

D designates T650 3K-135-8H / 7740
6th Character: Subpanel Number

The sub-panel(s) cut from each panel, with subpanel
numbers labeled increasing from reference edge.
3rd Character: Test Type

J designates 0 Tension
Strength and Modulus, other
test types will be clearly labeled
at the top of each sheet
4th Character: Prepreg Batch ID
See Table 2.1 for Fiberite Batch ID /
Sample Batch ID correlation.
7th Character: Sample Number

The sample(s) cut from each subpanel, with sample
numbers labeled increasing from reference edge.
8th Character: Test Condition
A --- RTD
B --- CTD
F --- ETW
G --- ETD
See Table 1.5.1 for condition parameters.
38
3.2.1 Raw Data Spreadsheets and Scatter Charts
39
0 Tension -- (RTD)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDJ12X1A
BDJ12X2A
BDJ12X3A
BDJ14X1A
BDJ14X2A
BDJ14X3A
BDJ21X6A
BDJ21X7A
BDJ21X8A
BDJ23X6A
BDJ23X7A
BDJ23X8A
BDJ31X6A
BDJ31X7A
BDJ31X8A
BDJ33X6A
BDJ33X7A
BDJ33X8A
Cure
Cycle
1
1
1
2
2
2
1
1
1
2
2
2
1
1
1
2
2
2
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
133.721
138.173
137.221
134.527
136.931
132.648
133.952
136.739
132.941
131.080
138.635
135.439
127.783
122.940
130.269
128.737
123.953
129.618
Modulus
[Msi]
10.122
Poisson's
Ratio
0.056
10.059
0.052
9.568
0.052
9.863
0.046
10.047
0.043
10.029
0.053
132.517
4.617
3.484
122.940
138.635
18
9.948
0.205
2.064
9.568
10.122
6
0.050
0.005
9.877
0.043
0.056
6
Avg. Specimen
Thickn. [in]
0.102
0.104
0.104
0.104
0.102
0.104
0.108
0.107
0.106
0.109
0.108
0.108
0.107
0.106
0.105
0.106
0.106
0.107
# Plies in
Laminate
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
Avg. tply
[in]
0.01461
0.01485
0.01492
0.01486
0.01463
0.01481
0.01550
0.01533
0.01520
0.01551
0.01545
0.01538
0.01524
0.01514
0.01505
0.01516
0.01518
0.01522
Averagenorm 0.01511
Standard Dev.norm
Coeff. of Var. [%]norm
Min.
0.0146
Max.
0.0155
Number of Spec.
Strengthnorm
[ksi]
130.219
136.770
136.459
133.245
133.519
130.942
138.396
139.713
134.714
135.533
142.816
138.900
129.791
124.053
130.745
130.106
125.449
131.531
Modulusnorm
[Msi]
9.857
133.494
4.922
3.687
124.053
142.816
18
10.041
0.158
1.571
9.857
10.205
6
9.963
9.885
10.198
10.205
10.136
40
Pooled Average = 133.494 [ksi]

Pooled Standard Deviation = 4.922 [ksi]
Pooled Coeff. of Variation = 3.687 [%]
0 Tension -- (RTD)
Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
25
50
75
100
125
150
175
200
225
250
275
0
300
0 Tension Strength [ksi]
Pooled Average = 10.041 [Msi]

Pooled Standard Deviation = 0.158 [Msi]
0 Tension -- (RTD)
Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
0 Tension Modulus [Msi]
41
0 Tension -- (CTD)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDJ12X5B
BDJ12X6B
BDJ12X7B
BDJ14X5B
BDJ14X6B
BDJ14X7B
BDJ22X5B
BDJ22X6B
BDJ22X7B
BDJ24X5B
BDJ24X6B
BDJ24X7B
BDJ32X6B
BDJ32X7B
BDJ32X8B
BDJ34X6B
BDJ34X8B
BDJ34X9B
Cure
Cycle
1
1
1
2
2
2
1
1
1
2
2
2
1
1
1
2
2
2
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
136.980
119.187
128.021
132.471
135.418
136.185
129.792
128.645
127.855
126.556
128.052
138.673
119.991
111.896
114.552
116.994
115.406
117.637
Modulus
[Msi]
10.178
Poisson's
Ratio
0.076
10.051
0.046
10.112
0.069
9.650
0.051
10.063
0.061
125.795
8.485
6.745
111.896
138.673
18
10.011
0.208
2.076
9.650
10.178
5
0.060
0.012
20.418
0.046
0.076
5
Avg. Specimen
Thickn. [in]
0.104
0.104
0.105
0.104
0.104
0.103
0.108
0.108
0.108
0.108
0.107
0.103
0.105
0.104
0.105
0.104
0.106
0.105
# Plies in
Laminate
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
Avg. tply
[in]
0.01486
0.01483
0.01493
0.01487
0.01481
0.01471
0.01548
0.01543
0.01547
0.01537
0.01526
0.01476
0.01500
0.01490
0.01499
0.01479
0.01518
0.01493
Averagenorm 0.01503
Standard Dev.norm
Min.
0.0147
Max.
0.0155
Number of Spec.
Strengthnorm
[ksi]
135.675
117.843
127.452
131.356
133.677
133.548
133.953
132.301
131.833
129.650
130.308
136.471
119.972
111.167
114.479
115.360
116.780
117.114
Modulusnorm
[Msi]
10.081
126.052
8.580
6.807
111.167
136.471
18
10.086
0.211
2.092
9.886
10.437
5
9.966
10.437
9.886
10.062
42
0 Tension -- (CTD)
Normalized Strength


6
3
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
25
50
75
100
125
150
175
200
225
250
275
0
300

Pooled Coeff . of Variation = 2.092 [%]
0 Tension -- (CTD)
Normalized Modulus
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
43
0 Tension -- (ETW)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDJ11X5F
BDJ11X6F
BDJ11X7F
BDJ11X8F
BDJ11X9F
BDJ13X5F
BDJ13X6F
BDJ13X7F
BDJ13X8F
BDJ13X9F
BDJ21X1F
BDJ21X2F
BDJ21X3F
BDJ21X4F
BDJ21X5F
BDJ23X1F
BDJ23X2F
BDJ23X3F
BDJ23X4F
BDJ23X5F
BDJ31X1F
BDJ31X2F
BDJ31X3F
BDJ31X4F
BDJ31X5F
BDJ33X1F
BDJ33X2F
BDJ33X3F
BDJ33X4F
BDJ33X5F
Cure
Cycle
1
1
1
1
1
2
2
2
2
2
1
1
1
1
1
2
2
2
2
2
1
1
1
1
1
2
2
2
2
2
Prepreg
Lot #
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
1
2
2
2
2
2
3
3
3
3
3
4
4
4
4
4
5
5
5
5
5
6
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
135.069
136.604
136.630
135.739
132.625
128.534
127.650
125.857
133.019
131.933
126.400
129.699
131.040
124.308
126.050
132.357
130.727
129.186
128.689
127.175
131.200
137.840
132.716
131.368
134.110
131.466
134.154
129.888
126.691
124.297
Modulus
[Msi]
9.893
Poisson's
Ratio
0.036
9.719
0.028
9.494
0.035
9.360
0.031
10.289
0.024
9.928
0.041
130.767
3.731
2.853
124.297
137.840
30
9.781
0.333
3.409
9.360
10.289
6
0.032
0.006
18.834
0.024
0.041
6
Avg. Specimen
Thickn. [in]
0.104
0.105
0.103
0.103
0.102
0.105
0.104
0.105
0.105
0.103
0.106
0.106
0.107
0.108
0.108
0.108
0.109
0.109
0.108
0.108
0.105
0.104
0.106
0.106
0.105
0.105
0.103
0.104
0.106
0.106
# Plies in
Laminate
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
Avg. tply
[in]
0.01488
0.01496
0.01475
0.01472
0.01464
0.01501
0.01490
0.01498
0.01497
0.01475
0.01514
0.01518
0.01535
0.01548
0.01544
0.01536
0.01561
0.01553
0.01542
0.01545
0.01500
0.01481
0.01513
0.01510
0.01499
0.01496
0.01467
0.01492
0.01521
0.01517
Averagenorm 0.01508
Standard Dev.norm
Min.
0.0146
Max.
0.0156
Number of Spec.
Strengthnorm
[ksi]
133.997
136.235
134.331
133.175
129.404
128.595
126.819
125.677
132.724
129.755
127.604
131.263
134.097
128.254
129.711
135.550
136.039
133.779
132.284
131.011
131.179
136.112
133.854
132.223
134.046
131.090
131.236
129.167
128.461
125.698
Modulusnorm
[Msi]
9.815
131.446
3.073
2.338
125.677
136.235
30
9.816
0.263
2.675
9.585
10.288
6
9.723
9.585
9.586
10.288
9.899
44

0 Tension -- (ETW)
Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
25
50
75
100
125
150
175
200
225
250
275
0
300

0 Tension -- (ETW)
Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
45
0 Tension -- (ETD)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDJ11X1G
BDJ11X2G
BDJ11X3G
BDJ13X1G
BDJ13X2G
BDJ13X3G
BDJ22X1G
BDJ22X2G
BDJ22X3G
BDJ24X2G
BDJ24X3G
BDJ24X8G
BDJ32X1G
BDJ32X2G
BDJ32X3G
BDJ34X1G
BDJ34X2G
BDJ34X3G
Cure
Cycle
1
1
1
2
2
2
1
1
1
2
2
2
1
1
1
2
2
2
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
139.769
141.042
138.180
134.234
136.404
136.449
134.299
137.304
131.389
131.635
123.708
132.799
121.746
122.392
125.203
118.959
123.771
118.022
Modulus
[Msi]
10.054
Poisson's
Ratio
0.040
10.195
0.032
9.581
0.028
9.557
0.020
10.222
0.040
9.858
0.023
130.406
7.510
5.759
118.022
141.042
18
9.911
0.295
2.974
9.557
10.222
6
0.030
0.009
28.121
0.020
0.040
6
Avg. Specimen
Thickn. [in]
0.103
0.103
0.104
0.102
0.104
0.104
0.107
0.105
0.106
0.108
0.108
0.107
0.105
0.105
0.103
0.104
0.104
0.105
# Plies in
Laminate
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
Avg. tply
[in]
0.01465
0.01476
0.01490
0.01463
0.01479
0.01493
0.01526
0.01493
0.01514
0.01545
0.01549
0.01528
0.01504
0.01505
0.01471
0.01486
0.01488
0.01495
Averagenorm 0.01498
Standard Dev.norm
Min.
0.0146
Max.
0.0155
Number of Spec.
Strengthnorm
[ksi]
136.464
138.804
137.303
130.889
134.521
135.778
136.623
136.693
132.599
135.584
127.753
135.244
122.094
122.820
122.818
117.883
122.809
117.610
Modulusnorm
[Msi]
9.817
130.238
7.288
5.596
117.610
138.804
18
9.895
0.187
1.892
9.747
10.251
6
9.941
9.747
9.843
10.251
9.769
46

Pooled Coef f. of Variation = 5.596 [%]
0 Tension -- (ETD)
Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
25
50
75
100
125
150
175
200
225
250
0
300
275

0 Tension -- (ETD)
Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
47
90 Tension-- (RTD)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDU12X1A
BDU12X2A
BDU12X3A
BDU14X1A
BDU14X2A
BDU14X3A
BDU21X6A
BDU21X7A
BDU21X8A
BDU23X6A
BDU23X7A
BDU23X8A
BDU32X1A
BDU32X2A
BDU32X3A
BDU34X5A
BDU34X6A
BDU34X7A
Cure
Cycle
1
1
1
2
2
2
1
1
1
2
2
2
1
1
1
2
2
2
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
119.760
120.597
123.191
131.497
127.730
121.694
126.203
129.937
122.987
129.936
133.727
133.589
117.174
121.342
123.525
123.829
120.981
127.640
Modulus
[Msi]
10.176
125.297
4.938
3.941
117.174
133.727
18
9.837
0.253
2.577
9.546
10.176
6
10.050
9.546
9.906
9.763
9.580
Avg. Specimen
Thickn. [in]
0.103
0.104
0.104
0.102
0.105
0.104
0.108
0.108
0.106
0.106
0.107
0.105
0.105
0.103
0.107
0.106
0.107
0.105
# Plies in
Laminate
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
Avg. tply
[in]
0.01478
0.01489
0.01480
0.01460
0.01498
0.01482
0.01548
0.01539
0.01520
0.01521
0.01524
0.01506
0.01501
0.01477
0.01525
0.01519
0.01524
0.01502
Averagenorm 0.01505
Standard Dev.norm
Min.
0.0146
Max.
0.0155
Number of Spec.
Strengthnorm
[ksi]
118.011
119.716
121.509
128.011
127.547
120.264
130.230
133.278
124.627
131.751
135.892
134.098
117.248
119.455
125.564
125.401
122.921
127.782
Modulusnorm
[Msi]
10.028
125.739
5.757
4.579
117.248
135.892
18
9.863
0.142
1.444
9.702
10.045
6
9.784
9.851
10.045
9.769
9.702
48

90 Tension -- (RTD)
Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
25
50
75
100
125
150
175
200
225
0
250

90 Tension -- (RTD)
Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
49
90 Tension-- (CTD)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDU12X5B
BDU12X6B
BDU12X7B
BDU14X5B
BDU14X6B
BDU14X7B
BDU24X5B
BDU24X6B
BDU24X7B
BDU22X5B
BDU22X6B
BDU22X7B
BDU33X6B
BDU33X7B
BDU33X8B
BDU31X6B
BDU31X7B
BDU31X8B
Cure
Cycle
1
1
1
2
2
2
2
2
2
1
1
1
2
2
2
1
1
1
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
116.364
113.681
116.322
130.931
122.990
123.179
118.148
130.395
125.101
122.510
116.496
116.356
117.350
118.724
117.663
124.415
115.832
123.503
Modulus
[Msi]
11.333
120.553
5.043
4.183
113.681
130.931
18
10.632
0.452
4.247
10.105
11.333
6
10.105
10.580
10.190
10.799
10.788
Avg. Specimen
Thickn. [in]
0.104
0.104
0.105
0.103
0.105
0.104
0.108
0.107
0.109
0.108
0.109
0.110
0.106
0.106
0.107
0.107
0.106
0.107
# Plies in
Laminate
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
Avg. tply
[in]
0.01488
0.01491
0.01494
0.01470
0.01501
0.01493
0.01548
0.01530
0.01561
0.01550
0.01563
0.01565
0.01509
0.01521
0.01530
0.01533
0.01521
0.01526
Averagenorm 0.01522
Standard Dev.norm
Min.
0.0147
Max.
0.0156
Number of Spec.
Strengthnorm
[ksi]
115.404
113.032
115.879
128.291
123.068
122.573
121.937
132.982
130.165
126.574
121.397
121.379
118.077
120.363
120.016
127.121
117.450
125.620
Modulusnorm
[Msi]
11.239
122.296
5.379
4.398
113.032
132.982
18
10.746
0.474
4.416
9.901
11.239
6
9.901
10.919
10.528
10.866
11.022
50

90 Tension -- (CTD)
Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
25
50
75
100
125
150
175
200
225
0
250

90 Tension -- (CTD)
Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
51
90 Tension-- (ETW)
Strength & Modulus
normalizing tply
[in]
0.0150
Fiberite 7740/T650 3K-135-8H Graphite Fabricite

Specimen
Number
BDU11X1F
BDU11X2F
BDU11X3F
BDU11X4F
BDU11X5F
BDU13X1F
BDU13X2F
BDU13X3F
BDU13X4F
BDU13X5F
BDU21X1F
BDU21X2F
BDU21X3F
BDU21X4F
BDU21X5F
BDU23X1F
BDU23X2F
BDU23X3F
BDU23X4F
BDU23X5F
BDU31X1F
BDU31X2F
BDU31X3F
BDU31X4F
BDU31X5F
BDU33X1F
BDU33X2F
BDU33X3F
BDU33X4F
BDU33X5F
Cure
Cycle
1
1
1
1
1
2
2
2
2
2
1
1
1
1
1
2
2
2
2
2
1
1
1
1
1
2
2
2
2
2
Prepreg
Lot #
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
1
2
2
2
2
2
3
3
3
3
3
4
4
4
4
4
5
5
5
5
5
6
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
109.996
124.566
128.413
121.993
120.888
126.419
135.222
131.725
131.746
127.880
114.065
124.089
121.877
117.860
125.144
123.537
127.399
130.544
129.043
127.718
115.015
116.873
122.299
118.611
119.168
126.751
123.860
120.060
118.910
122.792
Modulus
[Msi]
123.482
5.758
4.663
109.996
135.222
30
9.359
0.384
4.100
8.671
9.699
6
9.343
9.632
8.671
9.699
9.220
9.589
Avg. Specimen
Thickn. [in]
0.101
0.103
0.105
0.105
0.104
0.101
0.101
0.103
0.104
0.104
0.105
0.107
0.108
0.108
0.109
0.103
0.107
0.108
0.107
0.107
0.106
0.104
0.106
0.106
0.106
0.104
0.104
0.106
0.105
0.107
# Plies in
Laminate
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
Avg. tply
[in]
0.01445
0.01473
0.01495
0.01496
0.01488
0.01439
0.01448
0.01468
0.01483
0.01487
0.01502
0.01525
0.01547
0.01547
0.01552
0.01478
0.01531
0.01536
0.01528
0.01533
0.01508
0.01486
0.01518
0.01520
0.01520
0.01486
0.01487
0.01510
0.01506
0.01523
Averagenorm 0.01502
Standard Dev.norm
Min.
0.0144
Max.
0.0155
Number of Spec.
Strengthnorm
[ksi]
105.946
122.332
128.005
121.663
119.929
121.282
130.565
128.924
130.282
126.784
114.228
126.157
125.668
121.527
129.474
121.713
130.028
133.653
131.460
130.536
115.617
115.815
123.775
120.174
120.795
125.584
122.779
120.822
119.420
124.664
Modulusnorm
[Msi]
123.653
6.032
4.878
105.946
133.653
30
9.439
0.320
3.389
8.941
9.881
6
9.318
9.525
8.941
9.881
9.341
9.630
52

90 Tension -- (ETW)
Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
25
50
75
100
125
150
175
200
225
0
250

90 Tension -- (ETW)
Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
53
90 Tension-- (ETD)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDU11X6G
BDU11X7G
BDU11X8G
BDU13X6G
BDU13X7G
BDU13X8G
BDU22X1G
BDU22X2G
BDU22X3G
BDU24X1G
BDU24X2G
BDU24X3G
BDU32X5G
BDU32X6G
BDU32X7G
BDU34X1G
BDU34X2G
BDU34X3G
Cure
Cycle
1
1
1
2
2
2
1
1
1
2
2
2
1
1
1
2
2
2
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
123.807
129.918
132.931
130.868
126.288
127.880
130.932
124.876
125.417
118.925
127.153
130.912
124.218
118.315
123.308
125.015
116.540
117.080
Modulus
[Msi]
9.317
125.243
5.007
3.998
116.540
132.931
18
9.410
0.149
1.588
9.249
9.675
6
9.675
9.388
9.249
9.473
9.361
Avg. Specimen
Thickn. [in]
0.105
0.104
0.104
0.104
0.104
0.105
0.107
0.108
0.108
0.109
0.105
0.106
0.106
0.106
0.103
0.104
0.106
0.106
# Plies in
Laminate
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
Avg. tply
[in]
0.01493
0.01488
0.01484
0.01482
0.01479
0.01500
0.01527
0.01550
0.01547
0.01557
0.01506
0.01521
0.01521
0.01510
0.01469
0.01488
0.01507
0.01521
Averagenorm 0.01508
Standard Dev.norm
Min.
0.0147
Max.
0.0156
Number of Spec.
Strengthnorm
[ksi]
123.237
128.887
131.538
129.310
124.484
127.860
133.322
128.999
129.319
123.436
127.678
132.740
125.934
119.085
120.744
123.983
117.094
118.734
Modulusnorm
[Msi]
9.274
125.910
4.870
3.868
117.094
133.322
18
9.480
0.157
1.656
9.274
9.604
6
9.560
9.559
9.600
9.604
9.283
54

90 Tension -- (ETD)
Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
25
50
75
100
125
150
175
200
0
250
225

90 Tension -- (ETD)
Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
55
0 Compression -- (RTD)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDK1216A
BDK1217A
BDK1218A
BDL12X6A
BDK1129A
BDK112AA
BDK112BA
BDL11X6A
BDK2216A
BDK2217A
BDK2218A
BDL22X6A
BDK2117A
BDK2118A
BDK2119A
BDL2116A
BDK3126A
BDK3128A
BDK3129A
BDL31X6A
BDK3211A
BDK3213A
BDK3214A
BDL32X6A
Cure
Cycle
3
3
3
3
1
1
1
1
3
3
3
3
2
2
2
2
3
3
3
3
4
4
4
4
Prepreg
Lot #
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
2
3
3
3
3
4
4
4
4
5
5
5
5
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
101.467
111.790
107.161
Modulus
[Msi]
9.846
105.938
98.158
96.467
9.047
100.821
102.753
102.481
9.279
103.475
96.992
96.158
9.272
102.631
109.185
104.895
9.862
105.837
97.897
113.081
9.257
103.177
5.070
4.914
96.158
113.081
18
9.427
0.342
3.625
9.047
9.862
6
Avg. Specimen
Thickn. [in]
0.118
0.117
0.118
0.116
0.119
0.119
0.119
0.119
0.116
0.118
0.116
0.122
0.122
0.124
0.122
0.119
0.122
0.119
0.120
0.120
0.121
0.121
0.118
0.122
# Plies in
Laminate
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
Avg. tply
[in]
0.01471
0.01467
0.01473
0.01455
0.01484
0.01483
0.01486
0.01482
0.01454
0.01476
0.01450
0.01525
0.01525
0.01546
0.01526
0.01489
0.01522
0.01489
0.01495
0.01500
0.01511
0.01509
0.01478
0.01522
Averagenorm 0.01492
Standard Dev.norm
Min.
0.0145
Max.
0.0155
Number of Spec.
Strengthnorm
[ksi]
99.522
109.345
105.263
Modulusnorm
[Msi]
9.553
104.791
97.074
95.542
8.940
97.712
101.126
99.044
9.433
105.178
99.963
97.840
9.206
104.128
108.388
104.545
9.859
106.631
98.468
111.408
9.390
102.554
4.682
4.565
95.542
111.408
18
9.397
0.312
3.315
8.940
9.859
6
56

Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
20
40
60
80
100
120
140
160
180
0
200
0 Compression Strength [ksi]

Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
0 Compression Modulus [Msi]

57
0 Compression -- (CTD)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDK1125B
BDK1126B
BDK1127B
BDL11X9B
BDK1223B
BDK1224B
BDK1225B
BDL12X9B
Cure
Cycle
1
1
1
1
3
3
3
3
Prepreg
Lot #
1
1
1
1
1
1
1
1
ASAP
Batch #
1
1
1
1
2
2
2
2
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
97.162
105.642
107.119
Modulus
[Msi]
9.539
104.071
95.004
109.534
9.690
103.089
5.758
5.585
95.004
109.534
6
9.614
0.107
1.116
9.539
9.690
2
Avg. Specimen
Thickn. [in]
0.119
0.119
0.118
0.118
0.118
0.118
0.118
0.117
# Plies in
Laminate
8
8
8
8
8
8
8
8
Avg. tply
[in]
0.01489
0.01488
0.01469
0.01470
0.01473
0.01475
0.01477
0.01464
Averagenorm 0.01476
Standard Dev.norm
Min.
0.0146
Max.
0.0149
Number of Spec.
Strengthnorm
[ksi]
96.434
104.828
104.932
Modulusnorm
[Msi]
9.350
102.185
93.441
107.845
9.456
101.611
5.552
5.464
93.441
107.845
6
9.403
0.075
0.800
9.350
9.456
2
58

Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
20
40
60
80
100
120
140
160
0
200
180

Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
59
0 Compression -- (ETW)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDK1111F
BDK1112F
BDK1113F
BDK1114F
BDK1115F
BDL11X1F
BDK1211F
BDK1212F
BDK1213F
BDK1214F
BDK1215F
BDL12X1F
BDK2211F
BDK2212F
BDK2213F
BDK2214F
BDK2215F
BDL2111F
BDK2111F
BDK2112F
BDK2113F
BDK2114F
BDK2115F
BDL22X1F
BDK3121F
BDK3122F
BDK3123F
BDK3124F
BDK3125F
BDL31X1F
BDK3215F
BDK3217F
BDK3218F
BDK321AF
BDK321BF
BDL32X1F
Cure
Cycle
1
1
1
1
1
1
3
3
3
3
3
3
3
3
3
3
3
2
2
2
2
2
2
3
3
3
3
3
3
3
4
4
4
4
4
4
Prepreg
Lot #
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
4
4
4
4
4
4
5
5
5
5
5
5
6
6
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
64.891
68.540
54.777
47.840
50.907
Modulus
[Msi]
9.155
51.420
54.754
50.591
55.517
53.559
10.282
53.233
44.146
51.216
50.793
56.976
8.919
67.274
60.202
54.471
47.578
51.702
10.652
63.403
60.734
62.131
48.570
65.198
9.741
56.417
58.774
57.500
61.586
65.888
9.625
56.353
6.470
11.481
44.146
68.540
30
9.729
0.656
6.747
8.919
10.652
6
Avg. Specimen
Thickn. [in]
0.120
0.118
0.119
0.116
0.119
0.118
0.117
0.118
0.116
0.117
0.117
0.114
0.119
0.118
0.118
0.117
0.115
0.119
0.124
0.123
0.124
0.123
0.124
0.120
0.123
0.122
0.119
0.119
0.120
0.120
0.120
0.121
0.121
0.120
0.120
0.122
# Plies in
Laminate
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
Avg. tply
[in]
0.01505
0.01481
0.01483
0.01453
0.01484
0.01469
0.01465
0.01476
0.01454
0.01467
0.01460
0.01430
0.01483
0.01474
0.01474
0.01463
0.01435
0.01485
0.01548
0.01534
0.01551
0.01532
0.01544
0.01495
0.01532
0.01520
0.01493
0.01488
0.01503
0.01504
0.01502
0.01507
0.01508
0.01495
0.01501
0.01523
Averagenorm 0.01492
Standard Dev.norm
Min.
0.0143
Max.
0.0155
Number of Spec.
Strengthnorm
[ksi]
65.094
67.669
54.138
46.325
50.355
Modulusnorm
[Msi]
8.969
50.209
53.865
49.052
54.279
52.119
9.800
52.623
43.392
50.341
49.534
54.507
8.830
69.432
61.557
56.321
48.589
53.231
10.619
64.751
61.531
61.833
48.185
65.320
9.767
56.500
59.056
57.811
61.394
65.929
9.773
56.165
6.952
12.377
43.392
69.432
30
9.626
0.652
6.772
8.830
10.619
6
60

Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
20
40
60
80
100
120
140
160
0
200
180

Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
61
0 Compression -- (ETD)
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDK1121G
BDK1123G
BDK1124G
BDL11XCG
BDK1227G
BDK1228G
BDK1229G
BDL12XCG
BDK2221G
BDK2222G
BDK2223G
BDL22X9G
BDK2123G
BDK2124G
BDK2126G
BDL2119G
BDK31X5G
BDK31X6G
BDK31X7G
BDL31X9G
BDK3222G
BDK3224G
BDK3225G
BDL32X9G
Cure
Cycle
1
1
1
1
3
3
3
3
3
3
3
3
2
2
2
2
3
3
3
3
4
4
4
4
Prepreg
Lot #
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
2
3
3
3
3
4
4
4
4
5
5
5
5
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
82.162
77.893
77.762
Modulus
[Msi]
10.695
79.382
80.772
78.180
9.424
80.984
82.296
77.756
8.805
80.125
65.700
77.724
9.095
79.998
76.881
80.928
9.926
86.326
88.621
87.002
9.212
80.027
4.931
6.161
65.700
88.621
18
9.526
0.684
7.183
8.805
10.695
6
Avg. Specimen
Thickn. [in]
0.117
0.119
0.119
0.112
0.118
0.118
0.118
0.118
0.123
0.123
0.123
0.121
0.121
0.122
0.123
0.119
0.122
0.122
0.123
0.120
0.120
0.119
0.119
0.122
# Plies in
Laminate
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
Avg. tply
[in]
0.01464
0.01482
0.01484
0.01406
0.01471
0.01471
0.01470
0.01472
0.01538
0.01535
0.01534
0.01513
0.01518
0.01526
0.01536
0.01491
0.01529
0.01527
0.01532
0.01504
0.01505
0.01492
0.01490
0.01522
Averagenorm 0.01501
Standard Dev.norm
Min.
0.0141
Max.
0.0154
Number of Spec.
Strengthnorm
[ksi]
80.194
76.936
76.952
Modulusnorm
[Msi]
10.024
77.844
79.208
76.633
9.249
83.059
84.233
79.538
8.884
81.093
66.850
79.586
9.042
81.564
78.275
82.631
9.951
86.596
88.159
86.440
9.346
80.322
4.846
6.033
66.850
88.159
18
9.416
0.472
5.009
8.884
10.024
6
62

Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
20
40
60
80
100
120
140
160
0
200
180

Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
63
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDW1116A
BDW1117A
BDW1118A
BDZ11X6A
BDW1216A
BDW1217A
BDW1218A
BDZ12X6A
BDW2111A
BDW2112A
BDW2114A
BDZ21X6A
BDW2216A
BDW2217A
BDW2218A
BDZ22X6A
BDW3121A
BDW3122A
BDW3123A
BDW3216A
BDW3217A
BDW3218A
BDZ31X6A
BDZ32X6A
Cure
Cycle
1
1
1
1
3
3
3
3
2
2
2
2
3
3
3
3
3
3
3
4
4
4
4
4
Prepreg
Lot #
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
2
3
3
3
3
4
4
4
4
5
5
5
6
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
104.777
104.381
97.571
Modulus
[Msi]
9.491
100.807
111.558
106.991
9.642
112.733
103.872
99.832
8.857
102.100
98.868
108.216
9.106
108.601
112.677
106.012
103.530
108.220
115.865
9.408
9.203
105.923
5.159
4.871
97.571
115.865
18
9.285
0.285
3.070
8.857
9.642
6
Avg. Specimen
Thickn. [in]
0.120
0.120
0.120
0.119
0.118
0.118
0.118
0.118
0.123
0.121
0.122
0.121
0.122
0.121
0.122
0.120
0.123
0.123
0.122
0.120
0.121
0.118
0.121
0.121
# Plies in
Laminate
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
Avg. tply
[in]
0.01503
0.01498
0.01501
0.01487
0.01472
0.01473
0.01477
0.01476
0.01536
0.01510
0.01525
0.01517
0.01528
0.01517
0.01523
0.01505
0.01542
0.01542
0.01526
0.01502
0.01512
0.01477
0.01508
0.01512
Averagenorm 0.01507
Standard Dev.norm
Min.
0.0147
Max.
0.0154
Number of Spec.
Strengthnorm
[ksi]
104.995
104.229
97.632
Modulusnorm
[Msi]
9.406
98.917
109.536
105.364
9.485
115.411
104.564
101.496
8.959
104.015
99.960
109.861
9.137
111.633
115.823
107.845
103.660
109.077
114.078
9.459
9.278
106.561
5.475
5.138
97.632
115.823
18
9.287
0.207
2.224
8.959
9.485
6
64

Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
20
40
60
80
100
120
140
160
180
0
200

Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
65
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDW1127B
BDW1129B
BDW112AB
BDZ11X9B
BDW1227B
BDW1228B
BDW1229B
BDZ12X9B
Cure
Cycle
1
1
1
1
3
3
3
3
Prepreg
Lot #
1
1
1
1
1
1
1
1
ASAP
Batch #
1
1
1
1
2
2
2
2
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
108.139
107.222
105.930
Modulus
[Msi]
9.481
117.519
117.833
119.721
9.653
112.727
6.253
5.547
105.930
119.721
6
9.567
0.122
1.273
9.481
9.653
2
Avg. Specimen
Thickn. [in]
0.120
0.120
0.121
0.117
0.119
0.119
0.120
0.116
# Plies in
Laminate
8
8
8
8
8
8
8
8
Avg. tply
[in]
0.01498
0.01503
0.01507
0.01463
0.01493
0.01489
0.01494
0.01449
Averagenorm 0.01487
Standard Dev.norm
Min.
0.0145
Max.
0.0151
Number of Spec.
Strengthnorm
[ksi]
107.981
107.401
106.437
Modulusnorm
[Msi]
9.244
116.932
116.974
119.272
9.326
112.499
5.809
5.163
106.437
119.272
6
9.285
0.058
0.620
9.244
9.326
2
66

Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
20
40
60
80
100
120
140
160
180
0
200

Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
67
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDW1111F
BDW1112F
BDW1113F
BDW1114F
BDW1115F
BDZ11X1F
BDW1211F
BDW1212F
BDW1213F
BDW1214F
BDW1215F
BDZ12X1F
BDW2118F
BDW2119F
BDW211AF
BDW211BF
BDW211CF
BDZ21X1F
BDW2211F
BDW2212F
BDW2214F
BDW2215F
BDZ22X1F
BDW3111F
BDW3112F
BDW3113F
BDW3114F
BDZ31X1F
BDW321AF
BDW3211F
BDW3212F
BDW3213F
BDW3214F
BDW3215F
BDZ32X1F
Cure
Cycle
1
1
1
1
1
1
3
3
3
3
3
3
2
2
2
2
2
2
3
3
3
3
3
4
4
4
4
4
4
4
4
4
4
4
4
Prepreg
Lot #
1
1
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
4
4
4
4
4
5
5
5
5
5
6
6
6
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
58.183
51.573
52.084
48.560
51.432
Modulus
[Msi]
9.196
50.985
42.427
46.924
56.386
52.188
10.269
52.869
56.858
54.332
50.345
41.144
9.355
46.348
43.464
47.046
45.683
9.535
47.415
51.337
48.599
48.743
9.144
47.499
52.334
51.721
53.087
54.600
48.799
9.601
50.102
4.165
8.313
41.144
58.183
29
9.517
0.410
4.312
9.144
10.269
6
Avg. Specimen
Thickn. [in]
0.120
0.117
0.118
0.118
0.119
0.119
0.118
0.118
0.119
0.118
0.117
0.117
0.123
0.122
0.121
0.123
0.121
0.122
0.122
0.121
0.119
0.121
0.123
0.120
0.119
0.120
0.121
0.121
0.119
0.120
0.121
0.122
0.118
0.120
0.119
# Plies in
Laminate
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
Avg. tply
[in]
0.01497
0.01465
0.01471
0.01478
0.01493
0.01481
0.01480
0.01470
0.01483
0.01474
0.01464
0.01464
0.01533
0.01529
0.01517
0.01534
0.01516
0.01530
0.01526
0.01511
0.01487
0.01515
0.01533
0.01494
0.01490
0.01501
0.01511
0.01515
0.01490
0.01494
0.01509
0.01523
0.01474
0.01496
0.01489
Averagenorm 0.01498
Standard Dev.norm
Min.
0.0146
Max.
0.0153
Number of Spec.
Strengthnorm
[ksi]
58.050
50.380
51.064
47.852
51.175
Modulusnorm
[Msi]
9.081
50.316
41.587
46.386
55.411
50.938
10.023
54.026
57.971
54.954
51.489
41.590
9.542
47.160
43.772
46.644
46.140
9.741
47.217
50.994
48.640
49.088
9.234
47.182
52.115
52.045
53.917
53.667
48.677
9.531
50.015
4.204
8.406
41.587
58.050
29
9.525
0.340
3.568
9.081
10.023
6
68

Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
20
40
60
80
100
120
140
160
0
200
180

Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
69
Strength & Modulus
normalizing tply
[in]
0.0150

Specimen
Number
BDW1123G
BDW1124G
BDW1125G
BDZ11XCG
BDW1223G
BDW1224G
BDW1225G
BDZ12XDG
BDW2121G
BDW2122G
BDW2123G
BDZ21X9G
BDW2221G
BDW2222G
BDW2223G
BDZ22X9G
BDW3125G
BDW3126G
BDW3127G
BDW3223G
BDW3224G
BDW3225G
BDZ31X9G
BDZ32X9G
Cure
Cycle
1
1
1
1
3
3
3
3
2
2
2
2
3
3
3
3
3
3
3
4
4
4
4
4
Prepreg
Lot #
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
2
3
3
3
3
4
4
4
4
5
5
5
6
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
67.975
72.609
72.907
Modulus
[Msi]
8.775
74.729
85.327
82.319
9.834
86.420
74.411
82.048
9.143
69.967
73.866
79.925
9.370
77.532
81.059
82.909
78.857
75.970
75.655
9.488
8.811
77.471
5.219
6.737
67.975
86.420
18
9.237
0.410
4.438
8.775
9.834
6
Avg. Specimen
Thickn. [in]
0.120
0.121
0.120
0.119
0.119
0.119
0.119
0.117
0.122
0.124
0.123
0.123
0.121
0.120
0.119
0.120
0.123
0.123
0.123
0.121
0.121
0.122
0.119
0.122
# Plies in
Laminate
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
8
Avg. tply
[in]
0.01505
0.01510
0.01503
0.01484
0.01490
0.01491
0.01488
0.01467
0.01529
0.01544
0.01537
0.01533
0.01509
0.01505
0.01493
0.01498
0.01540
0.01536
0.01535
0.01510
0.01513
0.01522
0.01491
0.01523
Averagenorm 0.01511
Standard Dev.norm
Min.
0.0147
Max.
0.0154
Number of Spec.
Strengthnorm
[ksi]
68.201
73.093
73.059
Modulusnorm
[Msi]
8.684
74.247
84.794
81.684
9.619
88.077
76.597
84.048
9.343
70.390
74.127
79.526
9.357
79.616
83.018
84.861
79.399
76.603
76.759
9.431
8.945
78.228
5.493
7.022
68.201
88.077
18
9.230
0.346
3.752
8.684
9.619
6
70

Normalized Strength
6
4
2
3
2
Prepeg Lot #
ASAP Batch #
1
0
0
20
40
60
80
100
120
140
160
0
200
180

Pooled Coeff . of Variation = 3.752 [%]
Normalized Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
2.0
4.0
6.0
8.0
10.0
12.0
14.0
16.0
18.0
0
20.0
71
In-Plane Shear -- (RTD)

Strength & Modulus
Specimen
Number
BDN1112A
BDN1113A
BDN1114A
BDN1115A
BDN1228A
BDN1229A
BDN122AA
BDN2122A
BDN2123A
BDN2124A
BDN2125A
BDN2226A
BDN2229A
BDN222AA
BDN3112A
BDN3115A
BDN3116A
BDN3232A
BDN3233A
BDN3234A
Cure
Cycle
1
1
1
1
4
4
4
2
2
2
2
3
3
3
3
3
3
4
4
4
Prepreg
Lot #
1
1
1
1
1
1
1
2
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
2
2
2
3
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
17.548
18.075
18.010
18.454
18.319
17.875
18.064
17.791
17.520
17.427
17.522
18.437
17.698
17.775
19.103
19.012
18.629
17.900
18.565
18.044
Modulus
[Msi]
0.661
18.088
0.487
2.693
17.427
19.103
20
0.630
0.045
7.187
0.544
0.667
6
0.635
0.544
0.624
0.667
0.651
Avg. Specimen
Thickn. [in]
0.133
0.132
0.133
0.133
0.133
0.133
0.132
0.136
0.134
0.133
0.136
0.133
0.138
0.137
0.138
0.136
0.135
0.133
0.135
0.134
# Plies in
Laminate
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
Avg. tply
[in]
0.01473
0.01468
0.01478
0.01474
0.01475
0.01476
0.01466
0.01509
0.01492
0.01481
0.01508
0.01480
0.01532
0.01518
0.01533
0.01514
0.01498
0.01475
0.01505
0.01489
0.0149
Min.
Max.
0.0147
0.0153
72
Pooled Average 18.088 [ksi]


Measured Strength
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0
0
10
15
20
25
30
35
40
In-Plane Shear Strength [ksi]


Measured Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.0
1.1
0
1.2
In-Plane Shear Modulus [Msi]
73
In-Plane Shear -- (CTD)

Strength & Modulus
Specimen
Number
BDN1135B
BDN1136B
BDN1137B
BDN1213B
BDN1214B
BDN1215B
Cure
Cycle
1
1
1
4
4
4
Prepreg
Lot #
1
1
1
1
1
1
ASAP
Batch #
1
1
1
2
2
2
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
22.213
22.317
22.602
24.321
22.862
23.606
Modulus
[Msi]
0.750
22.987
0.821
3.574
22.213
24.321
6
0.789
0.056
7.063
0.750
0.828
2
0.828
Avg. Specimen
Thickn. [in]
0.133
0.133
0.129
0.133
0.134
0.135
# Plies in
Laminate
9
9
9
9
9
9
Avg. tply
[in]
0.01482
0.01477
0.01429
0.01482
0.01484
0.01498
0.0148
Min.
Max.
0.0143
0.0150
74


Measured Strength
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0
0
10
15
20
25
30
35
40


Measured Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.0
1.1
0
1.2
75
In-Plane Shear -- (ETW)

Strength & Modulus
Specimen
Number
BDN1121F
BDN1124F
BDN1127F
BDN1128F
BDN1129F
BDN1223F
BDN1224F
BDN1225F
BDN1226F
BDN1227F
BDN2126F
BDN2127F
BDN2128F
BDN2129F
BDN212AF
BDN2211F
BDN2213F
BDN2214F
BDN2216F
BDN2217F
BDN3117F
BDN3119F
BDN3127F
BDN3129F
BDN312AF
BDN3226F
BDN3227F
BDN3228F
BDN3229F
BDN322AF
Cure
Cycle
1
1
1
1
1
4
4
4
4
4
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
4
4
4
4
4
Prepreg
Lot #
1
1
1
1
1
1
1
1
1
1
2
2
2
2
2
2
2
2
2
2
3
3
3
3
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
1
2
2
2
2
2
3
3
3
3
3
4
4
4
4
4
5
5
5
5
5
6
6
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
9.993
8.779
9.391
8.056
8.685
9.525
8.391
8.084
8.283
8.380
9.234
8.495
8.977
8.223
9.122
8.958
8.346
7.853
8.131
8.654
10.190
9.339
8.866
9.219
8.998
9.568
9.345
9.127
8.812
8.837
Modulus
[Msi]
8.862
0.577
6.512
7.853
10.190
30
0.328
0.014
4.148
0.311
0.350
6
0.323
0.350
0.324
0.311
0.323
0.337
Avg. Specimen
Thickn. [in]
0.129
0.135
0.134
0.135
0.134
0.132
0.131
0.131
0.129
0.131
0.136
0.137
0.137
0.135
0.135
0.136
0.136
0.135
0.137
0.137
0.134
0.138
0.135
0.134
0.132
0.139
0.137
0.139
0.134
0.138
# Plies in
Laminate
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
Avg. tply
[in]
0.01437
0.01505
0.01489
0.01500
0.01491
0.01467
0.01460
0.01451
0.01435
0.01451
0.01513
0.01517
0.01519
0.01502
0.01503
0.01515
0.01510
0.01504
0.01524
0.01522
0.01488
0.01529
0.01495
0.01491
0.01471
0.01542
0.01520
0.01541
0.01491
0.01532
0.0150
Min.
Max.
0.0144
0.0154
76
Pooled Average 8.862 [ksi]


Measured Strength
6
4
2
3
Prepreg Lot #
ASAP Batch #
0
0
10
15
20
25
30
35
40


Measured Modulus
6
4
2
3
Prepreg Lot #
ASAP Batch #
0
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.0
1.1
0
1.2
77
In-Plane Shear -- (ETD)

Strength & Modulus
Specimen
Number
BDN1131G
BDN1132G
BDN1133G
BDN1217G
BDN1218G
BDN1219G
BDN2111G
BDN2113G
BDN2114G
BDN2223G
BDN2224G
BDN2225G
BDN3122G
BDN3123G
BDN3124G
BDN3235G
BDN3236G
BDN3237G
Cure
Cycle
1
1
1
4
4
4
2
2
2
3
3
3
3
3
3
4
4
4
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
2
2
2
3
3
3
4
4
4
5
5
5
6
6
6
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
12.829
13.529
12.527
12.664
13.240
12.526
12.475
13.535
12.874
12.226
13.060
12.653
14.381
13.579
13.537
13.000
13.547
13.163
Modulus
[Msi]
0.404
13.075
0.542
4.142
12.226
14.381
18
0.422
0.037
8.746
0.384
0.492
6
0.492
0.384
0.409
0.421
0.424
Avg. Specimen
Thickn. [in]
0.134
0.135
0.133
0.134
0.135
0.136
0.137
0.137
0.139
0.138
0.138
0.139
0.135
0.133
0.132
0.135
0.135
0.134
# Plies in
Laminate
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
9
Avg. tply
[in]
0.01491
0.01495
0.01482
0.01494
0.01501
0.01506
0.01523
0.01522
0.01542
0.01539
0.01538
0.01539
0.01497
0.01477
0.01465
0.01501
0.01501
0.01494
0.0151
Min.
Max.
0.0147
0.0154
78


Measured Strength
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0
0
10
15
20
25
30
35
40


Measured Modulus
6
4
2
3
2
Prepreg Lot #
ASAP Batch #
1
0
0.0
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1.0
1.1
0
1.2
79
Apparent Interlaminar Shear -- (RTD)

Strength
Specimen
Number
BDQ1111A
BDQ1112A
BDQ1113A
BDQ1114A
BDQ1115A
BDQ1121A
BDQ2111A
BDQ2112A
BDQ2113A
BDQ2114A
BDQ2115A
BDQ2121A
BDQ3111A
BDQ3112A
BDQ3113A
BDQ3114A
BDQ3115A
BDQ3121A
Cure
Cycle
Prepreg
Lot #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
ASAP
Batch #
1
1
1
1
1
1
2
2
2
2
2
2
3
3
3
3
3
3
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
10.695
10.595
11.227
10.701
10.660
10.651
10.197
9.755
10.005
9.598
9.972
10.285
10.678
10.296
10.424
10.755
10.258
10.351
10.395
0.400
3.848
9.598
11.227
18
Avg. Specimen
Thickn. [in]
0.113
0.119
0.114
0.118
0.115
0.113
0.104
0.104
0.102
0.101
0.103
0.103
0.100
0.101
0.099
0.101
0.101
0.100
# Plies in
Laminate
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
Avg. tply
[in]
0.01616
0.01693
0.01630
0.01688
0.01636
0.01614
0.01481
0.01488
0.01458
0.01446
0.01478
0.01471
0.01426
0.01446
0.01414
0.01436
0.01442
0.01435
0.0152
Min.
Max.
0.0141
0.0169
80

Apparent Interlaminar Shear -- (RTD)

Measured Strength
Prepreg Lot #
ASAP Batch #
0
0
10
12
14
16
18
20
Apparent Interlaminar Shear Strength [ksi]
81
3.2.2 Fluid Sensitivity Raw Data Spreadsheets and Scatter Charts
82
In-Plane Shear -- (MEK - RTD)

Strength
Specimen
Number
BDN3238T
BDN3239T
BDN323AT
BDN3222T
BDN3225T
Batch
Number
3
3
3
3
3
Strength
[ksi]
18.121
17.986
18.169
18.426
17.941
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Avg. Specimen
Thickn. [in]
0.135
0.135
0.133
0.136
0.134
18.128
0.191
1.053
17.941
18.426
5
Avg. tply
# Plies in
Laminate
9
9
9
9
9
[in]
0.01502
0.01504
0.01477
0.01514
0.01487
0.0150
Min.
Max.
0.0148
0.0151

In-Plane Shear -- (MEK - RTD)

Measured Strength
Batch #
0
0
10
15
20
25
30
35
40
83
In-Plane Shear -- (JP-4 JET FUEL - ETD)

Strength
Specimen
Number
BDN2116R
BDN2117R
BDN2118R
BDN2119R
BDN2121R
Batch
Number
2
2
2
2
2
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
12.778
12.406
12.244
12.285
11.985
Avg. Specimen
Thickn. [in]
0.138
0.136
0.138
0.139
0.137
12.340
0.289
2.343
11.985
12.778
5
# Plies in
Laminate
9
9
9
9
9
Avg. tply
[in]
0.01537
0.01508
0.01534
0.01546
0.01520
0.0153
Min.
Max.
0.0151
0.0155

In-Plane Shear -- (JP-4 JET FUEL - ETD)

Measured Strength
Batch #
0
0
10
15
20
25
30
35
40
84
In-Plane Shear -- (Hydraulic Fluid - ETD)

Strength
Specimen
Number
BDN1117V
BDN1118V
BDN111AV
BDN1139V
BDN113AV
Batch
Number
1
1
1
1
1
Average
Standard Dev.
Coeff. of Var. [%]
Min.
Max.
Number of Spec.
Strength
[ksi]
12.111
12.151
12.229
11.786
11.709
Avg. Specimen
Thickn. [in]
0.133
0.133
0.128
0.135
0.135
11.997
0.233
1.945
11.709
12.229
5
# Plies in
Laminate
9
9
9
9
9
Avg. tply
[in]
0.01474
0.01480
0.01426
0.01502
0.01496
0.0148
Min.
Max.
0.0143
0.0150

In-Plane Shear -- (Hydraulic Fluid - ETD)

Measured Strength
Batch #
0
0
10
15
20
25
30
35
40
85
Fluid Sensitivity Comparison:

Average In-Plane Shear Strength
with Fluid (ksi)
Same Environment In-Plane Shear

Strength without Fluid (ksi)
Worst Case Environment In-Plane

Shear Strength (ksi)
MEK (RTD)
(RTD)
(ETW)
18.13
18.09
8.86
The RTD average in-plane shear strength was not reduced after exposure to MEK.
with Fluid (ksi)


JP-4 JET FUEL (ETD)
(ETD)
(ETW)
12.34
13.08
8.86
The ETD average in-plane shear strength was reduced by 6% after exposure to JP-4 Jet Fuel. However it remained
39% higher than water exposure in ETW conditions.
with Fluid (ksi)

HYDRAULIC FLUID (ETD)
(ETD)
(ETW)
12.00
13.08
8.86

The ETD average in-plane shear strength was reduced by 8% after exposure to Hydraulic Fluid. However, it
remained 35% higher than water exposure in ETW conditions.
86
3.2.3 Representative Shear Stress-Strain Curve

The following stress-strain curve is representative of the T650 3K-135-8H / 7740 prepreg system. The tension and
compression stress-strain curves are not presented in graphical form. If strain design allowables from these tests
are required, simple one-dimensional linear stress-strain relationships may be used to obtain corresponding strain
design values. This process should approximate tensile and compressive strain behavior relatively well but may
produce extremely conservative strain values in shear due to the nonlinear behavior. A more realistic approach for
shear strain design allowables is to use a maximum strain value of 5% (reference MIL-HDBK-17-1E, section 5.7.6).
If a nonlinear analysis of the materials shear behavior is required, the curve-fit of the shear stress-strain curve may
be used. The representative shear stress-strain curve was obtained by taking the average of all the sample shear
curves and determining the best-fit line through the data. The actual data points also presented on the chart to
demonstrate material variability.
87
Shear Stress vs. Shear Strain, RTD

14000
12000
Shear Stress [psi]
10000
8000
6000
-1
y = a+blnx/x
2
r = 0.99999885
a = 7.4250665e-05
b = -2.167502e-07
4000
2000
0
0
0.02
0.04
0.06
0.08
0.1
0.12
Shear Strain [in/in]

88
3.3 Statistical Results
89
3.3.1 Plot by Condition
90
DISTRIBUTION OF GROUPED DATA FOR DIFFERENT TEST CONDITIONS

Cessna
1.20
CTD
RTD
ETD
ETW
NO DATA
1.00
PROBABILITY OF SURVIVAL
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.80
NORMAL CURVE
NORMAL CURVE
0.60
0.40
0.20
0.00
0.60
50.60
100.60
150.60
200.60
250.60
0 Tension - BDJXXXXX Measured
91

Cessna
1.20
CTD
RTD
ETD
ETW
NO DATA
1.00
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.80
NORMAL CURVE
NORMAL CURVE
0.60
0.40
0.20
0.00
0.60
50.60
100.60
150.60
200.60
250.60
0 Tension - BDJXXXXX Normalized
92

Cessna
1.20
CTD
RTD
ETD
ETW
NO DATA
1.00
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.80
NORMAL CURVE
NORMAL CURVE
0.60
0.40
0.20
0.00
0.60
50.60
100.60
150.60
200.60
250.60
90 Tension - BDUXXXXX Measured
93

Cessna
1.20
CTD
RTD
ETD
ETW
NO DATA
1.00
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.80
NORMAL CURVE
NORMAL CURVE
0.60
0.40
0.20
0.00
0.60
50.60
100.60
150.60
200.60
250.60
90 Tension - BDUXXXXX Normalized
94

Cessna
1.20
CTD
RTD
ETD
ETW
NO DATA
1.00
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.80
NORMAL CURVE
NORMAL CURVE
0.60
0.40
0.20
0.00
0.60
20.60
40.60
60.60
80.60
100.60
120.60
140.60
160.60
180.60
0 Compression - BDKXXXXX Measured
95

Cessna
1.20
CTD
RTD
ETD
ETW
NO DATA
1.00
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.80
NORMAL CURVE
NORMAL CURVE
0.60
0.40
0.20
0.00
0.60
20.60
40.60
60.60
80.60
100.60
120.60
140.60
160.60
180.60
0 Compression - BDKXXXXX Normalized
96

Cessna
1.20
CTD
RTD
ETD
ETW
NO DATA
1.00
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.80
NORMAL CURVE
NORMAL CURVE
0.60
0.40
0.20
0.00
0.60
20.60
40.60
60.60
80.60
100.60
120.60
140.60
160.60
180.60
90 Compression - BDWXXXXX Measured
97

Cessna
1.20
CTD
RTD
ETD
ETW
NO DATA
1.00
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.80
NORMAL CURVE
NORMAL CURVE
0.60
0.40
0.20
0.00
0.60
20.60
40.60
60.60
80.60
100.60
120.60
140.60
160.60
180.60
90 Compression - BDWXXXXX Normalized
98

Cessna
1.20
CTD
RTD
ETD
ETW
NO DATA
1.00
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.80
NORMAL CURVE
NORMAL CURVE
0.60
0.40
0.20
0.00
0.60
5.60
10.60
15.60
20.60
25.60
30.60
In-Plane Shear - BDNXXXXX Measured
99

Cessna
1.20
CTD
RTD
ETD
ETW
NO DATA
1.00
NORMAL CURVE
NORMAL CURVE
NORMAL CURVE
0.80
NORMAL CURVE
NORMAL CURVE
0.60
0.40
0.20
0.00
0.60
2.60
4.60
6.60
8.60
10.60
12.60
14.60
16.60
Apparent Interlaminar Shear - BDQXXXXX Measured
100
3.3.2 Plot of Pooled Data
101
DISTRIBUTION OF POOLED DATA

Cessna
0 Tension - BDJXXXXX Measured
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.40
0.50
0.60
0.70
0.80
0.90
1.00
1.10
1.20
NORMALIZED VALUE
102

Cessna
0 Tension - BDJXXXXX Normalized
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.40
0.50
0.60
0.70
0.80
0.90
1.00
1.10
1.20
NORMALIZED VALUE
103

Cessna
90 Tension - BDUXXXXX Measured
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.40
0.50
0.60
0.70
0.80
0.90
1.00
1.10
1.20
NORMALIZED VALUE
104

Cessna
90 Tension - BDUXXXXX Normalized
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.40
0.50
0.60
0.70
0.80
0.90
1.00
1.10
1.20
NORMALIZED VALUE
105

Cessna
0 Compression - BDKXXXXX Measured
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.40
0.60
0.80
1.00
1.20
1.40
1.60
NORMALIZED VALUE
106

Cessna
0 Compression - BDKXXXXX Normalized
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.40
0.60
0.80
1.00
1.20
1.40
1.60
NORMALIZED VALUE
107

Cessna
90 Compression - BDWXXXXX Measured
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.40
0.50
0.60
0.70
0.80
0.90
1.00
1.10
1.20
1.30
NORMALIZED VALUE
108

Cessna
90 Compression - BDWXXXXX Normalized
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.40
0.50
0.60
0.70
0.80
0.90
1.00
1.10
1.20
1.30
NORMALIZED VALUE
109

Cessna
In-Plane Shear - BDNXXXXX Measured
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.40
0.50
0.60
0.70
0.80
0.90
1.00
1.10
1.20
1.30
NORMALIZED VALUE
110

Cessna
Apparent Interlaminar Shear - BDQXXXXX Measured
1.0
0.9
0.8
0.7
0.6
0.5
0.4
0.3
0.2
0.1
0.0
0.40
0.50
0.60
0.70
0.80
0.90
1.00
1.10
1.20
NORMALIZED VALUE
111
3.4 Moisture Conditioning History Charts
112
Conditioning History Cessna

0.800
BDJ21X
0.700
BDJ23X
0.600
BDJ31X
0.500
BDJ33X
0.400
BDJ33X
BDJ13X
0.300
BDJ11X
0.200
0.100
0.000
0
10
20
30
40
50
60
70
Time (days)

0.800
BDU31X
0.700
BDU33X
0.600
BDU21X
BDU23X
0.500
BDU23X
0.400
BDU13X
0.300
BDU11X
0.200
0.100
0.000
0
10
20
30
40
50
60
Time (days)
113

0.900
BDK31
0.800
BDK32
0.700
BDK21
0.600
BDK22
0.500
BDK22
0.400
BDK12
0.300
BDK11
0.200
0.100
0.000
0
10
20
30
40
50
60
70
Time (days)

0.900
BDL31X
0.800
BDL32X
0.700
BDL21X
0.600
BDL22X
0.500
BDL22X
BDL11X
0.400
BDL12X
0.300
0.200
0.100
0.000
0
10
20
30
40
50
60
70
Time (days)
114

0.800
BDW21X
0.700
BDW22X
BDW31X
0.600
BDW11X
0.500
BDW11X
0.400
BDW32X
BDW12X
0.300
0.200
0.100
0.000
0
10
20
30
40
50
60
70
Time (days)

0.800
BDN11X
0.700
BDN31X
BDN22X
0.600
BDN32X
0.500
BDN32X
0.400
BDN21X
0.300
BDN12X
0.200
0.100
0.000
0
10
20
30
40
50
60
70
Time (days)
115

0.900
BDZ31X
0.800
BDZ32X
0.700
BDZ21X
0.600
BDZ22X
0.500
BDZ22X
0.400
BDZ11X
0.300
BDZ12X
0.200
0.100
0.000
0
10
20
30
40
50
60
70
Time (days)

0.800
0.700
0.600
BDD11
0.500
BDD21
0.400
BDD31
0.300
0.200
0.100
0.000
0
20
40
60
80
Time (days)
116
3.5 Physical Test Results
117
Physical Test Summary

Composite
Density
[g/cc]
Resin
Content
[wt%]
Fiber
Volume
[vol%]
Void
Content
[vol%]
0 Tension (BDJXXXXX)
No. of Specimens
Mean
Standard Deviation
12
1.528
0.007
12
34.139
1.755
12
56.712
1.553
12
2.203
0.720
90 Tension (BDUXXXXX)
No. of Specimens
Mean
Standard Deviation
12
1.520
0.010
12
35.010
2.075
12
55.665
1.926
12
2.431
0.797
0 Compression (BDKXXXXX)
No. of Specimens
Mean
Standard Deviation
7
1.516
0.011
7
35.345
2.656
7
55.227
2.372
7
2.581
1.079
90 Compression (BDWXXXXX)
No. of Specimens
Mean
Standard Deviation
6
1.523
0.003
6
36.716
2.944
6
54.285
2.498
6
1.693
1.068
In-Plane Shear (BDNXXXXX)

No. of Specimens
Mean
Standard Deviation
6
1.519
0.006
6
33.319
2.777
6
57.041
2.466
6
3.129
0.891
Interlaminar Shear (BDQXXXXX)

No. of Specimens
Mean
Standard Deviation
3
1.520
0.006
3
37.047
0.825
3
53.916
0.612
3
1.736
0.585
Overall No. of Specimens

Overall Mean
Overall Std. Deviation
46
1.522
0.009
46
34.969
2.421
46
55.757
2.158
46
2.344
0.920
118
COMPANY :
MATERIAL SYSTEM :
PROJECT :
Cessna
980409C1
DMA Results -- Onset Storage Modulus

DRY
Sample #
BDD1X1FA
BDD1X1GA
BDD1X1HA
BDD2X1GA
BDD2X1HA
BDD2X1IA
BDD3X1FA
BDD3X1GA
BDD3X1HA
WET
As Fabricated
Tg [C]
105.92
106.25
110.85
104.59
109.01
113.81
116.14
110.30
112.38
Tg [F]
222.66
223.25
231.53
220.26
228.22
236.85
241.05
230.53
234.28
Moisture Equilibirum at 85% RH

Sample #
Tg [C]
Tg [F]
BDD1X1BC
82.63
180.73
BDD1X1CC
83.63
182.53
BDD1X1DC
87.36
189.26
BDD2X1BC
81.91
179.44
BDD2X1CC
84.72
184.50
BDD2X1FC
84.57
184.23
BDD3X1BC
83.97
183.14
BDD3X1CC
82.97
181.34
BDD3X1DC
84.32
183.77
Average [F]
Standard Dev. [F]
Coeff. Of Var. [%]
229.85
6.96
3.03
Average [F]
Standard Dev. [F]
Coeff. Of Var. [%]
183.22
2.82
1.54
DMA Results - Peak Tan Delta

DRY
Sample #
BDD1X1FA
BDD1X1GA
BDD1X1HA
BDD2X1GA
BDD2X1HA
BDD2X1IA
BDD3X1FA
BDD3X1GA
BDD3X1HA
WET
As Fabricated
Tg [C]
123.83
126.16
123.88
122.94
124.26
125.37
126.39
124.64
124.93
Tg [F]
254.89
259.09
254.99
253.29
255.68
257.67
259.49
256.36
256.87
Moisture Equilibirum at 85% RH

Sample #
Tg [C]
Tg [F]
BDD1X1BC
101.57
214.83
BDD1X1CC
102.55
216.60
BDD1X1DC
101.91
215.44
BDD2X1BC
101.81
215.25
BDD2X1CC
106.74
224.14
BDD2X1FC
104.41
219.94
BDD3X1BC
102.07
215.72
BDD3X1CC
101.27
214.28
BDD3X1DC
102.93
217.28
Average [F]
Standard Dev. [F]
Coeff. Of Var. [%]
256.48
2.03
0.79
Average [F]
Standard Dev. [F]
Coeff. Of Var. [%]
217.05
3.14
1.45
119
BDD1X1FA
BDD1X1GA
120
BDD1X1HA
BDD2X1GA
121
BDD2X1HA
BDD2X1IA
122
BDD3X1FA
BDD3X1GA
123
BDD3X1HA
BDD1X1BC
124
BDD1X1CC
BDD1X1DC
125
BDD2X1BC
BDD2X1CC
126
BDD2X1FC
BDD3X1BC
127
BDD3X1CC
BDD3X1DC
128
4.0 TESTING AND REPORTING COMMENTS
129
All tests were conformed under Designated Option Authority (DOA) by Cessna
Aircraft Co. Inc.
130
APPENDIX A. PHYSICAL TEST DATA SUPPLIED BY MATERIAL VENDOR
131
132
133
134
135
136
137
138
139
140
141
APPENDIX B. DATES OF PANEL MANUFACTURE AND COPY OF FAA FORM

8130-3
142
143

B-Basis T650 3K-135-8H Fabric-7740

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B-Basis T650 3K-135-8H Fabric-7740

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Advanced General

B Basis Design Allowables for

J. Tomblin, J. McKenna, Y. Ng, K. S. Raju

1.1 Scope ................................................................................................................................................... 5

2.0 FIBERITE T650 3K-135-8H / 7740 PREPREG PROPERTIES................................18

3.0 FIBERITE T650 3K-135-8H / 7740 LAMINATE PROPERTIES...............................21

3.2 Raw Data ........................................................................................................................................... 38

TESTING AND REPORTING COMMENTS ........................................................129

APPENDIX A. PHYSICAL TEST DATA SUPPLIED BY MATERIAL VENDOR .........131

1.2 Symbols Used

major Poissons ratio, tension

1.3 Acronyms and Definitions

95% lower confidence limit on the first population percentile

Tensile Properties of Polymer Matrix Composite Materials

Compressive Properties of Oriented Fiber-Resin Composites

Table 1.5.1: Test Matrix and Standards Used

0o (warp) Tension Strength

Glass Transition Temperature

SACMA SRM 18-94

NO. OF REPLICATES PER

CTD1,5 RTD2,5 ETW3

SACMA SRM 1-94

1.5.2 Environmental Conditioning

W i = weight at current time

1.5.3 Fluid Sensitivity Screening

W i = weight at current time

1.5.4 Normalization Procedures

0 (warp) Tensile Strength and Modulus

The relationship between fiber volume fraction and ultimate laminate

Fiber volume is not commonly measured for each test sample, so

Additional information is detailed in FAA Document DOT/FAA/AR-00/47: Material

Average Sample Thickness

1.5.5 Statistical Analysis

1.5.6 Material Performance Envelope and Interpolation

B-Basis Strength Values (ksi)

Figure 1.5.1 Material performance envelope.

B MOL = B RTD where

(B RTD - BETD )(TRTD - TMOL )

BMOL = new application basis value interpolated to TMOL

BRTD = basis RTD strength value

BRTW = BRTD - ( BETD - BETW )

(BRTW - BETW )(TRTW - TMOL )

BMOL = new application basis value interpolated to TMOL

ETW : BMOL = 59.746 ksi

B-Basis Strength Values (ksi)

Figure 1.5.2 Example of 150o F interpolation for B-basis values.

2.0 FIBERITE T650 3K-135-8H / 7740 PREPREG PROPERTIES

2.1 Prepreg Documentation by Prepreg Lot

Fabric Batch or Lot #, Warp

Prepreg Manufacturer & Product ID:

Fiber/Fabric Manufacturer & Product ID: T650/35 3K 309NT

.93, 1.14, .97, 1.03, 1.09 %

.93, 1.14, .97, 1.03, 1.09 %

B3S0803, 804, 820

B3S0803, 804, 820

.97, 1.03, 1.09 %

.97, 1.03, 1.09 %

1.775 (warp), 1.776 ( fill ) g/cc

1.775 (warp), 1.776 ( fill ) g/cc

Resin Manufacturer & Product ID:

Matrix Batch or Lot #

2.2 Process Specification

3.0 FIBERITE T650 3K-135-8H / 7740 LAMINATE PROPERTIES

3.1 Test Results