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WHEN YOU COME IN, PLEASE:

• Put all of your stuff in the back.

• Only have a pen on table for the quiz @ 9:25. NOTHING ELSE.

• Raise your hand when you finish quiz.

• After I collect it, sign in and hand in work due today. Make sure you
name is on every paper!!!
TODAY

• Lab 3: Vapor Pressure and Heat of Vaporization

• Lab 4: The Synthesis and Analysis of Aspirin

• Part I. (Synthesize Aspirin)


DUE NEXT WEEK:
• Lab 3: Vapor Pressure and Heat of Vaporization

• Data Analysis questions (pg. 23)

• Make sure all graphs are properly labeled, formatted, and printed…

• Lab 4: The Synthesis and Analysis of Aspirin

• Pre Lab Report:

• Part 2 (Melting Temperature)

• Part 3 (Colorimetric Absorbance)

• All pre-lab questions on pg. 19

• Pre lab quiz next week will cover all of Aspirin Lab (parts 1, 2, and 3)
TODAY

• Lab 3: Vapor Pressure and Heat of


Vaporization

• Lab 4: The Synthesis and Analysis of Aspirin

• Part I. (Synthesize Aspirin)

The partner you get today will also be your partner next week!
(Since next week is just Parts 2 and 3 of Aspirin Lab)
• pg. 21

• Step 2. You do NOT need to use a hot plate. Just take a 400mL
beaker and go to the sink. Run the TAP water until its hot. Fill up
your beaker with hot tap water. You don’t have to do this right
away though. You don’t actually need this hot tap water until Step
13.
• At Step 5 - This is how your set up should
look.

• Don't let Figure 1 in the manual trip you up.


That picture should be located under step
9…

• Just follow the written steps.

• Notice how the valve is OPEN.

• You program your vernier according to


manual…

• In this picture, the temp probe is near the


flask. Allow your readings to stabilize. You
then have the room temp and initial air
pressure in the flask…

Make sure your pressure reading is


close to this value - otherwise your
99.42 equipment isn’t working right.

21.4
Step 8 - Place temp probe
in ROOM TEMP water bath.
Make sure flask is
submerged.

After 30 seconds, CLOSE


the VALVE on the white
stopper
Notice the water level height
Current
Apparatus

Draw up 3 mL
of ethanol

Unscrew
1. OPEN VALVE
2. DEPRESS SYRINGE syringe,
3. DRAW IT BACK UP keeping valve
4. SHUT VALVE shut. You’re
Thread syringe left with this set
on - KEEPING up.
VALVE SHUT
Allow a few seconds for ethanol
to evaporate…

Start Data Collection

(Hit Play)

Make sure flask is always submerged.


You are watching the temperature and
pressure readings.
When they stabilize, HIT KEEP.
Then you need to raise the
temperature atleast 1 degree C.

This is where the beaker of hot tap


water comes in.

Pour some of that in. Swirl it around.

Always make sure your flask is


submerged

When temperature raises a degree or


2 - wait for it to stabilize - along with
the pressure reading. HIT KEEP.

Do this 4 times.

Eventually you might need to scoop


water out of main beaker in order to
get more hot water in and raise temp.
Always keep flask submerged.
• After you have raised temp to complete all trials. Just stop data
collection. Tap table to see the temps and pressure values you
recorded. These must go in data table on pg. 22.

102.99

99.42

21.4 22.3

Initial Initial
Values from Values in
Step 7. water bath
102.99

99.42 You will calculate these values as you go through


Data Analysis questions on page 23. Show your
work!

21.4 22.3

Initial Initial
Values from Values in
Step 7. water bath

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