Acid and Base Standarization

reated by

sri Aminah 151411003

eptiani Rasidah 1514110

A Chemical Engineering

Objective

Result
&
Discussion

Methodology

Theory
Equilibriu
m

Tools
&
Ingredient

Outline Of
Presentation

Objective

To demonstrate the
basic laboratory
technique of titration

To learn to calculate
molarity based on
titrations

Theory

High purity
Stability (low reactivity)
Low hygroscopicity (to minimize
weight changes due to humidity)
High equivalent weight (to
minimize weighing errors)[3]
Non-toxicity
Ready and cheap availability

secondary standard is
usually standardized
against a primary
standard.

Theory
Hidrokloride
acid

Hydrochloric
acid is a clear,
colorless,
highly
pungent solution
of
hydrogen chloride
(HCl) in water
HCl can use for

Sodium
Hidrokside

Sodium hydroxide
(NaOH) is an a
white. NaOH is
available in pellets,
flakes, granules,
and as prepared
solutions at a
number of different

Theory
Titration is a method used in measuring the
amount of an analytical reagent necessary to react
quantitatively with the sample.
Acid-base titrations are important for counting
concentrations of acids and bases.
The point at which the equivalence point has been
reached is called the theoretical end point.
In titration used indicator to detected by some
physical change, such as colour change, to
indicate the endpoint.

Tools & Ingredients

1. Tools

Beaker

Spatula

Volumetric Flask

Erlenmeyer flask Pipet Filler

Pipet

Funnel

analytical balance

Stirrer stick

Buret, Klem & Statif

2. Ingredients

Aquadest
NaOH 1 N
HCl 1 N
Indicator PP
Indicator MM
Indicator MO

Methodology
1. Strandarization Acid
25
ml Aquadest
1 gram
Boraks

Solution 1

Aquadest
Solution 1

Solution 2

5 ml Solution
2
Indicator
MM 3 drop

Solution 3

sodium hidroxide

2. Strandarization Base
25 ml
Aquadest
0,63
Oxalic
acid

Aquadest1
Solution

Aquadest
50drop
ml2
10
ml Solution
Indicator
PP

Solution 1

Solution 2

Solution 3

Result and Discussion

Standarizasion of HCl
Trial 1

Trial 2

Trial 3

Volume of Boraks
used

5 mL

5 mL

5 mL

Molarity of
Boraks used

0,1 N

0,1 N

0,1 N

6,00 mL

5,55 mL

5,61 mL

Volume of HCl
used
Averange of
volume HCl
Molarity of NaOH
sol'n

5,72 mL
0,09 N

Result and Discussion

Standarizasion of NaOH
Trial 1

Trial 2

Trial 3

Volume of Oxalic
acid used

10 mL

10 mL

10 mL

Molarity of
Oxalic acid used

0,1 N

0,1 N

0,1 N

Volume of NaOH
used

11,85 mL

11,95 mL

12,00 mL

Averange of
volume NaOH
Molarity of NaOH
sol'n

11,93 mL
0,08 N

Result and Discussion

The end point of an acid-base titration is the point where
the indicator changes colour
Equivalence point is the point where there are equal
amounts (in moles) of acid and base
The indicator that we used in standarizasion of HCl is the
methyil red, where the ph range is around 4,8 to 6,0
The indicator that we used in standarizasion of NaOH is the
phenolphthalein, where the ph range is around 8.2 to 10.0
In order to make sure that sample dissolved completely,
we have to shake the flask thoroughly.

Result and Discussion

The titration curve