Additional Metode Penelitian

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 METODE PENELITIAN

Karakterisasi Fisik dan Kimia

Instrumen Magna-IR 560 ESP spectrophotometer
Bruker AXS D8 Advance X-ray Piridin FTIR
diffractometer Situs asam
Pola XRD ASAP2450 system
Quanta 200 Isoterm nitrogen
SEM Images Luas permukaan dan distribusi ukuran
Magna-IR 560 ESP infrared pori
spectrophotometer TPD/TPR 5079 analyzer
Spektra IR Analisis desorpsi amonia yang diprogram
Pelarutan dalam KBr dengan temperatur (Temperature-
Programmed Ammonia Desorption,
NH3-TPD) Nur Handayani Octaviyanti
 METODE PENELITIAN

Kondisi Instrumen
Bruker AXS D8 Advance X-ray Quanta 200
diffractometer SEM Images
Pola XRD operation voltage of 20 kV
Nickel-filtered Cu KaX-ray source The samples were coated with a thin
radiation and operated at 40 kV and 30 layer of gold
mA Magna-IR 560 ESP infrared
2 range 15-35 at a speed of 2/min spectrophotometer
with slit parameters DS = SS = 1 and RS
Spektra IR
= 0.3 mm
Resolusi 1/cm
Pelarutan dalam KBr

Nur Handayani Octaviyanti

 METODE PENELITIAN

Kondisi Instrumen
Magna-IR 560 ESP spectrophotometer
Piridin FTIR
The samples were finely ground and Subsequently, the samples were
pressed into a self-supporting wafer followed by the adsorption of purified
(diameter 12 mm) pyridine vapor at room temperature
The wafers were evacuated in the IR for 20 min
cell at 350C for 2 h under a vacuum of The Py-IR spectra were recorded after
1.33x10-3 Pa subsequent evacuation of the infrared
After the temperature decreased to cell at 200 and 350C, respectively
room temperature, IR spectra were
recorded in the range from 1700 to
1400 cm-1

Nur Handayani Octaviyanti

 METODE PENELITIAN

Kondisi Instrumen
ASAP2450 system
Isoterm Nitrogen
All the samples were degassed at The micropore volume and the
300C under vacuum for 24 h before external surface area were determined
analysis from the t-plot analysis
The specific surface areas were The PSD of the samples were
calculated using the Brunauer calculated using the BarrettJoyner
EmmettTeller (BET) model Halenda (BJH) method
The total volumes of micropores and
mesopores were calculated from the
amounts of nitrogen adsorbed at P/P0=
0.98

Nur Handayani Octaviyanti

 METODE PENELITIAN

Kondisi Instrumen
TPD/TPR 5079 analyzer
Analisis NH3-TPD
Initially, all the samples were heated to Then, the NH3-TPD profiles were
400C at a rate of 10C min-1 and obtained in the range of 100600C at
maintained at 400C for 1 h a heating rate of 10C min-1
The adsorption of ammonia on the
samples was performed at room
temperature
After saturation, the samples were
purged in flowing pure nitrogen at
100C for 1 h to eliminate the
physically adsorbed ammonia

Nur Handayani Octaviyanti