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Synthesis of CL
Figure 2 :
a) SEM Image of
b) TEM image of CL
Characterization of CL
b)
DMF as
solvent
Figure 4 : a)
Precepitate of
CH3NH3I b)
CH3NH3PbI3 PSCs
solution
Etching
Compact layer
IV
Characterizatio
n
FESEM
UV
Measurement
Back Contact
Mesoporous
Layer
HTM
Perovskite
Coating
MAPbICl
Perovskite
Coating
MAPbI
3. Mesoporous layer
2000rpm, 1500rpm
& 1000rpm for 60s
(using Spin coater)
0.1M TiCl4
60c for 1hr in
oven
Sintered at 475c
for 30min
4. Perovskite Coating
1000rpm for 50s
(Spin coater)
MAPbI3 & MAPbICl2
Spiro MeOTAD
75mg/ml of Cholorobenzene + 8l of TBP + 14.2l L
+ 525mg.ml acetonitril
6. Back contact
Platinum
3min
(20MA)
5min
(40MA)
10min
(40MA)
MAPbICl
2
Spiro
Planar &
Mesoporo
us
MAPbICl2
with
Planar &
Mesoporo
us MAPbI3
with
Cu2O
Only one
device
show high
voltage
~430 mv
out of 6
sample
tested
FF
Voc (V)
Jsc
(mA/cm2)
0.22
0.485
6.85
0.55
FESEM (1500rpm
Platin
um
Spiro
Mp TiO2 /
Perovskite
C
L
FT
O
What should we
modify our
experiment?
1. 3000rpm will used to
coat mesoporous
layer
2. Reduce time for dip
coating of compact
layer 60c for
30min.
3. Humidity of the room
should be controlled
~ 35%
The color of
perovskite change
Solutio
n
Encapsulation of PSCs
Timeline
I am
here
Synthesis
of
Perovskite
solution
Full device
fabrication
Stability
of
perovski
Wt
%
0
24
48
72
96
120
144
168
182
216
240
Hrs
0wt%
5wt%
10wt%
20wt%
XRD
UV-Vis
PL
FESEM