TESTS ON CEMENT

DETERMINATION OF FINENESS OF CEMENT 1.0 PURPOSE To establish the procedure for the determination of fineness of cement by dry sieving. 2.0 SCOPE The fineness of cement has an important bearing on the rate of hydration and ultimately the rate of gain of strength. 3.0 4.0 REFERENCE DOCUMET:IS: 4031 (Part-1) APPARATUS 1. 2. 3. 5.0 90 micron sieve with lid & pan Balance 0.01 accuracy Brush

PROCEDURE 1. 2. 3. 4. Weigh 100 (g) cement and sieve from a standard sieve 90 micron Sieve continuously cement sample giving circular and vertical motion for a period of 15 minutes. Weigh the retained mass left on sieve. After sieving the residue by weight on an IS 90 micron shall be weighed.

Acceptance criteria = Residue on the 90 micron sieve shall not exceed 10% of the total weight of sample.

DETERMINATION OF NORMAL CONSISTENCY FOR CEMENT 1.0 PURPOSE: To find out normal consistency of cement. 2.0 SCOPE: The SOP works method of find out normal consistency of cement as per IS: 4031 Part-4 3.0 4.0 REFERENCE DOCUMET:IS: 4031 (Part-4) APPARATUS: 1. 2. 3. 4. 5. 5.0 Vicat Apparatus Balance Gauging trowel Standard weights Non porous plate

DETAILED PROCEDURE: 1. 2. 3. 4. 5. 6. 7. 8. 9. Take 500 gms of cement Add 24% of water into cement The paste must be prepared in a standard manner and filled into vicat mould within 3-5 minutes. After filling the mould shake the mould to expel air. A standard plunger is brought down to touch the surface of the paste in the test block & quickly released allowing it to sink into paste by its own weight. Take the reading. Conduct 2nd trial with % of water at 25 & take the reading. Conduct similar trials with higher w/c ratio till plunger penetrates for a depth of 33-35 mm from the top. The percentage of water at which penetration gives 33-35 from the top or 5 to 7 mm from the bottom is a standard consistency. Acceptance criteria: Amount of water as a % by mass of the dry cement.

DETERMINATION OF SETTING TIMES FOR CEMENT 1.0 2.0 PURPOSE To determine Initial & final setting time. SCOPE The time interval is retained for the cement paste/mortar/concrete for its workability while mixing, transporting and placing. REFERENCE DOCUMENTS: APPARATUS: 1. 2. 3. 4. 5. 1.0 I. Vicat needle apparatus Trowel Balance Weights Stop watch IS-4031-1988 (Part-5)

3.0 4.0

DETAIL PROCEDURE :

INITIAL SETTING TIME a. Take 500(g) cement sample b. Add 85% of consistency water to produce paste. c. Fill paste in vicat mould within 2.5 minutes. d. In the beginning needle will pierce through test block but after sometime when the paste starts losing its plasticity, the needle may penetrate only to a depth 3335 mm from the top. e. Interval of time at which the needle penetrate to test block to a depth equal to 3335 mm from the top is taken as initial setting time.

II.

FINAL SETTING TIME: a. Replace vicat needle by a circular attachment cover the surface of the test block the concrete needle makes an impression. c. The circular arrangement impression not seen on the mould it considered as final setting time. Acceptance criteria: Initial Setting time should not be less than 30minutes Final Setting time should not be more than 600minutes

b. The cement shall be considered as finally set when upon lowering the attachment gently

DETERMINATION OF COMPRESSIVE SRENGTH OF CEMENT 1.0 2.0 3.0 4.0 PURPOSE: To establish the compressive strength of cement mortar. SCOPE: The scope is to determine compressive strength of hardened cement. REFERENCE DOCUMENTS: APPARATUS: 1. 2. 3. 4. 5. 6. 1.0 High frequency mortar cube vibrator. Mixing tools, frogs, trowels Ennore sand confirming IS-650-1960 Moulds of size 7.06x7.06x7.06 cm Poking rod Balance and graduated glass cylinder IS 4031 (Part-6) & IS: 8112-1989

DETAILS PROCEDURE : 1. Take Ennore sand class I, II & III with cement sample and mix with (1:3) proportion in tray. Mix the same for 1 minute in dry condition. 2. 3. 4. 5. 6. 7. Add water (P/4 + 3.0)% and mix thoroughly uniform upto 3.5 minute Immediately after mixing fill mortar in 7.06 x 7.06 mm moulds 9 Nos. Compact the filled cube mould by cube vibration machine up to 2 minutes at the specified speed 12000+/-400 vibrations per minute. Keep mortar cube mould at a temperature of 27 + 2C for 24 hours (may be kept under wet gunny bag to simulate 90% relative humidity. After 24 hours the cubes are removed from the mould and immersed in clean water, until takes out for testing. Three moulds shall be treated at age 3 days (72+/- 1 hour) Three moulds shall be treated at age 7 days (168+/- 2 hours) Three moulds shall be treated at age 28 days (672+/-4 hours) Comp. Strength of cement cube = Load (N) Area (mm2)

Acceptance criteria as per IS- 8112 (For OPC 43 grade): The average compressive strength
for cube not less than 23MPa for 3 days, 33MPa for 7 days & 43MPa for 28 days.

DETERMINATION OF SOUNDNESS FOR CEMENT 1.0 PURPOSE: To establish the procedure for the cement shows any appreciable subsequent expansion. 2.0 SCOPE: Cement shall not go a large expansion after setting and this will cause serious difficulty to the structure. 3.0 4.0 REFERENCE DOCUMENTS: APPARATUS: 1 2 3 4 5 5.0 Le-Chatelier apparatus Water bath Measuring scale Trowel Graduated glass cylinder IS 4031 -1988(Part-3)

DETAILS PROCEDURE: 1. 2. 3. Take 500 gm. Cement sample Add water 78% of consistency water and make a well mixed paste with in 5 minutes. Paste filled into the moulds kept on a glass plate and moulds are closed on the top with another glass plate and keep weight as given in set. Measure the distance between two indicator points before put in to the water. 4. 5. 6. Whole assembly is immersed in water at a temperature of 27 +/-20 c and kept for 24 hours and measure the distance between two indicators. Submerge the mould again water & heat the water at boiling point in @ 25-30 minutes & keep it boiling for 3 hours. Remove the mould from water, allow it to cool and measure the distance between indicator points. The distance between indicator points represent the expansion of cement. 7. It must not exceed 10 mm for OPC. Acceptance criteria: For OPC cement shall not have an expansion more than 10mm (tested by Lechateliers apparatus)

TESTS ON CONCRETE
DETERMINATION OF COMPRESSIVE STRENGTH OF CONCRETE CUBES 1.0 PURPOSE: To determine the compressive strength of concrete. 2.0 SCOPE :

The SOP covers test for determination of compressive strength of concrete. 3.0 4.0 RESPECTIVE DOCUMENTS: IS: 516

APPARATUS i. Compressive strength Test Machine (CTM-200MT) ii. Balance iii. Measuring scale DETAILS PROCEDURE: 1. 2. 3. 4. 5. 6. Specimen (CUBE) stored in water shall be tested immediately after removing from water tank. Size and Weight shall be noted before testing. Cube shall be placed in the machine in such a way that the load shall be applied to opposite sides of the cubes as cast that is not to the top and bottom. The Axis of the cube shall be carefully aligned with the center of thrust of the spherically seated platen. The spherically seated block is brought to bear on cube and the movable portion shall be rotated gently by hand. The load shall be applied continuously without shock and at the rate of 140 kg/Sq.cm/ min. until the resistance of cube to the increasing load breaks down and no greater load can be sustained. The maximum applied load is recorded. 7. Compressive strength is calculated by maximum load applied during the test divided by the cross section area. Comp. Strength of concrete cube = Load / Area (N / mm2) Acceptance criteria as per MoRT&H clause: 1716.2.5

5.0

a)

The mean strength determined from any group of four consecutive samples should exceed the specified characteristic compressive strength. b) Strength of any sample is not les than the specified characteristic compressive strength minus 3MPa.

DETERMINATION OF WORKABILITY OF CONCRETE BY SLUMP 1. SCOPE To determine workability of the concrete mix. 2. 3. REFERENCE DOCUMENTS: IS: 1199 APPARATUS 1. 2. 3. 4. Slump cone apparatus (With complete set) M.S Tray for concrete sample. Float, Trowel.

PROCEDURE: 1. 2. 3. 4. 5. 6. 7. 8. The internal surface of the mould shall be thoroughly cleaned. The mould shall be placed on a smooth, horizontal, rigid & non absorbent leveled surface. The operator shall hold the mould firmly in place while it is being filled with test specimen of concrete. The mould shall be filled in four layers each layer shall be tamped with twenty-five strokes of the rounded end of the tamping rod. After the top layer has been rodded the surplus concrete shall be struck off by trowel. Clean the concrete around the mould. Mould shall be removed form the concrete immediately after filling by raising it slowly and carefully in a vertical direction. The moulded concrete shall be allowed to subside and slump shall be measured immediately by determining the difference between the height of the subsided mould and that horizontal flat of the mould.

Note: Above operation shall be carried out a place free from vibration or shock. RESULT: The slump shall be measured in terms of millimeters.

Acceptance criteria: As per MoRT&H table 1700-4 and as observed in design mix trials, it varies with different grade of concrete. DETERMINATION OF WORKABILITY OF CONCRETE BY COMPACTION FACTOR 1.0 2.0 3.0 4.0 1. 2. 3. 4. 5. PURPOSE: - To determined the workability of the concrete mix. SCOPE: - To know the workability of the Mix for required level compaction factor. REFERENCE DOCUMENTS: APPARATUS: Compaction Factor apparatus Steel float Nos.2 25 mm Needle vibrator No.1 M.S.Tray 600 x 600 x 50 mm Electronic balance 30 kg Capacity IS: 1199-1959

Apparatus consist of two hoppers 1 & 2 , bottom of the hoppers consists of hinged doors. Distance of the hoppers from the base are fixed. Below the lower hopper 2 , one cylindrical mould having (30 cm ht. & 15 cm dia) is fitted. 5.0 DETAILS OF PROCEDURE : a. Fill the hopper No.1 & release the bottom door, the concrete falls from a specified height into the lower hopper No.2 b. Release the door of the lower hopper No.2 concrete will fall in cylindrical mould placed below. c. Remove the surplus concrete from mould by using steel floats. d. Take weight of concrete in mould W1 e. Make empty the cylindrical mould and refilled with concrete from the same sample in layers approximate 5cm deep. Layers being compacted by vibrator Remove surplus concrete & get weight W2 Compaction factor = W1/W2

METHOD OF TEST FOR SURFACE TEXTURE 1. PURPOSE To find out texture depth of rigid pavement concrete. 2. SCOPE The SOP covers the method to determine depth of texture for rigid pavement concrete. 3. APPARATUS : REFERENCE DOCUMENT MoRT&H Clause 602.12 1. 2. 3. 4. 4. Cylinderical container 25 ml capacity. Flat wooden disc (with hard rubber disc at bottom) with handle Measuring Scale Dry natural sand passing IS Sieve 300 micron and retained on 150micron sieve.

PROCEDURE: 1. 2. 3. 4. 5. 6. 7. 8. 9. Surface to be measured shall be dried. Any extraneous mortar or loose material shall be removed by wire brush (Bothlongitudinal & Transverse direction). The cylindrical container shall be filled with the sand, tamp its bottom 3 times on surface and ensure sand level up to the required mark. The sand in container shall be poured into a heap on the surface to be treated. The sand shall be spread over the surface, rotating the disc over sand in a circular motion so that the sand is spread into a circular patch with the surface depressions filled with sand to the level of peaks. The diameter of the patch shall be measured to the nearest 5 mm and five reading are to be taken for a particular location of a panel. Select 4 location in diagonally & one in centre of panel. The texture depth of concrete surface shall be calculated by formula 31000/(D x D) where D = Dia of patch in mm. Two times observations to be done for a particular panel. a. Between 24 hrs to 7 days b. Between 7 days to before 6 weeks.

Acceptance criteria: i. Between 24hours and 7 days 1+/-0.25mm. ii. Not later than 6 weeks before the road is opened to public traffic 1+0.25mmand 1-0.35mm

FLEXURAL STRENGTH OF CONCRETE BEAM 1.0 2.0 3.0 4.0 1. 5.0 PURPOSE: - To determined flexural strength of Pavement Concrete Beam. SCOPE: -This deals with the procedure for determining the flexural strength of moulded concrete flexure test specimen (i.e. beam) to represent PQC Strength. REFERENCE DOCUMENTS: APPARATUS: Flexural Strength M/c DETAILS OF PROCEDURE:a. Take out specimen from curing tank, clean it with water. b. Make a 5 cm mark vertically, on specimen on either ends. c. Specimen shall be placed in machine such a way that the load shall be applied to the upper most surface as cast in mould. d. The axis of the specimen shall be carefully aligned with the axis of the loading device. e. Load shall be applied continuously and without shock. f. The load shall be increased until the specimen fails and load applied is recorded at the failure. g. The appearance of the fractured faces is observed. h. Fractured line is measured to the nearest ends of specimen. Fractured face IS: 516

5cm a

60 cm

5cm

If a > 20 cm, use this formula for modulus rupture fb = p x l bxd2 If a < 20 cm, use this formula for modulus rupture fb = 3p x l bxd2 P = Applied Load (KN), l = Supported Length 60 cm b = Width of the Beam, d = depth of the beam Acceptance criteria: Characteristic flexural strength at 28 days 4.0MPa (As per Technical Specification sub clause 602.3.5)

TESTS ON AGGREGATE
DETERMINATION OF TEN PERCENT FINES VALUE FOR AGGREGATE 1.0 2.0
3.0

4.0

PURPOSE To find out 10% fines value. SCOPE The SOP covers to find out 10% fines value, which gives a measure of the resistance of an aggregate to crushing. REFERENCE DOCUMENTS : BS:812 Part-3 & IS:2386 (Part-IV) APPARATUS 1. Loading Machine 2. 15 cm dia cylinder 3. Plunger 4. IS sieves 12.5 mm, 10 mm & 2.36 mm. 5. Tamping rod 16 mm dia 6. Balance with 1 gm accuracy and 3kg capacity DETAIL PROCEDURE : 1. Take sample from 12.5 mm passing & 10 mm retained & put that sample into soaked condition (i.e. in water) for 24 hrs. 2. Fill the 10% fines mould with sample in 3 layers & tamped each layer 25 strokes with tamping rod. 3. Weight the mould with aggregate Reading A. 4. Put that mould into compressive loading machine & give load upto 15 mm penetration for rounded aggregates & 20 mm penetration for angular aggregates. 5. Note the load value at specified penetration. X 6. Take out the sample from the mould & sieved through 2.36 mm size. Take out of sample passing through.-B 7. Take reading of empty mould C 8. Now, find out % passing from 2.36 mm by formula. B Y = ---------- x 100 A-C 9. If, y is between 7.5 and 12.5 % then apply given formula to find out 10% times value. 10. Load required for 10% fines = 14 x X 4+Y Where X- Load in tones Y- Mean % fines from two tests at X tones load Acceptance criteria = Minimum 50KN (for sample in soaked condition for GSB) 5.0

DETERMINATION OF FLAKINESS INDEX OF AGGREGATE 1. PURPOSE This method of test lays down the procedure for determining the flakiness index of coarse aggregate. 2. SCOPE To find out particle size distribution of fine, coarse and all-in-aggregate by sieving and screening.. 3. 4. REFERENCE DOCUMENTS : IS-2386 (Part-I) - 1968 APPARATUS 1. 2. 3. 4. 5. Balance (0.1 of accuracy of the weight of the test sample) Metal thickness Gauge I.S. Sieves (given in table-I) conforming to IS:460-1962 (i.e, 63, 50, 40, 31.5, 25, 16, 12.5, 10 and 6.3mm) Container

PROCEDURE: I. SIEVING : The sample shall be sieved as per IS-2386 (Part-I) Table V in a fraction 63-50 mm, 50-40 mm, 40-25 mm, 31.5 25 mm, 25-20 mm, 20-16 mm, 16-12.5 mm, 12.5 10 mm & 10-6.3 mm. II. SEPRATION OF FLAKY MATERIALS: Each fraction shall be gauged in turn for thickness on a metal gauge of the pattern. The width of slot used in the gauge or sieve shall be of the dimensions specified in column-3 of Table V of IS-2386 (Part-I) 1963. III IV WEIGHING OF FLAKY MATERIAL: The total amount passing the gauge shall be weigh to an accuracy of at least 0.1% of the weight of the test sample. REPORTING OF RESULTS: The flakiness index is the total weight of the material passing the various thickness gauge, expresses as a % of the total weight of the sample gauged. Acceptance criteria: For concrete For WMM,DBM & BC (Flaki & Elongation combined) 35% max. 30% max.

DETERMINATION OF ELONGATION INDEX FOR AGGREGATE I PURPOSE: Method covers to determining the elongation index of coarse aggregate. II SCOPE: The SOP covers for determining the elongation index of coarse aggregate. III IV REFERENCE DOCUMENTS: IS 2386 (Part I) 1963 APPARATUS: 1. Balance 0.1g accuracy 2. 3. 4. V Metal length gauge IS Sieves Containers

PROCEDURE: 1. SEIVING : The sample shall be sieved as per IS-2386 (Part-I) Table V in fraction 6350 mm, 50-40 mm, 40-25 mm, 31.5 25 mm, 25-20 mm, 20-16 mm, 16-12.5 mm, 12.5 10 mm & 10-6.3 mm. 2. SEPERATION OF ELONGATED MATERIALS: Each fraction shall be gauged individually for length on a metal length of the pattern. The gauge length used shall be that specified in column 4 of Table IV of IS-2386 (Part-I) 1965. 3. 4. WEIGHING OF ELONGATION MATERIAL: The total amount retained by the length gauge shall be weighed. REPORT OF RESULTS: The elongation index is the total weight of the material retained on the various length gauge, expressed as a percentage of the total weight of the sample gauged. Acceptance criteria: For concrete For WMM,DBM & BC (Flaki & Elongation combined) Not applicable 30% max.

DETERMINATION OF AGGREGATE IMPACT VALUE FOR AGGREGATES 1.0 Purpose: 2.0 3.0 4.0 2. 3. 4. 5. 6. 5.0 To find out Aggregates Impact Value.

The SOP covers the finding out of aggregate Impact Value of the coarse aggregate. Reference Document : IS 2386 (Part-IV) Apparatus : Aggregate Impact value machine IS sieve size 12.5 mm 10 mm size & 2.36 mm Size Aggregate Impact Jar. Tamping rod with nose of cylinder 16 mm Dia Balance with 0.01 gm capacity.

Detailed Procedure 1. Take aggregate from source/ stock piles 2. 3. 4. 5. 6. 7. 8. 9. Make test sample of aggregates passing 12.5 mm IS sieve & retained on 10 mm IS sieve Put the sample in to oven for four hours at 1000 c 1100 c temperature & cool it. The aggregates are filled in measuring cylinder in 3 equal layer with 25 strokes by tamping rod. Weight the impact Jar with material. Take Reading A Now place the Impact cup into impact machine & set the bottom plate without deviating such that hammer falls from 380 + 5 mm height. Total 15 blows are carried out each being delivered at an interval of not less than the second. The crushed aggregate are taken out & sieved through 2.36 mm sieve & weigh the fraction passing out 2.36 mm IS Sieve. Take the Empty Wt. of impact cup Reading C Calculation: Aggregate Impact Value B = -------- x 100 A-C Conclusion B

Aggregate Impact Value = ------- x 100 AC

Acceptance criteria:

Specification

limits

as

per

For Concrete & WMM 30

MoRT&H Maximum ( % )

For DBM 27

For BC 24

DETERMINATION OF SPECIFIC GRAVITY AND WATER ABSORPTION FOR AGGREGATE LARGER THAN 10MM 1.0 2.0 Purpose: To find out water absorption & Specific gravity of aggregate greater than 10 mm size. SCOPE: The SOP covers the procedure for testing of aggregate for its water absorbing property & specific gravities. 3.0 Apparatus : Ref. Document : IS 2386 (Part III) : 1963 1. Wire basket. 2. Oven 3. Balance 4. Water Container 5. Suspension rod or ring 6. Two clothes of cotton 4.0 Detailed Procedure : 1. Take about 2 kg of aggregate sample & washed to remove fines & dust from it. 2. Place the aggregates in wire basket & immersed wire basket in distilled water container with the help of suspension rod ring. Such that wire basket get a cover of at least 5 cm above. The temperature at this time should be between 220 C & 320 c. After immersions to remove entrapped air from sample, jerk the wire basket for 25 times. The basket & aggregate should removed completing immersed in water for period of 24 + hours. Weigh after 24 hrs the sample with basket in water with use of suspension ring Reading A. Sample is taken out from basket & weigh the basket in water Reading B. The aggregates made surface dry with use of dry cotton cloths.

3. 4. 5. 6. 7. 8.

The aggregate should be weight Reading C.

9. Then after, aggregate placed in oven for 24 hours at 110 C then it is cooled & weight, Reading D. (I) Specific Gravity = D --------------C (A-B)

(II)

Apparatus Gravity = D ----------D (A-B)

Water Absorption = (C-D) -------------- x 100 D Acceptance criteria for water absorption = Maximum 2% for all types of works DETERMINATION OF SPECIFIC GRAVITY AND WATER ABSORPTION FOR AGGREGATE SMALLER THAN 10MM I II PURPOSE: To find out water absorption and specific gravity of aggregate smaller than 10 mm. SCOPE: The SOP covers for determining specific gravity of aggregate based on SSD, Oven dried and apparent specific gravity. REFERENCE DOCUMENTS : IS-2386 (Part-III) 1963 APPARATUS: 1. Balance 2. 3. V Oven Pycnometer

(III)

III IV

PROCEDURE: 1. A sample of about 1 kg for 10 mm- 4.75mm or 500 g. if finer than 4.75 mm, shall be placed in the tray and covered with the distilled water at a temperature of 22-320 C. 2. Soon after immersion, air entrapped in or bubbles on the surface of the aggregate shall be removed by gentle agitation with a rod. 3. The sample shall remain immersed for 24 + Hrs. 4. The water shall then be drained out carefully from the sample by cotton cloth / filter paper. 5. Surface moisture can be evaporated by rubbing cotton cloth on the aggregate. The saturated and surface dry sample shall be weighed say weight (A). 6. The aggregate shall be then placed into pycnometer which shall be filled with distilled water. 7. Any trapped air shall be eliminated by rotating the pycnometer on its sides, the hole in the apex of the cone being covered with a finger. 8. The pycnometer shall be filled up with distilled water up to top to remove if any air bubbles from the surface and so that the surface of the water in the hole is flat. The pycnometer shall be dried on the outside and weighed (B). 9. The content of the pycnometer shall be emptied into the tray, care being taken to ensure that all the aggregate is transferred. 10. The pycnometer shall be refilled with distilled water to the same level as before, drained on the outside and weighed say (C). 11. The water shall be carefully drained from the sample by cotton cloth.

12.

The sample shall be placed in oven in the tray at a temperature 1000 to1100C for 24 hrs. Then the same is cooled in airtight container and get weight (D). Two tests shall be made.

VI

CALCULATION: D Specific gravity -----------A - (B-C)

Where A = Weight of SSD condition (g) B = Weight of Pycnometer filled with water and sample (g)

D C = Weight of pycnometer filled with distilled water (g) Apparent Sp. Gr. -----------D = Weight of oven dried sample (g) D - (B-C) Acceptance criteria for water absorption = Maximum 2% for all types of works DETERMINATION OF STRIPPING VALUE OF AGGREGATES STANDARD IS: 6241-1971. DEFINITION The stripping value of aggregates is determined as the ratio of the uncovered area observed visually to the total area of aggregates, expressed as a percentage. APPARATUS Heat resistant glass beaker of 500 ml capacity. 20mm and 12.5mm IS sieves. Mixer. Balance of capacity 10Kg and sensitivity 1gram. Water bath preferably with a thermostat.

PROCEDURE Take 200 grams of dry and clean aggregates passing 20mm and retained on 12.5mm sieves and heat up to 1500C.

Take five percent by weight of bitumen binder and heat up to 1600C. Mix the aggregates and the binder till they are completely coated and transfer the mixture in to a 500ml beaker and allow to cool at room temperature for about 2 hours. Add distilled water to immerse the coated aggregates. Cover the beaker and keep in a water bath maintained at 400C taking care that the level of water in the water bath is at least half the height of the beaker.

After 24hours take the beaker out, cool at room temperature and estimate the extent of stripping visually while the specimen is still under the water.

REPORT Express the stripping value as the ratio of the uncovered area observed visually to the total area of aggregates in each test. Report the mean of three results as stripping value of the tested aggregates to the nearest whole number. Acceptance Criteria = Minimum 95% retained coating

DETERMINATION OF SAND EQUIVALENT VALUE STANDARD IS: 2720 (Part-3)-1976 SCOPE

The SOP covers the method for the determination of sand equivalent value of the soils and this method is intended to serve as a rapid field-correlation test.

APPARATUS Sand equivalent test, Graduated cylinder Irrigator tube, Flat pan Trimming device, Siphon assembly Weighted foot assembly, Measuring can IS Sieves, Funnel Calcium chloride solution

PROCEDURE

Fill the prepared calcium chloride solution up to 100+/-2mm indicated on the graduated cylinder. Pour the test specimen (4.75mm sieve passing) into the graduated cylinder using the funnel to avoid spillage. Tap the bottom of the cylinder sharply on the palm of the hand several times to replace air bubbles and to promote thorough wetting of the specimen. Allow the wetted specimen and cylinder to stand undisturbed for 10+/- 1 minute.

At the end of the 10minutes soaking period, stopper the cylinder, then loosen the material from the bottom by partially inverting the cylinder and shaking it simultaneously. After loosening the material from the bottom of the cylinder, shake the cylinder and contents by hand. Hold the cylinder in the horizontal position and shake it vigorously in a horizontal linear motion from end to end. Shake the cylinder 90cycles in approximately 30seconds using a throw of 230+/-5mm. Following the shaking operation, set the cylinder upright on the work table and remove the stopper. Insert the irrigator tube in the top of cylinder, remove the spring clamp from the hose and rinse the material from the cylinder wall as the irrigator is lowered. Continue to apply a stabbing and twisting action which flushing the fines upwards until the cylinder is filled to the 380mm graduation. Regulate the flow just before the irrigator tube is entirely with drawn and adjust the final level to the above 380mm graduation. Allow the cylinder and contents to stand undisturbed for 20minutes +/-15 seconds. After 20minutes sedimentation period read and record the level of the top of the clay suspension as clay reading. After the clay reading has been taken place the weighed foot assembly over cylinder and gently lower the assembly until it comes to rest on the sand. Subtract 250mm from the level indicated by the extreme top edge of the indicator and record this value as sand reading. Sr Calculate the sand equivalent (SE) = ---- x 100 Cr Where Sr- Sand reading Cr- Clay reading Acceptance Criteria = Minimum 50%

TESTS ON SOIL
DETERMINATION OF MOISTURE DENSITY RELATION FOR SOIL 1.0 PURPOSE To establish the relation between the Moisture content and Density by heavy compaction. 2.0 SCOPE The SOP covers the method for determination of the relation between the water content and the dry density of soil. 3.0 REFERENCE DOCUMENTS IS-2720 (Part-VIII) 4.0 APPARATUS i. Cylindrical metal mould. ii. Chisel & hammer iii. Balances 0.1 gm & 0.2 gm accuracy iv. Oven & Containers v. Steel Straight edge vi. Sieve 19 mm IS size vii. Metal Rammer 4.9 Kg & Mixing Tools 6.0 DETAIL PROCEDURE : i. Take 5.0 Kg of air dried soil (passing from 19 mm sieve and replaced retained particle by 4.75 mm) ii. iii. iv. v. vi. vii. viii. ix. x. Thoroughly mix the soil by adding uniform increments of water content. 1000 cm3 capacity mould with base plate & extension attached shall be placed on plain floor. Soil specimen is approximately divided in five equal parts, each layer being given 25 blows by 4.9 kg rammer dropped from height of 450 mm. The extension shall be removed after 5 layers and compacted soil shall be leveled off carefully by straightedge. Weigh the compacted soil with mould. Take approximate 50 gm soil sample in aluminum container from that mould after weighing and put container in oven for 24 hours. Repeat the same procedure with new soil sample with adding 2% of increments of water content for at least 5 times. Moisture content should be optimum of which the maximum DRY DENSITY occurs. Plot the graph with DRY DENSITY & MOISTURE CONTENT and derive MDD, OMC from the graph. Acceptance criteria Specification limits as per Embankment Embankment Subgrade&

MoRT&H table 300-1 Minimum (gm/cc)

upto3m height 1.52

exceeding 3m 1.60

Eart. shoulders 1.75

DETERMINATION OF LIQUID LIMIT FOR SOIL 1.0 2.0 PURPOSE To establish the procedure for the Determination of Liquid Limit. SCOPE Liquid Limit is defined as the water content at which the soil changes from liquid state to plastic state. 3.0 4.0 REFERENCE DOCUMENTS: IS: 2720 (Part 5) 1985. APPARATUS 1. Casagrande apparatus confirming to IS: 9259-1979. 2. Grooving tool. 3. Balance of capacity 500 grams and sensitivity 0.01gram.
4.

Thermostatically controlled oven with capacity up to 2500 C.

5. Porcelain evaporating dish about 12 to 15cm in diameter. 6. Spatula flexible with blade about 8cm long and 2cm wide. 7. Palette knives with the blade about 20cm long and 3cm wide. 8. Wash bottle or beaker containing distilled water. 9. Containers airtight and non- corrodible for determination of moisture content. DETAIL PROCEDURE: Take representative soil sample of approximately 120gms passing through 425 micron IS sieve and mix thoroughly with distilled water in the evaporating dish to a uniform paste. The paste shall have a consistency that will require 30 to 35 drops of the cup to cause the required closure of the standard groove. Leave the soil paste to stand for 24 hours to ensure uniform distribution of moisture through out the soil mass. Remix the soil thoroughly before the test. Place a portion of the paste in the cup above the spot where the cup rests on the base, squeeze down and spread in to position with a few strokes of the spatula as possible and at the same time trim to a depth of 1cm at the point of maximum thickness.

Make a clean, sharp groove by a grooving tool along the diameter through the centerline of the cam follower.

Drop the cup from a height of 10 + 0.25 mm by turning the crank at the rate of two-revolutions/ sec, until the two halves of the soil cake come in contact with the bottom of the groove along the distance of about 12mm.

Record the number of drops required to cause the groove close for the length of 12mm.

Collect a representative slice of sample of soil approximately the width of spatula, extending from about edge to edge of the soil cake at right angle to the groove in to an air tight container and keep in the oven for 24hrs, maintained at a temperature of 105 0 to 1100C and express its moisture content as the percentage of the oven dried weight.

Transfer the remaining soil in the cup to the evaporating dish and clean the cup and the grooving tool thoroughly. Repeat the operation specified above for at least three more additional trials (minimum of four in all) with soil collected in evaporating dish to which sufficient water has been added to bring the soil to more fluid condition.

In each case record the number of blows and determine the moisture content as before. The specimens shall be of such consistency that the number of drops required to close the groove shall not be less than 15 or more than 35.

REPORT Plot a flow curve with the points obtained from each determination on a semi logarithmic graph representing water content on the arithmetical scale and the no of drops on the logarithmic scale. The flow curve is a straight line drawn as nearly as possible through the four or more plotted points. The moisture content corresponding to 25 drops as read from the curve shall be rounded off to the nearest second decimal and is reported as liquid limit of the soil. Acceptance criteria Specification limits as per MoRT&H clause 305.2.1.1 Maximum ( % ) Embankment & Subgrade 70 GSB 25

DETERMINATION OF PLASTIC LIMIT & PLASTICITY INDEX FOR SOIL 2.0 PURPOSE To establish the procedure for the determination of plastic limit / plasticity index 3.0 SCOPE The SOP covers the determination of plastic limit of soils 4.0 REFERENCE DOCUMENTS : IS 2720 (Part-5) : 1985 APPARATUS 1. 2. 3. 4. 5. 6. 5.0 Porcelain dish Appx. 100 mm dia Flat glass 10 mm thick & 45 cm square Spatula flexible, cm in length & 2 cm in width Containers 2 Nos. at least Balance 0.01 g accuracy Oven a. A soil sample 20 gm aging through 425 micron sieve is taken in parceling dish and added known volume of distilled water until soil mass be comes plastic enough to be easily moulded into a ball with fingers. b. Take a portion of the ball and roll it on glass plate at the rate of 80 to 90 strokes /minutes by fingures. c. Care should taken while rolling soil mass to form a thread (Between fingers and glass plate) be uniform in diameter thought its length. d. Rolling shall be done till the threads are of 3 mm dia meter, the soil is remolded again into a ball. e. This process of rolling and remolding is repeated until the thread starts just crumbling at a diameter of 3 mm, and soil can no longer be rolled into a thread. f. The crushed thread are kept for water cement determination g. Repeat the test with two more sample h. The plastic limit is then taken as average of the three water content value PLASTICITY INDEX (Ip) = Liquid limit (WL) Plastic limit (Wp) Acceptance criteria for PI:

4.0

DETAIL PROCEDURE:

Specification limits as per MoRT&H clause 305.2.1.1 Maximum ( % )

Embankment & Subgrade 45

GSB & WMM 6

DETERMINATION OF GRAIN SIZE ANALYSIS FOR SOIL 2.0 PURPOSE To establish the procedure for the quantitive determination of grain size distribution. 3.0 SCOPE

The sop covers the determination the percentage of various size particles in a soil sample. 4.0 5.0 1. 2. REFERENCE DOCUMENTS : APPARATUS I.S. Sieve (size 19mm, 4.75 mm, 2.0 mm, 1.18 mm, 425 micron, 300 micron, 150 and 75 micron with lid & pan) Oven 3. 4. 5. 6. 5.0 Balance 0.01 g accuracy Tray Brush Mechanical sieve shaker IS-2720 (Part-4) : 1985

DETAIL PROCEDURE: 1. 2. 3. 4. 5. Take 500 gm of oven dried soil passing 4.75 mm sieve. Put this soil in a tray containing water for a period of 2-4 hours Wash the soil on 75 micron sieve by stirring the soil on sieve. Continue to pour the water till water passing the sieve is substantially clear. Oven dry soil mass is sieved on above sieve as per apparatus and record the weight get passing of on 75 micron sieve.

6.

The percentage of soil retained on each sieve shall be calculated on the bases of the total mass of soil sample taken.

Acceptance criteria:

Soil having different % variation in grain size gives identification of different types.

DETERMINATION OF FREE SWELL INDEX FOR SOIL 1.0 PURPOSE :

To establish the procedure for the Free Swell Index 2.0 SCOPE :

The SOP covers the test for the determination of free swell index of soils which help to identify / further detailed investigation. 3.0 REFERENCE DOCUMENTS: 5.0 1. 2. 5.0 APPARATUS : 425 microns sieve Graduated cylinders 2 Nos. 100 ml capacities. IS-2720 (Part XL) 1977

DETAIL PROCEDURE: a. b. c. d. e. Take two 10 (g) soil specimen of oven dry soil passing through 425 micron IS sieve. Each soil specimen shall be poured in each of the two glass (gradated) cylinder of 100 ml capacity. One cylinder shall be filled with kerosene oil and other with distilled water up to 100 ml mark. By gentle shaking the soil in both the cylinder shall be allowed to settle up to 24 hrs to attain equilibrium state of volume without disturbing the both cylinder. The final volume of soil in each of the cylinder shall be noted. Vd - Vk The free swell index = --------- x 100 (FSI) Vk Where Vd = Volume of soil read from cylinder with distilled water Vk Volume of soil read from cylinder with kerosene. Acceptance criteria = Maximum 50%

DETERMINATION OF CBR FOR SOIL 1.0 2.0 3.0 4.0 PURPOSE: Laboratory determination of CBR to establish the procedure for the testing of CBR SCOPE: The SOP covers the mould preparation for CBR, Testing of CBR & interpretation of CBR reports. REFERENCE DOCMENTS: IS 2720 (Part 16) - 1987 APPARATUS 1. Moulds with Base plate, stay rod & wing nut with collar. 9. Graduated cylinder 2. Spacer Disc. 10. CBR Apparatus

a.

3. Metal Rammer 8. Perforated plate 4. Expansion Measuring Apparatus (Swelling) 5. Weights 6. Loading Machine with plunger 7. Dial gauges 5.0 PROCEDURE: (A) MOULD PREPARATION First find out moisture density relation of soil, as per IS:2720 (Part-8) b. Take soil sample of about 5000 gms & add water in it as per OMC found. c. Fill the 3 CBR mould in 5 layers with 55 blows with 4.9 kg hammer. d. Put filter paper on mould with spacer disc on it. e. Put surcharge weigh of 5 kg on prepared mould & put those mould into water tank for soaking. f. Put Expansion Measuring apparatus on those moulds & take initial reading. (B) TESTING OF CBR: a. Take out CBR moulds after 4 days soaking & get air dried for 15 minutes, check swelling gauge reading. b. Place the CBR mould into CBR Testing machine & give the sitting load as per IS-2720 (Part-16) with penetration plunger. b. Take the reading of loading proving ring (CBR machine) at 0,0.5,1.0,1.5,2.0,2.5, 3.0,4.0,5.0,7.5,10 & 12.5 mm penetration for all three moulds respectively. c. Multiply the proving ring reading with proving ring factor (from calibration of loading machine) which gives load values for diff penetration & mould. d. Draw a graph between load v/s penetrations & make a smooth curve of it. e. Take out the load values at 2.5 mm & 5.0 mm penetration for different moulds. f. With use of formula. PT CBR = ------- x100 PS Where PT- Corrected unit test load corresponding to the chosen penetration from the load penetration curve and PS Unit standard load for the same depth of penetration as for PT taken from the standard table. Generally the CBR value at 2.5mm penetration will be greater than that at 5mm penetration and the same value of CBR taken for design. Acceptance criteria = Minimum 8 for soil & 30 for GSB

DETERMINATION OF MOISTURE CONTENT BY RAPID MOISTURE METER 1.0 2.0 PURPOSE: To determine moisture content of soil

SCOPE: This SOP covers a method for rapid determination of water content from the gas pressure developed by the reaction of calcium carbide with the free water of soil

3.0 4.0

REFERENCE DOCUMENTS: IS-2720 (Part-II) 1973 APPARATUS: 1. Metallic Pressure vessel 2. 3. 4. 5. 6. Counterpoised Balance Scoop Calcium Carbide Cleaning brush Steel Balls

PROCEDURE: 1. Set up the balance. Place the sample in pan till the mark on the balance arm mark lines up with the index mark. 2. Unclamp the clamping screw of the instrument sufficient to move the U-clamp off the Cup, Lift off the cup & check that cup and body are clean, otherwise clean it using a brush. 3. Hold the body horizontal and gently deposit one level scoop full calcium carbide half way inside the chamber. 4. Transfer the soil weighed out as above from the pan to the cap. 5. Place the 3-smaller balls into the cup along with the soil and larger one in the body along with the calcium carbide and clamp the U-clamp tightly. 6. Hold moisture meter vertical so that the material in the cup falls into the body. Now holding the unit horizontal rotate it for 10 seconds so that the balls are rolled round the i/s circumstances of the body. Rest for 20 seconds. 7. Repeat the rotation rest cycle until the gauge reading constant Note the reading. 8. Finally release the pressure slowly (away from the operator) opening the clamp screw and taking cup out, empty the contents clean the instrument with a brush. Acceptance criteria: The water content of the soil from the calibrated rapid moisture meter gives the actual moisture content available in soil.

DETERMINATION OF FIELD DENSITY BY SAND REPLACEMENT METHOD 1.0 PURPOPSE: To determine the field density by sand replacement method. 2.0 SCOPE: The method covers the determination, in-place of dry density (in g/cc) of natural or compacted soil. 3.0 REFERENCE DOCUMENS: IS 2720 (Part 28) 1974 6.0 APPARATUS 1. 2. 3. 4. 5. 6. 7.0 a. b. c. d. e. f. g. h. i. j. Sand Pouring cylinder Tools for excavating holes chisels, hammer, clamps, bent spoon and scrappers tools. Balance - 30 Kg capacity Metal tray with hole Standard sand. Rapid Moisture meter

PROCEDURE

Approx 450 mm square flat area shall be exposed and leveled. The metal tray with central hole shall be laid on the prepared surface. The hole in the soil shall be excavated using scrapped tools put excavated soil in tray to the depth of the layer to be tested (max. depth up to 150mm) Excavated soil shall be removed and weigh carefully. Pour the sand in excavated trench and weight the remain sand in pouring cylinder. After weighing cylinder is to be placed on excavated pit and shutter is opened till the sand fills the excavated hole. Care should be taken that theres no further movement of sand in the cylinder then shutter is closed. Weigh the sand pouring cylinder again and noted. Moisture from excavated soil is checked by moisture meter. Put all data in tabular format and get % of compaction.
Acceptance criteria:

Specification

limits

as

per

MoRT&H Minimum ( % )

Embankment 95

Subgrade & Eart. Shoulder 98

WMM, DBM & BC 98

TESTS ON BITUMEN
DETERMINATION OF SPECIFIC GRAVITY OF BITUMEN STANDARD IS: 1202 1978 DEFINITION Specific gravity is the ratio of the mass of a given volume of the substance to the mass of an equal volume of water. APPARATUS

Specific gravity bottle of 50ml capacity Constant temperature bath having a depth greater than that of Pycnometer capable of being maintained within 0.2 0C. Balance of capacity 500grams and sensitivity 0.01gm. Clean dry and weigh the specific gravity bottle together with the stopper (A). Fill it with freshly boiled and cooled distilled water and insert the stopper firmly. Keep the bottle up to its neck for not less than half an hour in beaker of distilled water at a temperature of 27 + 0.10C or any other temperature at which specific gravity is to be determined. Wipe all surplus moisture from the surface with a clean, dry cloth and weigh it (B). Bring the bituminous material to the fluid condition by gentle application of heat, care being taken to prevent loss by evaporation.

PROCEDURE

When the material is sufficiently fluid, pour the bitumen in to the clean, dry specific gravity

bottle to fill at least half. Slightly warm the bottle before filling the material Keep the material away from touching the sides above the final level of bottle and avoid the inclusion of air bubbles. The use of small funnel will prevent contamination of the neck of the bottle. To permit escape of entangled air bubbles, allow the partly filled bottle to stand for half an hour at a suitable temperature, then cool to the specified temperature, and weigh with the stopper (C).

Fill the specific gravity bottle containing the asphalt with freshly boiled and cooled distilled water placing the stopper loosely in the specific gravity bottle. Do not allow any air bubbles to remain in the specific gravity bottle. Place the specific gravity bottle in the water bath and press the stopper firmly in place. Allow the specific gravity bottle to remain in the water bath maintained at a temperature of 27 + 0.10C for a period of not less than 30 minutes.

Remove the specific gravity bottle from the water bath, wipe all surplus moisture from the

surface with a clean dry cloth and weigh it along with the stopper (D). Calculations C-A Specific gravity = ----------------(B-A) - (D-C) A = Weight of specific gravity bottle B = Weight of specific gravity bottle filled with distilled water. C = Weight of specific gravity bottle about half filled with the bituminous material D = Weight of specific gravity bottle about half filled with the material and the rest with distilled water. Report Express the ratio of mass of a given volume of the bituminous material to the mass of an equal volume of water. Acceptance criteria: Minimum 0.99 at 270C for 60/70 grade.

DETERMINATION OF PENETRATION OF BITUMEN STANDARD IS: 1203 1978 DEFINITION Penetration of a bituminous material is the distance in tenths of millimeter that standard needle will penetrate vertically into a sample under standard conditions of temperature, load and time. APPARATUS Standard Penetration apparatus A metal or glass cylindrical flat-bottomed container essentially with the following dimensions For penetration below 225 Diameter 55mm

Internal depth 35mm Needle shall be made up of straight, highly polished, cylindrical, hard steel rod. Water bath 10 liters capacity thermostatically Controlled and maintained within the temperature of 25 + 0.10C.

Thermometer capable of reading temperature up to 250 0C. Soften the material to a pouring consistency at a temperature not more than 60 0C for tars and pitches and not more than 90 0C for bitumen above the approximate respective softening points. Stir it thoroughly until it is homogeneous and free from air bubbles and water. Pour the melt in to the container to a depth of at least 10mm in excess of the expected penetration. Protect the sample from dust and allow it to cool in atmosphere at a temperature between 15 to 30
0

PROCEDURE

C for 11/2 to 2hours for 45mm deep container and 1 to 11/2 hours for 35mm deep container.

Unless otherwise specified carry out testing at a temperature of 25 + 0.1oC. Place it along with the transfer dish in the water bath at 25 + 0.10C and allow it remain for 11/2 to 2hours for 45mm deep container and 1 to 11/2 hours for 35mm deep container.

Fill the transfer dish with water from the water bath to a depth sufficient to cover the mould completely. Remove the transfer dish along with the mould from water bath after specified period of time and put it upon the stand of penetration apparatus. Adjust the needle (previously washed, cleaned well with benzene and dried) just to make contact with the surface of the sample. The sum of the weights of the needle, carrier and super imposed weights i.e. the total moving weight shall be 100 0.25grams.

Bring the pointer to zero. Release the needle for five seconds and measure the distance penetrated. Make at least three determinations at points on the surface of the sample not less than 10mm apart and not less than 10mm from the side of the dish. After each test, return the sample and transfer dish to the water bath and wash the needle with benzene and dry. In case of material of penetration greater than 225 make three determinations on each of two identical test specimens using a separate needle for each determination, leaving the needle in the sample on completion of each determination to avoid disturbance of the specimen.

REPORT Express the depth of penetration of the needle in tenths of mm. The value of penetration reported shall be the mean of not less than three determinations whose values. Acceptance criteria: Between 60 to 70 at 250C for 60/70 grade.

DETERMINATION OF SOFTENING POINT OF BITUMEN

STANDARD IS: 1205 1978.

DEFINITION Softening point is the temperature at which the substance attains a particular degree of softening under specified conditions of test. APPARATUS

Standard Ring and Ball Apparatus. Steel balls 2 No, each 9.5mm in diameter and weighing 3.5 + 0.05 grams. Brass rings 2 No, the rings shall be tampered and shall confirm to the following Depth : 6.4 + 0.1mm : 15.9 + 0.1mm : 20.6 + 0.1mm Inside diameter at bottom Outside diameter

Inside diameter at top : 17.5 + 0.1mm Thermometer capable of reading temperature up to 0 to 250 0 C. Water bath should be a heat resistant glass vessel not less than 85mm in diameter and 120mm in depth.

Stirrer shall be manual or mechanical to ensure uniform heat distribution at all times throughout the water bath.

PROCEDURE

Heat the material to a temperature between 75 to 100 0C above its softening point. Stir until it is completely fluid and free from air bubbles and water, and filter if necessary, through IS sieve 30. Place the rings, previously heated to a temperature approximately to that of molten material on a metal plate, which has been coated with a mixture of equal parts of glycerin and dextrin. Fill the mould with sufficient melt to give excess above the level of the ring.

Remove the excess material with a warmed sharp knife after cooling in air for 30 minutes. Assemble the apparatus with the rings, thermometer and ball guides in position Fill the bath to a height of 50mm above the upper surface of the rings with the freshly boiled distilled water or pure glycerin at a temperature of 5 0C. The water bath liquid shall be freshly boiled distilled water when testing materials having softening points below 80 0C and pure glycerin for material having softening points above 80 0C. There shall be exactly 25mm difference between the bottom of the rings and the top surface of the bottom plate of the support, if any, or the bottom of the bath. Maintain the bath at a temperature of 5 0C for 15 minutes after which place the balls previously cooled to a temperature of 5 0C by forceps in each ball guide. Apply heat to the bath and stir the liquid so that the temperature rises at a uniform rate of 5 + 0.5 0 C per minute until the material softens and allow the balls to pass through the ring. Record the temperature shown by the thermometer for each ring and ball at the instant the sample surrounding the ball touches the bottom plate of the support, if any or the bottom of the bath.

Report

Report to the nearest 0.5 0C the mean of the temperature recorded in duplicate as the softening point. Acceptance criteria: Between 45 to 55 for 60/70 grade.

DETERMINTION OF DUCTILITY OF BITUMEN STANDARD IS: 208-1978. The ductility of bituminous material is the distance in centimeters to which it will elongate before breaking when a briquette specimen of the materials is pulled at a specified speed and at specified temperature. APPARTUS

DEFINTION

Testing machine Mould made up of brass Water bath preferably with a thermostat, 10lit capacity and maintained with in 0.10C of the specified temperature Thermometer 2500C capable of reading up to 0.010C. Unless otherwise specified this test shall be conducted at a temperatures of 27 + 0.50C and at a rate of pull of 50 + 2.5mm /min. Melt the bitumen to be tested to a temperature of 75 to 100 0C above its approximate softening point till it becomes fluid. Assemble the mould on a brass plate and coated on all the sides with a mixture glycerin and dextrin of equal parts to avoid sticking of the material. Fill the mould until it is more than level full. In filling the mould, pour the material in a thin stream back and forth from end to end of the mould. Leave it to cool room temperature for 30 to 40 minutes and than place it in water bath maintained at a specific temperature for 30 minutes. Cut off excess bitumen by means of hot straight edged putty knife level full. Place the brass plate and mould with briquette specimen, in the water-bath and keep at the specified temperature for about 85 to 95 minutes. Remove the briquette from the plate, detach sidepieces and test the briquette immediately. While the test is being conducted, make sure that the water in the tank of the testing machine covers the specimen above by at least 25mm and is maintained continuously with in +0.50C of specified temperature.

PROCEDURE

Attach rings at each end of the clips to the hooks in the testing machine and pull the two clips apart horizontally at a uniform speed as specified until the briquette ruptures.

Measure the distance in centimeters through which the clips have been pulled to produce rupture. At least three determinations shall be made for each test.

REPORT

Report the average of three normal tests as ductility of the sample, provided that, the three determinations be with in + 5% of their mean value. If the value of three determinations do not lie with in + 5% of their mean but the two higher value are with in + 5% of their mean, then record the mean of the two higher values as the test result. Acceptance criteria: Minimum 75 cm at 270C for 60/70 grade.

DETERMINATION OF FLASH POINT FOR BITUMEN STANDARD IS: 1209 1978 (3). DEFINITION Flash Point The flash point of a material is the lowest temperature at which the application of test flame cause the vapors from the material momentarily catch fire in the form of a flash under specified conditions of test. APPARTUS

Pensky Martens Closed Tester consisting of cup, lid, stirring device, cover shutter and flame exposure device etc. Low range thermometer -7 to +1100C and capable of reading up to 0.50C. High range thermometer 90 to 3700C and capable of reading up to 2 0C.

PROCEDURE

Clean and dry all parts of the cup and its accessories thoroughly before the test. Take particular care to avoid the presence of any solvent used to clean the apparatus. Fill the cup with the material to be tested up to the level indicated by the filling mark. Place the lid on the cup and set the latter in the stove. Take care that the locating devices are properly engaged. Insert the thermometer, high or low range, as required. Light and adjust the test flame so that it is of the size of a bead of 4mm in diameter. Apply heat at such a rate that the temperature recorded by the thermometer increases between 5 to 60C per minute. Start stirring at a rate of 60 revolutions per minute. Apply the test flame at each temperature reading, which is a multiple of 10C up to 1040C. For the temperature range above 1040C, apply the test flame at each temperature reading, which is a multiple of 20C Apply initial test flame at least 170C below the expected flash point.

Apply the test flame by operating the device controlling the shutter and test flame burner so that the flame is lowered in 0.50 seconds, left in its lowered position for one second, and quickly raised to its high position.

Discontinue stirring during the application of test flame. Carefully observe the surface of the material during heating.

REPORT Flash Point The flash point shall be taken as the temperature read on the thermometer at the time of the flame application that causes a distinct flash in the interior of the cup. Acceptance criteria: Minimum 1750C for 60/70 grade.

DETERMINATION OF ELASTIC RECOVERY TEST ON CRMB SCOPE This procedure is mainly intended to access degree of bitumen modification and quality of modified bitumen. PURPOSE Test intended to optimize dose of polymeric and/or rubber additive in bitumen and help in accessing quality of PMB/RMB in laboratory. APPARTUS Ductility machine with moulds Thermometer Scissors Scale Hot plate Water bath

PROCEDURE Prepare three test specimens for one sample by heating CRMB at 163+/- 50C on hot plate. Pour the heated sample of CRMB in the moulds for test and keep at room temperature for 30 to 40 minutes and than place it into water bath at 150C trimming up to 30minutes. Place brass plate and moulds after with briquette specimen up to about 85 to 95 minutes at 150C after trimming. Elongate the test specimen in specified rate to a deformation 10cm at a rate of 5+/-0.25cm per minute at 150C temperature. Immediately cut the test specimen in to two halves at the midpoint using the scissors. Keep the test specimen in the water bath in an undisturbed condition for one hour at 15 0C temperature. After one hour time period, move the elongated half of the test specimen back position near the fixed half of the test specimen so that the two pieces of modified bitumen just touch. Record the length of the recombined specimen as X. Calculate the percentage/elastic recovery by the following procedure. 10-X Elastic recovery (%) =-------- x 100 10 Acceptance Criteria: Minimum 50%

DETERMINATION OF SEPERATION TEST ON CRMB SCOPE The separation of modifier and bitumen during hot storage is often seen and this can be evaluated by comparing the ring and ball softening point of the top and bottom portion of sample taken from crumbed rubber modified bitumen in a sealed tube. REFERENCE DOCUMENTS IRC-SP: 53-2002 APPARTUS Softening point apparatus

Aluminium tube, Freezer, Rack Oven, thermometer, Spatula & Hammer

PROCEDURE Place the empty tube (with sealed one end down) in rack.

Heat the CRMB sample at 163+/-50C and pass the molten sample of CRMB through IS sieve 600microns.

Pour the sample of 50 (g) into vertically held tube. Fold the excess tube over two times and crimp and seal. Place the rack containing the sealed tubes in a oven at 163+/-50C temperature for 48+/-4 hours. After 48+/-4 hours remove the rack from the oven and put it into freezer at 6.70+/-50C.

After remove the tube from the freezer place the tube on the flat surface and cut the tube into three equal lengths with knife. Discard the center portion of the sample and place the top & bottom in position of the tube into separate beakers. Place the beakers into a 163+/-50C in oven until the bitumen is sufficiently fluid and after thoroughly stirring, pour the samples into appropriately marked rings, for ring and ball softening point test.

Prepare the ring and ball apparatus accordingly to test method IS: 1205 and top & bottom sample from the same tube should be tested at the same time. Difference in the
o

C temperature, between the softening points of the respective top & bottom

samples in average of three specimens. Acceptance Criteria: Difference between softening points between top & bottom sample

should not be more than 40C.

TESTS ON ASPHALT MIX

DETERMINATION OF BINDER CONTENT FOR ASPHALT MIX STANDARD

IRC: SP 11 1988 (Appendix - 5), ASTM D 2172. To determine the binder content in the asphalt mix by cold solvent extraction Centrifuge bitumen extractor. Balance of capacity 500 gram and sensitivity 0.01grams. Thermostatically controlled oven with capacity up to 2500C. Beaker for collecting extracted material.

OBJECTIVE

APPARTUS

PROCEDURE

Take exactly 500 grams of representative sample and place in the bowl of extraction apparatus (W1). Add benzene to the sample until it is completely submerged. Dry and weigh the filter paper and place it over the bowl of the extraction apparatus containing the sample ( F1 ) . Clamp the cover of the bowl tightly. Place a beaker under the drainpipe to collect the extract Sufficient time (not more than an hour) is allowed for the solvent to disintegrate the sample before running the centrifuge. Run the centrifuge slowly and then gradually increase the speed to a maximum of 3600 rpm Maintain the same speed till the solvent ceases to flow from the drainpipe. Run the centrifuge until the bitumen and benzene are drained out completely. Stop the machine, remove the cover and add 200ml of benzene to the material in the extraction bowl and the extraction is done in the same process as described above. Repeat the same process not less than three times till the extraction is clear and not darker than a light straw colour. Collect the material from the bowl of the extraction machine along with the filter paper and dry it to constant weight in the oven at a temperature of 1050C to 1100C and cool to room temperature. Weigh the material ( W2 ) and the filter paper ( F2 ) separately to an accuracy of 0.01grams.

Weight of extracted filler shall be note as (W4) grams.

Calculations

W1 (W2 + W3+ W4) Percentage of binder in the total mix = ---------------------------- x 100 W1 W1 = Weight of sample taken W2 = Weight of sample after extraction W3 = Increased weight of filter paper ( F2 F1 ) W4 = Weight of extracted filler

REPORT The result obtained shall be reported as the percentage of binder content in the mix to the nearest second decimal.

Acceptance Criteria: For DBM (Grade-II) For BC (Grade-I) For BC (Grade-II) -

4.5% min. 5-6% 5-7%

DETERMINATION OF STABILITY ON ASPHALT MIX STANDARD MS-4 1989, ASTM D 1559 and AASHTO Designation: T 166 78.

OBJECTIVE

To determine the stability and flow of compacted asphalt mix. Marshall Testing Machine Compaction pedestal consisting of a 200x460x460mm wooden post capped with a 305x305x25mm steel plate. Compaction mould consisting of a base plate, forming mould and color extension. The internal diameter of forming mould should be 101.60mm and a height of approximately 75mm. Compaction hammer consisting of flat circular tamping face 98.40mm diameter and equipped with 4.50 Kilogram weight constructed to obtain a specified 457mm height of drop. Mould holder consisting of a spring tension device designed to hold compaction mould in place on compaction pedestal. Pans, metal, round, approximately 4 liters capacity for mixing of asphalt and aggregates. Thermostatically controlled oven and electrical hot plate. Scoop, mixing spoon, trowel and spatula. Mechanical mixer (optional) of 4lits capacity equipped with two metal mixing bowls and two wire stirrers. Thermostatically controlled water bath Gloves and welders for handling hot equipment. Marking crayons. Extrusion jack for extruding compacted specimens from mould. Balance of capacity 10 kgs and sensitivity 0.5 gms and of such a type and shape so as to permit the basket containing the sample to be suspended from the beam and weighed in water. Wire basket of not more than 6.3mm mesh or a perforated container of convenient size preferably chromium plated and polished, with wire hangers thickness not less than 1mm. A stout watertight container in which the basket may be freely suspended

APPARATUS

Two dry soft absorbent clothes each not less than 650 cm2

PROCEDURE Prepare test specimens either from Laboratory mix or from plant mix or from paved surface.

Preparation of Mix in the Laboratory

Take representative sample of aggregates and dry to constant weight at 1050 to 1100C. Separate the aggregates by dry sieving in to desired size of fraction. Weigh in to separate pans for each test specimen the amount of each size of fraction required to produce a batch that will result in a compacted specimen of height 63.5 + 1.3 mm which is generally of 1.20kg including asphalt percentage.

It is generally desirable to prepare a trial specimen prior to preparing aggregate batches. If the trial specimen height falls out side the limits, the amount of aggregate used for the specimen may be adjusted as follows Adjusted mass of aggregate = 63.50 (Mass of aggregate used) -------------------------------------------

Specimen height (mm) obtained Place the pans in the oven or on the hot plate and heat the aggregates to a temperature of approximately 280C above the mixing temperature Heat the asphalt cement to a temperature not more than 1600C. Charge the mixing bowl with heated aggregates and dry mix thoroughly. From a carter in the dry blended aggregates and weigh the required amount of asphalt cement in to the mixture accordance with the accumulative batch weights. The temperature to which the asphalt must be heated to produce viscosity of 170 + 20 centistokes shall be taken as the mixing temperature. Care shall be taken to maintain temperature of aggregates and asphalt cement be with in the limits of the mixing temperature. Mix aggregates and asphalt cement, preferably with a mechanical mixer or by hand with a trowel as quickly and thoroughly as possible to yield a mixture having a uniform distribution of asphalt through out.

Preparation of Mould and Hammer

Thoroughly clean the mould assembly and heat the face of the compaction hammer in a boiling water bath or on the hot plate to a temperature between 930C and 1490C.

Compaction of Specimens

Place a piece of waxed paper cut to size in the bottom of the mould before the mix is placed in the mould. Place the entire batch in the mould. Spade the mix vigorously with a heated spatula or trowel 5 times round the perimeter and 10 times over the interior. Remove the collar and smoothen the surface to a slightly rounded shape. The temperature of the mix immediately prior to compaction shall be with in the limits of the compaction temperature. Replace the collar, place the mould assembly on the compaction pedestal in the mould holder. Apply either 75 blows as specified according to the design traffic category with the compaction hammer using a free fall of 457mm. Hold the axis of the compaction hammer as nearly perpendicular to the base of the mould assembly during compaction.

Remove the base plate and collar, reverse and reassemble the mould. Apply the same number of compaction blows to the face of the reversed specimen. After compaction, remove the base plate and allow the specimen to cool in air until no deformation will result while removing it from the mould. Remove the specimen from the mould by means of extrusion jack and then place on a smooth level surface until ready for testing. Marking shall be done on the specimens for identification. Leave the specimens to cool over night.

Stability and Flow

Immerse the test specimens in a water bath maintained at 600C + 10C for 30 to 40 minutes before commencing the test. Thoroughly clean the inside surface of the testing head. Temperature of the testing head shall be maintained within 210C to 37.800C using a water bath whenever required. Lubricate guide rods with a thin film of oil so that upper test head will slide freely without binding. Check the dial indicator of the dial gauge to be firmly fixed and set to zero load position. With testing apparatus ready, remove test specimen from water bath and carefully wipe the surface.

Place the specimen in the lower testing head and center, and then fit the upper testing head into position and center complete loading device. Place flow meter over marked guide rod and set the needle to zero. Apply load on the specimen at the constant rate of deformation 51mm per minute. The point of failure is defined by the maximum load reading obtained. Maximum load taken by the specimen at 600C shall be recorded as its Stability value. Note the flow meter reading immediately when the load begins to decrease in load meter. This reading is the flow value of the specimen, expressed in units of 0.25mm. The entire procedure, both Stability and Flow tests, starting with removal of specimen from the water bath and testing shall be completed within a period of 30 seconds. Measured Stability values for specimens that depart from the standard 63.50mm thickness shall be converted to an equivalent 63.50mm value by means of conversion factor from the Table. Average the flow values and the converted Stability values for all specimens. Table: Stability Correlation Ratios Correlation Ratio 1.14 1.09 1.04 1.00 0.96 0.93 0.89 0.86

Thickness of specimen, in mm 58.70 60.30 61.90 63.50 64.00 65.10 66.70 68.30 Note*

The measured stability of a specimen multiplied by the correlation ratio for the specimen thickness equals the corrected stability for a 63.50 mm specimen. REPORT Report all the test results density, voids, stability and flow in a typical format.

Acceptance Criteria: For DBM (With Bitumen grade 60/70)

For BC (With CRMB-60)

917.43 Kg min. 1200Kg min.

SWELL TEST ON ASPHALT MIX STANDARD MS-4 1989

OBJECTIVE To determine the swelling of the compacted specimen under specified conditions of the test.

APPARTUS Mould of height 127mm and inside diameter 101.6mm tripod of height 170mm suitable to fix for the mould of 101.6mm diameter. Dial gauge sensitivity to 0.025mm. Deep aluminum pan of size 194mm x 64mm Perforated bronze plate with adjustable stem. Graduated scale capable of reading up to 1mm.

PROCEDURE

Compact the asphalt mix in to the mould as specified in MS-4 1989 Allow the mould to cool at room temperature for at least one hour (This is done to permit rebound after compaction). Place the mould and the specimen in the aluminum pan. Place a perforated bronze disc on the top of the specimen. Position tripod on the mould with dial gauge reading 2.54mm. Introduce 500ml of water in to the mould and measure distance (H) from top of the mould to the top of the water with a graduated scale and keep the set up undisturbed for 24 hours. After 24 hours again read dial gauge (R1) and record the change. Also measure the distance (H1) from top of the mould to the top of the water with graduated scale and record the change as permeability or the amount of water in millimeters that percolates in to and / or through the test specimen.

CALCULATIONS R1 R Swelling, (%) = ------------R R = Initial dial gauge reading R1 = Final dial gauge reading

Permeability = H - H1 H = Initial height of water from the top of the mould H1 = Final height of water from the top of the mould

REPORT Report the amount of swelling to the nearest second decimal and permeability to the nearest 1mm.

PRECAUTION Do not disturb the specimen during the period of swelling. 1.5% maximum

Acceptance Criteria: For BC (With CRMB-60)