( afFRT g;rmJl )

Indian Standard

ENAMEL, INTERIOR : (a) UNDERCOATING (0) FINISHING - SPECIFICATION

( Third Revision )

UDC

666.29 : 667-637.2

Q BIS 1993

BUREAU
MANAK

OF
BHAVAN, 9

INDIAN
BAHADUR DELHI NEW

STANDARDS
SHAH -110002 Price Gronp 3 ZAFAR MARG

December 1993

Paints ( Other than lndustrial

Paints ) and Allied Products

Sectional

Committee,

CHD 020

FOREWORD This Indian Standard was adopted by the Bureau of Indian Standards, after the draft finalized by the Paints ( Other than Industrial Paints ) and Allied Products Sectional Committee had been approved by the Chemical Division Council. This standard was first published in 1950 and then revised in 1965 and 1975. Through the use of this specification it was felt that for the same colour, suppliers had to submit two samples, one for each type, which increases the work of testing authorities. It was therefore prescribed that the material shall be supplied only in brushing consistency, but shall be suitable for spraying also using thinners. In this revision the minimum mass in kg per 10 litres of the material has been modified as 9.0 for finishing. This standard prescribes colour-wise requirement for wet opacity based on data collected on interior enamels by Ministry of Defence. Moreover fineness of grind and gloss values have been quantified. This revision achieves full alignment with JSS 3018 Specification for paint, RFU, enamel, interior, brushing ( lead restricted ), and JSS 3019 &Specification for paint, RFU, enamel, interior, brushing ( lead paint ), issued by the Department of Standardization, Ministry of Defence, Government of India. The composition in Annex E. of the technical committee responsible for preparation of this standard is given

For the purpose of deciding whether a particular requirement of this standard is complied with, the final value, observed or calculated, expressing the result of a test or analysis, shall be ro~unded offin accordance with IS 2 : 1960 Rules for rounding off numerical values ( revised ). The number of significant places retained in the rounded off value should be the same as that of the specified value in this standard.

IS 133 : 1993

ENAMEL, INTERIOR : (a) UNDERCOATING (b) FINlSHING - SPECIHCATION d Third Revision )

1 SCOPE 1.1 This standard prescribes requirements and methods of sampling and test for enamel, interior, undercoating and finishing, colour as required. 1.2 The material is used for the interior decoration and protection of buildings and is normally applied as a painting system comprising an appropriate primer followed by the undercoating and the finishing enamel. 2 REFERENCES The Indian Standards listed in Annex necessary adjuncts to this standard. 3 TERMINOLOGY For the purpose of this standard the definitions given in IS 1303 : 1983 shall apply. 4 TYPES The material shall be supplied in brushing consistency but shall be suitable for application by brushing and spraying after thinning with a between the suitable thinner as agreed to purchaser and the supplier. 5 REQUIREMENTS 5.1 Composition The material shall be of to satisfy the requirements 5.2 Freedom such a composition of this standard. as A are in 5.1 to 5.5 also be tested for restriction from lead in accordance with IS 101 (Part 8/Set 5) : middle brunswick green 1992 except for ( ISC 286 ) and golden yellow (lSC 356 ) colours. 5.4.1 When thus tested, the material shall not contain lead or compounds of lead or mixtures of both, calculated as lead monoxide ( PbO ), exceeding 5 -percent by mass. 5.5 The material shall also comp!y requirements given in Table 1. with the

5.6 The manufacturer( s ) may be permitted to mark their product synthetic according to this specification, if it contains minimum 10.0 percent by mass of phthalic anhydride content on non-volatile vehicle when tested as prescribed in 11 of IS 354 ( Part 2 ) : 1986. 6 PACKING 6.1 Packing Unless otherwise agreed to between the purchaser and the supplier the material shall be packed in metal containers conforming to IS 1407 : 1980 and IS 2552 : 1989. 6.2 Marking Each container shall following information: a) Name be marked material, with the AND MARKING

and type of the

from Yellowing

Enamel, interior, finishing, white, shall not show a greater degree of yellowing than the approved sample when tested as prescribed in ~Annex B. 5.3 Application The material by brushing sagging. Properties shall be suitable for application or spraying as specified without Material purposes stipulated 1

b) Indication of the source of manufacture, c) A statement synthetic if the material contains phthalic anhydride as prescribed under 5.6, d) Volume of the material, or othere) Batch No. or lot No. in code wise, and f) Month and year of manufacture. 6.3 Other details be in accordance the purchaser.

of packing and marking shall with the instructions given by for defence marked in

5.4 Lead-Restricted

The material intended for defence shall, in addition to the requirements

6.4 The material, when intended purposes, shall be packed and accordance with IS 5661 : 1970.

IS 133 : 1383

Table 1 Requirements for Enamel, Interior, Undercoating Finishing ( Clause 5.5 )

No. (1)

Sl

Characteristic
(2)

Requirement (3)

Method of Test, Ref to IS 101 (4) Part 2/Set 1 : 1988 Part 3/Set 1: 1986

i) ii)

z;;;rM;;tent, Drying time : a) Surface dry b) Hard dry c) Tack free

percent

by

0.5

Not more than 6 h Not more than 12 h Not more than 24 h 80 to 120 set ( For better application the mate. rial may be thinned to 50-60sec for brushing and 35-40 set for spraying ) Under coat Finish coat Under coat Finish coat 40 15 12.0 8.5 Part 3/Set 4 : 1987 Smooth and matt to egg shell gloss Smooth and glossy PartI/Sec4 Under coat Finish coat 20 61 Part 4/Set Off white to light grey Close match to the specified IS colour or to an approved sample where IS colour is not specified To pass the test 3 : 1986 : 1988 Part l/Set 7 : 1987 Part l/Set 5 : 1989

iii)

a) Consistency, ford cup No. 4

b) Fineness microns, iv) v)

of grind

Min,
1

Part 3/Set 5 : 1987

Mass in kg/l0 Finish: a) Undercoating

b) Finishing c) Gloss 60, Min

vi)

Colour a) Undercoating b) Finishing

vii)

viii) ix)

Fastness to light ( for finishing only ) ( with panel exposed for 100 hours ) Scratch -hardness Flexibility and adhesion a) Undercoating after 48 h air-drying b) Finishing after 96 h air-drying Resistance to water ( for finishing only )

Part 4/Set 3 : 1988

No such scratch bare metal No visible damage of film

as to show the

Part S/Set 1 : 1988 Part 5/Set 2 : 1988

3 L i

or detachment

x)

xi) xii) xiii)

Flash point Wet opacity ( see Note ) Volume solids, by mass, Min

peeling, or change in colour. Gloss retention shall not be less than 60 percent of the gloss of unimmersed portion Not below 30C Between-10 percent and +20 percent of the approved sample

Free

flaking and no undue

from

bisters,

Part 7jSec 1 : 1989

Part l/Set 6 : 1986 Part 4/Set 1 : 1988 Part 8jSec 6 : 1993

percent Under coat Finish coat Passes the test

Accelerated storage stability test, 60C, 96 h xv) Keeping properties NOTE - The values of wet opacities

xiv)

Annex

Not less than one year for supplies to defence are given in Annex C.

Part 6/Set 2 : 1989

IS 133 : 1993 7 SAMPLING Representative samples of the material shall be drawn as prescribed in IS 101 ( Part l/Set 1 ) : 1986. 8 TESTS 8.1 Tests shall be conducted as prescribed in various parts of IS 101. References to the relevant parts/sections are given in co1 4 of Table 1 and 5.3, 5.4, 5.6 and to Annex B in 5.2. 8.2 Quality of Reagents
Unless

distilled employed

water ( see IS 1070 : 1992 ) shall in tests.

be

NOTE - Pure chemicals do not contain impurities analysis.

shall mean chemicals that which affect the results of

8.3 For match against Indian IS 5 : 1993 shall be used.

Standard

colours,

9 CRITERIA FOR CONFORMITY A lot shall be declared as conforming to the requirements of this standard if the test results of the composite samples satisfy the requirements prescribed in 5.

specified

otherwise,

pure

chemicals

and

ANNEX A (Clause 2 )
LIST OF REFERRED INDIAN STANDARDS IS No. 5 : 1993 101 ( Part l/ Set 1 ) : 1986 Title Colours for ready mixed paints and enamels (fourth revision ) Methods of sampling and tests for paints, varnishes and related products : Part 1 Tests on liquid paints ( general and physical ), Section 1 Sampling ( third revision ) Section 3 Preparation of panels ( third revision ) Section revisjon Section revision 5 Consistency ) 6 Flash point ) ( third ( third IS No. 101 ( Part 4/ Set 3 ) : 1988 101 ( Part Set 4 ) : 101 ( Part Set 1 ) : 4/ 1988 5/ 1988 Title Section 3 Fastness ( third revision ) Section to light

4 Gloss ( third revision )

Part 5 Mechanical tests on paint films, Section 1 Hardness test ( third revision ) Section adhesion and 2 Flexibility ( third revision )

101 ( Part l,/ Set 3 ) : 1986 101 ( Part I/ Set 5 ) : 1989 101 ( Part~l/ Set 6 ) : 1987 101 ( Part l/ Set 7) : 1986 101 ( Part 2/ Set 1 ) : 1988

101 ( Part 5/ Set 2 ) : 1988 101 ( Part 6/ Set 2 ) : 1989 101 ( Part 8/ Set 5 ) : 1992 101 (Part 8/ Set 6 ) : 1993 354 ( Part 2 ) : 1986

Part 6 Durability tests on paint films, Section 2 Keeping properties ( third revision )
Part 8 Tests for pigments and other solids, Section 5 Lead restriction test

101 ( Part 3/ Set 1 ) : 1986 101 ( Part 3/ Set 4 ) : 1987 101 ( Part 3/ Set 5 ) : 1987 101 ( Part 4/ Set 1 ) : 1988 101 ( Part 4/ Set 2 ) : 1989

Section 7 Mass per ten litres ( third revision ) Part 2 Preliminary examination and preparation of samples for testing, Section 1 Water content ( third revision ) Part 3 Test on paint film formation, Section 1 Drying time ( third revision ) Section 4 Finish ( third revision) Section 5 Fineness ( third revision ) of grind

Section

6 Volume

solids

Methods of sampling and test for resins for paints: Part 2 Special test methods for alkyd resins ( second revision ) Reagent grade water ( third revision ) Glossary of terms relating to paints ( second revision ) tins ( second Round paint revision ) Petroleum hydrocarbon solvents ( second revision ) Steel drums ungalvanized ( galvanized and ) ( third revision )

1070 : 1992 1303 : 1983 1407 : 1980 1745 : 1978 2552 : 1989

Part 4 Optical tests on paint films, Section 1 Opacity ( third revision ) Section 2 Colour (third revision)

IS 133 : 1993

ANNEX B ( Clauses 5.2 and 8.1 )

TEST FOR FREEDOM FROM YELLOWING
B-l PROCEDURE

B-l.1 Apply two normal

coats of the material in accordance with IS 101 ( Part l/Set 3 ) : 1986 by brushing on 150 mm x 150 mm mild steel panel. Allow the first coat to dry for 12 hotirs, slightly rub down the surface and then

apply the second coat. Place the panel after 24 h in complete darkness for a period of 7 days
*

B-l.2 Compare with freshly prepared cured, for not less than 24 h and more 48 h, panel.

and than

ANNEX C ( Table 1 )
WET OPACITY VALUES,m2/10 I, Min
Value Colour Vahe Colour

350 250 290 150 90 100

Black Azure blue DaIk admiralty grey Middle brunswick green Signal Red Yellow golden

80 200 150 110

Pale green Light admiralty sea green Blue sky White

grey, and

ANNEX D
[ Table 1, SZNo. ( xiv ) ] ACCELERATEDSTORAGESTABILITY
D-l PROCEDURE

TEST

20 percent, and there

D-l.1 Store the paint sample in a closed 500 ml container and keep at 60C for 96 hours. D-l.2 After the test paint shall not gel, liver, curdle or increase in efffux time by more than

shall be no evidence of seeding. The paint shall meet the drying time requirements and shall produce dry film that is uniform in appearance and free from streaking, mottling and seediness. Further, in case of finishing paint, the change fin gloss value shall not be more than 5 units from that of original value.

IS 133, :1993
,

ANNEXE ( Forej4xwd)
COMMITTEE COMPOSITION

Paints
SHRI

( Other
MANI

than

Industrial

Paints

) and Allied
Addison9 Directorate

Products

Sectional

Committee,

CND 020

Chairman

Representing

T. K. S.
Members

Paints

and Chemicals of Technical Paints

Ltd, Madras Development, New Delhi

SHRI S. N.

AGAKWAL SHRI JASBIR SINGH (

General Nerolac of Defence

Alternate

) Goodlass
)

SHRI S. S. ANA~AIKAR SHRI JAMEELAHMAD ( Alternate SHRI S. K. ASTHANA SHRI K. N. MEBROTRA ( Ahmte SHRI V. M. WAYDEKAR SHRI S. G. SHFTYE ( Aliernnte SHRI~R. BEFIL Dr P. G. CHALJDHARI SHRI C. R. TRLTSE ( Alternate
DIRECTOR CHE~K~A~~

Ltd. Bombay j, New Delhi

Ministry
)

(DGQA

Asian Paints
)

( India ) Ltd, Bombay

ICI India Ltd, Culcutta GarwarePaints Ltd, Bombay

)
Development Shalimar Commissioner Ltd, Calcutta ( SSI ), Government of InGja

SHRI R. MU~HG~ADHAYA ( A~ternnte )

SHRI M. M. GHOSH
DR S. GHOSH SHRI K. NIRMAL KUMAR ( Alternate JOINT DIRECTOR ( CM ) SR ( CMT ) ( .dhwmte

Paints

Berger Paints

India Ltd, Calcutta New Delhi CO, Pune Calcutta New Delhi Plant ( HEC ), Ranchi Bombay

)
Railway Board, Tata Engg and Locomotive

)
)

SHRI JUNG BAHADLJR SHRI A. MAZUMDAR ; Ah%Ute SHRI ALOK MATHUR SHRI M. M. GHOSH ( Alternate SHRI ALOK MUKMERJIE SHRI S. P. GOEL ( Alternate SHRI D. P. MUKHERJEE SHRI A. P. SINHA ( Alternate

Tndian Paints )

Association,

The U K Paint Industries, ) Heavy Machine Building

)
Indian Small Scale Paint Association, Central Public Works Department, New Delhi Jenson and Nicholson ( lndia ) Ltd, Catcutta ) Ministry of Defence ( R and D ), New Delhi ~MinisLry of Environment and Forests, New Delhi National Test House, Calcutta ) Engineers India Ltd. New Delhi Oil Technologists Association of India, Kanpur ) The Punjab Bharat Paint Colour and Varnish Works Ltd. Kanpur

SHRIANIL A. PAREKH
SHRI RAMESHCHAND

SHRI G. K. LOYALKA ( -4lteunate)

DR GAUTAM RAY SHRI R. N. BANERJRE(Alternate REPRESENTATIVE REPRESWTATIVE SHRI A. K. SAMA SHRI S. K. SAHA ( Alternate DR G. SAHA DR M. S. SAXENA DR M. M. SHIRSALKAR( Alternate SHRI G. N. TEWARI SHRI P. K. KHANNA ( Alternate ) SHRI M. B. UNNI SHRI N. I). GUPTA (Alternate SHRI A. K. BASU ( Ahmute

Heavy Electricals

Ltd, New Delhi Research, Technology,

Member)

) )
Shriram Institute Indian
)

SHRI V. K. VEXMA SHRI A. K. AGARWAL ( .-ibernate ) DR M. YA~EEN DR B. G. K. MURTHY (Alternate DR R. K. SINGH,

for Industrial of Chemical

New Delhi Hyderabad

1r;stitute General,
Secretary

Director
Member

BIS ( Ex-officio

Director ( Chem j
SHRI R. NARULA Joint Director ( Chemicals ), BIS

IS 133 : 1993
RMPs
Convener SHRI S. S. ANAKAIKAR

Enamels and Adjuncts

Goodlass

Sub-committee,
Representing Nerolac Paints

CHD 020 : 02
Ltd, Bombay

Members
SHRI R. N. BANERJEE SHRI R. BEHL DR P. G. CHAUDHARI SHRI A. P. SHENOY ( Alternate DR M. B. GUHA SHRI D. K. SEN ( Alternate SHRI JAMEELAHMAD SHR~ A. V. KALE SHRI N. K. KAUSHAL SHRI P. JAYAKUMARANA ( Alternate

Indian Paints Association, Calcutta ICI India Ltd, Calcutta Garware Paints Ltd, Bombay ) Shalimar Paints, Calcutta

, Goodlass Snowcem Directorate ) The U K Paint ) Berger Paints, Calcutta Addisons Paints, Madras Ministry of Defence ( DGQA ), New Delhi ) Jenson and Nicholson ( India ) Ltd, Calcutta Central Building Research Institute, Roorkee Railway Board, New Delhi National Test House, Calcutta ) Asian Paints India Ltd, Bombay The Punjab Paint Colour and Varnish Works Ltd, Kanpur Industries, New Delhi Nerolac Paints Ltd, Bombay India Ltd, Bombay General of Supplies and Disposals, New Delhi

SHRI ALOK MUKHERJEE

SHKI K. NIRMAL KUMAR

SHRI S. P. GOEL ( rllternnte

SHRI K. S. RAMACHANDRAN SHRI S. S. RAO SHRI M. H. ALAM ( Alternate DR GAUTAM RAY REPRESENTATIVE REPRESENTATIVE SHRI S. K. SAHA SHRI T. K. CHAKARABORTY( Alternate SHRI S. Go. SHETYE SHRI G. N. TEWARI

Standard Mark

Mark is governed by the provisions of the Bureau of Indian made thereunder. The Standard Mark on products covered by an Indian Standard conveys the assurance that they have been produced to comply with the requirements of that standard under a well defined system of inspection, testing and quality control which is devised and supervised by BtS and operated by the producer. Standard marked products are also continuously checked by BIS for conformity to that standard as a further safeguard. Details of conditions under which a licence for the use of the Standard Mark may be granted to manufacturers or produceres may be obtained from the Bureau of Indian Standards.
Standards Act, 1986 and the Rules and Regulations

The use of the Standard

Bureau of Indian Standards

, .

BIS is a statutory institution established under the Bureau of Indian Standards Act, 1986 to promote harmoious development of the activities of standardization, marking and quality certification of goods and attending to connected matters in the country. Copyright BIS,has the copyright of all its publications. No part of these publications may be reproduced in any form without the prior permission in writing of BIS. This does not preclude the free use, in the course of implementing the standard, of necessary details, such as symbols and sizes, type or grade designations. Enquiries relating to copyright be addressed to the Director ( Publications ), BIS. Revision of Indian Standards

Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewed periodically; a standard along with amendments is reaffirmed when such review indicates that no changes are needed; if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standards should ascertain that they are in possession of the latest amendments or edition by referring to the latest issue of BIS Handbook and GStandards Comments on this Indian Standard may be sent to BIS giving the following Monthly Addition. reference: Dot : No. CHD 020 ( 0452 ) Amendments Issued Since Publication Amend No. Date of Issue Text Affected

BUREAU Headquarters: Manak Bhavan, Telephones 9 Bahadur Shah Zafar 331 13 75

OF INDIAN Marg,

STANDARDS 110002 Telegrams ( Common : Manaksanstha to all Offices Telephone )

New Delhi

: 331 01 31,

Regional Central

Offices : Manak

: Bhavan, 9 Bahadur 110002 VIII M, V. I. P. Road, Maniktola f37 84 99, I 37 86 26, f53 38 43, 35-C, CHANDIGARH Road, MADRAS Andheri 160036 600113 Shah Zafar Marg

C 331 01 31 331 13 75 37 85 61 37 86 62 53 16 40 235 04 42 235 23 15 632 78 58 632 78 92

NEW DELHI Eastern

: l/14 C. I. T. Scheme CALCUTTA 700054 Sector

Northern Southern Western

: SC0 445-446,

153 23 84 f235 02 16, 1235 15 19,

: C. I. T. Campus, : Manakalaya, BOMBAY

IV Cross

E9 MIDC, 400093

Marol,

( East )

f632 92 95, 1632 78 9 1,

Branch

: AHMADABAD. FARIDABAD. LUCKNOW.

BANGALORE. BHOPAL. BHUBANESHWAR. COIMBATORE. GHAZIABAD, GUWAHATI. HYDERABAD. JAIPUR. KANPUR PATNA. THIRUVANANTHPURAM.

Printed at Prirrtwell Printers,

Aligarh.

India

NO. 1 TO IS 133 : 1993 ENAMEL INTERIOR: (a) UNDERCOATING (b) FINISHING - SPECIFICATION ( Third Revision)
(Foreword,para
Part 4iSec 3 : 1986. [

AMENDMENT

3, line 1) -

Substitute 8.5 for 9.0. Substitute Substitute

Part 4Eiec 3

[ Page 2, Table 1, SZNo. (vi), coZ4 ] Page 2, Table 1, Sl No. (xi), coZ4 ] -

: 1988 for for

Part l/Set 6 : 1987

Part l/Set 6 : 1986.

(Page 3,Annex A, line 2 ) -

Substitute 1994for 1993. Substitute 101 ( Part l/Set 7 ) : 1987 for

(Page 3, Annex A, line 16 ) ( 101 Part l/ Set 7 ) : 1986.

( Page 3, Annex A ) - Add at the end IS 5661 : 1970 Code of practice for packing and marking for packages of paints, enamels varnishes and allied products.

(CHD20)

Rwwvhy

Unit, BE, New Delhi, India

AMENDMENT NO. 2 JULY 1997 TO IS 133 : 1993 ENAMEL, INTERIOR: (a) UNDERCOATING (b) FINISHING SPECIFICATION

(Page 1, clause 4, he 3 ) - Insert ( recommended consistency is 50-60 set ) after the word brushing and ( recommended consistency is 35-40 set ) after the word spraying.
[ Page 2, Table 1,SZNo. (iii)(a), coZ3 ] spraying). [ Win. [ Page 2, Table 1, SZNo. (iii) (b), coi 3 ] - Stibstitute Not more than 40 microns for 40 against Under coat and Not more than 15 microns for 15 against Finish coat.

Delete the following:

( For better application the material may be thinned to 50-60 set for brushing and 35-40 set for

Page 2, Table 1, SI No. (iii)(b), co2 2, line 2 ] .- IMete the word

microns,

[ Page 2, Table 1, SZ No. (iv), coZ2 ] kg/l0 1.

Insert the word

Part 4/set 2

Mitt

after Massin
3

(Amendment No. 1, line 2 ) 1988.

Substitute

: 1989

for Part 4&c

(CHDO20)

Reprography Unit, BE, New Delhi, India

NO. 3 MARCH 1999 TO IS 133 : 1993 ENAMEL, INTERIOR: (a) UNDERCOATING (b) FINISHING - SPECIFICATION ( Third Revision)
(Page 1, clause 1.2 ) Substitute the following for the existing:

AMENDMENT

1.2 The material is used for protection and decoration of interior surfaces and is normally applied as a painting system comprising an appropriate primer tollowed by the undercoating and the finishing enamei. [ Page 2, T&e existirrg: c) Gloss 60
Under coal, Max finish coat, Min [ Edge 2,

1, Si No. (v)(c), cd 2 ] -

Substitute the following for the

Y&le 1: Sb Xo. (x), coi 3 ] -

Substitute the following

for the

existblp;:
Free from blisters, peeling or flaking and no undue change in colour. Gloss retenaion shall not be less than 60 percen; cf the gloss of unimmersed portion. when tested as follows: in 5 of IS 101 (Part l&c 3) to give a dry film

Apply a coat of material OII glass panels as @bed mass commensurate Al!ow :he pane! to air dry in a horizontal

with ?he mass per 10 litre as specified

in Table 1 of IS 101 (Part 3/Set 4).

position for 48 h. Immerse the panel in distilled water

(see IS 1070) at room temperature for 48 h. Remove the panels from water and examine it after 4 h.

(CHD30)

Reprography

Unit, BIS, New Delhi, India